CN106665681A - Plant-growth regulator preparation method - Google Patents
Plant-growth regulator preparation method Download PDFInfo
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- CN106665681A CN106665681A CN201610990715.5A CN201610990715A CN106665681A CN 106665681 A CN106665681 A CN 106665681A CN 201610990715 A CN201610990715 A CN 201610990715A CN 106665681 A CN106665681 A CN 106665681A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/26—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/22—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom rings with more than six members
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/26—Phosphorus; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/38—Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
- C05F11/08—Organic fertilisers containing added bacterial cultures, mycelia or the like
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
Abstract
The invention discloses a plant-growth regulator preparation method, which belongs to the technical field of pesticide preparation. The plant-growth regulator preparation method comprises the following steps: processing mushroom and tremella to powder, stirring the powder with fish oil to obtain a coating agent, mixing tomato, enteromorpha, and mushroom bran for fermentation to obtain deacetic acid, vitamin and polysaccharide which are in favor of plant growth, mixing eggshell, a hydrochloric acid solution, and calcium hydrogen phosphate to obtain a mineral solution, mixing the materials with brassinolide, performing freeze drying, coating by the coating agent to obtain the plant-growth regulator. The plant-growth regulator has good broad spectrum activity, is suitable for each growth phase of different crops, has obvious regulation and promotion effects for vegetation, reduces plant insect disease after usage, increases plant resistance capability, has good storage stability, is benefit for long-term storage, and has good application prospect.
Description
Technical field
The invention discloses the preparation method of a plant growth regulators, belongs to preparation technique of pesticide field.
Background technology
The growth and development dynamics of plant are generally regulated and controled by plant endogenous hormones, because of world's frequent natural calamity, plant
Existence is faced with various adverse circumstance factor serious challenges.Due to many factors such as various historical reasons and natural environment, artificial behavior
Cause Desertification Soil area constantly to extend, fall sharply using land resource, Land capability fails, the natural calamity such as sandstorm
Evil takes place frequently, and deepens desertificated area poverty, has had a strong impact on Agriculture Production, social stability and people's lives rich.These
Factor directly results in plant percent, storage rate reduction, plant growth rate and yield, quality decline.
Plant growth regulator is the non-nutritive chemical substance of external source, can be used to regulate and control nucleic acid, the albumen in plant body
The synthesis of matter and enzyme, the different phase in plant growth and development process can such as be germinateed, be taken root, cell elongation, Organ Differentiation, flower
Bud breaks up, blooms, regulation and control action are played in result, fallen leaves, dormancy etc., generally can conduct to service portion in plant body
Position, is allowed to develop to the needs for meeting the mankind.China is one of most widely used country of plant growth regulator in the world, is planted
Thing growth regulator is China's agricultural production and development in terms of adjusting the growth promoter of crops, improving yield and improveing quality
It is made that significant contribution.
The plant growth regulator for occurring on the market at present is varied, and the species of plant growth regulator presses biochemical efficacy
Point, there are growth promoter, growth inhibitor and the big class of growth retardant 3, have more than 100 kind.Headed by agricultural production
Plant utilize among, how effectively to allow plant growing this problem to be asking of being concerned about always for plant user
Topic.The regulator of common promotion plant growing mainly has immediate effect diethyl aminoethyl hexanoate (DA-6), CPPU, compound sodium nitrophenolate, brassin, red
Mycin etc., their general character is to urge Seedling as means to reach the purpose of increasing both production and income with supplementary fertilizer, the negative consequence brought therewith
It is that the branch of plant and the strong of root system do not catch up with, causes the resistance capacity of plant low, simultaneously because existing plant growing is adjusted
Section agent broad spectrum activity is poor, is only applicable to single plant and the particular growth phase uses, and improper use can also cause poisoning, can be to plant
Growth produces inhibitory action, and existing plant growth regulator less stable, is easily affected by external environment condition change, it is difficult to
Long term storage.
The content of the invention
Present invention mainly solves technical problem：It is poor for the existing plant growth regulator wide spectrum suitability, use
Easily causing the resistance capacity of plant afterwards reduces, and improper use can also cause poisoning, and inhibitory action is produced to plant growing, and stores
Less stable, is difficult the defect of long-term preservation, there is provided a kind of organic matter and inorganic mineral compounding do growth regulatory substance, with perfume (or spice)
Mushroom, shitosan and fish oil mixed liquor do the method that coating agent prepares plant growth regulator, and the present invention is first by Lentinus Edodess and Tremella
Make and stir to obtain coating agent with fish oil etc. after powder, then by Fructus Lycopersici esculenti, Entermorpha and mushroom bran mixed fermentation, obtain desacetoxy, vitamin
With the material that polysaccharide etc. is conducive to plant growing, then eggshell is made be mixed to get mineral with hydrochloric acid, calcium hydrogen phosphate etc. after powder
Solution, finally mixes with brassin lactones etc. again, after freeze-drying process, carries out peplos with coating agent, you can obtain plant life
Long regulator, after plant growth regulator is mixed with water, coating agent can solve nutrition soluble in water, to contain in Lentinus Edodess and Tremella
Material can also promote the growth of plant, plant growth regulator of the present invention to have preferable broad spectrum activity, it is adaptable to Different Crop
Each growth stage, to plant growing have considerably adjust and facilitation, plant pest can be reduced after use, improve
The resistance capacity of plant, and bin stability is preferably, beneficial to long-term storage, with preferable application prospect.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is：
（1）100~200g Lentinus Edodess and 60~80g Tremella are weighed, after being washed with deionized 3~5 times, in being placed in baking oven, 95
1~2h of drying at~105 DEG C, dried Lentinus Edodess and Tremella is added in pulverizer and crushes 20~30min, and excessively 100~
120 mesh sieves, obtain sieving, and sieving is added in beaker, add 30~40g fish oil, 8~12g shitosans and 60~
70mL deionized waters, stirring 40~50min of mixing, obtain mixed liquor, standby；
（2）100~200g Fructus Lycopersici esculenties and 200~400g Entermorpha are weighed, the 5~10min that squeezes the juice is added in juice extractor, mixed juice is obtained
Liquid, and be added in beaker, 600~700g mushroom brans are added, after stirring 5~10min of mixing, in being transferred to fermentation tank, then divide
Not An inoculum concentration 6~8% and 8~10% to inoculation yeast bacterium and bacillus subtilises in fermentation tank, at 35~45 DEG C sealing send out
Ferment 3~4 days, treats fermentation ends, collects fermented product, in being placed in centrifuge, under 2000~3000r/min centrifugation 20~
30min, collects supernatant, and is spray-dried, and obtains dried object, standby；
（3）100~200g eggshells are weighed, 20~30min of crushing in jet mill is added to, and crosses 100~120 mesh sieves, obtained
To egg-shell meal, and it is added in beaker, adds 300~400mL mass fractions for 10% hydrochloric acid, stirring 10~15min of mixing
Afterwards, 10~15g calcium hydrogen phosphate, 6~8g magnesium chlorides and 3~5g potassium chloride are sequentially added, 10~20min is stirred, mineral are obtained
Solution；
（4）Count by weight, weigh 40~50 parts of steps（2）Standby dried object, 40~50 parts of above-mentioned Mineral Solutions, 6~8
Part humic acid and 1~3 part of brassin lactones, in being added to beaker, after stirring 3~5min of mixing, are placed in vacuum freezing drying oven
In, 24~26h is dried at -45~-30 DEG C, obtain lyophilized powder；
（5）Above-mentioned lyophilized powder is added in coating machine, then to lyophilized powder spray lyophilized powder quality 10~20% the step of（1）It is standby
Mixed liquor, to lyophilized powder peplos are carried out, and after the completion for the treatment of peplos, material are taken out, and 2~3h of natural air drying, place into powder
Crushed in broken machine, and crossed 80~100 mesh sieves, you can obtained plant growth regulator.
The present invention application process be：In mass ratio 1:1500~1:2000, by plant growth regulating obtained in the present invention
Agent is mixed homogeneously with water and is fitted in spraying machine, subsequently by medicine liquid spray after Fructus Vitis viniferae full-bloom stage 5~7 days, start grow Portugal
On the fruit ear of grape young fruit, sprayed once every 20~30 days, spray altogether 2 times, control each spray plant growth regulator consumption
For 30~50g/mu.After testing, growth of the obtained plant growth regulator of the present invention to crop has and preferably adjust and promote
To enter effect, when being relatively not used using the fruit-setting rate of ensuing crop 50~60% are improve, crop yield improves 20 when being relatively not used~
30%, while there is plant growth regulator of the present invention preferable prevention and elimination of disease and pests to act on, subtracted using ensuing crop pest and disease damage incidence rate
Lack more than 80%, effectively increased 1~2 grade of fruit quality, and plant growth regulator of the present invention has preferably storage stable
Property, under room temperature sealed environment, the shelf life was up to 3~5 years.
The invention has the beneficial effects as follows：
（1）Obtained plant growth regulator effect is significant of the invention, residual hazard are few, and just plant can be given birth to using in the case of low concentration
Important adjustment effect, and the overgrowing of energy effective control crop top are played in long, development, promote root system and branch growth, are increased and are tied
Real rate, improves fruit quality, promotees to receive so as to increase production；
（2）Plant growth regulator of the invention obtained is applicable to the multiple kinds of crops such as Semen Tritici aestivi, Semen sojae atricolor, Semen Maydiss, broad spectrum activity compared with
It is good, while the growth demand in crop each stage can effectively be met, the exceeded problem of pesticide, chemical fertilizer is reduced, crops are improved to fertilizer
The utilization rate of material, can be with controlling crop diseases and insect pests.
Specific embodiment
100~200g Lentinus Edodess and 60~80g Tremella are weighed first, after being washed with deionized 3~5 times, in being placed in baking oven,
1~2h is dried at 95~105 DEG C, dried Lentinus Edodess and Tremella are added to into 20~30min of crushing in pulverizer, and mistake
100~120 mesh sieves, obtain sieving, and sieving is added in beaker, add 30~40g fish oil, 8~12g shitosans and
60~70mL deionized waters, stirring 40~50min of mixing, obtain mixed liquor, standby；Subsequently weigh 100~200g Fructus Lycopersici esculenties and 200
~400g Entermorpha, is added in juice extractor the 5~10min that squeezes the juice, and obtains mixing juice, and is added in beaker, add 600~
700g mushroom brans, after stirring 5~10min of mixing, in being transferred to fermentation tank, then respectively by inoculum concentration 6~8% and 8~10% to fermentation
Fermentation ends are treated in inoculation yeast bacterium and bacillus subtilises in tank, sealing and fermenting 3~4 days at 35~45 DEG C, collect fermentation
Thing, in being placed in centrifuge, is centrifuged 20~30min under 2000~3000r/min, collects supernatant, and is spray-dried,
Dried object is obtained, it is standby；100~200g eggshells are weighed again, are added in jet mill and are crushed 20~30min, and excessively 100~
120 mesh sieves, obtain egg-shell meal, and are added in beaker, add 300~400mL mass fractions for 10% hydrochloric acid, stirring mixing
After 10~15min, 10~15g calcium hydrogen phosphate, 6~8g magnesium chlorides and 3~5g potassium chloride are sequentially added, stir 10~20min,
Obtain Mineral Solution；Count by weight again, weigh 40~50 parts of standby dried objects of above-mentioned steps, 40~50 parts of above-mentioned mineral
Solution, 6~8 parts of humic acid and 1~3 part of brassin lactones, in being added to beaker, after stirring 3~5min of mixing, are placed in vacuum cold
In freezing drying baker, 24~26h is dried at -45~-30 DEG C, obtains lyophilized powder；Finally above-mentioned lyophilized powder is added to into coating machine
In, then the standby mixed liquor of lyophilized powder quality 10~20% is sprayed to lyophilized powder, and peplos are carried out to lyophilized powder, treat that peplos are completed
Afterwards, material is taken out, and 2~3h of natural air drying, place in pulverizer and crushed, and cross 80~100 mesh sieves, you can obtain
Plant growth regulator.
Example 1
100g Lentinus Edodess and 60g Tremella are weighed first, after being washed with deionized 3 times, in being placed in baking oven, at 95 DEG C 1h are dried,
Dried Lentinus Edodess and Tremella are added in pulverizer and crush 20min, and cross 100 mesh sieves, obtain sieving, by sieving plus
Enter in beaker, add 30g fish oil, 8g shitosans and 60mL deionized waters, stirring mixing 40min obtains mixed liquor, standby
With；100g Fructus Lycopersici esculenties and 200g Entermorpha are subsequently weighed, the 5min that squeezes the juice is added in juice extractor, obtains mixing juice, and be added to burning
In cup, 600g mushroom brans are added, after stirring mixing 5min, in being transferred to fermentation tank, then respectively by inoculum concentration 6% and 8% to fermentation
Fermentation ends are treated in inoculation yeast bacterium and bacillus subtilises in tank, sealing and fermenting 3 days at 35 DEG C, collect fermented product, are placed in
In centrifuge, 20min is centrifuged under 2000r/min, collects supernatant, and be spray-dried, obtain dried object, it is standby；Again
100g eggshells are weighed, is added in jet mill and is crushed 20min, and cross 100 mesh sieves, obtain egg-shell meal, and be added to beaker
In, it is 10% hydrochloric acid to add 300mL mass fractions, after stirring mixing 10min, sequentially adds 10g calcium hydrogen phosphate, 6g chlorinations
Magnesium and 3g potassium chloride, stir 10min, obtain Mineral Solution；Count by weight again, weigh 40 parts of standby dryings of above-mentioned steps
Thing, 40 parts of above-mentioned Mineral Solutions, 6 parts of humic acid and 1 part of brassin lactones, in being added to beaker, after stirring mixing 3min, are placed in
In vacuum freezing drying oven, 24h is dried at -45 DEG C, obtains lyophilized powder；Finally above-mentioned lyophilized powder is added in coating machine,
Spray the standby mixed liquor of lyophilized powder quality 10% to lyophilized powder again, peplos are carried out to lyophilized powder, after the completion for the treatment of peplos, by thing
Material takes out, and natural air drying 2h, places in pulverizer and is crushed, and crosses 80 mesh sieves, you can obtain plant growth regulator.
This example operation is easy, when using, in mass ratio 1:1500, by plant growth regulator obtained in the present invention and water
Mix homogeneously is simultaneously fitted in spraying machine, subsequently by medicine liquid spray after Fructus Vitis viniferae full-bloom stage 5 days, start grow Fructus Vitis viniferae young fruit fruit
On fringe, sprayed once every 20 days, spray altogether 2 times, control each spray plant growth regulator consumption for 30g/mu.Jing is examined
Survey, growth of the obtained plant growth regulator of the present invention to crop has and preferably adjust and facilitation, using ensuing crop
Fruit-setting rate improve 50% when being relatively not used, crop yield improves 20% when being relatively not used, while plant growing of the present invention tune
There is preferable prevention and elimination of disease and pests to act on for section agent, and using ensuing crop pest and disease damage incidence rate 83% is reduced, and effectively increase fruit product
1 grade of matter, and plant growth regulator of the present invention has preferable bin stability, under room temperature sealed environment, the shelf life is up to 3
Year.
Example 2
150g Lentinus Edodess and 70g Tremella are weighed first, after being washed with deionized 4 times, in being placed in baking oven, at 100 DEG C 1h are dried,
Dried Lentinus Edodess and Tremella are added in pulverizer and crush 25min, and cross 110 mesh sieves, obtain sieving, by sieving plus
Enter in beaker, add 35g fish oil, 10g shitosans and 65mL deionized waters, stirring mixing 45min obtains mixed liquor, standby
With；150g Fructus Lycopersici esculenties and 300g Entermorpha are subsequently weighed, the 8min that squeezes the juice is added in juice extractor, obtains mixing juice, and be added to burning
In cup, 650g mushroom brans are added, after stirring mixing 8min, in being transferred to fermentation tank, then respectively by inoculum concentration 7% and 9% to fermentation
Fermentation ends are treated in inoculation yeast bacterium and bacillus subtilises in tank, sealing and fermenting 3 days at 40 DEG C, collect fermented product, are placed in
In centrifuge, 25min is centrifuged under 2500r/min, collects supernatant, and be spray-dried, obtain dried object, it is standby；Again
150g eggshells are weighed, is added in jet mill and is crushed 25min, and cross 110 mesh sieves, obtain egg-shell meal, and be added to beaker
In, it is 10% hydrochloric acid to add 350mL mass fractions, after stirring mixing 13min, sequentially adds 13g calcium hydrogen phosphate, 7g chlorinations
Magnesium and 4g potassium chloride, stir 15min, obtain Mineral Solution；Count by weight again, weigh 45 parts of standby dryings of above-mentioned steps
Thing, 45 parts of above-mentioned Mineral Solutions, 7 parts of humic acid and 2 parts of brassin lactones, in being added to beaker, after stirring mixing 4min, are placed in
In vacuum freezing drying oven, 25h is dried at -37 DEG C, obtains lyophilized powder；Finally above-mentioned lyophilized powder is added in coating machine,
Spray the standby mixed liquor of lyophilized powder quality 15% to lyophilized powder again, peplos are carried out to lyophilized powder, after the completion for the treatment of peplos, by thing
Material takes out, and natural air drying 2h, places in pulverizer and is crushed, and crosses 90 mesh sieves, you can obtain plant growth regulator.
This example operation is easy, when using, in mass ratio 1:1800, by plant growth regulator obtained in the present invention and water
Mix homogeneously is simultaneously fitted in spraying machine, subsequently by medicine liquid spray after Fructus Vitis viniferae full-bloom stage 6 days, start grow Fructus Vitis viniferae young fruit fruit
On fringe, sprayed once every 25 days, spray altogether 2 times, control each spray plant growth regulator consumption for 40g/mu.Jing is examined
Survey, growth of the obtained plant growth regulator of the present invention to crop has and preferably adjust and facilitation, using ensuing crop
Fruit-setting rate improve 55% when being relatively not used, crop yield improves 20% when being relatively not used, while plant growing of the present invention tune
There is preferable prevention and elimination of disease and pests to act on for section agent, and using ensuing crop pest and disease damage incidence rate 85% is reduced, and effectively increase fruit product
1 grade of matter, and plant growth regulator of the present invention has preferable bin stability, under room temperature sealed environment, the shelf life is up to 3
Year.
Example 3
200g Lentinus Edodess and 80g Tremella are weighed first, after being washed with deionized 5 times, in being placed in baking oven, at 105 DEG C 2h are dried,
Dried Lentinus Edodess and Tremella are added in pulverizer and crush 30min, and cross 120 mesh sieves, obtain sieving, by sieving plus
Enter in beaker, add 40g fish oil, 12g shitosans and 70mL deionized waters, stirring mixing 50min obtains mixed liquor, standby
With；200g Fructus Lycopersici esculenties and 400g Entermorpha are subsequently weighed, the 10min that squeezes the juice is added in juice extractor, obtains mixing juice, and be added to burning
In cup, 700g mushroom brans are added, after stirring mixing 10min, in being transferred to fermentation tank, then respectively by inoculum concentration 8% and 10% to sending out
Fermentation ends are treated in inoculation yeast bacterium and bacillus subtilises in fermentation tank, sealing and fermenting 4 days at 45 DEG C, collect fermented product, juxtaposition
In centrifuge, 30min is centrifuged under 3000r/min, collects supernatant, and be spray-dried, obtain dried object, it is standby；
200g eggshells are weighed again, is added in jet mill and is crushed 30min, and cross 120 mesh sieves, obtain egg-shell meal, and be added to burning
In cup, it is 10% hydrochloric acid to add 400mL mass fractions, after stirring mixing 15min, sequentially adds 15g calcium hydrogen phosphate, 8g chlorine
Change magnesium and 5g potassium chloride, stir 20min, obtain Mineral Solution；Count by weight again, weigh standby dry of 50 parts of above-mentioned steps
Dry thing, 50 parts of above-mentioned Mineral Solutions, 8 parts of humic acid and 3 parts of brassin lactones, in being added to beaker, after stirring mixing 5min, put
In vacuum freezing drying oven, 26h is dried at -30 DEG C, obtains lyophilized powder；Finally above-mentioned lyophilized powder is added to into coating machine
In, then the standby mixed liquor of lyophilized powder quality 20% is sprayed to lyophilized powder, and peplos are carried out to lyophilized powder, after the completion for the treatment of peplos, will
Material takes out, and natural air drying 3h, places in pulverizer and is crushed, and crosses 100 mesh sieves, you can obtain plant growth regulating
Agent.
This example operation is easy, when using, in mass ratio 1:2000, by plant growth regulator obtained in the present invention and water
Mix homogeneously is simultaneously fitted in spraying machine, subsequently by medicine liquid spray after Fructus Vitis viniferae full-bloom stage 7 days, start grow Fructus Vitis viniferae young fruit fruit
On fringe, sprayed once every 30 days, spray altogether 2 times, control each spray plant growth regulator consumption for 50g/mu.Jing is examined
Survey, growth of the obtained plant growth regulator of the present invention to crop has and preferably adjust and facilitation, using ensuing crop
Fruit-setting rate improve 60% when being relatively not used, crop yield improves 30% when being relatively not used, while plant growing of the present invention tune
There is preferable prevention and elimination of disease and pests to act on for section agent, and using ensuing crop pest and disease damage incidence rate 88% is reduced, and effectively increase fruit product
Matter surpasses 2 grades, and plant growth regulator of the present invention has preferable bin stability, under room temperature sealed environment, the shelf life
Up to 5 years.
Claims (1)
1. the preparation method of a plant growth regulators, it is characterised in that concrete preparation process is：
（1）100~200g Lentinus Edodess and 60~80g Tremella are weighed, after being washed with deionized 3~5 times, in being placed in baking oven, 95
1~2h of drying at~105 DEG C, dried Lentinus Edodess and Tremella is added in pulverizer and crushes 20~30min, and excessively 100~
120 mesh sieves, obtain sieving, and sieving is added in beaker, add 30~40g fish oil, 8~12g shitosans and 60~
70mL deionized waters, stirring 40~50min of mixing, obtain mixed liquor, standby；
（2）100~200g Fructus Lycopersici esculenties and 200~400g Entermorpha are weighed, the 5~10min that squeezes the juice is added in juice extractor, mixed juice is obtained
Liquid, and be added in beaker, 600~700g mushroom brans are added, after stirring 5~10min of mixing, in being transferred to fermentation tank, then divide
Not An inoculum concentration 6~8% and 8~10% to inoculation yeast bacterium and bacillus subtilises in fermentation tank, at 35~45 DEG C sealing send out
Ferment 3~4 days, treats fermentation ends, collects fermented product, in being placed in centrifuge, under 2000~3000r/min centrifugation 20~
30min, collects supernatant, and is spray-dried, and obtains dried object, standby；
（3）100~200g eggshells are weighed, 20~30min of crushing in jet mill is added to, and crosses 100~120 mesh sieves, obtained
To egg-shell meal, and it is added in beaker, adds 300~400mL mass fractions for 10% hydrochloric acid, stirring 10~15min of mixing
Afterwards, 10~15g calcium hydrogen phosphate, 6~8g magnesium chlorides and 3~5g potassium chloride are sequentially added, 10~20min is stirred, mineral are obtained
Solution；
（4）Count by weight, weigh 40~50 parts of steps（2）Standby dried object, 40~50 parts of above-mentioned Mineral Solutions, 6~8
Part humic acid and 1~3 part of brassin lactones, in being added to beaker, after stirring 3~5min of mixing, are placed in vacuum freezing drying oven
In, 24~26h is dried at -45~-30 DEG C, obtain lyophilized powder；
（5）Above-mentioned lyophilized powder is added in coating machine, then to lyophilized powder spray lyophilized powder quality 10~20% the step of（1）It is standby
Mixed liquor, to lyophilized powder peplos are carried out, and after the completion for the treatment of peplos, material are taken out, and 2~3h of natural air drying, place into powder
Crushed in broken machine, and crossed 80~100 mesh sieves, you can obtained plant growth regulator.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107473866A (en) * | 2017-09-30 | 2017-12-15 | 百色阳生农业开发有限公司 | A kind of tomato growth accelerator and preparation method thereof |
| CN108308206A (en) * | 2018-01-24 | 2018-07-24 | 合肥华盖生物科技有限公司 | A kind of fish pelargonium is aestivated special resistance reinforcing agent |
| CN108513991A (en) * | 2018-05-18 | 2018-09-11 | 赵建平 | The preparation method of one plant growth regulators |
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| CN103833459A (en) * | 2012-11-23 | 2014-06-04 | 深圳市高杰斯科技有限公司 | Drug fertilizer composition for preventing and treating green turf diseases and application thereof |
| CN105924241A (en) * | 2016-04-28 | 2016-09-07 | 平顶山市绿禾农业科技开发有限公司 | Phytohormone-containing slow-release fertilizer for soybeans and preparation method thereof |
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2016
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103833459A (en) * | 2012-11-23 | 2014-06-04 | 深圳市高杰斯科技有限公司 | Drug fertilizer composition for preventing and treating green turf diseases and application thereof |
| CN105924241A (en) * | 2016-04-28 | 2016-09-07 | 平顶山市绿禾农业科技开发有限公司 | Phytohormone-containing slow-release fertilizer for soybeans and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107473866A (en) * | 2017-09-30 | 2017-12-15 | 百色阳生农业开发有限公司 | A kind of tomato growth accelerator and preparation method thereof |
| CN108308206A (en) * | 2018-01-24 | 2018-07-24 | 合肥华盖生物科技有限公司 | A kind of fish pelargonium is aestivated special resistance reinforcing agent |
| CN108513991A (en) * | 2018-05-18 | 2018-09-11 | 赵建平 | The preparation method of one plant growth regulators |
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