CN105454329B - Oil of Cymbopogon winterianus vaporizer mosquito liquid and preparation method thereof - Google Patents
Oil of Cymbopogon winterianus vaporizer mosquito liquid and preparation method thereof Download PDFInfo
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- CN105454329B CN105454329B CN201610059331.1A CN201610059331A CN105454329B CN 105454329 B CN105454329 B CN 105454329B CN 201610059331 A CN201610059331 A CN 201610059331A CN 105454329 B CN105454329 B CN 105454329B
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- 241000255925 Diptera Species 0.000 title claims abstract description 53
- 239000007788 liquid Substances 0.000 title claims abstract description 42
- 241000744766 Cymbopogon winterianus Species 0.000 title claims abstract description 35
- 239000006200 vaporizer Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 15
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 15
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- CUYTYLVEYFUAAX-UHFFFAOYSA-N 4-methylbenzenesulfonic acid;sodium Chemical compound [Na].CC1=CC=C(S(O)(=O)=O)C=C1 CUYTYLVEYFUAAX-UHFFFAOYSA-N 0.000 claims abstract description 5
- JZODKRWQWUWGCD-UHFFFAOYSA-N 2,5-di-tert-butylbenzene-1,4-diol Chemical compound CC(C)(C)C1=CC(O)=C(C(C)(C)C)C=C1O JZODKRWQWUWGCD-UHFFFAOYSA-N 0.000 claims description 6
- OPLCSTZDXXUYDU-UHFFFAOYSA-N 2,4-dimethyl-6-tert-butylphenol Chemical class CC1=CC(C)=C(O)C(C(C)(C)C)=C1 OPLCSTZDXXUYDU-UHFFFAOYSA-N 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical class CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- GQNBIMLHUAWKHJ-UHFFFAOYSA-N [4-(methoxymethyl)phenyl]methyl 2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound C1=CC(COC)=CC=C1COC(=O)C1C(C)(C)C1C=C(C)C GQNBIMLHUAWKHJ-UHFFFAOYSA-N 0.000 claims 1
- YREQHYQNNWYQCJ-UHFFFAOYSA-N etofenprox Chemical compound C1=CC(OCC)=CC=C1C(C)(C)COCC1=CC=CC(OC=2C=CC=CC=2)=C1 YREQHYQNNWYQCJ-UHFFFAOYSA-N 0.000 claims 1
- 239000000077 insect repellent Substances 0.000 abstract description 19
- 230000000694 effects Effects 0.000 abstract description 10
- 230000000857 drug effect Effects 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 2
- 239000003921 oil Substances 0.000 description 24
- 238000012360 testing method Methods 0.000 description 13
- PXOYOCNNSUAQNS-AGNJHWRGSA-N alantolactone Chemical group C1[C@H]2OC(=O)C(=C)[C@H]2C=C2[C@@H](C)CCC[C@@]21C PXOYOCNNSUAQNS-AGNJHWRGSA-N 0.000 description 11
- IQVQXVFMNOFTMU-FLIBITNWSA-N (Z)-ligustilide Chemical compound C1CC=CC2=C1C(=C/CCC)/OC2=O IQVQXVFMNOFTMU-FLIBITNWSA-N 0.000 description 6
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- IQVQXVFMNOFTMU-DHZHZOJOSA-N Z-ligustilide Natural products C1CC=CC2=C1C(=C/CCC)\OC2=O IQVQXVFMNOFTMU-DHZHZOJOSA-N 0.000 description 5
- OOWCJRMYMAMSOH-UHFFFAOYSA-N [2,3,5,6-tetrafluoro-4-(methoxymethyl)phenyl]methyl 2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound FC1=C(F)C(COC)=C(F)C(F)=C1COC(=O)C1C(C)(C)C1C=C(C)C OOWCJRMYMAMSOH-UHFFFAOYSA-N 0.000 description 5
- PXOYOCNNSUAQNS-UHFFFAOYSA-N alantolactone Natural products C1C2OC(=O)C(=C)C2C=C2C(C)CCCC21C PXOYOCNNSUAQNS-UHFFFAOYSA-N 0.000 description 5
- 239000003814 drug Substances 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 230000002147 killing effect Effects 0.000 description 4
- 239000002728 pyrethroid Substances 0.000 description 4
- 208000035473 Communicable disease Diseases 0.000 description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 3
- VXSIXFKKSNGRRO-MXOVTSAMSA-N [(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate;[(1s)-2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-3-[(e)-3-methoxy-2-methyl-3-oxoprop-1-enyl Chemical group CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1.CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VXSIXFKKSNGRRO-MXOVTSAMSA-N 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 description 3
- 229940070846 pyrethrins Drugs 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 231100000419 toxicity Toxicity 0.000 description 3
- 230000001988 toxicity Effects 0.000 description 3
- 241000700159 Rattus Species 0.000 description 2
- 208000000705 Rift Valley Fever Diseases 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000001154 acute effect Effects 0.000 description 2
- 150000001335 aliphatic alkanes Chemical class 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 230000037213 diet Effects 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 208000015181 infectious disease Diseases 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- ZCVAOQKBXKSDMS-AQYZNVCMSA-N (+)-trans-allethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(CC=C)C(=O)C1 ZCVAOQKBXKSDMS-AQYZNVCMSA-N 0.000 description 1
- FZSPYHREEHYLCB-UHFFFAOYSA-N 1-tert-butyl-3,5-dimethylbenzene Chemical class CC1=CC(C)=CC(C(C)(C)C)=C1 FZSPYHREEHYLCB-UHFFFAOYSA-N 0.000 description 1
- FMTFEIJHMMQUJI-NJAFHUGGSA-N 102130-98-3 Natural products CC=CCC1=C(C)[C@H](CC1=O)OC(=O)[C@@H]1[C@@H](C=C(C)C)C1(C)C FMTFEIJHMMQUJI-NJAFHUGGSA-N 0.000 description 1
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 1
- -1 4- toluenesulfonic acid sodium salts Chemical class 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 240000004784 Cymbopogon citratus Species 0.000 description 1
- 235000017897 Cymbopogon citratus Nutrition 0.000 description 1
- 239000005946 Cypermethrin Substances 0.000 description 1
- 208000001490 Dengue Diseases 0.000 description 1
- 206010012310 Dengue fever Diseases 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
- 108010000912 Egg Proteins Proteins 0.000 description 1
- 206010015150 Erythema Diseases 0.000 description 1
- 206010015946 Eye irritation Diseases 0.000 description 1
- 201000006353 Filariasis Diseases 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 206010033799 Paralysis Diseases 0.000 description 1
- 208000005374 Poisoning Diseases 0.000 description 1
- 241000382353 Pupa Species 0.000 description 1
- 206010041896 St. Louis Encephalitis Diseases 0.000 description 1
- 208000003152 Yellow Fever Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 231100000921 acute inhalation toxicity Toxicity 0.000 description 1
- 231100000460 acute oral toxicity Toxicity 0.000 description 1
- 229940024113 allethrin Drugs 0.000 description 1
- 238000009534 blood test Methods 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 229960005424 cypermethrin Drugs 0.000 description 1
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 208000025729 dengue disease Diseases 0.000 description 1
- 239000007933 dermal patch Substances 0.000 description 1
- 125000004177 diethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 206010014599 encephalitis Diseases 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 231100000321 erythema Toxicity 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 231100000013 eye irritation Toxicity 0.000 description 1
- 238000003197 gene knockdown Methods 0.000 description 1
- 230000007688 immunotoxicity Effects 0.000 description 1
- 231100000386 immunotoxicity Toxicity 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 230000001537 neural effect Effects 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- SMKRKQBMYOFFMU-UHFFFAOYSA-N prallethrin Chemical compound CC1(C)C(C=C(C)C)C1C(=O)OC1C(C)=C(CC#C)C(=O)C1 SMKRKQBMYOFFMU-UHFFFAOYSA-N 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000004577 thatch Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Environmental Sciences (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Pest Control & Pesticides (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Toxicology (AREA)
- Catching Or Destruction (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of oil of Cymbopogon winterianus vaporizer mosquito liquid and preparation method thereof.The oil of Cymbopogon winterianus vaporizer mosquito liquid is made up of the raw material of following weight parts：0.5 2.5 parts of dimefluthrins, 0.1 0.5 parts of oil of Cymbopogon winterianus, 50 60 parts of butyls, 0.05 0.15 parts of p-methyl benzenesulfonic acid sodium, 0.1 0.5 parts of synergist, 0.1 0.5 parts of antioxidant, 35 45 parts of water.The oil of Cymbopogon winterianus vaporizer mosquito liquid of the present invention, the pure and fresh fragrance of taste, effect is killed with stronger to mosquito, it is a kind of environment-friendly liquid mosquito-repellent incense, it has that drug effect is powerful, safety is non-combustible, volatilization is stable, moreover it is possible to reduces indoor organic volatile matter content, is the ideal chose of healthy life staying idle at home.
Description
Technical field：
The present invention relates to a kind of mosquito-repellent incense, and in particular to a kind of oil of Cymbopogon winterianus vaporizer mosquito liquid and preparation method thereof.
Background technology：
Mosquito is a kind of worldwide sanitary insect pest, and its all one's life passes through ovum, larva, pupa, four periods of adult.Mosquito is main
Be to be that it is one of communication media of infectious disease.It was found that the disease of mosquitoes spread is up to as many as kind more than 80.In the whole world, about
There are 1,200,000 people to infect filariasis.The disease of the mosquito meeting infectious disease toxicity of most of kind, including yellow fever, dengue fever, Japan
Encephalitis, St. Louis encephalitis, polyarthirtis, Rift Valley fever (Rift Valley fever), contract elder brother Gen Yare and West Nile
Heat.On earth, then without which kind of animal than mosquito there is bigger harm to the mankind.The mosquito serious threat mankind as can be seen here
Health, these disgusting mosquitoes are only driven, epidemic infectious diseases could be controlled, human health could be ensured, improve people
Quality of life.
For many years, people develop and have used substantial amounts of hygienic insecticide product, for killing mosquitoes.Mosquito-repellent incense is most ancient
Natural drug mosquito repellent method.Just there is culicifuge incense rod made of Chinese medicine early in Southern Song Dynasty's period.In modern mosquito-repellent incense containing effectively into
It is pyrethrins to divide, and it plays the role of mosquito.After burning mosquito incense, pyrethrins in mosquito-repellent incense evaporates with smog,
Send out in the air of interior, make the neural paralysis of mosquito, then mosquito or it is born get killed, or four dissipate and escape, and are driven so as to play
The current mosquito-repellent incense production industry insecticidal active ingredient of effect of mosquito-killing, mainly cypermethrin, Prallethrin, allethrin, life
The pyrethrins such as thing chrysanthemum ester, the nerve that can benumb mosquito cause it dead.
Electric liquid device is actually mosquito liquid and the general name for making the electronic thermostatic heater that decoction uniformly volatilizees, preceding
Person claims mosquito-driving liquid, and the latter claims electric heater.In electric liquid device work, after electric heater accesses power supply, PTCR elements are just
Heating is started to warm up, afterwards by the PTCR elements temp regulating function of itself, its temperature is remained certain value.PTCR members
Heat caused by part is volatilized core by radiant heat transfer to decoction, is drawn to from medicinal liquid bottle decoction by core capillarity of volatilizing
Plug upper end, decoction is improved under heat radiation heating and be vaporized speed, after the insecticidal active ingredient in space reaches finite concentration,
Just mosquito is produced and driven, so as to knock down and kill mosquito.Electric liquid device because its using it is light, smokelessly without dust, drug effect
The features such as stabilization, high-efficiency low-toxicity, welcome by consumer.
Existing electric liquid device formula system is with alkane solvent, pyrethroid, antioxidant and essence etc. for group
Point, form homogeneous system by mixing, stirring solvent.Alkane solvent is due to being that rectifying etc. is formed, and its carbochain is distributed more widely, especially
It is that wherein low-carbon paraffin easily forms organic volatile i.e. VOC, in the daily life staying idle at home of consumer, electric heating liquid mosquito can be passed through
Fragrant heating brings certain influence using the pollution that domestic environment is caused with volatilization naturally to consumer health.
The invention provides a kind of oil of Cymbopogon winterianus vaporizer mosquito liquid, is a kind of vaporizer mosquito liquid of safety and environmental protection.
The content of the invention：
For deficiencies of the prior art, one of the technical problems to be solved by the invention are to provide a kind of lemongrass
Essential oil vaporizer mosquito liquid.
One of technical problems to be solved by the invention are to provide the preparation method of above-mentioned oil of Cymbopogon winterianus vaporizer mosquito liquid.
The technical problem of the present invention, is achieved by following technical proposals：
A kind of oil of Cymbopogon winterianus vaporizer mosquito liquid, is made up of the raw material of following weight parts：0.5-2.5 parts dimefluthrin,
0.1-0.5 parts oil of Cymbopogon winterianus, 50-60 parts butyl, 0.05-0.15 part p-methyl benzenesulfonic acids sodium, 0.1-0.5 part synergy
Agent, 0.1-0.5 parts antioxidant, 35-45 part water.
Preferably, described synergist is alantolactone and/or Ligustilide.
It is highly preferred that described synergist is made up of 40-60wt% alantolactones and 40-60wt% Ligustilides.
Preferably, described antioxidant is 2,4- dimethyl -6- tert-butyl phenols and/or 2,5- di-t-butyl to benzene two
Phenol.
It is highly preferred that described antioxidant is by 40-60wt%2,4- dimethyl -6- tert-butyl phenols and 40-60wt%2,
5- di-tert-butyl hydroquinones form.
Present invention also offers the preparation method of above-mentioned oil of Cymbopogon winterianus vaporizer mosquito liquid, by dimefluthrin, oil of Cymbopogon winterianus,
Butyl, synergist, antioxidant are well mixed, and are added p-methyl benzenesulfonic acid sodium and are well mixed, are eventually adding water and mix
Close uniform.
Specifically, in the present invention：
Dimefluthrin, No. CAS：271241-14-6.
Oil of Cymbopogon winterianus, No. CAS：73049-78-2.
Butyl, No. CAS：112-34-5.
P-methyl benzenesulfonic acid sodium, Chinese nickname：4- toluenesulfonic acid sodium salts, No. CAS：657-84-1.
Alantolactone, No. CAS：546-43-0.
Ligustilide, No. CAS：4431-01-0.
2,4- dimethyl -6- tert-butyl phenols, No. CAS：1879-09-0.
2,5- di-tert-butyl hydroquinones, No. CAS：88-58-4.
The oil of Cymbopogon winterianus vaporizer mosquito liquid of the present invention, the pure and fresh fragrance of taste, effect is killed with stronger to mosquito, is a kind of
Environment-friendly liquid mosquito-repellent incense, it has, and drug effect is powerful, safety is non-combustible, volatilization is stable, moreover it is possible to indoor organic volatile matter content is reduced,
It is the ideal chose of healthy life staying idle at home.
Embodiment：
With reference to embodiment, the present invention is described further, as described below, is only the preferable implementation to the present invention
Example, is not limited the present invention, any person skilled in the art is possibly also with the disclosure above
Technology contents be changed to the equivalent embodiment changed on an equal basis.It is every of the invention without departing from the present invention program content, foundation
Technical spirit any simple modification that following examples are made or equivalent variations, all fall within protection scope of the present invention.
Embodiment 1
Oil of Cymbopogon winterianus vaporizer mosquito liquid raw material (parts by weight)：1.2 parts of dimefluthrins, 0.2 part of oil of Cymbopogon winterianus, 55 parts of diethyls
Glycol butyl ether, 0.1 part of p-methyl benzenesulfonic acid sodium, 0.3 part of synergist, 0.3 part of antioxidant, 40 parts of deionized waters.
Described synergist is obtained by 50wt% alantolactones and 50wt% Ligustilides are well mixed.
Described antioxidant is by 50wt%2,4- dimethyl -6- tert-butyl phenols and 50wt%2,5- di-t-butyls to benzene two
Phenol is well mixed to be obtained.
The preparation method of oil of Cymbopogon winterianus vaporizer mosquito liquid：
Dimefluthrin, oil of Cymbopogon winterianus, butyl, synergist, antioxidant are mixed and stirred for uniformly, then added
Enter p-methyl benzenesulfonic acid sodium be mixed and stirred for uniformly, be eventually adding deionized water and be mixed and stirred for uniformly.Obtain the perfume (or spice) of embodiment 1
Thatch essential oil vaporizer mosquito liquid.
Embodiment 2
It is substantially the same manner as Example 1, differ only in：Described synergist is only alantolactone.Obtain embodiment 2
Oil of Cymbopogon winterianus vaporizer mosquito liquid.
Embodiment 3
It is substantially the same manner as Example 1, differ only in：Described synergist is only Ligustilide.Obtain embodiment 3
Oil of Cymbopogon winterianus vaporizer mosquito liquid.
Embodiment 4
It is substantially the same manner as Example 1, differ only in：Described antioxidant is only 2,4- dimethyl -6- tert-butyl benzenes
Phenol.Obtain the oil of Cymbopogon winterianus vaporizer mosquito liquid of embodiment 4.
Embodiment 5
It is substantially the same manner as Example 1, differ only in：Described antioxidant is only 2,5 di tert butyl hydroquinone.
Obtain the oil of Cymbopogon winterianus vaporizer mosquito liquid of embodiment 5.
Test case 1
Indoor harmacological effect test is carried out to embodiment 1-5 oil of Cymbopogon winterianus vaporizer mosquito liquid, defended using GB18418-2009 family expenses
Raw desinsection articles for use electric liquid device standard, is tested.In the standard, KT50 values (boxing method)≤10 minute can be judged to
Qualified, the time is shorter, and explanation is better to mosquito driving and killing effect, and test data is shown in Table 1.
Table 1：Vaporizer mosquito liquid indoor harmacological effect table (boxing method)
| KT50 values | |
| Embodiment 1 | 3 points 24 seconds |
| Embodiment 2 | 5 points 57 seconds |
| Embodiment 3 | 5 points 40 seconds |
| Embodiment 4 | 4 points 41 seconds |
| Embodiment 5 | 4 points 58 seconds |
Comparing embodiment 1-3, embodiment 1 (alantolactone, Ligustilide compounding) mosquito driving and killing effect, hence it is evident that better than reality
Apply a 2-3 (single raw material in alantolactone, Ligustilide)；Comparing embodiment 1 and embodiment 4-5, embodiment 1 (2,4- bis-
Methyl-6-tert-butylphenol, 2,5- di-tert-butyl hydroquinones compounding) mosquito driving and killing effect, hence it is evident that better than embodiment 4-5 (2,
Single raw material in 4- dimethyl -6- tert-butyl phenols, 2,5 di tert butyl hydroquinone).
Test case 2
Toxotest is carried out to embodiment 1-5 oil of Cymbopogon winterianus vaporizer mosquito liquid, with reference to health ministry《Management of occupational acute
Learn thing Poisoning disease in the blood system diagnostic criteria》And《Chinese medicine, technological guidance's principle of natural drug immunotoxicity research》Mark
Standard, formulate test case of the present invention.
Test species：Two young age small white mouses.
Experimental method：
(1) experiment condition：Laboratory temperature (27 ± 2) DEG C
(2) experimental provision：In two 25 square metres of mutually synthermal laboratories, each one size same size of placement
80 × 80 × 80cm is fine and closely woven ventilative netted to be shrouded.
(3) experimental procedure：By two young age small white mouses be separately respectively put in two laboratories it is netted shroud in, and be divided into pair
According to group and mosquito-repellent incense group of the present invention is smoked, gives respectively and does not smoke mosquito-repellent incense of the present invention and smoke mosquito-repellent incense of the present invention, measure young age small white mouse body weight,
The biochemical index of observation hematology, changes in histopathology and stopping smoke recovery situation after mosquito-repellent incense of the present invention etc..Place this hair
During bright mosquito-repellent incense will be arranged on it is netted shroud it is interior from the centimeters of bottom 30.Dosage：Electrical heating mosquito-repellent incense, keeps for a long time making for 24 hours
With.Time：Continuous use one month, observation control group and the young age small white mouse for smoking mosquito-repellent incense group of the present invention, long-term use of present invention
Toxicity and side effect of the mosquito-repellent incense to young age small white mouse.Cleaning：Clean once within two days in shrouding.
As a result：After two young age small white mouse blood tests, every biochemical indicator is normal, shows mosquito-repellent incense of the present invention to children
Age small white mouse has no toxic side effect, and when only more than 24 hours, indoor mosquito-repellent incense smog is too dense, need to open a window ventilation 10-15 minutes, blood drawing
Do not fed to two young age small white mouses within first 8 hours.
Conclusion：Long-term use of mosquito-repellent incense of the present invention is to young age small white mouse without any toxicity.
Test case 3
Acute oral toxicity test, 5 minutes activities in rats after contamination are carried out to embodiment 1-5 oil of Cymbopogon winterianus vaporizer mosquito liquid
Increase, continues 2 minutes or so, and activity switchs to normally, and diet is normal, and the observation period is more than 5000 mgs/kg without death, LD50,
Belong to actual nontoxic.
Test case 4
Acute inhalation toxicity experiment, rat diet activity after contamination are carried out to embodiment 1-5 oil of Cymbopogon winterianus vaporizer mosquito liquid
No abnormality seen, observation period are more than 10 grams/cubic metre without death, LD50, belong to actual nontoxic.
Test case 5
Skin patch test, experimental group erythema and oedema shape are carried out to embodiment 1-5 oil of Cymbopogon winterianus vaporizer mosquito liquid
It is 0 into scoring sum, explanation has no stimulation of the skin.
Test case 6
Eye irritant test, the acute Eye irritation integration number of experimental group are carried out to embodiment 1-5 oil of Cymbopogon winterianus vaporizer mosquito liquid
For 0, illustrate to have no stimulation to mucous membrane.
Claims (4)
1. a kind of oil of Cymbopogon winterianus vaporizer mosquito liquid, it is characterised in that be made up of the raw material of following weight parts：0.5-2.5 part tetrafluoro first
Ethofenprox, 0.1-0.5 parts oil of Cymbopogon winterianus, 50-60 parts butyl, 0.05-0.15 part p-methyl benzenesulfonic acids sodium, 0.1-
0.5 part of synergist, 0.1-0.5 parts antioxidant, 35-45 part water；Described synergist is by 40-60wt% alantolactones and 40-
60wt% Ligustilides form.
2. oil of Cymbopogon winterianus vaporizer mosquito liquid as claimed in claim 1, it is characterised in that：Described antioxidant be 2,4- dimethyl-
6- tert-butyl phenols and/or 2,5 di tert butyl hydroquinone.
3. oil of Cymbopogon winterianus vaporizer mosquito liquid as claimed in claim 2, it is characterised in that：Described antioxidant by 40-60wt%2,
4- dimethyl -6- tert-butyl phenols and 40-60wt%2,5- di-tert-butyl hydroquinones composition.
4. the preparation method of oil of Cymbopogon winterianus vaporizer mosquito liquid as any one of claim 1-3, it is characterised in that：By tetrafluoro
Methothrin, oil of Cymbopogon winterianus, butyl, synergist, antioxidant are well mixed, and add the mixing of p-methyl benzenesulfonic acid sodium
Uniformly, water is eventually adding to be well mixed.
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| CN106237366A (en) * | 2016-08-31 | 2016-12-21 | 防城港市绿华源农林科技有限公司 | A kind of Herba Cymbopogonis Citrari incense and preparation method thereof |
| CN106386901A (en) * | 2016-08-31 | 2017-02-15 | 防城港市绿华源农林科技有限公司 | Lemongrass aromatherapy mosquito-repellent incense |
| CN111771921A (en) * | 2019-12-09 | 2020-10-16 | 湖南省九喜日化有限公司 | Electric heating mosquito-repellent incense liquid and preparation method thereof |
| CN111955492A (en) * | 2020-09-01 | 2020-11-20 | 张增香 | Mosquito-repellent incense liquid and preparation method thereof |
| CN114903058A (en) * | 2022-06-17 | 2022-08-16 | 汕头市金龙日化实业有限公司 | Electric mosquito repellent liquid and preparation method thereof |
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