CN105519600B - Lemon vaporizer mosquito liquid and preparation method thereof - Google Patents
Lemon vaporizer mosquito liquid and preparation method thereof Download PDFInfo
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- CN105519600B CN105519600B CN201610058311.2A CN201610058311A CN105519600B CN 105519600 B CN105519600 B CN 105519600B CN 201610058311 A CN201610058311 A CN 201610058311A CN 105519600 B CN105519600 B CN 105519600B
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- lemon
- mosquito
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- vaporizer
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a kind of lemon vaporizer mosquito liquids and preparation method thereof.The lemon vaporizer mosquito liquid is made of the raw material of following weight parts：0.5 2.5 parts of dimefluthrins, 0.1 0.5 parts of lemons, 50 60 parts of butyls, 0.05 0.15 part of 4 cumene sodium sulfonate, 0.1 0.5 parts of synergist, 0.1 0.5 parts of antioxidant, 35 45 parts of water.The lemon vaporizer mosquito liquid of the present invention, the pure and fresh fragrance of taste kill effect to mosquito with stronger, it is a kind of environment-friendly liquid mosquito-repellent incense, it is powerful with drug effect, safety is non-combustible, volatilization is stablized, moreover it is possible to reduce indoor organic volatile matter content, be the ideal chose of healthy home life.
Description
Technical field：
The present invention relates to a kind of mosquito-repellent incenses, and in particular to a kind of lemon vaporizer mosquito liquid and preparation method thereof.
Background technology：
Mosquito is a kind of worldwide sanitary insect pest, its all one's life passes through ovum, larva, pupa, four periods of adult.Mosquito is main
Be to be that it is one of communication media of infectious disease.It was found that the disease of mosquitoes spread is up to as many as more than 80 kinds.In the whole world, about
There are 1,200,000 people to infect filariasis.The disease of the mosquito meeting infectious disease toxicity of most of kind, including yellow fever, dengue fever, Japan
Encephalitis, St. Louis encephalitis, polyarthirtis, Rift Valley fever (Rift Valley fever), contract elder brother Gen Yare and West Nile
Heat.On earth, then without which kind of animal than mosquito there is the harm of bigger to the mankind.It can be seen that mosquito has seriously threatened the mankind
Health only drives these disgusting mosquitoes, could control epidemic infectious diseases, could ensure human health, improves people
Quality of life.
For many years, people develop and have used a large amount of hygienic insecticide product, are used for killing mosquitoes.Mosquito-repellent incense is most ancient
Natural drug mosquito repellent method.Just there is culicifuge incense stick made of Chinese medicine early in Southern Song Dynasty's period.In modern mosquito-repellent incense containing effectively at
It is pyrethrins to divide, it plays the role of mosquito.After burning mosquito incense, pyrethrins in mosquito-repellent incense is evaporated with smog,
Send out in indoor air, make the neural paralysis of mosquito, then mosquito or it is born get killed or four dissipate escape, to play drive
The current mosquito-repellent incense production industry insecticidal active ingredient of effect of mosquito-killing, mainly cypermethrin, Prallethrin, allethrin, life
The pyrethrins such as object pyrethroids, the nerve that can benumb mosquito cause its death.
Electric liquid device is actually mosquito liquid and makes the general name for the electronic thermostatic heater that liquid uniformly volatilizees, preceding
Person claims mosquito repellent liquid, the latter to claim electric heater.In electric liquid device work, after electric heater accesses power supply, PTCR elements are just
Fever is started to warm up, the PTCR elements temp regulating function of itself is relied on later, its temperature is made to remain certain value.PTCR members
The heat that part generates is volatilized core by radiant heat transfer to liquid, is drawn to from medicinal liquid bottle liquid by volatilization core capillarity
Plug upper end makes liquid be improved under heat radiation heating and is vaporized speed, after the insecticidal active ingredient in space reaches a certain concentration,
Just mosquito is generated and is driven, to knock down and kill mosquito.Electric liquid device because its using it is light, smokelessly without dust, drug effect
It the features such as stabilization, high-efficiency low-toxicity, is welcome by consumer.
Existing electric liquid device formula system is with alkane solvent, pyrethroid, antioxidant and essence etc. for group
Point, form homogeneous system by mixing, stirring solvent.For alkane solvent due to being the formation such as rectifying, carbochain is distributed more widely, especially
It is that wherein low-carbon paraffin easily forms organic volatile i.e. VOC, in the daily home life of consumer, electric heating liquid mosquito can be passed through
Fragrant heating brings certain influence using the pollution for causing domestic environment with volatilization naturally to consumer health.
The present invention provides a kind of lemon vaporizer mosquito liquids, are a kind of vaporizer mosquito liquids of safety and environmental protection.
Invention content：
For deficiencies of the prior art, the first technical problem to be solved by the present invention is to provide a kind of lemon
Essential oil vaporizer mosquito liquid.
The first technical problem to be solved by the present invention is to provide the preparation method of above-mentioned lemon vaporizer mosquito liquid.
The technical problem of the present invention, is achieved by following technical proposals：
A kind of lemon vaporizer mosquito liquid, is made of the raw material of following weight parts：0.5-2.5 parts of dimefluthrins,
0.1-0.5 parts of lemons, 50-60 parts of butyls, 0.05-0.15 parts of 4- cumene sodium sulfonates, 0.1-0.5 parts of synergy
Agent, 0.1-0.5 parts of antioxidant, 35-45 parts of water.
Preferably, the synergist is alantolactone and/or menthalactone.
It is highly preferred that the synergist is made of 40-60wt% alantolactones and 40-60wt% menthalactones.
Preferably, the antioxidant is 2,4- dimethyl -6- tert-butyl phenols and/or 2,6- di-t-butyl -4- methyl
Phenol.
It is highly preferred that the antioxidant is by 40-60wt%2,4- dimethyl -6- tert-butyl phenols and 40-60wt%2,
6- di-tert-butyl-4-methy phenols form.
The present invention also provides the preparation method of above-mentioned lemon vaporizer mosquito liquid, by dimefluthrin, lemon,
Butyl, synergist, antioxidant are uniformly mixed, and add that 4- cumene sodium sulfonates are uniformly mixed, to be eventually adding water mixed
It closes uniform.
Specifically, in the present invention：
Dimefluthrin, No. CAS：271241-14-6.
Lemon, i.e. lemon oil, No. CAS：8008-56-8.
Butyl, No. CAS：112-34-5.
4- cumene sodium sulfonates, No. CAS：32073-22-6.
Alantolactone, No. CAS：546-43-0.
Menthalactone, No. CAS：13341-72-5.
2,4- dimethyl -6- tert-butyl phenols, No. CAS：1879-09-0.
2,6- di-tert-butyl-4-methy phenols, No. CAS：128-37-0.
The lemon vaporizer mosquito liquid of the present invention, the pure and fresh fragrance of taste kill effect with stronger to mosquito, are a kind of
Environment-friendly liquid mosquito-repellent incense, powerful with drug effect, safe non-combustible, volatilization are stablized, moreover it is possible to indoor organic volatile matter content is reduced,
It is the ideal chose of healthy home life.
Specific implementation mode：
With reference to embodiment, the present invention is described further, as described below, is only the preferable implementation to the present invention
Example, not limits the present invention, any person skilled in the art is possibly also with the disclosure above
Technology contents be changed to the equivalent embodiment changed on an equal basis.Without departing from the concept of the present invention, according to the present invention
Technical spirit any simple modification that following embodiment is made or equivalent variations, all fall in protection scope of the present invention.
Embodiment 1
Lemon vaporizer mosquito liquid raw material (parts by weight)：1.2 parts of dimefluthrins, 0.2 part of lemon, 55 parts of diethyls
Glycol butyl ether, 0.1 part of 4- cumene sodium sulfonate, 0.3 part of synergist, 0.3 part of antioxidant, 40 parts of deionized waters.
The synergist is uniformly mixed by 50wt% alantolactones and 50wt% menthalactones and is obtained.
The antioxidant is by 50wt%2,4- dimethyl -6- tert-butyl phenols and 50wt%2,6- di-t-butyl -4- first
Base phenol is uniformly mixed and obtains.
The preparation method of lemon vaporizer mosquito liquid：
Dimefluthrin, lemon, butyl, synergist, antioxidant are mixed and stirred for uniformly, then added
Enter 4- cumene sodium sulfonates be mixed and stirred for uniformly, be eventually adding deionized water and be mixed and stirred for uniformly.Obtain the lemon of embodiment 1
Lemon essential oil vaporizer mosquito liquid.
Embodiment 2
It is substantially the same manner as Example 1, it differs only in：The synergist is only alantolactone.Obtain embodiment 2
Lemon vaporizer mosquito liquid.
Embodiment 3
It is substantially the same manner as Example 1, it differs only in：The synergist is only menthalactone.Obtain embodiment 3
Lemon vaporizer mosquito liquid.
Embodiment 4
It is substantially the same manner as Example 1, it differs only in：The antioxidant is only 2,4- dimethyl -6- tert-butyl benzenes
Phenol.Obtain the lemon vaporizer mosquito liquid of embodiment 4.
Embodiment 5
It is substantially the same manner as Example 1, it differs only in：The antioxidant is only 2,6- di-t-butyl -4- methylbenzenes
Phenol.Obtain the lemon vaporizer mosquito liquid of embodiment 5.
Test case 1
Indoor harmacological effect test is carried out to the lemon vaporizer mosquito liquid of embodiment 1-5, is defended using GB18418-2009 households
Raw desinsection articles for use electric liquid device standard, is tested.In the standard, KT50 values (boxing method)≤10 minute can be judged to
Qualification, the time is shorter, and explanation is better to mosquito driving and killing effect, and test data is shown in Table 1.
Table 1：Vaporizer mosquito liquid indoor harmacological effect table (boxing method)
| KT50 values | |
| Embodiment 1 | 3 points 31 seconds |
| Embodiment 2 | 5 points 53 seconds |
| Embodiment 3 | 6 points 06 second |
| Embodiment 4 | 5 points 19 seconds |
| Embodiment 5 | 5 points 32 seconds |
Comparing embodiment 1-3, embodiment 1 (alantolactone, menthalactone compounding) mosquito driving and killing effect, hence it is evident that better than real
Apply a 2-3 (single raw material in alantolactone, menthalactone)；Comparing embodiment 1 and embodiment 4-5, embodiment 1 (2,4- bis-
Methyl-6-tert-butylphenol, 2,6- di-tert-butyl-4-methy phenols compounding) mosquito driving and killing effect, hence it is evident that it is better than embodiment 4-5
(single raw material in 2,4 dimethyl 6 tert butyl phenol, 2,6 di tert butyl 4 methyl phenol).
Test case 2
Toxotest is carried out to the lemon vaporizer mosquito liquid of embodiment 1-5, with reference to health ministry《Management of occupational acute
Learn object Poisoning disease in the blood system diagnostic criteria》And《Technological guidance's principle that Chinese medicine, natural drug immunotoxicity are studied》Mark
Standard formulates test case of the present invention.
Test type：Two young age small white mouses.
Experimental method：
(1) experiment condition：Laboratory temperature (27 ± 2) DEG C
(2) experimental provision：In two 25 square metres of mutually synthermal laboratories, each one size same size of placement
80 × 80 × 80cm is fine and closely woven ventilative netted to be shrouded.
(3) experimental procedure：Two young age small white mouses are separated respectively be put in two laboratories it is netted shroud in, and be divided into pair
According to group and mosquito-repellent incense group of the present invention is smoked, gives respectively and does not smoke mosquito-repellent incense of the present invention and smoke mosquito-repellent incense of the present invention, measure young age small white mouse weight,
The biochemical index of observation hematology, changes in histopathology and stopping smoke the recovery situation etc. after mosquito-repellent incense of the present invention.Place this hair
When bright mosquito-repellent incense will be mounted on it is netted shroud it is interior from 30 centimeters of bottom.Dosage：Electrical heating mosquito-repellent incense, keeps for a long time making for 24 hours
With.Time：The present invention is used for a long time in continuous use one month, observation control group and the young age small white mouse for smoking mosquito-repellent incense group of the present invention
Toxicity and side effect of the mosquito-repellent incense to young age small white mouse.Cleaning：Cleaning in two days is primary in shrouding.
As a result：After two young age small white mouse blood tests, every biochemical indicator is normal, shows mosquito-repellent incense of the present invention to children
Age small white mouse has no toxic side effect, and when interior mosquito-repellent incense smog is too dense within only more than 24 hours, need to open a window ventilation 10-15 minutes, blood drawing
Two young age small white mouses is not given to feed within first 8 hours.
Conclusion：Mosquito-repellent incense of the present invention is used for a long time to young age small white mouse without any toxicity.
Test case 3
Acute oral toxicity test, 5 minutes activities in rats after contamination are carried out to the lemon vaporizer mosquito liquid of embodiment 1-5
Increasing, continues 2 minutes or so, activity switchs to normally, and diet is normal, and the observation period is more than 5000 mgs/kg without death, LD50,
Belong to practical nontoxic.
Test case 4
Acute inhalation toxicity experiment, rat diet activity after contamination are carried out to the lemon vaporizer mosquito liquid of embodiment 1-5
No abnormality seen, observation period are more than 10 grams/cubic metre without death, LD50, belong to practical nontoxic.
Test case 5
Skin patch test, experimental group erythema and oedema shape are carried out to the lemon vaporizer mosquito liquid of embodiment 1-5
It is 0 at the sum of scoring, explanation has no stimulation of the skin.
Test case 6
Eye irritant test is carried out to the lemon vaporizer mosquito liquid of embodiment 1-5, the acute Eye irritation of experimental group integrates number
It is 0, illustrates to have no stimulation to mucous membrane.
Claims (4)
1. a kind of lemon vaporizer mosquito liquid, which is characterized in that be made of the raw material of following weight parts：0.5-2.5 parts of tetrafluoro first
Ethofenprox, 0.1-0.5 part lemon, 50-60 parts of butyls, 0.05-0.15 parts of 4- cumene sodium sulfonates, 0.1-
0.5 part of synergist, 0.1-0.5 parts of antioxidant, 35-45 parts of water；
The synergist is made of 40-60wt% alantolactones and 40-60wt% menthalactones.
2. lemon vaporizer mosquito liquid as described in claim 1, it is characterised in that：The antioxidant is 2,4- dimethyl-
6- tert-butyl phenols and/or 2,6 di tert butyl 4 methyl phenol.
3. lemon vaporizer mosquito liquid as claimed in claim 2, it is characterised in that：The antioxidant by 40-60wt%2,
4- dimethyl -6- tert-butyl phenols and 40-60wt%2,6- di-tert-butyl-4-methy phenols composition.
4. the preparation method of lemon vaporizer mosquito liquid as described in any one of claim 1-3, it is characterised in that：By tetrafluoro first
Ethofenprox, lemon, butyl, synergist, antioxidant are uniformly mixed, and it is equal to add the mixing of 4- cumene sodium sulfonates
It is even, be eventually adding water be uniformly mixed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610058311.2A CN105519600B (en) | 2016-01-28 | 2016-01-28 | Lemon vaporizer mosquito liquid and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610058311.2A CN105519600B (en) | 2016-01-28 | 2016-01-28 | Lemon vaporizer mosquito liquid and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105519600A CN105519600A (en) | 2016-04-27 |
| CN105519600B true CN105519600B (en) | 2018-07-13 |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101558767A (en) * | 2009-05-12 | 2009-10-21 | 江西山峰日化有限公司 | Composition for driving and killing mosquitoes and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
-
2016
- 2016-01-28 CN CN201610058311.2A patent/CN105519600B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101558767A (en) * | 2009-05-12 | 2009-10-21 | 江西山峰日化有限公司 | Composition for driving and killing mosquitoes and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
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| Publication number | Publication date |
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| CN105519600A (en) | 2016-04-27 |
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