CN105724374B - Geranium Essential vaporizer mosquito liquid and preparation method thereof - Google Patents
Geranium Essential vaporizer mosquito liquid and preparation method thereof Download PDFInfo
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- CN105724374B CN105724374B CN201610058738.2A CN201610058738A CN105724374B CN 105724374 B CN105724374 B CN 105724374B CN 201610058738 A CN201610058738 A CN 201610058738A CN 105724374 B CN105724374 B CN 105724374B
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- 241000255925 Diptera Species 0.000 title claims abstract description 51
- 239000007788 liquid Substances 0.000 title claims abstract description 40
- 241000208152 Geranium Species 0.000 title claims abstract description 32
- 239000006200 vaporizer Substances 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 14
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 14
- COBPKKZHLDDMTB-UHFFFAOYSA-N 2-[2-(2-butoxyethoxy)ethoxy]ethanol Chemical compound CCCCOCCOCCOCCO COBPKKZHLDDMTB-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- QUCDWLYKDRVKMI-UHFFFAOYSA-M sodium;3,4-dimethylbenzenesulfonate Chemical compound [Na+].CC1=CC=C(S([O-])(=O)=O)C=C1C QUCDWLYKDRVKMI-UHFFFAOYSA-M 0.000 claims description 8
- 229940048842 sodium xylenesulfonate Drugs 0.000 claims description 7
- 150000002989 phenols Chemical class 0.000 claims description 6
- KVIZNNVXXNFLMU-AIIUZBJTSA-N [2,3,5,6-tetrafluoro-4-(methoxymethyl)phenyl]methyl (1r,3r)-2,2-dimethyl-3-[(e)-prop-1-enyl]cyclopropane-1-carboxylate Chemical compound FC1=C(F)C(COC)=C(F)C(F)=C1COC(=O)[C@H]1C(C)(C)[C@@H]1\C=C\C KVIZNNVXXNFLMU-AIIUZBJTSA-N 0.000 claims description 5
- -1 Benzyl Flumethrin Chemical compound 0.000 claims description 3
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 claims description 2
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical class OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 2
- RFXSFVVPCLGHAU-UHFFFAOYSA-N benzene;phenol Chemical group C1=CC=CC=C1.OC1=CC=CC=C1.OC1=CC=CC=C1 RFXSFVVPCLGHAU-UHFFFAOYSA-N 0.000 claims 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims 1
- 239000000077 insect repellent Substances 0.000 abstract description 19
- 230000000694 effects Effects 0.000 abstract description 8
- 230000000857 drug effect Effects 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 2
- 229910052708 sodium Inorganic materials 0.000 abstract description 2
- 239000011734 sodium Substances 0.000 abstract description 2
- 238000012360 testing method Methods 0.000 description 13
- PXOYOCNNSUAQNS-AGNJHWRGSA-N alantolactone Chemical group C1[C@H]2OC(=O)C(=C)[C@H]2C=C2[C@@H](C)CCC[C@@]21C PXOYOCNNSUAQNS-AGNJHWRGSA-N 0.000 description 11
- BGEBZHIAGXMEMV-UHFFFAOYSA-N 5-methoxypsoralen Chemical compound O1C(=O)C=CC2=C1C=C1OC=CC1=C2OC BGEBZHIAGXMEMV-UHFFFAOYSA-N 0.000 description 6
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- JZODKRWQWUWGCD-UHFFFAOYSA-N 2,5-di-tert-butylbenzene-1,4-diol Chemical class CC(C)(C)C1=CC(O)=C(C(C)(C)C)C=C1O JZODKRWQWUWGCD-UHFFFAOYSA-N 0.000 description 5
- PXOYOCNNSUAQNS-UHFFFAOYSA-N alantolactone Natural products C1C2OC(=O)C(=C)C2C=C2C(C)CCCC21C PXOYOCNNSUAQNS-UHFFFAOYSA-N 0.000 description 5
- 239000003814 drug Substances 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 230000002147 killing effect Effects 0.000 description 4
- 239000002728 pyrethroid Substances 0.000 description 4
- 208000035473 Communicable disease Diseases 0.000 description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 3
- VXSIXFKKSNGRRO-MXOVTSAMSA-N [(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate;[(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-3-[(e)-3-methoxy-2-methyl-3-oxoprop-1-enyl Chemical group CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1.CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VXSIXFKKSNGRRO-MXOVTSAMSA-N 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 description 3
- 229940070846 pyrethrins Drugs 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 231100000419 toxicity Toxicity 0.000 description 3
- 230000001988 toxicity Effects 0.000 description 3
- 239000000341 volatile oil Substances 0.000 description 3
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 2
- 241000208181 Pelargonium Species 0.000 description 2
- 241000700159 Rattus Species 0.000 description 2
- 208000000705 Rift Valley Fever Diseases 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000001154 acute effect Effects 0.000 description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000037213 diet Effects 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 208000015181 infectious disease Diseases 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 239000002917 insecticide Substances 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- ZCVAOQKBXKSDMS-AQYZNVCMSA-N (+)-trans-allethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(CC=C)C(=O)C1 ZCVAOQKBXKSDMS-AQYZNVCMSA-N 0.000 description 1
- WIXDSJRJFDWTNY-UHFFFAOYSA-N 1,3-ditert-butyl-5-methylbenzene Chemical class CC1=CC(C(C)(C)C)=CC(C(C)(C)C)=C1 WIXDSJRJFDWTNY-UHFFFAOYSA-N 0.000 description 1
- FMTFEIJHMMQUJI-NJAFHUGGSA-N 102130-98-3 Natural products CC=CCC1=C(C)[C@H](CC1=O)OC(=O)[C@@H]1[C@@H](C=C(C)C)C1(C)C FMTFEIJHMMQUJI-NJAFHUGGSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 239000005946 Cypermethrin Substances 0.000 description 1
- 208000001490 Dengue Diseases 0.000 description 1
- 206010012310 Dengue fever Diseases 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- 206010015946 Eye irritation Diseases 0.000 description 1
- 201000006353 Filariasis Diseases 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- KVIZNNVXXNFLMU-AATRIKPKSA-N Metofluthrin Chemical compound FC1=C(F)C(COC)=C(F)C(F)=C1COC(=O)C1C(C)(C)C1\C=C\C KVIZNNVXXNFLMU-AATRIKPKSA-N 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 206010033799 Paralysis Diseases 0.000 description 1
- 208000005374 Poisoning Diseases 0.000 description 1
- 241000382353 Pupa Species 0.000 description 1
- 206010041896 St. Louis Encephalitis Diseases 0.000 description 1
- 208000003152 Yellow Fever Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 231100000921 acute inhalation toxicity Toxicity 0.000 description 1
- 231100000460 acute oral toxicity Toxicity 0.000 description 1
- 229940024113 allethrin Drugs 0.000 description 1
- 238000009534 blood test Methods 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 235000010354 butylated hydroxytoluene Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 229960005424 cypermethrin Drugs 0.000 description 1
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 208000025729 dengue disease Diseases 0.000 description 1
- 239000007933 dermal patch Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 206010014599 encephalitis Diseases 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 231100000013 eye irritation Toxicity 0.000 description 1
- 238000003197 gene knockdown Methods 0.000 description 1
- 230000007688 immunotoxicity Effects 0.000 description 1
- 231100000386 immunotoxicity Toxicity 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 230000001537 neural effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- SMKRKQBMYOFFMU-UHFFFAOYSA-N prallethrin Chemical compound CC1(C)C(C=C(C)C)C1C(=O)OC1C(C)=C(CC#C)C(=O)C1 SMKRKQBMYOFFMU-UHFFFAOYSA-N 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Pest Control & Pesticides (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
The invention discloses a kind of Geranium Essential vaporizer mosquito liquid and preparation method thereof.The Geranium Essential vaporizer mosquito liquid is made up of the raw material of following weight parts：0.5 2.5 parts of metofluthrins, 0.1 0.5 parts of Geranium Essentials, 50 60 parts of triethylene glycol butyl ether, 0.05 0.15 parts of sodium xylene sulfonates, 0.1 0.5 parts of synergist, 0.1 0.5 parts of antioxidant, 35 45 parts of water.The Geranium Essential vaporizer mosquito liquid of the present invention, the pure and fresh fragrance of taste, effect is killed with stronger to mosquito, it is a kind of environment-friendly liquid mosquito-repellent incense, it has that drug effect is powerful, safety is non-combustible, volatilization is stable, moreover it is possible to reduces indoor organic volatile matter content, is the ideal chose of healthy life staying idle at home.
Description
Technical field：
The present invention relates to a kind of mosquito-repellent incense, and in particular to a kind of Geranium Essential vaporizer mosquito liquid and preparation method thereof.
Background technology：
Mosquito is a kind of worldwide sanitary insect pest, and its all one's life passes through ovum, larva, pupa, four periods of adult.Mosquito is main
Be to be that it is one of communication media of infectious disease.It was found that the disease of mosquitoes spread is up to as many as kind more than 80.In the whole world, about
There are 1,200,000 people to infect filariasis.The disease of the mosquito meeting infectious disease toxicity of most of kind, including yellow fever, dengue fever, Japan
Encephalitis, St. Louis encephalitis, polyarthirtis, Rift Valley fever (Rift Valley fever), contract elder brother Gen Yare and West Nile
Heat.On earth, then without which kind of animal than mosquito there is bigger harm to the mankind.The mosquito serious threat mankind as can be seen here
Health, these disgusting mosquitoes are only driven, epidemic infectious diseases could be controlled, human health could be ensured, improve people
Quality of life.
For many years, people develop and have used substantial amounts of hygienic insecticide product, for killing mosquitoes.Mosquito-repellent incense is most ancient
Natural drug mosquito repellent method.Just there is culicifuge incense rod made of Chinese medicine early in Southern Song Dynasty's period.In modern mosquito-repellent incense containing effectively into
It is pyrethrins to divide, and it plays the role of mosquito.After burning mosquito incense, pyrethrins in mosquito-repellent incense evaporates with smog,
Send out in the air of interior, make the neural paralysis of mosquito, then mosquito or it is born get killed, or four dissipate and escape, and are driven so as to play
The current mosquito-repellent incense production industry insecticidal active ingredient of effect of mosquito-killing, mainly cypermethrin, Prallethrin, allethrin, life
The pyrethrins such as thing chrysanthemum ester, the nerve that can benumb mosquito cause it dead.
Electric liquid device is actually mosquito liquid and the general name for making the electronic thermostatic heater that decoction uniformly volatilizees, preceding
Person claims mosquito-driving liquid, and the latter claims electric heater.In electric liquid device work, after electric heater accesses power supply, PTCR elements are just
Heating is started to warm up, afterwards by the PTCR elements temp regulating function of itself, its temperature is remained certain value.PTCR members
Heat caused by part is volatilized core by radiant heat transfer to decoction, is drawn to from medicinal liquid bottle decoction by core capillarity of volatilizing
Plug upper end, decoction is improved under heat radiation heating and be vaporized speed, after the insecticidal active ingredient in space reaches finite concentration,
Just mosquito is produced and driven, so as to knock down and kill mosquito.Electric liquid device because its using it is light, smokelessly without dust, drug effect
The features such as stabilization, high-efficiency low-toxicity, welcome by consumer.
Existing electric liquid device formula system is with alkane solvent, pyrethroid, antioxidant and essence etc. for group
Point, form homogeneous system by mixing, stirring solvent.Alkane solvent is due to being that rectifying etc. is formed, and its carbochain is distributed more widely, especially
It is that wherein low-carbon paraffin easily forms organic volatile i.e. VOC, in the daily life staying idle at home of consumer, electric heating liquid mosquito can be passed through
Fragrant heating brings certain influence using the pollution that domestic environment is caused with volatilization naturally to consumer health.
The invention provides a kind of Geranium Essential vaporizer mosquito liquid, is a kind of vaporizer mosquito liquid of safety and environmental protection.
The content of the invention：
For deficiencies of the prior art, one of the technical problems to be solved by the invention are to provide a kind of India
Certain herbaceous plants with big flowers essential oil vaporizer mosquito liquid.
One of technical problems to be solved by the invention are to provide the preparation method of above-mentioned Geranium Essential vaporizer mosquito liquid.
The technical problem of the present invention, is achieved by following technical proposals：
A kind of Geranium Essential vaporizer mosquito liquid, is made up of the raw material of following weight parts：0.5-2.5 parts metofluthrin,
0.1-0.5 parts Geranium Essential, 50-60 part triethylene glycols butyl ether, 0.05-0.15 parts sodium xylene sulfonate, 0.1-0.5 part synergy
Agent, 0.1-0.5 parts antioxidant, 35-45 part water.
Preferably, described synergist is alantolactone and/or majudin.
It is highly preferred that described synergist is made up of 40-60wt% alantolactones and 40-60wt% majudins.
Preferably, described antioxidant is 2,6- di-tert-butyl-4-methy phenols and/or 2,5- di-t-butyl to benzene two
Phenol.
It is highly preferred that described antioxidant is by 40-60wt%2,6- di-tert-butyl-4-methy phenols and 40-60wt%2,
5- di-tert-butyl hydroquinones form.
Present invention also offers the preparation method of above-mentioned Geranium Essential vaporizer mosquito liquid, by metofluthrin, fish pelargonium
Essential oil, triethylene glycol butyl ether, synergist, antioxidant are well mixed, and are added sodium xylene sulfonate and are well mixed, are eventually adding water
It is well mixed.
Specifically, in the present invention：
Metofluthrin, No. CAS：240494-70-6.
Geranium Essential, i.e. pelargonium oil, No. CAS：8000-46-2.
Triethylene glycol butyl ether, No. CAS：143-22-6.
Sodium xylene sulfonate, Chinese nickname：3,5- acid dimethyl sodium, No. CAS：1300-72-7.
Alantolactone, No. CAS：546-43-0.
Majudin, No. CAS：484-20-8.
2,6- di-tert-butyl-4-methy phenols, No. CAS：128-37-0.
2,5- di-tert-butyl hydroquinones, No. CAS：88-58-4.
The Geranium Essential vaporizer mosquito liquid of the present invention, the pure and fresh fragrance of taste, effect is killed with stronger to mosquito, is one
Kind environment-friendly liquid mosquito-repellent incense, it has, and drug effect is powerful, safety is non-combustible, volatilization is stable, moreover it is possible to reduces indoor organic volatile matter and contains
Amount, it is the ideal chose of healthy life staying idle at home.
Embodiment：
With reference to embodiment, the present invention is described further, as described below, is only the preferable implementation to the present invention
Example, is not limited the present invention, any person skilled in the art is possibly also with the disclosure above
Technology contents be changed to the equivalent embodiment changed on an equal basis.It is every of the invention without departing from the present invention program content, foundation
Technical spirit any simple modification that following examples are made or equivalent variations, all fall within protection scope of the present invention.
Embodiment 1
Geranium Essential vaporizer mosquito liquid raw material (parts by weight)：1.2 parts of metofluthrins, 0.2 part of Geranium Essential, 55 parts
Triethylene glycol butyl ether, 0.1 part of sodium xylene sulfonate, 0.3 part of synergist, 0.3 part of antioxidant, 40 parts of deionized waters.
Described synergist is obtained by 50wt% alantolactones and 50wt% majudins are well mixed.
Described antioxidant is by 50wt%2,6- di-tert-butyl-4-methy phenols and 50wt%2,5- di-t-butyls to benzene two
Phenol is well mixed to be obtained.
The preparation method of Geranium Essential vaporizer mosquito liquid：
Metofluthrin, Geranium Essential, triethylene glycol butyl ether, synergist, antioxidant are mixed and stirred for uniformly, then
Add sodium xylene sulfonate be mixed and stirred for uniformly, be eventually adding deionized water and be mixed and stirred for uniformly.Obtain the day of embodiment 1
Zhu Kui essential oil vaporizer mosquito liquids.
Embodiment 2
It is substantially the same manner as Example 1, differ only in：Described synergist is only alantolactone.Obtain embodiment 2
Geranium Essential vaporizer mosquito liquid.
Embodiment 3
It is substantially the same manner as Example 1, differ only in：Described synergist is only majudin.Obtain embodiment 3
Geranium Essential vaporizer mosquito liquid.
Embodiment 4
It is substantially the same manner as Example 1, differ only in：Described antioxidant is only 2,6- di-t-butyl -4- methylbenzenes
Phenol.Obtain the Geranium Essential vaporizer mosquito liquid of embodiment 4.
Embodiment 5
It is substantially the same manner as Example 1, differ only in：Described antioxidant is only 2,5 di tert butyl hydroquinone.
Obtain the Geranium Essential vaporizer mosquito liquid of embodiment 5.
Test case 1
Indoor harmacological effect test is carried out to embodiment 1-5 Geranium Essential vaporizer mosquito liquid, using GB18418-2009 family expenses
Sanitary insecticide article electric liquid device standard, is tested.In the standard, KT50 values (boxing method)≤10 minute can be sentenced
To be qualified, the time is shorter, and explanation is better to mosquito driving and killing effect, and test data is shown in Table 1.
Table 1：Vaporizer mosquito liquid indoor harmacological effect table (boxing method)
| KT50 values | |
| Embodiment 1 | 4 points 13 seconds |
| Embodiment 2 | 7 points 02 second |
| Embodiment 3 | 6 points 50 seconds |
| Embodiment 4 | 6 points 24 seconds |
| Embodiment 5 | 6 points 33 seconds |
Comparing embodiment 1-3, embodiment 1 (alantolactone, majudin compounding) mosquito driving and killing effect, hence it is evident that be better than
Embodiment 2-3 (single raw material in alantolactone, majudin)；Comparing embodiment 1 and embodiment 4-5, embodiment 1 (2,
6- di-tert-butyl-4-methy phenols, 2,5- di-tert-butyl hydroquinones compounding) mosquito driving and killing effect, hence it is evident that better than embodiment 4-5
(single raw material in 2,6 di tert butyl 4 methyl phenol, 2,5 di tert butyl hydroquinone).
Test case 2
Toxotest is carried out to embodiment 1-5 Geranium Essential vaporizer mosquito liquid, with reference to health ministry《Management of occupational acute
Chemicals Poisoning disease in the blood system diagnostic criteria》And《Chinese medicine, technological guidance's principle of natural drug immunotoxicity research》
Standard, formulate test case of the present invention.
Test species：Two young age small white mouses.
Experimental method：
(1) experiment condition：Laboratory temperature (27 ± 2) DEG C
(2) experimental provision：In two 25 square metres of mutually synthermal laboratories, each one size same size of placement
80 × 80 × 80cm is fine and closely woven ventilative netted to be shrouded.
(3) experimental procedure：By two young age small white mouses be separately respectively put in two laboratories it is netted shroud in, and be divided into pair
According to group and mosquito-repellent incense group of the present invention is smoked, gives respectively and does not smoke mosquito-repellent incense of the present invention and smoke mosquito-repellent incense of the present invention, measure young age small white mouse body weight,
The biochemical index of observation hematology, changes in histopathology and stopping smoke recovery situation after mosquito-repellent incense of the present invention etc..Place this hair
During bright mosquito-repellent incense will be arranged on it is netted shroud it is interior from the centimeters of bottom 30.Dosage：Electrical heating mosquito-repellent incense, keeps for a long time making for 24 hours
With.Time：Continuous use one month, observation control group and the young age small white mouse for smoking mosquito-repellent incense group of the present invention, long-term use of present invention
Toxicity and side effect of the mosquito-repellent incense to young age small white mouse.Cleaning：Clean once within two days in shrouding.
As a result：After two young age small white mouse blood tests, every biochemical indicator is normal, shows mosquito-repellent incense of the present invention to children
Age small white mouse has no toxic side effect, and when only more than 24 hours, indoor mosquito-repellent incense smog is too dense, need to open a window ventilation 10-15 minutes, blood drawing
Do not fed to two young age small white mouses within first 8 hours.
Conclusion：Long-term use of mosquito-repellent incense of the present invention is to young age small white mouse without any toxicity.
Test case 3
Acute oral toxicity test is carried out to embodiment 1-5 Geranium Essential vaporizer mosquito liquid, 5 minutes rats live after contamination
Dynamic increase, continues 2 minutes or so, and activity switchs to normally, and diet is normal, and the observation period, LD50 was more than 5000 milligrams/public affairs without death
Jin, belong to actual nontoxic.
Test case 4
Acute inhalation toxicity experiment is carried out to embodiment 1-5 Geranium Essential vaporizer mosquito liquid, rat diet is lived after contamination
Dynamic no abnormality seen, observation period are more than 10 grams/cubic metre without death, LD50, belong to actual nontoxic.
Test case 5
Skin patch test, experimental group erythema and oedema are carried out to embodiment 1-5 Geranium Essential vaporizer mosquito liquid
It is 0 to form scoring sum, and explanation has no stimulation of the skin.
Test case 6
Eye irritant test, the acute Eye irritation integration branch of experimental group are carried out to embodiment 1-5 Geranium Essential vaporizer mosquito liquid
Number is 0, illustrates to have no stimulation to mucous membrane.
Claims (2)
1. a kind of Geranium Essential vaporizer mosquito liquid, it is characterised in that be made up of the raw material of following weight parts：0.5-2.5 part methoxies
Benzyl Flumethrin, 0.1-0.5 parts Geranium Essential, 50-60 part triethylene glycols butyl ether, 0.05-0.15 parts sodium xylene sulfonate, 0.1-
0.5 part of synergist, 0.1-0.5 parts antioxidant, 35-45 part water；
Described synergist is made up of 40-60wt% alantolactones and 40-60wt% majudins；
Described antioxidant is by 40-60wt%2,6- di-tert-butyl-4-methy phenols and 40-60wt%2,5- di-t-butyls to benzene
Diphenol forms.
2. the preparation method of Geranium Essential vaporizer mosquito liquid as claimed in claim 1, it is characterised in that：By metofluthrin,
Geranium Essential, triethylene glycol butyl ether, synergist, antioxidant are well mixed, and it is well mixed, last to add sodium xylene sulfonate
Water is added to be well mixed.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101558767A (en) * | 2009-05-12 | 2009-10-21 | 江西山峰日化有限公司 | Composition for driving and killing mosquitoes and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
| CN103704279A (en) * | 2013-12-13 | 2014-04-09 | 青岛安信医疗器械有限公司 | Electric heated liquid mosquito-repellent incense |
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| JPH04145076A (en) * | 1990-10-05 | 1992-05-19 | Morishita Jintan Kk | Preventive for anisakiasis |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101558767A (en) * | 2009-05-12 | 2009-10-21 | 江西山峰日化有限公司 | Composition for driving and killing mosquitoes and preparation method thereof |
| CN102742572A (en) * | 2012-07-27 | 2012-10-24 | 广州立白企业集团有限公司 | Water-based electric heating liquid mosquito-repellent incense and preparation method thereof |
| CN103704279A (en) * | 2013-12-13 | 2014-04-09 | 青岛安信医疗器械有限公司 | Electric heated liquid mosquito-repellent incense |
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