CN105724445A - Rosemary essential oil mosquito-repellent incense liquid and preparation method thereof - Google Patents
Rosemary essential oil mosquito-repellent incense liquid and preparation method thereof Download PDFInfo
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- CN105724445A CN105724445A CN201610059883.2A CN201610059883A CN105724445A CN 105724445 A CN105724445 A CN 105724445A CN 201610059883 A CN201610059883 A CN 201610059883A CN 105724445 A CN105724445 A CN 105724445A
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- mosquito
- ethereal oil
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Pest Control & Pesticides (AREA)
- Catching Or Destruction (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses rosemary essential oil mosquito-repellent incense liquid and a preparation method thereof. The rosemary essential oil mosquito-repellent incense liquid is prepared from the following raw materials in parts by weight: 0.5-2.5 parts of transfluthrin, 0.1-0.5 part of rosemary essential oil, 50-60 parts of triethylene glycol monobuthyl ether, 0.05-0.15 part of sodium xylene sulfonate, 0.1-0.5 part of a synergist, 0.1-0.5 part of an antioxidant and 35-45 parts of water. The rosemary essential oil mosquito-repellent incense liquid disclosed by the invention has fresh and fragrant aroma and has a relatively strong repelling and exterminating effect on mosquitoes; as environment-friendly mosquito-repellent incense liquid, the mosquito-repellent incense liquid has a relatively strong pesticide effect, is safe and non-combustible, can be volatilized stably, can also be used for reducing the content of indoor organic volatile matter and is an ideal option of healthy home livings.
Description
Technical field:
The present invention relates to a kind of mosquito incense, be specifically related to a kind of rosemary ethereal oil vaporizer mosquito liquid and preparation method thereof.
Background technology:
Mosquito is a kind of worldwide sanitary insect pest, and its all one's life, larva, when pupa, adult four through ovum
Phase.Mosquito is importantly that it is one of communication media of infectious disease.It was found that the disease of mosquitoes spread
Disease reaches more than kind more than 80.In the whole world, there are about 1,200,000 people and infect filaricide.The mosquito of major part kind
Can the disease of infectious disease toxicity, including yellow fever, dengue fever, Japanese encephalitis, St. Louis encephalitis, multiple
Property arthritis, Rift Valley fever (Rift Valley fever), contract elder brother Gen Yare and west Nile fever.On earth,
Which kind of animal is not had to have bigger harm to the mankind than mosquito again.The mosquito serious threat mankind as can be seen here
Health, only drives these disgusting mosquitoes, could control epidemic infectious diseases, could ensure people
Class is healthy, improves the quality of life of people.
For many years, people develop and employ substantial amounts of hygienic insecticide product, for killing mosquitoes.Mosquito
Perfume (or spice) is the most ancient natural drug anophelifuge way.As far back as the Southern Song Dynasty, just there is the culicifuge incense that Chinese medicine is made in period
Rod.Containing effective ingredient in modern mosquito incense is pyrethrin, and it has the effect of mosquito.After burning mosquito incense,
Pyrethrin in mosquito incense evaporates along with smog, sends out in indoor air, makes the nerve of mosquito
Paralysis, then mosquito or born get killed, or four dissipate and run away, thus the current mosquito of effect playing mosquito killer
Fragrant production industry insecticidal active ingredient, mainly cypermethrin, Prallethrin, allethrin, biological chrysanthemum
The pyrethrins such as ester, the nerve that can benumb mosquito causes its death.
Electric liquid device actually mosquito liquid and the electronic thermostatic heater making medicinal liquid uniformly volatilize
General name, the former claims mosquito-driving liquid, the latter to claim electric heater.In electric liquid device work, work as electric heater
After accessing power supply, PTCR element begins to the heating that heats up, and relies on the temperature of PTCR element self afterwards
Regulatory function, makes its temperature remain certain value.The heat that PTCR element produces is passed by heat radiation
It is delivered to medicinal liquid volatilization core, is drawn to plug upper end, make from medicinal liquid bottle by medicinal liquid by volatilization core capillarity
Medicinal liquid raising under heat radiation heats is vaporized speed, after the insecticidal active ingredient in space reaches finite concentration,
Just mosquito is produced and drive, thus knock down and kill mosquito.Electric liquid device is because of its light, nothing of use
Cigarette, without features such as dust, efficacy stability, high-efficiency low-toxicities, is welcome by consumer.
Existing electric liquid device formula system is with alkane solvent, pyrethroid, antioxidant and perfume (or spice)
Essences etc. are component, form homogeneous system by mixing, stirring solvent.Alkane solvent is owing to being the shapes such as rectification
Becoming, its carbochain is distributed more widely, and wherein low-carbon paraffin is easily formed organic volatile i.e. VOC,
In the daily life staying idle at home of consumer, can be used by the heating of electric liquid device and volatilization causes house naturally
The pollution of habitat environment, brings certain impact to consumer health.
The invention provides a kind of rosemary ethereal oil vaporizer mosquito liquid, be the vaporizer mosquito liquid of a kind of safety and environmental protection.
Summary of the invention:
For deficiencies of the prior art, one of the technical problem to be solved is to provide
A kind of rosemary ethereal oil vaporizer mosquito liquid.
One of the technical problem to be solved is to provide the preparation of above-mentioned rosemary ethereal oil vaporizer mosquito liquid
Method.
The technical problem of the present invention, is achieved by following technical proposals:
A kind of rosemary ethereal oil vaporizer mosquito liquid, is made up of the raw material of following weight parts: 0.5-2.5 part phenyl tetrafluoride
Chrysanthemum ester, 0.1-0.5 part rosemary ethereal oil, 50-60 part triethylene glycol butyl ether, 0.05-0.15 part dimethylbenzene sulphur
Acid sodium, 0.1-0.5 part synergist, 0.1-0.5 part antioxidant, 35-45 part water.
Preferably, described synergist is alantolactone and/or Griffonilide.
It is highly preferred that described synergist is by 40-60wt% alantolactone and 40-60wt% lattice row wind
Ester forms.
Preferably, described antioxidant is 2,4-dimethyl-6-tert-butyl phenol and/or 2,6-di-t-butyl-4-
Methylphenol.
It is highly preferred that described antioxidant by 40-60wt%2,4-dimethyl-6-tert-butyl phenol and
40-60wt%2,6-di-tert-butyl-4-methy phenol forms.
Present invention also offers the preparation method of above-mentioned rosemary ethereal oil vaporizer mosquito liquid, by transfluthrin,
Rosemary ethereal oil, triethylene glycol butyl ether, synergist, antioxidant mix homogeneously, add xylene monosulfonic acid
Sodium mix homogeneously, it is eventually adding water mix homogeneously.
Concrete, in the present invention:
Transfluthrin, No. CAS: 118712-89-3.
Rosemary ethereal oil, No. CAS: 8000-25-7.
Triethylene glycol butyl ether, No. CAS: 143-22-6.
Sodium xylene sulfonate, Chinese another name: 3,5-acid dimethyl sodium, No. CAS: 1300-72-7.
Alantolactone, No. CAS: 546-43-0.
Griffonilide, No. CAS: 61371-55-9.
2,4-dimethyl-6-tert-butyl phenols, No. CAS: 1879-09-0.
2,6-di-tert-butyl-4-methy phenols, No. CAS: 128-37-0.
The rosemary ethereal oil vaporizer mosquito liquid of the present invention, the pure and fresh fragrance of taste, mosquito is had stronger killing
Effect, is a kind of environment-friendly liquid mosquito incense, and it has, and drug effect is powerful, safety is non-combustible, volatilization is stable,
Indoor organic volatile matter content can also be reduced, be the ideal chose of healthy life staying idle at home.
Detailed description of the invention:
Below in conjunction with embodiment, the present invention is described further, the following stated, only to the present invention
Preferred embodiment, not does the restriction of other forms, any technology being familiar with this specialty to the present invention
Personnel are changed to the Equivalent embodiments changed on an equal basis possibly also with the technology contents of the disclosure above.Every
Without departing from the present invention program content, any letter following example done according to the technical spirit of the present invention
Single amendment or equivalent variations, all fall within protection scope of the present invention.
Embodiment 1
Rosemary ethereal oil vaporizer mosquito liquid raw material (weight portion): 1.2 parts of transfluthrins, 0.2 part of Herba Rosmarini Officinalis
Quintessence oil, 55 parts of triethylene glycol butyl ether, 0.1 part of sodium xylene sulfonate, 0.3 part of synergist, 0.3 part of antioxygen
Agent, 40 parts of deionized waters.
Described synergist is obtained by 50wt% alantolactone and 50wt% Griffonilide mix homogeneously.
Described antioxidant is by 50wt%2,4-dimethyl-6-tert-butyl phenol and 50wt%2,6-di-t-butyl
-4-methylphenol mix homogeneously obtains.
The preparation method of rosemary ethereal oil vaporizer mosquito liquid:
Transfluthrin, rosemary ethereal oil, triethylene glycol butyl ether, synergist, antioxidant are mixed and stirs
Mix uniformly, add sodium xylene sulfonate and be mixed and stirred for uniformly, be eventually adding deionized water and mix and stir
Mix uniformly.Obtain the rosemary ethereal oil vaporizer mosquito liquid of embodiment 1.
Embodiment 2
Substantially the same manner as Example 1, differ only in: described synergist is only alantolactone.
Obtain the rosemary ethereal oil vaporizer mosquito liquid of embodiment 2.
Embodiment 3
Substantially the same manner as Example 1, differ only in: described synergist is only Griffonilide.
Obtain the rosemary ethereal oil vaporizer mosquito liquid of embodiment 3.
Embodiment 4
Substantially the same manner as Example 1, differ only in: described antioxidant is only 2,4-dimethyl-6-
Tert-butyl phenol.Obtain the rosemary ethereal oil vaporizer mosquito liquid of embodiment 4.
Embodiment 5
Substantially the same manner as Example 1, differ only in: described antioxidant is only 2,6-di-t-butyl
-4-methylphenol.Obtain the rosemary ethereal oil vaporizer mosquito liquid of embodiment 5.
Test case 1
The rosemary ethereal oil vaporizer mosquito liquid of embodiment 1-5 is carried out indoor harmacological effect test, uses
GB18418-2009 domestic sanitary parasite killing articles for use electric liquid device standard, tests.In this standard
In, it is qualified that KT50 value (boxing method)≤10 minute can be judged to, and the time, the shortest explanation was to mosquito driving and killing
Effect is the best, and test data are shown in Table 1.
Table 1: vaporizer mosquito liquid indoor harmacological effect table (boxing method)
| KT50 value | |
| Embodiment 1 | 4 points 18 seconds |
| Embodiment 2 | 6 points 27 seconds |
| Embodiment 3 | 6 points 54 seconds |
| Embodiment 4 | 5 points 32 seconds |
| Embodiment 5 | 6 points 02 second |
Comparing embodiment 1-3, embodiment 1 (alantolactone, Griffonilide are compounding) mosquito driving and killing effect
Really, hence it is evident that be better than embodiment 2-3 (single raw material in alantolactone, Griffonilide)；The most real
Execute example 1 and embodiment 4-5, embodiment 1 (2,4-dimethyl-6-tert-butyl phenols, 2,6-di-t-butyl-4-
Methylphenol compounds) mosquito driving and killing effect, hence it is evident that it is better than embodiment 4-5 (2,4-dimethyl-6-tert-butyl benzenes
Single raw material in phenol, 2,6 di tert butyl 4 methyl phenol).
Test case 2
The rosemary ethereal oil vaporizer mosquito liquid of embodiment 1-5 is carried out toxotest, with reference to health ministry " duty
Industry impatient property chemicals toxic disease in the blood system diagnostic criteria " and " Chinese medicine, natural drug immunity poison
Technological guidance's principle of Journal of Sex Research " standard, formulate test case of the present invention.
Experiment kind: two young age white mice.
Experimental technique:
(1) experiment condition: laboratory temperature (27 ± 2) DEG C
(2) experimental provision: in two 25 square metres of mutually synthermal laboratorys, each placement one is big
80 × 80 × 80cm of little same size is fine and closely woven ventilative netted to be shrouded.
(3) experimental procedure: by two young age white mice be separately respectively put in the netted of two laboratorys and shroud
In, and be divided into matched group and smoke mosquito incense group of the present invention, give respectively do not smoke mosquito incense of the present invention and smoke the present invention
Mosquito incense, measures children's white mice body weight in age, observes hematology's biochemical indexes, changes in histopathology and stop
Only smoke the recovery situation etc. after mosquito incense of the present invention.Place mosquito incense of the present invention time to be arranged on netted shroud in from
The end 30 centimeters.Dosage: electrical heating mosquito incense, keeps 24 hours life-time service.Time: continuously
Use one month, observe matched group and smoke the white mice in young age of mosquito incense group of the present invention, the life-time service present invention
Mosquito incense to children age white mice toxicity and side effect.Cleaning: shroud interior two days cleanings once.
Result: after two young age white mice blood tests, every biochemical indicator is normally, shows this
Children white mice in age is had no side effect by bright mosquito incense, when only having more than that indoor mosquito incense smog is the denseest 24 hours, needs
Window and take a breath 10-15 minute, draw blood first 8 hours not to two children's white mice in age feeds.
Conclusion: life-time service mosquito incense of the present invention to children age white mice without any toxicity.
Test case 3
The rosemary ethereal oil vaporizer mosquito liquid of embodiment 1-5 is carried out acute oral toxicity test, after contamination 5
Minute activities in rats increases, and continues about 2 minutes, and activity transfers to normally, diet normally, the observation period without
Death, LD50 is more than 5000 mgs/kg, belongs to actual nontoxic.
Test case 4
The rosemary ethereal oil vaporizer mosquito liquid of embodiment 1-5 is carried out acute inhalation toxicity test, big after contamination
Mus diet activity no abnormality seen, the observation period, LD50, more than 10 grams/cubic metre, belonged to actual without death
Nontoxic.
Test case 5
The rosemary ethereal oil vaporizer mosquito liquid of embodiment 1-5 is carried out skin patch test, and experimental group skin is red
It is 0 that speckle and edema form scoring sum, illustrates to have no stimulation skin.
Test case 6
The rosemary ethereal oil vaporizer mosquito liquid of embodiment 1-5 is carried out eye irritant test, and experimental group acute ocular stings
Swashing integration number is 0, illustrates to have no stimulation mucosa.
Claims (6)
1. a rosemary ethereal oil vaporizer mosquito liquid, it is characterized in that, be made up of the raw material of following weight parts: 0.5-2.5 part transfluthrin, 0.1-0.5 part rosemary ethereal oil, 50-60 part triethylene glycol butyl ether, 0.05-0.15 part sodium xylene sulfonate, 0.1-0.5 part synergist, 0.1-0.5 part antioxidant, 35-45 part water.
2. rosemary ethereal oil vaporizer mosquito liquid as claimed in claim 1, it is characterised in that: described synergist is alantolactone and/or Griffonilide.
3. rosemary ethereal oil vaporizer mosquito liquid as claimed in claim 2, it is characterised in that: described synergist is made up of 40-60wt% alantolactone and 40-60wt% Griffonilide.
4. the rosemary ethereal oil vaporizer mosquito liquid as according to any one of claim 1-3, it is characterised in that: described antioxidant is 2,4-dimethyl-6-tert-butyl phenol and/or 2,6-di-tert-butyl-4-methy phenol.
5. rosemary ethereal oil vaporizer mosquito liquid as claimed in claim 4, it is characterised in that: described antioxidant is made up of 40-60wt%2,4-dimethyl-6-tert-butyl phenol and 40-60wt%2,6-di-tert-butyl-4-methy phenol.
6. the preparation method of rosemary ethereal oil vaporizer mosquito liquid as according to any one of claim 1-5, it is characterized in that: by transfluthrin, rosemary ethereal oil, triethylene glycol butyl ether, synergist, antioxidant mix homogeneously, add sodium xylene sulfonate mix homogeneously, be eventually adding water mix homogeneously.
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| CN201610059883.2A CN105724445B (en) | 2016-01-28 | 2016-01-28 | Rosemary Oil vaporizer mosquito liquid and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610059883.2A CN105724445B (en) | 2016-01-28 | 2016-01-28 | Rosemary Oil vaporizer mosquito liquid and preparation method thereof |
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| CN105724445A true CN105724445A (en) | 2016-07-06 |
| CN105724445B CN105724445B (en) | 2018-06-19 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109805033A (en) * | 2019-01-16 | 2019-05-28 | 佛山市南海添惠日化有限公司 | A kind of tea tree ethereal oil mosquito liquid |
| CN110037020A (en) * | 2019-03-21 | 2019-07-23 | 佛山市南海添惠日化有限公司 | A kind of tea tree ethereal oil mosquito liquid |
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| CN101558767A (en) * | 2009-05-12 | 2009-10-21 | 江西山峰日化有限公司 | Composition for driving and killing mosquitoes and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
| CN103931673A (en) * | 2014-04-08 | 2014-07-23 | 许银亚 | Rosemary liquid mosquito-repellent incense |
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2016
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| CN101558767A (en) * | 2009-05-12 | 2009-10-21 | 江西山峰日化有限公司 | Composition for driving and killing mosquitoes and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109805033A (en) * | 2019-01-16 | 2019-05-28 | 佛山市南海添惠日化有限公司 | A kind of tea tree ethereal oil mosquito liquid |
| CN110037020A (en) * | 2019-03-21 | 2019-07-23 | 佛山市南海添惠日化有限公司 | A kind of tea tree ethereal oil mosquito liquid |
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| CN105724445B (en) | 2018-06-19 |
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Effective date of registration: 20210715 Address after: 322000 No.212, Shenzhou Road, Houzhai Industrial Zone, Yiwu City, Jinhua City, Zhejiang Province Patentee after: ZHEJIANG LANJIAN BIOTECHNOLOGY Co.,Ltd. Address before: 311825 Zhejiang, Shaoxing, Zhuji, Zhuji City pat Tun Town, Keng West Village, No. 199 Patentee before: Xu Yinya |