CN105924241A - Phytohormone-containing slow-release fertilizer for soybeans and preparation method thereof - Google Patents

Phytohormone-containing slow-release fertilizer for soybeans and preparation method thereof Download PDF

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CN105924241A
CN105924241A CN201610271755.4A CN201610271755A CN105924241A CN 105924241 A CN105924241 A CN 105924241A CN 201610271755 A CN201610271755 A CN 201610271755A CN 105924241 A CN105924241 A CN 105924241A
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water
release fertilizer
mixed liquor
phytohormone
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郭亚培
秦丽敏
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Pingdingshan Lvhe Agricultural Technology Development Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C3/00Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
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    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
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    • C05FERTILISERS; MANUFACTURE THEREOF
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    • C05F1/00Fertilisers made from animal corpses, or parts thereof
    • C05F1/005Fertilisers made from animal corpses, or parts thereof from meat-wastes or from other wastes of animal origin, e.g. skins, hair, hoofs, feathers, blood
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/30Layered or coated, e.g. dust-preventing coatings
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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Abstract

The invention discloses phytohormone-containing slow-release fertilizer for soybeans and a preparation method thereof. The preparation method comprises mixing peanut shells, chicken manure, shell powder, pyrethrum, mint leaves and egg shell powder according to a certain ratio to obtain a ferment material, adding fine-pored silica gel into the ferment material, mixing the ferment material, Chinese medical stone, diatomite, carbendazim, kaolin and phoxim missible oil to obtain a mixture as a coating component, mixing manganese sulfate, urea, sodium alginate, peat, borax, ammonium molybdate and a growth stimulator to obtain a core, putting the core into a coating machine and carrying out processing to obtain the phytohormone-containing slow-release fertilizer. The phytohormone-containing slow-release fertilizer is novel fertilizer with effects of killing inserts, supplying elements for plants and promoting plant growth through phytohormone, contains rhizobia for helping nitrogen fixation to improve a yield, satisfies soybean growth rule requirements on elements, does not pollute the environment, observably improves a soybean yield and is suitable for promotion and development in the soybean planting industry.

Description

A kind of Semen sojae atricolor slow-release fertilizer containing phytohormone and preparation method thereof
Technical field
The invention belongs to the Technology field of fertilizer, a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone and preparation method thereof.
Background technology
Semen sojae atricolor is distributed in China various places as one of the staple crops of China, plantation, and annual cultivated area is big, the market demand is big, for Semen sojae atricolor typically all refers to its seed, it contains rich in protein, is commonly used to make various bean product, squeeze Oleum Glycines, make soy sauce and extract protein.Plantation Semen sojae atricolor must take into account yield and quality, the rule found out during the plantation for a long time of existing soybean planting technology Dou Shi peasant household oneself, the most extensive plantation can cause the element using fertilizer in planting process and each element ratio to grasp bad, do not reach the effect of optimization, cause the waste of fertilizer, and soybean yields can be caused to reduce, the adverse consequences such as deficiency in economic performance.
Abscisic acid is again dormin, is a kind of material with sesquiterpene structure of isolated from children's phase cotton boll the earliest, is one of six big natural phytohormones, is widely present and plant kingdom being present in various organ.In the tissue of normal growth, the content of abscisic acid is the lowest, but in ripe and aging tissues maybe will enter the organ of resting state, the content of abscisic acid is the highest.Under adverse environmental factor, plant endogenous ABA content increases sharply, and abscisic acid has promotion Stoma of Leaves to close, and strengthens stress resistance of plant, promotes seed normal development, promotes and maintain seed dormancy, the physiological action of suppression seed germination.
Gibberellins, is the class phytohormone being widely present, and its chemical constitution belongs to Diterpenes acid, Fourth Ring skeleton derive and obtain.The growth of leaf and bud can be stimulated.Known gibberellins kind at least 38 kinds.Gibberellins is applied to agricultural production, has better effects in some aspects.Such as improve Zante currant yield, break Rhizoma Solani tuber osi dormancy;When beer brewing, promote to prepare the sprouting of the barley seed of maltose with gibberellins;When late rice is met overcast and rainy low temperature and ears slow, heading can be promoted with gibberellin treatment;Or in breeding of hybrid rice florescence alternation so that Parent flower synchronization etc..
The compound that ethylene is made up of two carbon atoms and four hydrogen atoms.Connect with double bond between two carbon atoms.Ethylene is present in some tissue, organ of plant, methionine be transformed under conditions of oxygen supply abundance.Ethylene is the basic chemical raw materials of synthetic fibers, synthetic rubber, synthetic plastic, synthesizing alcohol, it is also used for manufacturing vinyl chloride, styrene, oxirane, acetic acid, acetaldehyde, ethanol and explosive etc., still can be used as the ripener of fruits and vegetables, be a kind of certified phytohormone.Ethylene is one of chemical products that yield is maximum in the world, and ethylene industry is the core of petrochemical industry, and ethylene product accounts for more than the 75% of petroleum chemicals, occupies an important position in national economy.The most using ethylene yield as one of important symbol weighing a national oil development of chemical industry level.Physiological action is: triple response, promote fruit maturation, promote leaf senile, inducing adventitious root and root hair are raw, break plant seed and the dormancy of bud, the many flowering of plant of suppression, can change the sex differentiation direction etc. of flower in synoecy plant in early days at flower development.
At present, there is not yet and use various plants hormone with the use of to improve reporting for work of soybean yields in plant slow-release fertilizer.
Summary of the invention
In order to solve the problems referred to above, it is an object of the invention to a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone and preparation method thereof, on the one hand common farm manure is utilized, on the other hand in conventional fertilizers, with the addition of growth stimulator, slowly discharge during plant growing, it is possible to significantly improve the yield of Semen sojae atricolor.
The present invention is to solve that the technical scheme that the problems referred to above are taked is:
A kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, according to weight ratio, described slow-release fertilizer is by 50-70 part Pericarppium arachidis hypogaeae, 15-25 part conch meal, 20-45 part kieselguhr, 20-40 part chicken manure, 5-15 part Kiselgel A, 15-35 part Maifanitum, 5-8 part manganese sulfate, 25-40 part agstone, 25-40 part plant ash, 25-40 part carbamide, 2-4 part sodium alginate, 10-14 part carbendazim, 25-40 part Kaolin, 2-4 part mentha leave, 3-10 part phoxim emulsifiable concentrate, 3-10 part Pyrethrum, 15-40 part peat, 3-10 part Borax, 25-40 part egg shell powder, 2-4 part ammonium molybdate, 4-8 part growth stimulator, 2-4 part nutritional solution and 4-10 part peplos agent composition;
The preparation process of described nutritional solution is: calcium phosphate 20-30g, potassium dihydrogen phosphate 30-50g, heteroauxing potassium 0.3-0.5g, rihizobium japonicum 5-10mL, ammonium sulfate 6-10g and magnesium sulfate 10-15g is joined in 5L distilled water and fully dissolves and mix homogeneously, gained is nutritional solution, and the living bacteria count content every milliliter of described rihizobium japonicum is more than or equal to 2,000,000,000;
nullDescribed peplos agent is made up of following raw material according to weight ratio: 1-3 part divinylbenzene、0.5-1 part potassium peroxydisulfate、2-4 part glycerol、2-4 part acetic acid、5-10 part bamboo charcoal powder、5-15 part calcium carbonate、3-7 part melamine resin、5-15 part isopropanol、5-8 part ethanol、8-16 part agstone、2-6 part Oleum Terebinthinae、5-10 part cyclodextrin、8-16 part sodium peroxide、3-6 part stearic acid、3-5 part formaldehyde and 40-60 part water,The preparation method of described peplos agent is to take isopropanol according to aforementioned proportion to add the water of 4 times amount and be diluted obtaining mixed liquor a,Again by Oleum Terebinthinae、Divinylbenzene and melamine resin join mix homogeneously in ethanol and obtain mixed liquor b,By mixed liquor a、Mixed liquor b and potassium peroxydisulfate、Glycerol、Agstone、Bamboo charcoal powder、Acetic acid、Calcium carbonate、Cyclodextrin、Sodium peroxide、Stearic acid、Formaldehyde、After remaining water is mixed into Emulsion,Be dried to water content be 35% prepare;
nullThe process for preparation of described growth stimulator is to choose the abscisic acid of 20-60mg to be dissolved completely in the dehydrated alcohol of 50mL,It is settled to 1.5L with distilled water,It is subsequently adding the 2-acrylic acrylic acid of 0.2-1.5g and the gibberellins diluent mix homogeneously of 15-30mL,The sucrose stirring of the potassium dihydrogen phosphate and 3-4.5g that add 0.3-1.1g is melted and mix homogeneously,With this mixed liquor of distilled water constant volume to 2L,Mixed liquor is injected airtight water storage box,Water storage box is bled and makes negative pressure state,Start the gas-liquid mixing pump in water storage box,Mix with the obtained mixeding liquid volume ratio than 1:500-1:300 according to ethylene,Mixed process continues 30-60min,Make mixed liquor is formed small suspension ethylene bubble,After the mixed liquor of the band suspended bubble prepared and the water dilution proportion according to mass ratio 1:10,The diluent obtained is growth stimulator;
Described gibberellins diluent is to add pure for 1g gibberellins in 3-5mL dehydrated alcohol to dissolve, and is settled to 100L with distilled water and i.e. obtains the diluent of 10ppm.
Described slow-release fertilizer includes 60 parts of Pericarppium arachidis hypogaeaes, 20 parts of conch meals, 32 parts of kieselguhr, 30 parts of chicken manures, 10 parts of Kiselgel As, 25 parts of Maifanitums, 6.5 parts of manganese sulfates, 32 parts of agstones, 32 parts of plant ash, 32 parts of carbamide, 3 parts of sodium alginates, 12 parts of carbendazim, 32 parts of Kaolin, 3 parts of mentha leavves, 6.5 parts of phoxim emulsifiable concentrates, 6.5 portions of Pyrethrum, 28 parts of peat, 6.5 parts of Boraxs, 32 parts of egg shell powders, 3 parts of ammonium molybdates, 6 parts of growth stimulators, 3 parts of nutritional solutions and 7 parts of peplos agent.
Described peplos agent is made up of following raw material according to weight ratio: 2 parts of divinylbenzene, 0.75 part of potassium peroxydisulfate, 3 parts of glycerol, 2-4 part acetic acid, 8 parts of bamboo charcoal powder, 10 parts of calcium carbonate, 5 parts of melamine resins, 10 parts of isopropanols, 6 parts of ethanol, 12 parts of agstones, 4 parts of Oleum Terebinthinaes, 8 parts of cyclodextrin, 12 parts of sodium peroxides, 5 parts of stearic acid, 4 parts of formaldehyde and 50 parts of water.
The preparation method of a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone: comprise the following steps:
Step one, according to aforementioned proportion mixing Pericarppium arachidis hypogaeae, chicken manure, conch meal, Pyrethrum, mentha leave and egg shell powder, be crushed to 50 mesh, spray suitable quantity of water to adjust water content to 40%, heap fermentation 30 days, stir every day twice, obtain fermentation material;
Step 2, Kiselgel A is joined in fermentation material, and mix with Maifanitum, kieselguhr, carbendazim, Kaolin and phoxim emulsifiable concentrate, grind to form the homogenate that fineness is 200 mesh, as outsourcing composition;
Step 3, carry out being mixed to get compound by manganese sulfate, carbamide, sodium alginate, peat, Borax, ammonium molybdate and growth stimulator, the water adding 4 times amount in compound carries out heated and stirred, heating-up temperature is 56 DEG C, add agstone and plant ash is slowly stirred 1h, make the kernel of diameter 5mm after drying;
Step 4, kernel is put in coating machine, at 60-80 DEG C, outsourcing composition is uniformly wrapped in core surface, Jacket thickness is 3mm, be bundled into outside point outer the most uniformly sprays nutritional solution, outermost layer sprays 4-10 part peplos agent, thickness is 0.2mm, and cold air drying to water content is 10%, obtains the Semen sojae atricolor slow-release fertilizer containing phytohormone.
Beneficial effects of the present invention:
A kind of Semen sojae atricolor slow-release fertilizer containing phytohormone of the present invention and preparation method thereof, it is added with Pyrethrum in the raw material of slow-release fertilizer, controllably descend the generation of insect, yield is improved from side, and slow-release fertilizer slowly discharges the efficacy of a drug, extend the lasting period, comparatively safe for plant and surrounding, N P and K reasonable mixture ratio in the dispensing of slow-release fertilizer, the release of nutritional labeling meets Semen sojae atricolor needs fertile rule, separately in nutritional solution, with the addition of rihizobium japonicum, belong to bio-bacterial manure, seedling absorbed nitrogen element can be helped at the beginning of soybean kernel is sprouted, improve germination and the survival rate of soybean kernel;And the effective ingredient in raw material of the present invention is released in the vicinity of soybean root system and can play the effect of protection soybean root system, containing abscisic acid in growth stimulator, can be metabolized by Oxidation and combination.Abscisic acid can stimulate the generation of ethylene, urge fruit maturation, its suppression DNA (deoxyribonucleic acid) and synthesis of protein, ethylene bubble then can promote the synthesis of RNA and protein, and the saturating property of cell membrane can be made in higher plant body to increase, and accelerates Repiration, thus when in fruit, ethylene contents increases, the auxin synthesized can be decomposed by the light of the enzyme in plant or the external world again, promotes the conversion of wherein organic substance, hasting of maturity further.
In sum, Semen sojae atricolor slow-release fertilizer containing phytohormone of the present invention and preparation method thereof, it is collection deinsectization, supplements needed for plant element and utilize phytohormone to promote the new-type fertilizer of its growth triplicity, and in slow-release fertilizer, with the addition of root nodule bacteria, help Semen sojae atricolor fixed nitrogen to improve yield, each component proportion science in described slow-release fertilizer, meet the Semen sojae atricolor growth rhythm demand to each element, the yield of Semen sojae atricolor can be significantly improved on the premise of free from environmental pollution, be suitable to Popularization And Development in soybean planting industry.
Detailed description of the invention
In conjunction with specific examples below, the present invention is described in further detail, and protection scope of the present invention is not limited to following example.Implementing the process of the present invention, condition, reagent, experimental technique etc., outside the lower content mentioned specially, be universal knowledege and the common knowledge of this area, the present invention is not particularly limited content.
Embodiment 1
The preparation method of a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, comprises the following steps:
Step one, according to aforementioned proportion 50 parts of Pericarppium arachidis hypogaeaes of mixing, 20 parts of chicken manures, 15 parts of conch meals, 3 portions of Pyrethrum, 2 parts of mentha leavves and 25 parts of egg shell powders, it is crushed to 50 mesh, sprays suitable quantity of water with adjustment water content to 40%, heap fermentation 30 days, stir every day twice, obtain fermentation material;
Step 2,5 parts of Kiselgel As are joined in fermentation material, and mix with 15 parts of Maifanitums, 20 parts of kieselguhr, 10 parts of carbendazim, 25 parts of Kaolin and 3 parts of phoxim emulsifiable concentrates, grind to form the homogenate that fineness is 200 mesh, as outsourcing composition;
Step 3, carry out being mixed to get compound by 5-8 part manganese sulfate, 25 parts of carbamide, 2 parts of sodium alginates, 15 parts of peat, 3 parts of Boraxs, 2 parts of ammonium molybdates and 4 parts of growth stimulators, the water adding 4 times amount in compound carries out heated and stirred, heating-up temperature is 56 DEG C, add 25 parts of agstones and 25 parts of plant ash are slowly stirred 1h, make the kernel of diameter 5mm after drying;
Step 4, kernel is put in coating machine, at 60 DEG C, outsourcing composition is uniformly wrapped in core surface, Jacket thickness is 3mm, be bundled into outside point outer the most uniformly sprays nutritional solution, outermost layer sprays 4 parts of peplos agent, thickness is 0.2mm, and cold air drying to water content is 10%, obtains the Semen sojae atricolor slow-release fertilizer containing phytohormone.
The preparation process of described nutritional solution is: described nutritional solution fully dissolves and mix homogeneously for calcium phosphate 20g, potassium dihydrogen phosphate 30g, heteroauxing potassium 0.3g, rihizobium japonicum 5mL, ammonium sulfate 6g and magnesium sulfate 10g being joined in 5L distilled water, gained is nutritional solution, and the living bacteria count content every milliliter of described rihizobium japonicum is more than or equal to 2,000,000,000;
nullWherein said peplos agent is made up of following raw material according to weight ratio: 1 part of divinylbenzene、0.5 part of potassium peroxydisulfate、2 parts of glycerol、2 parts of acetic acid、5 parts of bamboo charcoal powder、5 parts of calcium carbonate、3 parts of melamine resins、5 parts of isopropanols、5 parts of ethanol、8 parts of agstones、2 parts of Oleum Terebinthinaes、5 parts of cyclodextrin、8 parts of sodium peroxides、3 parts of stearic acid、3 parts of formaldehyde and 40 parts of water,The preparation method of described peplos agent is to take isopropanol according to aforementioned proportion to add the water of 4 times amount and be diluted obtaining mixed liquor a,Again by Oleum Terebinthinae、Divinylbenzene and melamine resin join mix homogeneously in ethanol and obtain mixed liquor b,By mixed liquor a、Mixed liquor b and potassium peroxydisulfate、Glycerol、Agstone、Bamboo charcoal powder、Acetic acid、Calcium carbonate、Cyclodextrin、Sodium peroxide、Stearic acid、Formaldehyde、After remaining water is mixed into Emulsion,Be dried to water content be 35% prepare;
nullThe process for preparation of described growth stimulator is to choose the abscisic acid of 20mg to be dissolved completely in the dehydrated alcohol of 50mL,It is settled to 1.5L with distilled water,It is subsequently adding the 2-acrylic acrylic acid of 0.2g and the gibberellins diluent mix homogeneously of 15mL,The sucrose stirring of the potassium dihydrogen phosphate and 3g that add 0.3g is melted and mix homogeneously,With this mixed liquor of distilled water constant volume to 2L,Mixed liquor is injected airtight water storage box,Water storage box is bled and makes negative pressure state,Start the gas-liquid mixing pump in water storage box,Mix with the obtained mixeding liquid volume ratio than 1:500 according to ethylene,Mixed process continues 30min,Make mixed liquor is formed small suspension ethylene bubble,After the mixed liquor of the band suspended bubble prepared and the water dilution proportion according to mass ratio 1:10,The diluent obtained is growth stimulator;
Described gibberellins diluent is to add pure for 1g gibberellins in 3mL dehydrated alcohol to dissolve, and is settled to 100L with distilled water and i.e. obtains the diluent of 10ppm.
Embodiment 2
The preparation method of a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, comprises the following steps:
Step one, according to aforementioned proportion 55 parts of Pericarppium arachidis hypogaeaes of mixing, 25 parts of chicken manures, 17 parts of conch meals, 5 portions of Pyrethrum, 2.5 parts of mentha leavves and 28 parts of egg shell powders, it is crushed to 50 mesh, sprays suitable quantity of water with adjustment water content to 40%, heap fermentation 30 days, stir every day twice, obtain fermentation material;
Step 2,8 parts of Kiselgel As are joined in fermentation material, and mix with 20 parts of Maifanitums, 27 parts of kieselguhr, 11 parts of carbendazim, 28 parts of Kaolin and 4.5 parts of phoxim emulsifiable concentrates, grind to form the homogenate that fineness is 200 mesh, as outsourcing composition;
Step 3, carry out being mixed to get compound by 6 parts of manganese sulfates, 28 parts of carbamide, 2.5 parts of sodium alginates, 21 parts of peat, 4 parts of Boraxs, 2.5 parts of ammonium molybdates and 5 parts of growth stimulators, the water adding 4 times amount in compound carries out heated and stirred, heating-up temperature is 56 DEG C, add 28 parts of agstones and 28 parts of plant ash are slowly stirred 1h, make the kernel of diameter 5mm after drying;
Step 4, kernel is put in coating machine, at 65 DEG C, outsourcing composition is uniformly wrapped in core surface, Jacket thickness is 3mm, be bundled into outside point outer the most uniformly sprays nutritional solution, outermost layer sprays 5.5 parts of peplos agent, thickness is 0.2mm, and cold air drying to water content is 10%, obtains the Semen sojae atricolor slow-release fertilizer containing phytohormone.
The preparation process of described nutritional solution is: described nutritional solution fully dissolves and mix homogeneously for calcium phosphate 23g, potassium dihydrogen phosphate 35g, heteroauxing potassium 0.35g, rihizobium japonicum 6mL, ammonium sulfate 7g and magnesium sulfate 11g being joined in 5L distilled water, gained is nutritional solution, and the living bacteria count content every milliliter of described rihizobium japonicum is more than or equal to 2,000,000,000;
nullWherein said peplos agent is made up of following raw material according to weight ratio: 1.5 parts of divinylbenzene、0.6 part of potassium peroxydisulfate、2.5 parts of glycerol、2.5 parts of acetic acid、6 parts of bamboo charcoal powder、8 parts of calcium carbonate、4 parts of melamine resins、8 parts of isopropanols、5.5 parts of ethanol、10 parts of agstones、3 parts of Oleum Terebinthinaes、6 parts of cyclodextrin、10 parts of sodium peroxides、4 parts of stearic acid、3.5 parts of formaldehyde and 45 parts of water,The preparation method of described peplos agent is to take isopropanol according to aforementioned proportion to add the water of 4 times amount and be diluted obtaining mixed liquor a,Again by Oleum Terebinthinae、Divinylbenzene and melamine resin join mix homogeneously in ethanol and obtain mixed liquor b,By mixed liquor a、Mixed liquor b and potassium peroxydisulfate、Glycerol、Agstone、Bamboo charcoal powder、Acetic acid、Calcium carbonate、Cyclodextrin、Sodium peroxide、Stearic acid、Formaldehyde、After remaining water is mixed into Emulsion,Be dried to water content be 35% prepare;
nullThe process for preparation of described growth stimulator is to choose the abscisic acid of 30mg to be dissolved completely in the dehydrated alcohol of 50mL,It is settled to 1.5L with distilled water,It is subsequently adding the 2-acrylic acrylic acid of 0.6g and the gibberellins diluent mix homogeneously of 18mL,The sucrose stirring of the potassium dihydrogen phosphate and 3.5g that add 0.6g is melted and mix homogeneously,With this mixed liquor of distilled water constant volume to 2L,Mixed liquor is injected airtight water storage box,Water storage box is bled and makes negative pressure state,Start the gas-liquid mixing pump in water storage box,Mix with the obtained mixeding liquid volume ratio than 1:400 according to ethylene,Mixed process continues 40min,Make mixed liquor is formed small suspension ethylene bubble,After the mixed liquor of the band suspended bubble prepared and the water dilution proportion according to mass ratio 1:10,The diluent obtained is growth stimulator;
Described gibberellins diluent is to add pure for 1g gibberellins in 3.5mL dehydrated alcohol to dissolve, and is settled to 100L with distilled water and i.e. obtains the diluent of 10ppm.
Embodiment 3
The preparation method of a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, comprises the following steps:
Step one, according to aforementioned proportion 60 parts of Pericarppium arachidis hypogaeaes of mixing, 30 parts of chicken manures, 20 parts of conch meals, 6.5 portions of Pyrethrum, 3 parts of mentha leavves and 32 parts of egg shell powders, it is crushed to 50 mesh, sprays suitable quantity of water with adjustment water content to 40%, heap fermentation 30 days, stir every day twice, obtain fermentation material;
Step 2,10 parts of Kiselgel As are joined in fermentation material, and mix with 25 parts of Maifanitums, 32 parts of kieselguhr, 12 parts of carbendazim, 32 parts of Kaolin and 6.5 parts of phoxim emulsifiable concentrates, grind to form the homogenate that fineness is 200 mesh, as outsourcing composition;
Step 3, carry out being mixed to get compound by 6.5 parts of manganese sulfates, 32 parts of carbamide, 3 parts of sodium alginates, 28 parts of peat, 6.5 parts of Boraxs, 3 parts of ammonium molybdates and 6 parts of growth stimulators, the water adding 4 times amount in compound carries out heated and stirred, heating-up temperature is 56 DEG C, add 32 parts of agstones and 32 parts of plant ash are slowly stirred 1h, make the kernel of diameter 5mm after drying;
Step 4, kernel is put in coating machine, at 70 DEG C, outsourcing composition is uniformly wrapped in core surface, Jacket thickness is 3mm, be bundled into outside point outer the most uniformly sprays nutritional solution, outermost layer sprays 7 parts of peplos agent, thickness is 0.2mm, and cold air drying to water content is 10%, obtains the Semen sojae atricolor slow-release fertilizer containing phytohormone.
The preparation process of described nutritional solution is: described nutritional solution fully dissolves and mix homogeneously for calcium phosphate 25g, potassium dihydrogen phosphate 40g, heteroauxing potassium 0.4g, rihizobium japonicum 7mL, ammonium sulfate 8g and magnesium sulfate 12g being joined in 5L distilled water, gained is nutritional solution, and the living bacteria count content every milliliter of described rihizobium japonicum is more than or equal to 2,000,000,000;
nullWherein said peplos agent is made up of following raw material according to weight ratio: 2 parts of divinylbenzene、0.75 part of potassium peroxydisulfate、3 parts of glycerol、2-4 part acetic acid、8 parts of bamboo charcoal powder、10 parts of calcium carbonate、5 parts of melamine resins、10 parts of isopropanols、6 parts of ethanol、12 parts of agstones、4 parts of Oleum Terebinthinaes、8 parts of cyclodextrin、12 parts of sodium peroxides、5 parts of stearic acid、4 parts of formaldehyde and 50 parts of water,The preparation method of described peplos agent is to take isopropanol according to aforementioned proportion to add the water of 4 times amount and be diluted obtaining mixed liquor a,Again by Oleum Terebinthinae、Divinylbenzene and melamine resin join mix homogeneously in ethanol and obtain mixed liquor b,By mixed liquor a、Mixed liquor b and potassium peroxydisulfate、Glycerol、Agstone、Bamboo charcoal powder、Acetic acid、Calcium carbonate、Cyclodextrin、Sodium peroxide、Stearic acid、Formaldehyde、After remaining water is mixed into Emulsion,Be dried to water content be 35% prepare;
nullThe process for preparation of described growth stimulator is to choose the abscisic acid of 40mg to be dissolved completely in the dehydrated alcohol of 50mL,It is settled to 1.5L with distilled water,It is subsequently adding the 2-acrylic acrylic acid of 0.8g and the gibberellins diluent mix homogeneously of 23mL,The sucrose stirring of the potassium dihydrogen phosphate and 3.8g that add 0.8g is melted and mix homogeneously,With this mixed liquor of distilled water constant volume to 2L,Mixed liquor is injected airtight water storage box,Water storage box is bled and makes negative pressure state,Start the gas-liquid mixing pump in water storage box,Mix with the obtained mixeding liquid volume ratio than 1:450 according to ethylene,Mixed process continues 45min,Make mixed liquor is formed small suspension ethylene bubble,After the mixed liquor of the band suspended bubble prepared and the water dilution proportion according to mass ratio 1:10,The diluent obtained is growth stimulator;
Described gibberellins diluent is to add pure for 1g gibberellins in 4mL dehydrated alcohol to dissolve, and is settled to 100L with distilled water and i.e. obtains the diluent of 10ppm.
Embodiment 4
The preparation method of a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, comprises the following steps:
Step one, according to aforementioned proportion 65 parts of Pericarppium arachidis hypogaeaes of mixing, 35 parts of chicken manures, 23 parts of conch meals, 9 portions of Pyrethrum, 3.5 parts of mentha leavves and 38 parts of egg shell powders, it is crushed to 50 mesh, sprays suitable quantity of water with adjustment water content to 40%, heap fermentation 30 days, stir every day twice, obtain fermentation material;
Step 2,13 parts of Kiselgel As are joined in fermentation material, and mix with 31 parts of Maifanitums, 40 parts of kieselguhr, 13 parts of carbendazim, 38 parts of Kaolin and 8 parts of phoxim emulsifiable concentrates, grind to form the homogenate that fineness is 200 mesh, as outsourcing composition;
Step 3, carry out being mixed to get compound by 7.5 parts of manganese sulfates, 38 parts of carbamide, 3.5 parts of sodium alginates, 35 parts of peat, 9 parts of Boraxs, 3.5 parts of ammonium molybdates and 7.5 parts of growth stimulators, the water adding 4 times amount in compound carries out heated and stirred, heating-up temperature is 56 DEG C, add 38 parts of agstones and 38 parts of plant ash are slowly stirred 1h, make the kernel of diameter 5mm after drying;
Step 4, kernel is put in coating machine, at 75 DEG C, outsourcing composition is uniformly wrapped in core surface, Jacket thickness is 3mm, be bundled into outside point outer the most uniformly sprays nutritional solution, outermost layer sprays 8 parts of peplos agent, thickness is 0.2mm, and cold air drying to water content is 10%, obtains the Semen sojae atricolor slow-release fertilizer containing phytohormone.
The preparation process of described nutritional solution is: described nutritional solution fully dissolves and mix homogeneously for calcium phosphate 28g, potassium dihydrogen phosphate 45g, heteroauxing potassium 0.45g, rihizobium japonicum 9mL, ammonium sulfate 9g and magnesium sulfate 14g being joined in 5L distilled water, gained is nutritional solution, and the living bacteria count content every milliliter of described rihizobium japonicum is more than or equal to 2,000,000,000;
nullWherein said peplos agent is made up of following raw material according to weight ratio: 2.5 parts of divinylbenzene、0.9 part of potassium peroxydisulfate、3.5 parts of glycerol、3.5 parts of acetic acid、9 parts of bamboo charcoal powder、13 parts of calcium carbonate、5.5 parts of melamine resins、13 parts of isopropanols、5-8 part ethanol、14 parts of agstones、5.5 parts of Oleum Terebinthinaes、9 parts of cyclodextrin、14 parts of sodium peroxides、5.5 parts of stearic acid、4.5 parts of formaldehyde and 55 parts of water,The preparation method of described peplos agent is to take isopropanol according to aforementioned proportion to add the water of 4 times amount and be diluted obtaining mixed liquor a,Again by Oleum Terebinthinae、Divinylbenzene and melamine resin join mix homogeneously in ethanol and obtain mixed liquor b,By mixed liquor a、Mixed liquor b and potassium peroxydisulfate、Glycerol、Agstone、Bamboo charcoal powder、Acetic acid、Calcium carbonate、Cyclodextrin、Sodium peroxide、Stearic acid、Formaldehyde、After remaining water is mixed into Emulsion,Be dried to water content be 35% prepare;
nullThe process for preparation of described growth stimulator is to choose the abscisic acid of 50mg to be dissolved completely in the dehydrated alcohol of 50mL,It is settled to 1.5L with distilled water,It is subsequently adding the 2-acrylic acrylic acid of 1.3g and the gibberellins diluent mix homogeneously of 25mL,The sucrose stirring of the potassium dihydrogen phosphate and 4.2g that add 0.9g is melted and mix homogeneously,With this mixed liquor of distilled water constant volume to 2L,Mixed liquor is injected airtight water storage box,Water storage box is bled and makes negative pressure state,Start the gas-liquid mixing pump in water storage box,Mix with the obtained mixeding liquid volume ratio than 1:450 according to ethylene,Mixed process continues 50min,Make mixed liquor is formed small suspension ethylene bubble,After the mixed liquor of the band suspended bubble prepared and the water dilution proportion according to mass ratio 1:10,The diluent obtained is growth stimulator;
Described gibberellins diluent is to add pure for 1g gibberellins in 4.5mL dehydrated alcohol to dissolve, and is settled to 100L with distilled water and i.e. obtains the diluent of 10ppm.
Embodiment 5
The preparation method of a kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, comprises the following steps:
Step one, according to aforementioned proportion 70 parts of Pericarppium arachidis hypogaeaes of mixing, 40 parts of chicken manures, 25 parts of conch meals, 10 portions of Pyrethrum, 4 parts of mentha leavves and 40 parts of egg shell powders, it is crushed to 50 mesh, sprays suitable quantity of water with adjustment water content to 40%, heap fermentation 30 days, stir every day twice, obtain fermentation material;
Step 2,15 parts of Kiselgel As are joined in fermentation material, and mix with 35 parts of Maifanitums, 45 parts of kieselguhr, 14 parts of carbendazim, 40 parts of Kaolin and 10 parts of phoxim emulsifiable concentrates, grind to form the homogenate that fineness is 200 mesh, as outsourcing composition;
Step 3, carry out being mixed to get compound by 8 parts of manganese sulfates, 40 parts of carbamide, 4 parts of sodium alginates, 40 parts of peat, 10 parts of Boraxs, 4 parts of ammonium molybdates and 8 parts of growth stimulators, the water adding 4 times amount in compound carries out heated and stirred, heating-up temperature is 56 DEG C, add 40 parts of agstones and 40 parts of plant ash are slowly stirred 1h, make the kernel of diameter 5mm after drying;
Step 4, kernel is put in coating machine, at 80 DEG C, outsourcing composition is uniformly wrapped in core surface, Jacket thickness is 3mm, be bundled into outside point outer the most uniformly sprays nutritional solution, outermost layer sprays 10 parts of peplos agent, thickness is 0.2mm, and cold air drying to water content is 10%, obtains the Semen sojae atricolor slow-release fertilizer containing phytohormone.
The preparation process of described nutritional solution is: calcium phosphate 30g, potassium dihydrogen phosphate 50g, heteroauxing potassium 0.5g, rihizobium japonicum 10mL, ammonium sulfate 10g and magnesium sulfate 15g is joined in 5L distilled water and fully dissolves and mix homogeneously, gained is nutritional solution, and the living bacteria count content every milliliter of described rihizobium japonicum is more than or equal to 2,000,000,000;
nullWherein said peplos agent is made up of following raw material according to weight ratio: 3 parts of divinylbenzene、1 part of potassium peroxydisulfate、4 parts of glycerol、4 parts of acetic acid、10 parts of bamboo charcoal powder、15 parts of calcium carbonate、7 parts of melamine resins、15 parts of isopropanols、8 parts of ethanol、16 parts of agstones、6 parts of Oleum Terebinthinaes、10 parts of cyclodextrin、16 parts of sodium peroxides、6 parts of stearic acid、5 parts of formaldehyde and 60 parts of water,The preparation method of described peplos agent is to take isopropanol according to aforementioned proportion to add the water of 4 times amount and be diluted obtaining mixed liquor a,Again by Oleum Terebinthinae、Divinylbenzene and melamine resin join mix homogeneously in ethanol and obtain mixed liquor b,By mixed liquor a、Mixed liquor b and potassium peroxydisulfate、Glycerol、Agstone、Bamboo charcoal powder、Acetic acid、Calcium carbonate、Cyclodextrin、Sodium peroxide、Stearic acid、Formaldehyde、After remaining water is mixed into Emulsion,Be dried to water content be 35% prepare;
nullThe process for preparation of described growth stimulator is to choose the abscisic acid of 60mg to be dissolved completely in the dehydrated alcohol of 50mL,It is settled to 1.5L with distilled water,It is subsequently adding the 2-acrylic acrylic acid of 1.5g and the gibberellins diluent mix homogeneously of 30mL,The sucrose stirring of the potassium dihydrogen phosphate and 4.5g that add 1.1g is melted and mix homogeneously,With this mixed liquor of distilled water constant volume to 2L,Mixed liquor is injected airtight water storage box,Water storage box is bled and makes negative pressure state,Start the gas-liquid mixing pump in water storage box,Mix with the obtained mixeding liquid volume ratio than 1:300 according to ethylene,Mixed process continues 60min,Make mixed liquor is formed small suspension ethylene bubble,After the mixed liquor of the band suspended bubble prepared and the water dilution proportion according to mass ratio 1:10,The diluent obtained is growth stimulator;
Described gibberellins diluent is to add pure for 1g gibberellins in 5mL dehydrated alcohol to dissolve, and is settled to 100L with distilled water and i.e. obtains the diluent of 10ppm.

Claims (4)

1. the Semen sojae atricolor slow-release fertilizer containing phytohormone, it is characterized in that: according to weight ratio, described slow-release fertilizer is by 50-70 part Pericarppium arachidis hypogaeae, 15-25 part conch meal, 20-45 part kieselguhr, 20-40 part chicken manure, 5-15 part Kiselgel A, 15-35 part Maifanitum, 5-8 part manganese sulfate, 25-40 part agstone, 25-40 part plant ash, 25-40 part carbamide, 2-4 part sodium alginate, 10-14 part carbendazim, 25-40 part Kaolin, 2-4 part mentha leave, 3-10 part phoxim emulsifiable concentrate, 3-10 part Pyrethrum, 15-40 part peat, 3-10 part Borax, 25-40 part egg shell powder, 2-4 part ammonium molybdate, 4-8 part growth stimulator, 2-4 part nutritional solution and 4-10 part peplos agent composition;
The preparation process of described nutritional solution is: calcium phosphate 20-30g, potassium dihydrogen phosphate 30-50g, heteroauxing potassium 0.3-0.5g, rihizobium japonicum 5-10mL, ammonium sulfate 6-10g and magnesium sulfate 10-15g is joined in 5L distilled water and fully dissolves and mix homogeneously, gained is nutritional solution, and the living bacteria count content every milliliter of described rihizobium japonicum is more than or equal to 2,000,000,000;
nullDescribed peplos agent is made up of following raw material according to weight ratio: 1-3 part divinylbenzene、0.5-1 part potassium peroxydisulfate、2-4 part glycerol、2-4 part acetic acid、5-10 part bamboo charcoal powder、5-15 part calcium carbonate、3-7 part melamine resin、5-15 part isopropanol、5-8 part ethanol、8-16 part agstone、2-6 part Oleum Terebinthinae、5-10 part cyclodextrin、8-16 part sodium peroxide、3-6 part stearic acid、3-5 part formaldehyde and 40-60 part water,The preparation method of described peplos agent is to take isopropanol according to aforementioned proportion to add the water of 4 times amount and be diluted obtaining mixed liquor a,Again by Oleum Terebinthinae、Divinylbenzene and melamine resin join mix homogeneously in ethanol and obtain mixed liquor b,By mixed liquor a、Mixed liquor b and potassium peroxydisulfate、Glycerol、Agstone、Bamboo charcoal powder、Acetic acid、Calcium carbonate、Cyclodextrin、Sodium peroxide、Stearic acid、Formaldehyde、After remaining water is mixed into Emulsion,Be dried to water content be 35% prepare;
nullThe process for preparation of described growth stimulator is to choose the abscisic acid of 20-60mg to be dissolved completely in the dehydrated alcohol of 50mL,It is settled to 1.5L with distilled water,It is subsequently adding the 2-acrylic acrylic acid of 0.2-1.5g and the gibberellins diluent mix homogeneously of 15-30mL,The sucrose stirring of the potassium dihydrogen phosphate and 3-4.5g that add 0.3-1.1g is melted and mix homogeneously,With this mixed liquor of distilled water constant volume to 2L,Mixed liquor is injected airtight water storage box,Water storage box is bled and makes negative pressure state,Start the gas-liquid mixing pump in water storage box,Mix with the obtained mixeding liquid volume ratio than 1:500-1:300 according to ethylene,Mixed process continues 30-60min,Make mixed liquor is formed small suspension ethylene bubble,After the mixed liquor of the band suspended bubble prepared and the water dilution proportion according to mass ratio 1:10,The diluent obtained is growth stimulator;
Described gibberellins diluent is to add pure for 1g gibberellins in 3-5mL dehydrated alcohol to dissolve, and is settled to 100L with distilled water and i.e. obtains the diluent of 10ppm.
A kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, it is characterized in that: described slow-release fertilizer includes 60 parts of Pericarppium arachidis hypogaeaes, 20 parts of conch meals, 32 parts of kieselguhr, 30 parts of chicken manures, 10 parts of Kiselgel As, 25 parts of Maifanitums, 6.5 parts of manganese sulfates, 32 parts of agstones, 32 parts of plant ash, 32 parts of carbamide, 3 parts of sodium alginates, 12 parts of carbendazim, 32 parts of Kaolin, 3 parts of mentha leavves, 6.5 parts of phoxim emulsifiable concentrates, 6.5 portions of Pyrethrum, 28 parts of peat, 6.5 parts of Boraxs, 32 parts of egg shell powders, 3 parts of ammonium molybdates, 6 parts of growth stimulators, 3 parts of nutritional solutions and 7 parts of peplos agent.
A kind of Semen sojae atricolor slow-release fertilizer containing phytohormone, it is characterised in that: described peplos agent is made up of following raw material according to weight ratio: 2 parts of divinylbenzene, 0.75 part of potassium peroxydisulfate, 3 parts of glycerol, 2-4 part acetic acid, 8 parts of bamboo charcoal powder, 10 parts of calcium carbonate, 5 parts of melamine resins, 10 parts of isopropanols, 6 parts of ethanol, 12 parts of agstones, 4 parts of Oleum Terebinthinaes, 8 parts of cyclodextrin, 12 parts of sodium peroxides, 5 parts of stearic acid, 4 parts of formaldehyde and 50 parts of water.
A kind of preparation method of the Semen sojae atricolor slow-release fertilizer containing phytohormone, it is characterised in that: comprise the following steps:
Step one, according to aforementioned proportion mixing Pericarppium arachidis hypogaeae, chicken manure, conch meal, Pyrethrum, mentha leave and egg shell powder, be crushed to 50 mesh, spray suitable quantity of water to adjust water content to 40%, heap fermentation 30 days, stir every day twice, obtain fermentation material;
Step 2, Kiselgel A is joined in fermentation material, and mix with Maifanitum, kieselguhr, carbendazim, Kaolin and phoxim emulsifiable concentrate, grind to form the homogenate that fineness is 200 mesh, as outsourcing composition;
Step 3, carry out being mixed to get compound by manganese sulfate, carbamide, sodium alginate, peat, Borax, ammonium molybdate and growth stimulator, the water adding 4 times amount in compound carries out heated and stirred, heating-up temperature is 56 DEG C, add agstone and plant ash is slowly stirred 1h, make the kernel of diameter 5mm after drying;
Step 4, kernel is put in coating machine, at 60-80 DEG C, outsourcing composition is uniformly wrapped in core surface, Jacket thickness is 3mm, be bundled into outside point outer the most uniformly sprays nutritional solution, outermost layer sprays 4-10 part peplos agent, thickness is 0.2mm, and cold air drying to water content is 10%, obtains the Semen sojae atricolor slow-release fertilizer containing phytohormone.
CN201610271755.4A 2016-04-28 2016-04-28 Phytohormone-containing slow-release fertilizer for soybeans and preparation method thereof Pending CN105924241A (en)

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CN106665681A (en) * 2016-11-10 2017-05-17 董晓 Plant-growth regulator preparation method
CN107500827A (en) * 2017-09-10 2017-12-22 惠州市欧野科技有限公司 It is a kind of suitable for green fertilizer of soybean and preparation method thereof
CN107739239A (en) * 2017-10-26 2018-02-27 石阡县龙腾农牧农民专业合作社 The base manure and preparation method of a kind of SHUIHUANGLIAN
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CN104292018A (en) * 2014-10-22 2015-01-21 肥东县花生原种场 High-efficiency peanut planting controlled release fertilizer and preparation method thereof
CN104871684A (en) * 2015-06-12 2015-09-02 安徽徽大农业有限公司 Soybean seed germinating method
CN105461457A (en) * 2015-12-30 2016-04-06 民勤县巴腾生物有机肥料有限公司 Bio-organic fertilizer and preparing method thereof

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Publication number Priority date Publication date Assignee Title
CN1669424A (en) * 2004-03-19 2005-09-21 中国科学院过程工程研究所 Drought resisting water-loss reducing seed capsule agent and uses thereof
CN104292018A (en) * 2014-10-22 2015-01-21 肥东县花生原种场 High-efficiency peanut planting controlled release fertilizer and preparation method thereof
CN104871684A (en) * 2015-06-12 2015-09-02 安徽徽大农业有限公司 Soybean seed germinating method
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106665681A (en) * 2016-11-10 2017-05-17 董晓 Plant-growth regulator preparation method
CN107500827A (en) * 2017-09-10 2017-12-22 惠州市欧野科技有限公司 It is a kind of suitable for green fertilizer of soybean and preparation method thereof
CN107739239A (en) * 2017-10-26 2018-02-27 石阡县龙腾农牧农民专业合作社 The base manure and preparation method of a kind of SHUIHUANGLIAN
RU2690187C1 (en) * 2018-11-06 2019-05-31 Государственное бюджетное учреждение Республики Башкортостан "Научно-исследовательский технологический институт гербицидов и регуляторов роста растений с опытно-экспериментальным производством Академии наук Республики Башкортостан" Novel compound of methyl ester of 2-benzimidazolylcarbamic acid with urea modifications, having fungicidal properties, and a fungicidal agent based thereon

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