CN105935151B - Do not burnt suitable for low temperature the processing methods of cigarette shreds - Google Patents
Do not burnt suitable for low temperature the processing methods of cigarette shreds Download PDFInfo
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- CN105935151B CN105935151B CN201610248666.8A CN201610248666A CN105935151B CN 105935151 B CN105935151 B CN 105935151B CN 201610248666 A CN201610248666 A CN 201610248666A CN 105935151 B CN105935151 B CN 105935151B
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- pipe tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/42—Treatment of tobacco products or tobacco substitutes by chemical substances by organic and inorganic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/18—Other treatment of leaves, e.g. puffing, crimpling, cleaning
- A24B3/182—Puffing
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention provides a kind of processing method for the cigarette shreds that do not burnt suitable for low temperature, pipe tobacco is put into after being soaked more than 0.5 hour in ethanol solution and is filtrated to get the pipe tobacco after immersion, the pipe tobacco after above water cleaning and dipping makes removing ethanol in three times, dries the pipe tobacco after cleaning in the environment for drying ventilation afterwards；Mixed aqueous solution containing hemicellulase and pectase is sprayed onto in cigarette shreds, then Room-temperature seal is preserved 24 hours, high-temperature steam inactivator is used after taking out pipe tobacco, dried for standby after more than 2 times is repeated, then pipe tobacco is handled again with the aqueous solution of cellulase；After pipe tobacco is enzyme treated, spray plus appropriate weak caustic solution in pipe tobacco, placement heat pipe tobacco more than 2 hours after more than 24 hours under lower pressure；This method technique is simple, and the raw material of cigarette of making can be used for heating non-burning cigarette, does not produce tar and harmful smoke, substantially reduces the murder by poisoning that flue gas is caused to human body.
Description
Technical field
The present invention relates to a kind of processing method for the cigarette shreds that do not burnt suitable for low temperature.
Background technology
In recent years, while world's cigarette products year volume of production and marketing has declined, various non-traditional tobacco products, which are presented, to be increased
Long situation, the product structure in World tobacco market constantly occurs to change, and actively development complete series tobacco product is increasingly becoming
The strategic decisions of each transnational tobacco company.The representational non-traditional tobacco product of in the market mainly has heating non-combustion-type tobacco
Several classes such as product, smoke-free tobacco product.Heating non-combustion-type tobacco product has " heating pipe tobacco or tobacco extract and it is non-combustible
Burn pipe tobacco " the characteristics of, it reduces the harmful components that the cracking of tobacco high-temp combustion is produced, and makes main flume chemical constituent burst size
Substantially reduce.Meanwhile, glowed difference with conventional cigarette, its pipe tobacco when aspirating interval is in non-burning/non-heated state, therefore
Side-stream smoke and environment flue gas are also greatly lowered.According to the difference of heating source, heating non-combustion-type tobacco product can be divided into " electricity
Hot type tobacco product ", " combustion heating type tobacco product " and " physical and chemical reaction hot type tobacco product ".
The operating temperature of low-temperature heat non-combustion type cigarette silk is normally less than 300 degrees Celsius, and traditional cigarette burning is split
The temperature of solution is at 800 degrees Celsius, therefore the chemical composition that identical pipe tobacco is discharged in the different products of above two has larger
Difference, so that both have larger difference in terms of the organoleptic attributes such as fragrance, excitant.Therefore, it is highly desirable to exploitation one
Plant new pipe tobacco handling process, it is adaptable to heat non-burning cigarette, reduce its difference with traditional cigarette in terms of mouthfeel, improve
It aspirates comfort level.
The content of the invention
It is an object of the invention to provide a kind of processing method solution prior art for the cigarette shreds that do not burnt suitable for low temperature
Present in how to reduce heating non-burning cigarette and difference of the traditional cigarette in terms of mouthfeel, improve it and aspirate asking for comfort level
Topic.
The present invention technical solution be：
A kind of processing method for the cigarette shreds that do not burnt suitable for low temperature, including：
Step 1, by pipe tobacco be put into ethanol solution soak more than 0.5 hour after be filtrated to get immersion after pipe tobacco, divide
Make removing ethanol with the pipe tobacco after water cleaning and dipping more than three times, dry the cigarette after cleaning in the environment for drying ventilation afterwards
Silk；
Step 2, the aqueous solution containing hemicellulase and pectase is sprayed onto in cigarette shreds, pipe tobacco cell membrane of degrading
In cellulose and pectin, then Room-temperature seal preserve more than 24 hours, take out pipe tobacco after use high-temperature steam inactivator, enter repeatedly
Dried for standby after row more than 2 times；The aqueous solution containing cellulase is sprayed onto after processing in the cigarette shreds of dried for standby,
Cellulose in degraded pipe tobacco cell membrane, then Room-temperature seal preservation more than 24 hours, is inactivated after taking out pipe tobacco with high-temperature steam
Enzyme, is repeated dried for standby after more than 2 times；
After step 3, pipe tobacco are enzyme treated, spray plus appropriate weak caustic solution, neutralize the acid-base value of pipe tobacco in pipe tobacco, place
Pipe tobacco more than 2 hours is heated after more than 24 hours under 60~80kpa lower pressure.
Further, the concentration of aqueous solution containing hemicellulase and pectase and pH value do not reduce enzyme in the step 2
Activity, be specially：100g pipe tobaccos are taken, 1g hemicellulases and 3-5g pectases are dissolved in water, PH is adjusted by citric acid
Value is to 5.5, and solution temperature is maintained at 40-50 DEG C of processing pipe tobacco.
Further, the concentration and pH value of the aqueous solution containing cellulase do not reduce the activity of enzyme, are specially：Take 100g
Pipe tobacco, 3-6g cellulases are dissolved in water, adjust pH value to 5.5 by citric acid, solution temperature is maintained at 30 DEG C and located again
Manage pipe tobacco.
Further, pipe tobacco is added after enzyme in the step 2, and the moisture of final pipe tobacco is not higher than 25%.
Further, the heating-up temperature of pipe tobacco is 40-60 DEG C in the step 3.
Further, the moisture in cut tobacco after being heated more than 2 hours in the step 3 is maintained at 20-25%.
Further, weak caustic solution is ammonium carbonate, ammonium hydrogen carbonate or sodium acid carbonate any one molten in the step 3
Liquid.
Further, in step 3, spray plus appropriate weak caustic solution in pipe tobacco make the acid-base value of neutralization pipe tobacco to pH value
For 6.6-6.9.
Further, in step 3, spray plus appropriate weak caustic solution in pipe tobacco make the acid-base value of neutralization pipe tobacco to pH value
For 6.8.
The beneficial effects of the invention are as follows：This kind is applied to low temperature and not burnt the processing methods of cigarette shreds, first using second
Alcohol processing pipe tobacco suitably reduces volatile stimulating component and nicotine content in pipe tobacco；Then with enzyme degraded pipe tobacco cell membrane
Fiber and pectin, for intracellular matter volatilize provide condition and suitably increase reduced sugar content；Add appropriate weak base
Property material, neutralize the acid-base value of pipe tobacco, and reacting precursor thing is provided for the Maillard reaction that may occur, coordination cigarette perfume, simultaneously
It is that the volatilization of pipe tobacco intracellular matter under cryogenic is created using by the appropriate expanded cut tobacco of thermogenetic atmospheric carbon dioxide
Advantage.This method technique is simple, and the raw material of cigarette of making can be used for heating non-burning cigarette, and tar and harmful cigarette are not produced
Gas, substantially reduces the murder by poisoning that flue gas is caused to human body.
Brief description of the drawings
Fig. 1 is the handling process schematic diagram of the embodiment of the present invention.
Embodiment
The preferred embodiment that the invention will now be described in detail with reference to the accompanying drawings.
A kind of processing method for the cigarette shreds that do not burnt suitable for low temperature, as shown in figure 1, including：
Step 1, by pipe tobacco be put into ethanol solution soak more than 0.5 hour after be filtrated to get immersion after pipe tobacco, divide
Make removing ethanol with the pipe tobacco after water cleaning and dipping more than three times, dry the cigarette after cleaning in the environment for drying ventilation afterwards
Silk；
Step 2, will be right successively containing hemicellulase, the mixed aqueous solution of pectase and the aqueous solution containing cellulase
Pipe tobacco carries out ferment treatment：Enzyme aqueous solution is sprayed onto in cigarette shreds, then Room-temperature seal is preserved more than 24 hours, takes out pipe tobacco
High-temperature steam inactivator is used afterwards, and dried for standby after more than 2 times is repeated；
After step 3, pipe tobacco are enzyme treated, spray plus appropriate weak caustic solution, neutralize the acid-base value of pipe tobacco in pipe tobacco, place
Pipe tobacco more than 2 hours is heated after more than 24 hours under lower pressure.
Embodiment 1
Pipe tobacco is put into after being soaked 0.5 hour in ethanol solution and filtered, cleaned pipe tobacco with water in three times and remove ethanol, it
Afterwards pipe tobacco is dried in the environment for drying ventilation.The step is mainly used in suitably reducing in pipe tobacco nicotine content and with stimulation
The volatile ingredient of property.
The aqueous solution containing cellulase is sprayed onto in cigarette shreds, then Room-temperature seal is preserved 24 hours, takes out cigarette
High-temperature steam inactivator is used after silk, dried for standby after 2 times is repeated.After being degraded through enzyme, content of cellulose will be reduced in pipe tobacco,
Cell membrane is also conducive to fragrance matter in tobacco cell to distribute under cryogenic by thinning, is beneficial to improve tobacco aroma.
After pipe tobacco is enzyme treated, sal volatile is added in pipe tobacco, with heating under lower pressure after placing 24 hours
Temperature is 40-60 DEG C and heats pipe tobacco 2 hours, moisture in cut tobacco is maintained at 20-25%, and processing is completed.
The sensory evaluating smoking's table of table 1
| Sample | Aroma quality | Perfume quantity | Concentration | Strength | Miscellaneous gas | Excitant | Pleasant impression |
| Control sample | 6.0 | 6.0 | 5.0 | 5.0 | 5.0 | 5.0 | 5.5 |
| Test sample 1 | 7.0 | 6.5 | 5.0 | 5.0 | 5.5 | 5.5 | 6.0 |
In table 1, control sample：Pipe tobacco without any processing；Test sample 1：Pipe tobacco after being handled through embodiment 1.
By above-mentioned table of smokeing panel test as can be seen that pipe tobacco the step of embodiment 1 after handling, aroma quality, perfume quantity have been carried
Rise, reduce miscellaneous gas, improve pleasant impression, improve the harmony and applicability of pipe tobacco.
Embodiment 2
Pipe tobacco is put into after being soaked 0.7 hour in ethanol solution and filtered, cleaned pipe tobacco with water in three times and remove ethanol, it
Afterwards pipe tobacco is dried in the environment for drying ventilation.The step is mainly used in suitably reducing in pipe tobacco nicotine content and with stimulation
The volatile ingredient of property.
The aqueous solution containing hemicellulase is sprayed onto in cigarette shreds, then Room-temperature seal is preserved 24 hours, taken out
High-temperature steam inactivator is used after pipe tobacco, dried for standby after 2 times is repeated.After being degraded through enzyme, content of cellulose will drop in pipe tobacco
Low, cell membrane is also conducive to fragrance matter in tobacco cell to distribute under cryogenic by thinning, is beneficial to improve tobacco perfume
Gas.
After pipe tobacco is enzyme treated, ammonium bicarbonate soln is added in pipe tobacco, to add under lower pressure after placing 24 hours
Hot temperature is 40 DEG C and heats pipe tobacco 2 hours, moisture in cut tobacco is maintained at 25%, processing is completed.
The sensory evaluating smoking's table of table 2
| Sample | Aroma quality | Perfume quantity | Concentration | Strength | Miscellaneous gas | Excitant | Pleasant impression |
| Control sample | 6.0 | 6.0 | 5.0 | 5.0 | 5.0 | 5.0 | 5.5 |
| Test sample 2 | 7.0 | 6.5 | 5.0 | 5.0 | 5.5 | 5.5 | 6.0 |
In table 2, control sample：Pipe tobacco without any processing；Test sample 2：Pipe tobacco after being handled through embodiment 2.
By above-mentioned table of smokeing panel test as can be seen that pipe tobacco the step of embodiment 2 after handling, aroma quality, perfume quantity have been carried
Rise, reduce miscellaneous gas, improve pleasant impression, improve the harmony and applicability of pipe tobacco.
Embodiment 3
Pipe tobacco is put into after being soaked 0.5 hour in ethanol solution and filtered, cleaned pipe tobacco with water in three times and remove ethanol, it
Afterwards pipe tobacco is dried in the environment for drying ventilation.The step is mainly used in suitably reducing in pipe tobacco nicotine content and with stimulation
The volatile ingredient of property.
The aqueous solution containing pectase is sprayed onto in cigarette shreds, then Room-temperature seal is preserved 24 hours, takes out pipe tobacco
High-temperature steam inactivator is used afterwards, and dried for standby after 2 times is repeated.After being degraded through enzyme, in pipe tobacco pectin content will reduce, it is water-soluble
Property glucide increase, be conducive to improving cigarette perfume, reduce miscellaneous gas.
After pipe tobacco is enzyme treated, sodium bicarbonate solution is added in pipe tobacco, to add under lower pressure after placing 24 hours
Hot temperature is 50 DEG C and heats pipe tobacco 2.5 hours, moisture in cut tobacco is maintained at 22%, processing is completed.
The sensory evaluating smoking's table of table 3
| Sample | Aroma quality | Perfume quantity | Concentration | Strength | Miscellaneous gas | Excitant | Pleasant impression |
| Control sample | 6.0 | 6.0 | 5.0 | 5.0 | 5.0 | 5.0 | 5.5 |
| Test sample 3 | 6.5 | 7.0 | 5.0 | 5.0 | 6.0 | 5.5 | 6.0 |
In table 3, control sample：Pipe tobacco without any processing；Test sample 3：Pipe tobacco after being handled through embodiment 3.
By above-mentioned table of smokeing panel test as can be seen that pipe tobacco the step of embodiment 3 after handling, aroma quality has been lifted, fragrance
Amount increase, miscellaneous gas is reduced, and is improved pleasant impression, is improved the harmony and applicability of pipe tobacco.
Claims (4)
1. a kind of processing method for the cigarette shreds that do not burnt suitable for low temperature, it is characterised in that including：
Step 1, by pipe tobacco be put into ethanol solution soak more than 0.5 hour after be filtrated to get soak after pipe tobacco, in three times
Make removing ethanol with the pipe tobacco after water cleaning and dipping above, dry the pipe tobacco after cleaning in the environment for drying ventilation afterwards；
Step 2, the aqueous solution containing hemicellulase and pectase is sprayed onto in cigarette shreds, in degraded pipe tobacco cell membrane
Cellulose and pectin, then Room-temperature seal preservation more than 24 hours, uses high-temperature steam inactivator after taking out pipe tobacco, is repeated 2
Dried for standby after more than secondary；The aqueous solution containing cellulase is sprayed onto after processing in the cigarette shreds of dried for standby, dropped
The cellulose in pipe tobacco cell membrane is solved, then Room-temperature seal is preserved more than 24 hours, high-temperature steam inactivator is used after taking out pipe tobacco,
Dried for standby after more than 2 times is repeated, the moisture of final pipe tobacco is not higher than 25%；
After step 3, pipe tobacco are enzyme treated, spray plus appropriate weak caustic solution in pipe tobacco, weak caustic solution is ammonium carbonate, ammonium hydrogen carbonate
Or the sodium acid carbonate solution of any one, neutralize the acid-base value of pipe tobacco, make the acid-base value of neutralization pipe tobacco to pH value be 6.6-6.9,
Heating-up temperature heats pipe tobacco more than 2 hours for 40-60 DEG C under 60~80kpa lower pressure after placing more than 24 hours, cigarette
Silk water tariff collection is in 20-25%.
2. the processing method for the cigarette shreds that do not burnt suitable for low temperature as claimed in claim 1, it is characterised in that：The step
Concentration of aqueous solution and pH value containing hemicellulase and pectase in 2 are specially：Take 100g pipe tobaccos, by 1g hemicellulases and
3-5g pectases are dissolved in water, adjust pH value to 5.5 by citric acid, solution temperature is maintained at 40-50 DEG C of processing pipe tobacco.
3. the processing method for the cigarette shreds that do not burnt suitable for low temperature as claimed in claim 1, it is characterised in that：Contain fiber
The concentration of aqueous solution and pH value of plain enzyme be specially：100g pipe tobaccos are taken, 3-6g cellulases are dissolved in water, adjusted by citric acid
PH value is to 5.5, and solution temperature is maintained at 30 DEG C of processing pipe tobaccos.
4. the processing method for the cigarette shreds that do not burnt suitable for low temperature as claimed in claim 1, it is characterised in that：In step 3,
Spray plus appropriate weak caustic solution in pipe tobacco, make the acid-base value of neutralization pipe tobacco to pH value be 6.8.
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| CN201610248666.8A CN105935151B (en) | 2016-04-20 | 2016-04-20 | Do not burnt suitable for low temperature the processing methods of cigarette shreds |
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| CN105935151B true CN105935151B (en) | 2017-09-19 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107156897B (en) * | 2017-07-07 | 2019-03-19 | 重庆中烟工业有限责任公司 | A kind of device and method preparing tobacco tar |
| CN108077997A (en) * | 2017-12-12 | 2018-05-29 | 江西中烟工业有限责任公司 | A kind of preparation method and applications of cigarette filter combination |
| CN108095185B (en) * | 2017-12-14 | 2020-05-05 | 江西中烟工业有限责任公司 | Tobacco shred pretreatment process |
| CN110946316A (en) * | 2018-09-27 | 2020-04-03 | 浙江中烟工业有限责任公司 | Method for treating non-burning tobacco shreds by heating |
| CN112293788B (en) * | 2019-07-31 | 2022-12-09 | 湖南中烟工业有限责任公司 | Pretreated tobacco raw material for heating non-combustion tobacco products and preparation and application thereof |
| CN110680024B (en) * | 2019-10-10 | 2022-02-22 | 黑龙江黑科科技有限责任公司 | Preparation method of cannabis electronic tobacco shreds and cannabis electronic cigarette cartridge |
| CN110522064A (en) * | 2019-10-14 | 2019-12-03 | 中国烟草总公司郑州烟草研究院 | A kind of throwing method improving discarded tobacco leaf quality |
| CN116268540A (en) * | 2022-09-08 | 2023-06-23 | 广东中烟工业有限责任公司 | Method for improving sensory quality of heated cigarettes |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3513857A (en) * | 1967-12-26 | 1970-05-26 | Philip Morris Inc | Process for the treatment of tobacco stems |
| CN101228967B (en) * | 2007-12-26 | 2010-12-08 | 广东中烟工业有限责任公司 | Method of improving cabo quality |
| CN102894472B (en) * | 2012-09-29 | 2014-12-24 | 福建中烟工业有限责任公司 | Method for improving sensory quality of tobacco leaves by using compound enzymic preparation |
| CN104366688B (en) * | 2014-11-27 | 2016-03-23 | 湖南中烟工业有限责任公司 | A kind of method improving inapplicable upper tobacco leaf material quality |
| CN104705779B (en) * | 2015-01-28 | 2016-08-17 | 中国烟草总公司郑州烟草研究院 | A kind of processing method improving cut stem quality |
| CN105326086A (en) * | 2015-11-25 | 2016-02-17 | 红云红河烟草(集团)有限责任公司 | Method for increasing alcohol thickness and sweet smell of tobacco flakes by using compound enzyme preparation |
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