CN105935151A - Processing method suitable for low-temperature non-combustion cigarette tobacco - Google Patents

Processing method suitable for low-temperature non-combustion cigarette tobacco Download PDF

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Publication number
CN105935151A
CN105935151A CN201610248666.8A CN201610248666A CN105935151A CN 105935151 A CN105935151 A CN 105935151A CN 201610248666 A CN201610248666 A CN 201610248666A CN 105935151 A CN105935151 A CN 105935151A
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China
Prior art keywords
tobacco
tobacco shred
cigarette
processing method
temperature
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CN201610248666.8A
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Chinese (zh)
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CN105935151B (en
Inventor
吴佳
陈晶波
张建彭
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China Tobacco Jiangsu Industrial Co Ltd
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China Tobacco Jiangsu Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/20Biochemical treatment
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/42Treatment of tobacco products or tobacco substitutes by chemical substances by organic and inorganic substances
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/18Other treatment of leaves, e.g. puffing, crimpling, cleaning
    • A24B3/182Puffing

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The present invention provides a processing method suitable for low-temperature non-combustion cigarette tobacco. The processing method comprises putting the tobacco into an ethanol solution and immersing for 0.5 hours and then obtaining immersed tobacco after filtering, cleaning the immersed tobacco by water for more than three times to remove ethanol, drying the cleaned tobacco in a dry and ventilated environment; spraying mixed aqueous solution containing hemicellulase and pectinase to the cigarette tobacco, sealedly preserving the cigarette tobacco at room temperature for 24 hours, taking the tobacco out and inactivating the enzymes by high-temperature steam repeatedly for two times, drying the tobacco for standby application, and then processing the tobacco again by using a aqueous solution containing cellulase; and spraying proper amount of weak base solution to the tobacco after the tobacco is processed by the enzyme, disposing the tobacco for more than 24 hours, and then heating the tobacco under a low pressure condition for more than 2 hours. The method is simple in technology, the produced cigarette raw material can be used for heating non-combustion cigarette, tar and harmful smoke are prevented, and toxicity to a human body caused by the smoke is largely reduced.

Description

It is applicable to low temperature do not burn the processing method of cigarette shreds
Technical field
The present invention relates to a kind of low temperature that is applicable to do not burn the processing method of cigarette shreds.
Background technology
In recent years, while cigarette products year volume of production and marketing in the world's has declined, various non-traditional tobacco products in Existing growing trend, the product structure in World tobacco market constantly occurs to change, actively development complete series Nicotiana tabacum L. system Product are increasingly becoming the strategic decisions of each transnational tobacco company.Representational non-traditional tobacco product master on market There are several classes such as heating non-combustion-type tobacco goods, smoke-free tobacco product.Heating non-combustion-type tobacco goods tool There is the feature of " heating tobacco shred or tobacco extract and non-burning tobacco shred ", which reduce the cracking of Nicotiana tabacum L. high-temp combustion The harmful components produced, make main flume chemical constituent burst size be substantially reduced.Meanwhile, glow with conventional cigarette Difference, its tobacco shred when suction interval is in non-burning/non-heated state, therefore side-stream smoke and environment flue gas Also it is greatly lowered.According to the difference of heating source, heating non-combustion-type tobacco goods can be divided into " electric heating type cigarette Straw-made articles ", " combustion heating type tobacco product " and " physical and chemical reaction hot type tobacco product ".
The operating temperature of low-temperature heat non-combustion type cigarette silk is normally less than 300 degrees Celsius, and traditional cigarette combustion Hardening crack the temperature of solution at 800 degrees Celsius, the change that thus like tobacco shred discharges in above two difference goods Studying point has larger difference, so that both have larger difference in terms of the organoleptic attribute such as fragrance, zest. Therefore, it is highly desirable to develop a kind of new cigarette wire processing technique, it is adaptable to heating non-burning Medicated cigarette, reduces it With traditional cigarette difference in terms of mouthfeel, improve its suction comfort level.
Summary of the invention
It is an object of the invention to provide a kind of be applicable to low temperature do not burn cigarette shreds processing method solve existing How to reduce heating non-burning Medicated cigarette and traditional cigarette difference in terms of mouthfeel present in technology, improve it and take out The problem inhaling comfort level.
The technical solution of the present invention is:
A kind of low temperature that is applicable to does not burns the processing method of cigarette shreds, including:
Step 1, tobacco shred is put into the cigarette soaked in ethanol solution after being filtrated to get immersion after more than 0.5 hour Silk, makes removing ethanol with the tobacco shred after water cleaning and dipping above in three times, dries in the air afterwards in the environment of dry ventilation Tobacco shred after dry cleaning;
Step 2, the aqueous solution containing hemicellulase and pectase is sprayed onto in cigarette shreds, tobacco shred of degrading Cellulose in cell wall and pectin, then Room-temperature seal preserves more than 24 hours, uses high temperature after taking out tobacco shred Steam inactivator, dried for standby after being repeated more than 2 times;Aqueous solution containing cellulase is sprayed onto through After process in the cigarette shreds of dried for standby, the cellulose in degraded tobacco shred cell wall, then Room-temperature seal preserves More than 24 hours, after taking out tobacco shred, use high-temperature steam inactivator, dried for standby after being repeated more than 2 times;
After step 3, tobacco shred are enzyme treated, in tobacco shred, spray adds appropriate weak caustic solution, neutralizes the soda acid of tobacco shred Degree, heats tobacco shred more than 2 hours after placing more than 24 hours under the lower pressure of 60~80kpa.
Further, in described step 2 containing hemicellulase and the concentration of aqueous solution of pectase and pH value not Reduce the activity of enzyme, particularly as follows: take 100g tobacco shred, 1g hemicellulase and 3-5g pectase are dissolved in water In, by citric acid regulation pH value to 5.5, solution temperature is maintained at 40-50 DEG C and processes tobacco shred.
Further, the concentration of the aqueous solution containing cellulase and pH value do not reduce the activity of enzyme, particularly as follows: Take 100g tobacco shred, 3-6g cellulase is dissolved in water, by citric acid regulation pH value to 5.5, solution Temperature is maintained at 30 DEG C and again processes tobacco shred.
Further, after in described step 2, tobacco shred adds enzyme, the moisture of final tobacco shred is not higher than 25%.
Further, in described step 3, the heating-up temperature of tobacco shred is 40-60 DEG C.
Further, the moisture in cut tobacco after heating more than 2 hours in described step 3 is maintained at 20-25%.
Further, in described step 3 weak caustic solution be ammonium carbonate, ammonium hydrogen carbonate or sodium bicarbonate any one Solution.
Further, in step 3, in tobacco shred, spray adds appropriate weak caustic solution, makes the acid-base value of neutralization tobacco shred It is 6.6-6.9 to pH value.
Further, in step 3, in tobacco shred, spray adds appropriate weak caustic solution, makes the acid-base value of neutralization tobacco shred It is 6.8 to pH value.
The invention has the beneficial effects as follows: this kind is applicable to low temperature and does not burn the processing method of cigarette shreds, first should Volatile stimulating component and nicotine content in tobacco shred is suitably reduced with Ethanol Treatment tobacco shred;Then enzymatic degradation is used Fiber in tobacco shred cell wall and pectin, for intracellular matter volatilization offer condition suitable increase the containing of reducing sugar Amount;Add appropriate alkalescence material, neutralize the acid-base value of tobacco shred, and be contingent Maillard reaction Reacting precursor thing is provided, coordinates cigarette fragrant, utilize simultaneously and by thermogenetic atmospheric carbon dioxide appropriateness expanded cut tobacco be The volatilization under cryogenic of tobacco shred intracellular matter creates favorable conditions.The method technique is simple, the volume of making Cigarette raw material can be used for heating non-burning Medicated cigarette, does not produce tar and harmful smoke, is substantially reduced flue gas and makes human body The murder by poisoning become.
Accompanying drawing explanation
Fig. 1 is the handling process schematic diagram of the embodiment of the present invention.
Detailed description of the invention
Describe the preferred embodiments of the present invention below in conjunction with the accompanying drawings in detail.
A kind of low temperature that is applicable to does not burns the processing method of cigarette shreds, as it is shown in figure 1, include:
Step 1, tobacco shred is put into the cigarette soaked in ethanol solution after being filtrated to get immersion after more than 0.5 hour Silk, makes removing ethanol with the tobacco shred after water cleaning and dipping above in three times, dries in the air afterwards in the environment of dry ventilation Tobacco shred after dry cleaning;
Step 2, by containing hemicellulase, mixed aqueous solution and the aqueous solution containing cellulase of pectase Tobacco shred carrying out ferment treatment successively: be sprayed onto in cigarette shreds by enzyme aqueous solution, then Room-temperature seal preserves 24 More than hour, after taking out tobacco shred, use high-temperature steam inactivator, dried for standby after being repeated more than 2 times;
After step 3, tobacco shred are enzyme treated, in tobacco shred, spray adds appropriate weak caustic solution, neutralizes the soda acid of tobacco shred Degree, heats tobacco shred more than 2 hours after placing more than 24 hours under lower pressure.
Embodiment 1
Tobacco shred is put into and filters after ethanol solution soaks 0.5 hour, clean tobacco shred with water in three times and remove second Alcohol, dries tobacco shred afterwards in the environment of dry ventilation.This step is mainly used in suitably reducing nicotine in tobacco shred and contains Measure and there is irritating volatile ingredient.
Being sprayed onto in cigarette shreds by aqueous solution containing cellulase, then Room-temperature seal preserves 24 hours, High-temperature steam inactivator is used, dried for standby after being repeated 2 times after taking out tobacco shred.After enzymatic degradation, in tobacco shred Content of cellulose will reduce, and cell wall is also conducive to fragrance matter in tobacco cell to dissipate under cryogenic by thinning Send out, be beneficial to improve tobacco aroma.
After tobacco shred is enzyme treated, tobacco shred adds sal volatile, after placing 24 hours under lower pressure Heating tobacco shred 2 hours with heating-up temperature for 40-60 DEG C, make moisture in cut tobacco be maintained at 20-25%, process completes.
Table 1 sensory evaluating smoking's table
Sample Aroma quality Perfume quantity Concentration Strength Miscellaneous QI Zest Pleasant impression
Control sample 6.0 6.0 5.0 5.0 5.0 5.0 5.5
Test sample 1 7.0 6.5 5.0 5.0 5.5 5.5 6.0
In table 1, control sample: without the tobacco shred of any process;Test sample 1: the cigarette after embodiment 1 processes Silk.
By above-mentioned table of smokeing panel test it can be seen that tobacco shred is after the step process of embodiment 1, aroma quality, perfume quantity Promote, reduced miscellaneous QI, improve pleasant impression, improve harmony and the suitability of tobacco shred.
Embodiment 2
Tobacco shred is put into and filters after ethanol solution soaks 0.7 hour, clean tobacco shred with water in three times and remove second Alcohol, dries tobacco shred afterwards in the environment of dry ventilation.This step is mainly used in suitably reducing nicotine in tobacco shred and contains Measure and there is irritating volatile ingredient.
Being sprayed onto in cigarette shreds by aqueous solution containing hemicellulase, then Room-temperature seal preserves 24 hours, High-temperature steam inactivator is used, dried for standby after being repeated 2 times after taking out tobacco shred.After enzymatic degradation, in tobacco shred Content of cellulose will reduce, and cell wall is also conducive to fragrance matter in tobacco cell to dissipate under cryogenic by thinning Send out, be beneficial to improve tobacco aroma.
After tobacco shred is enzyme treated, tobacco shred adds ammonium bicarbonate soln, at lower pressure after placing 24 hours Under be 40 DEG C of heating tobacco shreds 2 hours with heating-up temperature, make moisture in cut tobacco be maintained at 25%, process completes.
Table 2 sensory evaluating smoking's table
Sample Aroma quality Perfume quantity Concentration Strength Miscellaneous QI Zest Pleasant impression
Control sample 6.0 6.0 5.0 5.0 5.0 5.0 5.5
Test sample 2 7.0 6.5 5.0 5.0 5.5 5.5 6.0
In table 2, control sample: without the tobacco shred of any process;Test sample 2: the cigarette after embodiment 2 processes Silk.
By above-mentioned table of smokeing panel test it can be seen that tobacco shred is after the step process of embodiment 2, aroma quality, perfume quantity Promote, reduced miscellaneous QI, improve pleasant impression, improve harmony and the suitability of tobacco shred.
Embodiment 3
Tobacco shred is put into and filters after ethanol solution soaks 0.5 hour, clean tobacco shred with water in three times and remove second Alcohol, dries tobacco shred afterwards in the environment of dry ventilation.This step is mainly used in suitably reducing nicotine in tobacco shred and contains Measure and there is irritating volatile ingredient.
Being sprayed onto in cigarette shreds by aqueous solution containing pectase, then Room-temperature seal preserves 24 hours, takes High-temperature steam inactivator is used, dried for standby after being repeated 2 times after going out tobacco shred.After enzymatic degradation, fruit in tobacco shred Glue content will reduce, water-soluble saccharides material increases, and be conducive to improving cigarette fragrant, reduce miscellaneous QI.
After tobacco shred is enzyme treated, tobacco shred adds sodium bicarbonate solution, at lower pressure after placing 24 hours Under be 50 DEG C of heating tobacco shreds 2.5 hours with heating-up temperature, make moisture in cut tobacco be maintained at 22%, process completes.
Table 3 sensory evaluating smoking's table
Sample Aroma quality Perfume quantity Concentration Strength Miscellaneous QI Zest Pleasant impression
Control sample 6.0 6.0 5.0 5.0 5.0 5.0 5.5
Test sample 3 6.5 7.0 5.0 5.0 6.0 5.5 6.0
In table 3, control sample: without the tobacco shred of any process;Test sample 3: the cigarette after embodiment 3 processes Silk.
By above-mentioned table of smokeing panel test it can be seen that tobacco shred is after the step process of embodiment 3, aroma quality promoted, Perfume quantity increases, and miscellaneous QI reduces, and improves pleasant impression, improves harmony and the suitability of tobacco shred.

Claims (9)

1. one kind is applicable to low temperature and does not burn the processing method of cigarette shreds, it is characterised in that including:
Step 1, tobacco shred is put into the cigarette soaked in ethanol solution after being filtrated to get immersion after more than 0.5 hour Silk, makes removing ethanol with the tobacco shred after water cleaning and dipping above in three times, dries in the air afterwards in the environment of dry ventilation Tobacco shred after dry cleaning;
Step 2, the aqueous solution containing hemicellulase and pectase is sprayed onto in cigarette shreds, tobacco shred of degrading Cellulose in cell wall and pectin, then Room-temperature seal preserves more than 24 hours, uses high temperature after taking out tobacco shred Steam inactivator, dried for standby after being repeated more than 2 times;Aqueous solution containing cellulase is sprayed onto through After process in the cigarette shreds of dried for standby, the cellulose in degraded tobacco shred cell wall, then Room-temperature seal preserves More than 24 hours, after taking out tobacco shred, use high-temperature steam inactivator, dried for standby after being repeated more than 2 times;
After step 3, tobacco shred are enzyme treated, in tobacco shred, spray adds appropriate weak caustic solution, neutralizes the soda acid of tobacco shred Degree, heats tobacco shred more than 2 hours after placing more than 24 hours under the lower pressure of 60~80kpa.
Being applicable to low temperature the most as claimed in claim 1 do not burn the processing method of cigarette shreds, its feature exists In: described step 2 does not reduce the work of enzyme containing hemicellulase and the concentration of aqueous solution of pectase and pH value Property, particularly as follows: take 100g tobacco shred, 1g hemicellulase and 3-5g pectase are dissolved in water, pass through lemon Lemon acid regulation pH value is to 5.5, and solution temperature is maintained at 40-50 DEG C and processes tobacco shred.
Being applicable to low temperature the most as claimed in claim 1 do not burn the processing method of cigarette shreds, its feature exists In: concentration of aqueous solution containing cellulase and pH value do not reduce the activity of enzyme, particularly as follows: take 100g cigarette Silk, dissolves in water by 3-6g cellulase, and by citric acid regulation pH value to 5.5, solution temperature is maintained at 30 DEG C process tobacco shred again.
Being applicable to low temperature the most as claimed in claim 1 do not burn the processing method of cigarette shreds, its feature exists In: after in described step 2, tobacco shred adds enzyme, the moisture of final tobacco shred is not higher than 25%.
5. the low temperature that is applicable to as described in any one of claim 1-4 does not burn the processing method of cigarette shreds, It is characterized in that: in described step 3, the heating-up temperature of tobacco shred is 40-60 DEG C.
6. the low temperature that is applicable to as described in any one of claim 1-4 does not burn the processing method of cigarette shreds, It is characterized in that: the moisture in cut tobacco after heating more than 2 hours in described step 3 is maintained at 20-25%.
7. the low temperature that is applicable to as described in any one of claim 1-4 does not burn the processing method of cigarette shreds, It is characterized in that: in described step 3 weak caustic solution be ammonium carbonate, ammonium hydrogen carbonate or sodium bicarbonate any one Solution.
8. the low temperature that is applicable to as described in any one of claim 1-4 does not burn the processing method of cigarette shreds, It is characterized in that: in step 3, in tobacco shred, spray adds appropriate weak caustic solution, makes the acid-base value of neutralization tobacco shred arrive PH value is 6.6-6.9.
Being applicable to low temperature the most as claimed in claim 8 do not burn the processing method of cigarette shreds, its feature exists In: in step 3, in tobacco shred, spray adds appropriate weak caustic solution, and the acid-base value making neutralization tobacco shred to pH value is 6.8。
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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107156897A (en) * 2017-07-07 2017-09-15 重庆中烟工业有限责任公司 A kind of apparatus and method for preparing tobacco tar
CN108077997A (en) * 2017-12-12 2018-05-29 江西中烟工业有限责任公司 A kind of preparation method and applications of cigarette filter combination
CN108095185A (en) * 2017-12-14 2018-06-01 江西中烟工业有限责任公司 A kind of pipe tobacco pretreating process
CN110522064A (en) * 2019-10-14 2019-12-03 中国烟草总公司郑州烟草研究院 A kind of throwing method improving discarded tobacco leaf quality
CN110680024A (en) * 2019-10-10 2020-01-14 黑龙江黑科科技有限责任公司 Preparation method of cannabis electronic tobacco shreds and cannabis electronic cigarette cartridge
CN110946316A (en) * 2018-09-27 2020-04-03 浙江中烟工业有限责任公司 Method for treating non-burning tobacco shreds by heating
CN112293788A (en) * 2019-07-31 2021-02-02 湖南中烟工业有限责任公司 Pretreated tobacco raw material for heating non-combustion tobacco products and preparation and application thereof
CN116268540A (en) * 2022-09-08 2023-06-23 广东中烟工业有限责任公司 Method for improving sensory quality of heated cigarettes

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CN102894472A (en) * 2012-09-29 2013-01-30 福建中烟工业有限责任公司 Method for improving sensory quality of tobacco leaves by using compound enzymic preparation
CN104366688A (en) * 2014-11-27 2015-02-25 湖南中烟工业有限责任公司 Method for improving inapplicable upper tobacco leaf raw material quality
CN104705779A (en) * 2015-01-28 2015-06-17 中国烟草总公司郑州烟草研究院 Processing method for improving cut stem quality
CN105326086A (en) * 2015-11-25 2016-02-17 红云红河烟草(集团)有限责任公司 Method for increasing alcohol thickness and sweet smell of tobacco flakes by using compound enzyme preparation

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US3513857A (en) * 1967-12-26 1970-05-26 Philip Morris Inc Process for the treatment of tobacco stems
CN101228967A (en) * 2007-12-26 2008-07-30 广东中烟工业公司 Method of improving cabo quality
CN102894472A (en) * 2012-09-29 2013-01-30 福建中烟工业有限责任公司 Method for improving sensory quality of tobacco leaves by using compound enzymic preparation
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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107156897A (en) * 2017-07-07 2017-09-15 重庆中烟工业有限责任公司 A kind of apparatus and method for preparing tobacco tar
CN108077997A (en) * 2017-12-12 2018-05-29 江西中烟工业有限责任公司 A kind of preparation method and applications of cigarette filter combination
CN108095185A (en) * 2017-12-14 2018-06-01 江西中烟工业有限责任公司 A kind of pipe tobacco pretreating process
CN108095185B (en) * 2017-12-14 2020-05-05 江西中烟工业有限责任公司 Tobacco shred pretreatment process
CN110946316A (en) * 2018-09-27 2020-04-03 浙江中烟工业有限责任公司 Method for treating non-burning tobacco shreds by heating
CN112293788A (en) * 2019-07-31 2021-02-02 湖南中烟工业有限责任公司 Pretreated tobacco raw material for heating non-combustion tobacco products and preparation and application thereof
CN110680024A (en) * 2019-10-10 2020-01-14 黑龙江黑科科技有限责任公司 Preparation method of cannabis electronic tobacco shreds and cannabis electronic cigarette cartridge
CN110522064A (en) * 2019-10-14 2019-12-03 中国烟草总公司郑州烟草研究院 A kind of throwing method improving discarded tobacco leaf quality
CN116268540A (en) * 2022-09-08 2023-06-23 广东中烟工业有限责任公司 Method for improving sensory quality of heated cigarettes

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