CN105902733A - Preparation with thyroid cancer resisting function for ultrasonography and preparation method thereof - Google Patents
Preparation with thyroid cancer resisting function for ultrasonography and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/81—Solanaceae (Potato family), e.g. tobacco, nightshade, tomato, belladonna, capsicum or jimsonweed
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/02—Algae
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/11—Pteridophyta or Filicophyta (ferns)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/27—Asclepiadaceae (Milkweed family), e.g. hoya
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/30—Boraginaceae (Borage family), e.g. comfrey, lungwort or forget-me-not
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/40—Cornaceae (Dogwood family)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/66—Papaveraceae (Poppy family), e.g. bloodroot
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/888—Araceae (Arum family), e.g. caladium, calla lily or skunk cabbage
- A61K36/8884—Arisaema, e.g. Jack in the pulpit
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/888—Araceae (Arum family), e.g. caladium, calla lily or skunk cabbage
- A61K36/8888—Pinellia
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
Abstract
The invention discloses a preparation with a thyroid cancer resisting function for ultrasonography and a preparation method thereof. The preparation is prepared mainly from the following active pharmaceutical ingredients in parts by weight: 5-8 parts of solanum nigrum, 4-7 parts of curculigo capitulate, 6-10 parts of great willowherb herb, 7-12 parts of seaweed, 3-6 parts of fermented soybean, 8-14 parts of alkanet, 5-9 parts of typhonium giganteum, 7-13 parts of corylopsis sinensis root, 6-10 parts of hylomecon vernalis, 3-7 parts of longhairy antenoron herb, 5-8 parts of sonchus arvensis, 4-9 parts of radix cynanchi atrati, 3-7 parts of vittaria flexuosa and 5-11 parts of littleleaf dogwood root. The preparation disclosed by the invention realizes a remarkable treatment effect, takes effect quickly, avoids easy relapse and has the functions of clearing heat and removing toxin, calming and invigorating spleen, moistening lung and resolving phlegm, softening hard mass and relieving swelling, dispersing wind and harmonizing stomach, relaxing sinew and activating collaterals, dissipating stasis and eliminating swelling and clearing heat and replenishing yin, and can enhance the immune function of the body, inhibit the growth of cancer cells, quickly reduce the lumps, control the metastasis, relieve the pain of patients, stabilize the state, prolong the life and realize clinical healing.
Description
Technical field
The present invention relates to traditional Chinese medicine field, particularly relate to a kind of preparation with antithyroid cancer effect and preparation method.
Background technology
Thyroid cancer is modal thyroid malignancy, is derived from the malignant tumour of Thyroid follicular epithelial cell.First
Shape gland cancer early clinical manifestation is inconspicuous, and patient or household chance on neck thyroid gland with doctor has matter hard and rugged
Lump, many no conscious symptons, neck region lump is often asymmetry lump, and thyroid nodule lump can be gradually increased, with swallowing
Up and down, and can invade tracheae and fix, lump easily earlier generates pressure symptom, as with hoarseness, and unsmooth breath,
Dysphagia, or the local pressure symptom such as tenderness, during jugular vein pressurized, may occur in which the bodies such as Ipsilateral venous engorgement and facial edema
Levy, for one of the feature of thyroid cancer, such as Lung metastases and Bone tumour etc., pathologic fracture even occurs.
Application publication number CN 105327205 A(application number 201510872293.7) Chinese patent literature disclose one
Kind treating the Chinese medicine preparation of thyroid cancer, the Chinese medicine preparation of this invention includes following raw material: Poria cocos, Radix Codonopsis, parasitic loranthus, mushroom,
Red bean, the root bark of white mulberry, the bark of eucommia, akebi, dalbergia wood, the bighead atractylodes rhizome, fiveleaf akebia fruit, Rhizoma Arisaematis (processed), pawpaw, hairyvein agrimony, coix seed, garden burnet, Cynanchum glaucescens, half
Bian Lian, folium cycas, Herba Hedyotidis Diffusae, indigo naturalis, Chinese cassia tree, subprostrate sophora, polygala root, rhizoma alismatis, honeysuckle, pseudo-ginseng, peach kernel, centipede, trachelospermum jasminoide
Rattan.Application publication number CN 104398831 A(application number 201410757776.8) Chinese patent literature disclose one and control
Treating the Chinese medicine preparation of thyroid cancer, the Chinese medicine material by following parts by weight is formulated: Chinese honey locust 12-15 part, bulb of fritillary 10-13
Part, edible tulip 12-15 part, seed of cowherb 12-18 part, kelp 10-12 part, Siberian cocklebur grass 8-12 part, Sculellaria barbata 10-13 part, spend in vain
HERBA HEDYOTIS DIFFUSAE 10-12 part, red sage root 12-18 part, fructus polygoni orientalis 14-17 part, oyster 13-16 part, rhizoma arisaematis 6-8 part, Radix Codonopsis 8-12 part,
Radix Astragali 6-12 part and root of Dahurain angelica 8-10 part.Application publication number CN 105456670 A(application number 201510985277.9) China specially
Profit document discloses a kind of Chinese medicine treating thyroid cancer, is made up of the Chinese medicine material of following weight portion: calculus bovis factitius 35-46
Part, kamuning 23-36 part, two female peaceful 22-28 parts, radix berberidis 18-26 part, dried lacquer 16-28 part, elecampane 13-18
Part, indian adenosma herb 12-17 part, halite 9-15 part, Rabdosia amethystoides 3-8 part, Glabrous Sarcandra Herb 3-6 part, rascal 5-12 part, bavin
6-12 part recklessly.
Currently, western medical treatment thyroid cancer typically uses operative treatment and chemicotherapy, matching medication after postoperative and chemicotherapy,
Need to take high amount of drug, and it is higher to recur probability.Although the Chinese medicine for the treatment of thyroid cancer has a variety of, but, it is still
So there are two aspect deficiencies: one is that effect is obvious not, two is that the comparison that takes effect is slow.
Summary of the invention
For the deficiencies in the prior art, it is an object of the invention to provide a kind of preparation with antithyroid cancer effect and system
Method.Result for the treatment of of the present invention is notable, instant effect, is difficult to recurrence, has invigorating the spleen clearing heat and detoxicating, calm, moistening lung for removing phlegm, soft heavily fortified point move back
Swollen, dispelling wind and stomach, stimulate the circulation of the blood and cause the muscles and joints to relax, dissipate that stagnation resolvation is swollen, the effect of heat-clearing benefit the moon, it is possible to enhancing body's immunity, inhibition cancer cell
Growth, rapid drop lump, control transfer, alleviate patient suffering, stablize the state of an illness, extend life cycle, reach clinical cure.
The technical scheme is that
A kind of preparation with antithyroid cancer effect, takes off and states the primary raw material medicine of weight proportion and be prepared from: black nightshade 5-8,
Great Ye thizoma curculiginis 4-7, red chopsticks 6-10, marine alga 7-12, Fermented Soybean 3-6, alkanet 8-14, Typhonium giganteum 5-9, winterhazel root 7-13,
Japanese hylomecon root 6-10, desmodium 3-7, sowthistle 5-8, radix cynanchi atrati 4-9, ribbed value 3-7, littleleaf dogwood root 5-11.
A kind of preparation with antithyroid cancer effect, preferred scheme is, takes off the primary raw material medicine stating weight proportion
It is prepared from: black nightshade 6-7, great Ye thizoma curculiginis 5-6, red chopsticks 7-9, marine alga 8-11, Fermented Soybean 4-5, alkanet 9-13, Typhonium giganteum 6-
8, winterhazel root 9-11, japanese hylomecon root 7-9, desmodium 4-6, sowthistle 6-7, radix cynanchi atrati 5-8, ribbed value 4-6, littleleaf dogwood root 7-10.
A kind of preparation with antithyroid cancer effect, scheme more preferably is, takes off and states the most former of weight proportion
Material medicine is prepared from: black nightshade 6.5, great Ye thizoma curculiginis 5.5, red chopsticks 8, marine alga 9, Fermented Soybean 4.5, alkanet 12, Typhonium giganteum 7, wax
Hemp nettle root 10, japanese hylomecon root 8, desmodium 5, sowthistle 6.6, radix cynanchi atrati 7, ribbed value 5, littleleaf dogwood root 9.
Present invention also offers and the aforementioned preparation with antithyroid cancer effect is made pharmaceutically acceptable powder, ball
The preparation method of agent, granule and capsule.
The preparation method of described powder is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
The amount of the preferred barley wine of 1/6-1/4(of Hua Gen, japanese hylomecon root and radix cynanchi atrati four taste bulk drug gross weight be great Ye thizoma curculiginis, winterhazel root,
Japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight), 30-50 minute (the most vexed profit 40 minutes) of vexed profit, slow fire stir-fries 14-
20 minutes (preferably slow fire stir-fries 18 minutes), takes out, dries, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, with 5g often bag subpackage, sterile packaged and get final product.
The preparation method of described pill is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
The amount of the preferred barley wine of 1/6-1/4(of Hua Gen, japanese hylomecon root and radix cynanchi atrati four taste bulk drug gross weight be great Ye thizoma curculiginis, winterhazel root,
Japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight), 30-50 minute (the most vexed profit 40 minutes) of vexed profit, slow fire stir-fries 14-
20 minutes (preferably slow fire stir-fries 18 minutes), takes out, dries, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, with the general ball of vinegar, make the pill that particle diameter is 3mm, packing,
Obtain.
The preparation method of described granule is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
The amount of the preferred barley wine of 1/6-1/4(of Hua Gen, japanese hylomecon root and radix cynanchi atrati four taste bulk drug gross weight be great Ye thizoma curculiginis, winterhazel root,
Japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight), 30-50 minute (the most vexed profit 40 minutes) of vexed profit, slow fire stir-fries 14-
20 minutes (preferably slow fire stir-fries 18 minutes), takes out, dries, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, add the starch slurry that concentration is 10%-15% and (be preferably added to
Concentration is the starch slurry of 12%), the amount of starch slurry is step (1), step (2) and the 1/5 of step (3) gained gross weight, makes soft
Material, crosses 16-20 mesh sieve (preferably crossing 18 mesh sieves), makes particle, be dried, whole grain, and packaging to obtain final product.
The preparation method of described capsule is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
The amount of the preferred barley wine of 1/6-1/4(of Hua Gen, japanese hylomecon root and radix cynanchi atrati four taste bulk drug gross weight be great Ye thizoma curculiginis, winterhazel root,
Japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight), 30-50 minute (the most vexed profit 40 minutes) of vexed profit, slow fire stir-fries 14-
20 minutes (preferably slow fire stir-fries 18 minutes), takes out, dries, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, add the starch slurry that concentration is 10%-15% and (be preferably added to
Concentration is the starch slurry of 12%), the amount of starch slurry is step (1), step (2) and step (3) gained gross weight 1/5, makes soft
Material, crosses 20 mesh sieves, makes particle, is dried, and loads capsule, equipped with medicine 0.4g in every seed lac capsule, to obtain final product.
The preparation recipe science with antithyroid cancer effect that the present invention provides, the preparation method of various formulations is simple,
Products obtained therefrom taking convenience, it is easy to carry.In addition, the excellent results of the present invention is also manifested by:
1, result for the treatment of is notable, instant effect, is difficult to recurrence；
2, there is invigorating the spleen clearing heat and detoxicating, calm, moistening lung for removing phlegm, soft hard detumescence, dispelling wind and stomach, stimulate the circulation of the blood and cause the muscles and joints to relax, dissipate stagnation resolvation
Swollen, the effect of heat-clearing benefit the moon, it is possible to strengthen body's immunity, the growth of inhibition cancer cell, rapid drop lump, controls to turn
Move, alleviate patient suffering, stablize the state of an illness, extend life cycle, reach clinical cure.
Detailed description of the invention
Describe technical scheme in detail below in conjunction with embodiment and experimental example, but protection domain is not limited to this.
Embodiment 1 one kinds has the preparation of antithyroid cancer effect, and the primary raw material medicine taking following weight parts is prepared from
(every part is 900g): black nightshade 5 parts, great Ye thizoma curculiginis 4 parts, red chopsticks 6 parts, marine alga 7 parts, Fermented Soybean 3 parts, alkanet 8 parts, Typhonium giganteum
5 parts, winterhazel root 7 parts, japanese hylomecon root 6 parts, desmodium 3 parts, sowthistle 5 parts, radix cynanchi atrati 4 parts, ribbed value 3 parts, littleleaf dogwood root 5 parts.
The preparation method of the above-mentioned preparation powder with antithyroid cancer effect is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
Hua Gen, japanese hylomecon root and the 1/6 of radix cynanchi atrati four taste bulk drug gross weight, vexed profit 30 minutes, slow fire stir-fries 14 minutes, takes out, dries, powder
It is broken into fine powder, sieves；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50 DEG C, takes out, cools, be ground into fine powder,
Sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5 times of 9 taste bulk drug gross weights, decocts 1.4 hours every time, merges twice liquid, stands
12 hours, upper liquid is condensed into the thick paste that relative density is 1.4, dry, pulverize into fine powder, sieve；
(4) step (1), step (2) and step (3) gained are mixed, with 5g often bag subpackage, sterile packaged and get final product.
The instructions of taking of the preparation powder that gained of the present invention has antithyroid cancer effect is: oral, twice on the one, every time
5g, boiling water is taken after mixing it with water.
Embodiment 2 one kinds has the preparation of antithyroid cancer effect, and the primary raw material medicine taking following weight parts is prepared from
(every part is 900g): black nightshade 8 parts, great Ye thizoma curculiginis 7 parts, red chopsticks 10 parts, marine alga 12 parts, Fermented Soybean 6 parts, alkanet 14 parts, solely
9 parts of angle lotus, winterhazel root 13 parts, japanese hylomecon root 10 parts, desmodium 7 parts, sowthistle 8 parts, radix cynanchi atrati 9 parts, ribbed value 7 parts, littleleaf dogwood root
11 parts.
The preparation method of the above-mentioned preparation pill with antithyroid cancer effect is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
Hua Gen, japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight, vexed profit 40 minutes, slow fire stir-fries 18 minutes, takes out, dries, powder
It is broken into fine powder, sieves；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 60 DEG C, takes out, cools, be ground into fine powder,
Sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 8 times of 9 taste bulk drug gross weights, decocts 1.4 hours every time, merges twice liquid, stands
12 hours, upper liquid is condensed into the thick paste that relative density is 1.43, dry, pulverize into fine powder, sieve；
(4) step (1), step (2) and step (3) gained are mixed, with the general ball of vinegar, make the pill that particle diameter is 3mm, packing,
Obtain.
Model case one: honest and just XX, man, 47 years old.Before more than 2 years, patient suffers from right thyroid cancer.Perform the operation at local hospital row
Excision, postoperative recurs after radiotherapy repeatedly, comes to go to a doctor.Examine and see patient throat goiter and tumor protuberantia, fix and do not move, chest distress, gas
Short weak, god is tired to become thin, and appetite stimulator, two is the most uncomfortable.The dark violet few tongue of tongue nature, arteries and veins is the most puckery.Take the present embodiment gained and have anti-
The preparation pill of thyroid cancer effect, three times on the one, each 6 balls, warm water takes.Taking 1 month, Thyroid Tumors reduces.Clothes
With two months, recovery from illness, follow up a case by regular visits to without recurrence.
Embodiment 3 one kinds has the preparation of antithyroid cancer effect, and the primary raw material medicine taking following weight parts is prepared from
(every part is 900g): black nightshade 6 parts, great Ye thizoma curculiginis 5 parts, red chopsticks 7 parts, marine alga 8 parts, Fermented Soybean 4 parts, alkanet 9 parts, Typhonium giganteum
6 parts, winterhazel root 9 parts, japanese hylomecon root 7 parts, desmodium 4 parts, sowthistle 6 parts, radix cynanchi atrati 5 parts, ribbed value 4 parts, littleleaf dogwood root 7 parts.
The preparation method of the above-mentioned preparation granules agent with antithyroid cancer effect is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
Hua Gen, japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight, vexed profit 40 minutes, slow fire stir-fries 18 minutes, takes out, dries, powder
It is broken into fine powder, sieves；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 60 DEG C, takes out, cools, be ground into fine powder,
Sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 8 times of 9 taste bulk drug gross weights, decocts 1.4 hours every time, merges twice liquid, stands
12 hours, upper liquid is condensed into the thick paste that relative density is 1.43, dry, pulverize into fine powder, sieve；
(4) step (1), step (2) and step (3) gained being mixed, adding concentration is the starch slurry of 12%, and the amount of starch slurry is
Step (1), step (2) and the 1/5 of step (3) gained gross weight, make softwood, crosses 18 mesh sieves, makes particle, is dried, whole grain,
Packaging, to obtain final product.
Model case two: XX slowly, female, 33 years old.Before more than 1 year, patient goes to a doctor in local hospital because of the left neck thing that swells, and looks into first shape
Gland B ultrasonic shows that left lobe of thyroid gland swells thing, looks into thyroid hormone and shows: FT3, FT4 all increase, and TSH lowers, and carry out left lobe of thyroid gland and gorge
Portion's resection, postoperative pathological return: thyroid papillary carcinoma.Poor effect after treatment.Take the present embodiment gained and there is anti-first
The preparation granules agent of shape gland cancer effect, three times on the one, each 12g, boiling water is taken after mixing it with water.Taking 1 month, neck region lump reduces.Take
Two months, recovery from illness, follow up a case by regular visits to without recurrence.
Embodiment 4 one kinds has the preparation of antithyroid cancer effect, and the primary raw material medicine taking following weight parts is prepared from
(every part is 900g): black nightshade 7 parts, great Ye thizoma curculiginis 6 parts, red chopsticks 9 parts, marine alga 11 parts, Fermented Soybean 5 parts, alkanet 13 parts, only angle
8 parts of lotus, winterhazel root 11 parts, japanese hylomecon root 9 parts, desmodium 6 parts, sowthistle 7 parts, radix cynanchi atrati 8 parts, ribbed value 6 parts, littleleaf dogwood root 10
Part.
The preparation method of the above-mentioned preparation capsule with antithyroid cancer effect is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
Hua Gen, japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight, vexed profit 40 minutes, slow fire stir-fries 18 minutes, takes out, dries, powder
It is broken into fine powder, sieves；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 60 DEG C, takes out, cools, be ground into fine powder,
Sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 8 times of 9 taste bulk drug gross weights, decocts 1.4 hours every time, merges twice liquid, stands
12 hours, upper liquid is condensed into the thick paste that relative density is 1.43, dry, pulverize into fine powder, sieve；
(4) step (1), step (2) and step (3) gained being mixed, adding concentration is the starch slurry of 12%, and the amount of starch slurry is
Step (1), step (2) and step (3) gained gross weight 1/5, make softwood, crosses 20 mesh sieves, makes particle, is dried, and loads glue
Capsule, equipped with medicine 0.4g in every seed lac capsule, to obtain final product.
Model case three: poplar XX, man, 40 years old.Before more than 2 years, patient finds that unintentionally neck swells thing, and right side is relatively big, hard
Not moving, show left lobe of thyroid gland multiple nodules, thyroid gland diffusivity pathology at local hospital row thyroid gland B ultrasonic, carry out bilateral first shape
Gland cuts art entirely, and postoperative pathological return is right thyroid papillary carcinoma.Drug administration is treated, without being clearly better.Take this enforcement
Example gained has the preparation capsule of antithyroid cancer effect, and three times on the one, each 3, warm water takes.Take 1 month, neck
Mass reduction.Take two months, recovery from illness, follow up a case by regular visits to without recurrence.
Embodiment 5 one kinds has the preparation of antithyroid cancer effect, and the primary raw material medicine taking following weight parts is prepared from
(every part is 900g): black nightshade 6.5 parts, great Ye thizoma curculiginis 5.5 parts, red chopsticks 8 parts, marine alga 9 parts, Fermented Soybean 4.5 parts, alkanet 12
Part, Typhonium giganteum 7 parts, winterhazel root 10 parts, japanese hylomecon root 8 parts, desmodium 5 parts, sowthistle 6.6 parts, radix cynanchi atrati 7 parts, ribbed value 5 parts,
Littleleaf dogwood root 9 parts.
The preparation method of the above-mentioned preparation powder with antithyroid cancer effect is:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
Hua Gen, japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight, vexed profit 40 minutes, slow fire stir-fries 18 minutes, takes out, dries, powder
It is broken into fine powder, sieves；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 60 DEG C, takes out, cools, be ground into fine powder,
Sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 8 times of 9 taste bulk drug gross weights, decocts 1.4 hours every time, merges twice liquid, stands
12 hours, upper liquid is condensed into the thick paste that relative density is 1.43, dry, pulverize into fine powder, sieve；
(4) step (1), step (2) and step (3) gained are mixed, with 5g often bag subpackage, sterile packaged and get final product.
Used by the present invention, the pharmacology of main Chinese medicine material is as follows:
Black nightshade: base: for the herb of Solanaceae nightshade black nightshade.The property of medicine: bitter, cold.Slightly poisonous.Function cures mainly: clearing heat and detoxicating, profit
Water is subsided a swelling.For cat fever, toothache, chronic bronchitis, dysentery, urinary infection, mastitis, leukorrhea, cancer；External application is controlled
Carbuncle furuncle furunculosis, pemphigus, snake bite.
Great Ye thizoma curculiginis: base: Hypoxidaceae Curculigo great Ye thizoma curculiginis, is used as medicine with root and root-like stock.The property of medicine: bitter, puckery,
Flat.Function cures mainly: moistening lung for removing phlegm, relieving cough and asthma, calm invigorating the spleen, invigorates the kidney and stops nocturnal emission.For dyspnea and cough due to deficiency of the kidney, soreness of waist and knee joint, leukorrhea, lose
Essence.
Red chopsticks: base: for the herb of onagraceae plant willow herb.The property of medicine: bitter；Property flat.Function cures mainly: Li Shui oozes
Wet, dissipate-swelling of regulating the flow of vital energy, promoting blood circulation for regulating menstruation.Main oedema, has loose bowels, dyspepsia turgor, irregular menstruation, alactation, scrotum enlargement, and sore rash is itched
Bitterly.
Marine alga: base: for Sargassaceae plant sargassum fusifome and the frond of Sargassum.The property of medicine: bitter, salty, cold.Return lung, spleen,
Kidney, liver stomach warp.Function cures mainly: soft heavily fortified point, dissolving phlegm, Li Shui, detumescence.Main scrofula, goiter and tumor, accumulation, oedema, tinea pedis, testiclar gall,
(Epileptic is ruined) hernia.
Fermented Soybean: base: the mature seed for the black of legume soybean processes through steaming net for catching birds or fish fermentation etc..The property of medicine:
Bitter, pungent, flat.Return lung, stomach, the heart, bladder, small intestine, tri-jiao channel.Function cures mainly: expelling pathogenic factors from muscles and skin is delivered, and declares strongly fragrant relieving restlessness.Main diseases caused by external factors table is demonstrate,proved, cold
Heat headache, vexed, uncomfortable in chest.
Alkanet: base: alkanet section plant lithospermum euchromum Royle root, alkanet or the dry root of arnebia guttata Bunge root.The property of medicine:
Sweet, salty, cold.The thoughts of returning home, Liver Channel.Function cures mainly: cool blood, invigorates blood circulation, promoting eruption of detoxifying.Containing for blood-head poison, macula purple is black, and measles is not
Thoroughly, sore, eczema, scald.
Typhonium giganteum: base: for the herb of aroid Typhonium giganteum.Function cures mainly: controls venomous snake bite, scrofula, fall and beat
Damage.
Winterhazel root: base: for root or the root skin of Hamamelidaceae Plants China winterhazel.The property of medicine: sweet；Flat.Return stomach, the heart
Warp.Function cures mainly: dispelling wind and stomach, antitoxic heart-soothing and sedative.Main diseases caused by external factors ailment said due to cold or exposure, headache, n and V, palpitaition, have the fidgets.
Japanese hylomecon root: base: for the root of bloodroot japanese hylomecon root.The property of medicine: " Shaanxi Chinese herbal medicine ": " bitter, property is put down." function
Cure mainly: " Shaanxi Chinese herbal medicine ": " wines used as antirheumatic, stimulates the circulation of the blood and cause the muscles and joints to relax, and dissipates stagnation resolvation and swells, analgesic hemostatic.Treating rheumatic arthritis, internal lesion caused by overexertion, fall and beat
Damage.”
Desmodium: base: for the herb of Ofthe Primulaceae Lysimachia christinae.The property of medicine: hardship sweet, micro-, cool.Return liver, courage, kidney, bladder warp.
Function cures mainly: promoting diuresis for stranguria, clearing heat and detoxicating, dissipates stagnation resolvation and swells.Main liver and gall and stone in urinary system, heat pouring, nephritic dropsy, damp and hot Huang
Subcutaneous ulcer, sore carbuncle swells, venomous snake bite, traumatic injury.
Sowthistle: base: the herb of composite family sonchus plant sowthistle.The property of medicine: bitter, cold.Function cures mainly: heat-clearing solution
Poison, cool blood dampness removing.For acpuei pharyngitis, acute bacillary dysentery, spit blood, hematuria, hemorrhoid gall.
Radix cynanchi atrati: base: for trailing plants section plant radix cynanchi atrati or the root of Cynanchum versicolor Bunge.Heat-clearing benefit is cloudy；Inducing diuresis for treating strangurtia；Detoxification sore treatment.
Bitter；Salty；Cold in nature.Enter lung, stomach, kidney channel.Cure mainly warm；Body hot spot rash；Hectic fever hectic fever due to yin；Cough with lung heat；Postpartum dysphoria；Heat
Drench；Blood drenches；Abscess of throat；Sore and toxic；Venomous snake bite.For the heating of temperature evil wound battalion, fever due to yin deficiency, hectic fever due to yin labor heat, postpartum blood
Shooting without hitting the target heat, heat is drenched, and blood drenches, swollen ulcer drug.
Ribbed value: base: for the herb of Vittariaceae plant ribbed value.The property of medicine: bitter, puckery, cool.The thoughts of returning home, Liver Channel.Function master
Controlling: wind and heat dispersing, relaxing muscles and tendons pain relieving, invigorating the spleen disappears infantile malnutrition due to digestive disturbances or intestinalparasites, hemostasis.Main acute infantile convulsion wind, mesh screen, traumatic injury, arthralgia due to wind-dampness, children's's infantile malnutrition due to digestive disturbances or intestinalparasites
Long-pending, women's type of tubercular disease found in women, spitting of blood, spit blood.
Littleleaf dogwood root: base: for the complete stool of the little wood of Cornaceae plant.The property of medicine: bitter, puckery, cool.Function cures mainly: only dissipate the stasis of blood
Bitterly, hemostasis, synthetism.
Test example 1 gained of the present invention has a clinical practice of the preparation (embodiment 5) of antithyroid cancer effect: 2011 1
In August ,-2012 moon, screen 240 example thyroid cancer patients in 3 hospitals.It is randomly divided into two groups, experimental group and control group (often group
120 examples).Between two groups of patients, the aspect such as sex, age, course of disease compares, and no significant difference (P ＞ 0.05) has
Comparativity.
Methods for the treatment of: experimental group uses gained of the present invention to have the preparation of antithyroid cancer effect, and using method is: mouth
Clothes, twice on the one, each 5g, boiling water is taken after mixing it with water.Control group uses the medicines such as compound cantharidin capsule, XIAOAIPING PIAN, ginseng pellet dissipating bind capsule
Thing is treated.Two groups of patients carry out comparitive study after all treating 1 month.
Curative effect judging standard: cure: throat lump, clinical symptom disappearance, pathological biopsy cancer-free cell finds；Take a turn for the better: neck
Front mass reduction, clinical symptom relief；Invalid: throat lump does not reduces, clinical symptoms are without improving.
Table 1: gained of the present invention has the preparation compliance test result of antithyroid cancer effect
Efficacy analysis: experimental group cures 55 examples, take a turn for the better 63 examples, invalid 2 examples, total effective rate 98.33%；Control group cures 10 examples, good
Turn 72 examples, invalid 38 examples, total effective rate 68.33%.The cure rate of experimental group and total effective rate are apparently higher than control group.Test table
Bright, the clinical efficacy of experimental group is substantially better than control group, significant difference (P ＜ 0.05), has statistical significance.
The present invention, with black nightshade, great Ye thizoma curculiginis, red chopsticks and marine alga etc. as primary raw material, makes and has antithyroid cancer effect
Preparation.In side, black nightshade is clearing heat and detoxicating, inducing diuresis for removing edema.Great Ye thizoma curculiginis moistening lung for removing phlegm, relieving cough and asthma, calm invigorating the spleen, invigorate the kidney and stop nocturnal emission.
Red chopsticks clearing damp and promoting diuresis, dissipate-swelling of regulating the flow of vital energy, promoting blood circulation for regulating menstruation.The soft heavily fortified point of marine alga, dissolving phlegm, Li Shui, detumescence.Fermented Soybean expelling pathogenic factors from muscles and skin is delivered, Xuan Yu
Relieving restlessness.The cool blood of alkanet, invigorates blood circulation, promoting eruption of detoxifying.Typhonium giganteum controls venomous snake bite, scrofula, traumatic injury.Winterhazel root dispelling wind and
Stomach, antitoxic heart-soothing and sedative.Japanese hylomecon root wines used as antirheumatic, stimulates the circulation of the blood and cause the muscles and joints to relax, and dissipates stagnation resolvation and swells, analgesic hemostatic.Desmodium promoting diuresis for stranguria, clearing heat and detoxicating,
Dissipate stagnation resolvation to swell.Sowthistle is clearing heat and detoxicating, cool blood dampness removing.Radix cynanchi atrati heat-clearing benefit is cloudy；Inducing diuresis for treating strangurtia；Detoxification sore treatment.Ribbed value dispelling wind is clear
Heat, relaxing muscles and tendons pain relieving, invigorating the spleen disappears infantile malnutrition due to digestive disturbances or intestinalparasites, hemostasis.Littleleaf dogwood root blood stasis removing analgesic, hemostasis, synthetism.All medicines share, and play clearing heat and detoxicating, calm altogether
Invigorating the spleen, moistening lung for removing phlegm, soft hard detumescence, dispelling wind and stomach, stimulate the circulation of the blood and cause the muscles and joints to relax, dissipate that stagnation resolvation is swollen, the effect of heat-clearing benefit the moon, it is possible to enhancing body is exempted from
Epidemic disease function, the growth of inhibition cancer cell, rapid drop lump, control transfer, alleviate patient suffering, stablize the state of an illness, extend existence
Phase, reach clinical cure.
Finally it should be noted that embodiment is the optimum detailed description of the invention of the present invention, be not limited to this
Invention, although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it depends on
So the technical scheme described in foregoing embodiments can be modified, or wherein portion of techniques feature is carried out equivalent replace
Change.All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention
Protection domain within.
Claims (10)
1. a preparation with antithyroid cancer effect, it is characterised in that take off and state the primary raw material medicine of weight proportion and prepare
Form: black nightshade 5-8, great Ye thizoma curculiginis 4-7, red chopsticks 6-10, marine alga 7-12, Fermented Soybean 3-6, alkanet 8-14, Typhonium giganteum 5-9,
Winterhazel root 7-13, japanese hylomecon root 6-10, desmodium 3-7, sowthistle 5-8, radix cynanchi atrati 4-9, ribbed value 3-7, littleleaf dogwood root 5-11.
There is the preparation of antithyroid cancer effect the most as claimed in claim 1, it is characterised in that take off the master stating weight proportion
Bulk drug is wanted to be prepared from: black nightshade 6-7, great Ye thizoma curculiginis 5-6, red chopsticks 7-9, marine alga 8-11, Fermented Soybean 4-5, alkanet 9-13,
Typhonium giganteum 6-8, winterhazel root 9-11, japanese hylomecon root 7-9, desmodium 4-6, sowthistle 6-7, radix cynanchi atrati 5-8, ribbed value 4-6, littleleaf dogwood root
7-10。
There is the preparation of antithyroid cancer effect the most as claimed in claim 1, it is characterised in that take off the master stating weight proportion
Bulk drug is wanted to be prepared from: black nightshade 6.5, great Ye thizoma curculiginis 5.5, red chopsticks 8, marine alga 9, Fermented Soybean 4.5, alkanet 12, Typhonium giganteum
7, winterhazel root 10, japanese hylomecon root 8, desmodium 5, sowthistle 6.6, radix cynanchi atrati 7, ribbed value 5, littleleaf dogwood root 9.
4. the preparation method of the preparation powder with antithyroid cancer effect as described in claims 1 to 3 is arbitrary, its feature exists
In, step is as follows:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
Hua Gen, japanese hylomecon root and the 1/6-1/4 of radix cynanchi atrati four taste bulk drug gross weight, vexed profit 30-50 minute, slow fire stir-fries 14-20 minute, takes
Go out, dry, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, with 5g often bag subpackage, sterile packaged and get final product.
5. the preparation method of the preparation pill with antithyroid cancer effect as described in claims 1 to 3 is arbitrary, its feature exists
In, step is as follows:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
The amount of the preferred barley wine of 1/6-1/4(of Hua Gen, japanese hylomecon root and radix cynanchi atrati four taste bulk drug gross weight be great Ye thizoma curculiginis, winterhazel root,
Japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight), 30-50 minute (the most vexed profit 40 minutes) of vexed profit, slow fire stir-fries 14-
20 minutes (preferably slow fire stir-fries 18 minutes), takes out, dries, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, with the general ball of vinegar, make the pill that particle diameter is 3mm, packing,
Obtain.
6. the preparation method of the preparation granules agent with antithyroid cancer effect as described in claims 1 to 3 is arbitrary, its feature
Being, step is as follows:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
The amount of the preferred barley wine of 1/6-1/4(of Hua Gen, japanese hylomecon root and radix cynanchi atrati four taste bulk drug gross weight be great Ye thizoma curculiginis, winterhazel root,
Japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight), 30-50 minute (the most vexed profit 40 minutes) of vexed profit, slow fire stir-fries 14-
20 minutes (preferably slow fire stir-fries 18 minutes), takes out, dries, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, add the starch slurry that concentration is 10%-15% and (be preferably added to
Concentration is the starch slurry of 12%), the amount of starch slurry is step (1), step (2) and the 1/5 of step (3) gained gross weight, makes soft
Material, crosses 16-20 mesh sieve (preferably crossing 18 mesh sieves), makes particle, be dried, whole grain, and packaging to obtain final product.
7. the preparation method of the preparation capsule with antithyroid cancer effect as described in claims 1 to 3 is arbitrary, its feature
Being, step is as follows:
(1) taking great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and radix cynanchi atrati, add barley wine, the amount of barley wine is great Ye thizoma curculiginis, wax lobe
The amount of the preferred barley wine of 1/6-1/4(of Hua Gen, japanese hylomecon root and radix cynanchi atrati four taste bulk drug gross weight be great Ye thizoma curculiginis, winterhazel root,
Japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight), 30-50 minute (the most vexed profit 40 minutes) of vexed profit, slow fire stir-fries 14-
20 minutes (preferably slow fire stir-fries 18 minutes), takes out, dries, be ground into fine powder, sieve；
(2) taking marine alga, be soaked in water 3 days, every day changes water twice, is dried 12 hours in 50-70 DEG C and (is preferable over 60 DEG C and is dried 12 little
Time), take out, cool, be ground into fine powder, sieve；
(3) remaining the 9 taste bulk drug in addition to great Ye thizoma curculiginis, marine alga, winterhazel root, japanese hylomecon root and radix cynanchi atrati are put in pot, add water
Decocting twice, each amount of water is 5-9 times of 9 taste bulk drug gross weights, and (amount of water is 9 taste bulk drug gross weights preferably every time
8 times of amount), decoct 1.4 hours every time, merge twice liquid, stand 12 hours, it is 1.4-that upper liquid is condensed into relative density
The thick paste (upper liquid is preferably condensed into the thick paste that relative density is 1.43) of 1.45, dry, pulverize into fine powder, sieves；
(4) step (1), step (2) and step (3) gained are mixed, add the starch slurry that concentration is 10%-15% and (be preferably added to
Concentration is the starch slurry of 12%), the amount of starch slurry is step (1), step (2) and step (3) gained gross weight 1/5, makes soft
Material, crosses 20 mesh sieves, makes particle, is dried, and loads capsule, equipped with medicine 0.4g in every seed lac capsule, to obtain final product.
There is the preparation method of the preparation powder of antithyroid cancer effect the most as claimed in claim 4, it is characterised in that step
(1) amount of barley wine is great Ye thizoma curculiginis, winterhazel root, japanese hylomecon root and the 1/5 of radix cynanchi atrati four taste bulk drug gross weight.
There is the preparation method of the preparation powder of antithyroid cancer effect the most as claimed in claim 4, it is characterised in that step
(1) vexed profit 40 minutes.
There is the preparation method of the preparation powder of antithyroid cancer effect the most as claimed in claim 4, it is characterised in that step
Suddenly (1) slow fire stir-fries 18 minutes.
Priority Applications (1)
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| CN106511694A (en) * | 2016-11-14 | 2017-03-22 | 吉林大学 | Preparation with function of resisting thyroid cancer in ultrasound department and preparation method |
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| CN104840747A (en) * | 2015-05-18 | 2015-08-19 | 南京中医药大学 | Traditional Chinese medicine composition capable of resisting thyroid cancer activity and preparation method and application thereof |
| CN105169149A (en) * | 2015-10-26 | 2015-12-23 | 山东省肿瘤医院 | Traditional Chinese medicine composition for treating pyrophlegm stasis accumulation type thyroid cancer, preparation method and application |
| CN105327205A (en) * | 2015-12-02 | 2016-02-17 | 青岛市中心医院 | Traditional Chinese medicine preparation for treating thyroid cancer |
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| CN104840747A (en) * | 2015-05-18 | 2015-08-19 | 南京中医药大学 | Traditional Chinese medicine composition capable of resisting thyroid cancer activity and preparation method and application thereof |
| CN105169149A (en) * | 2015-10-26 | 2015-12-23 | 山东省肿瘤医院 | Traditional Chinese medicine composition for treating pyrophlegm stasis accumulation type thyroid cancer, preparation method and application |
| CN105327205A (en) * | 2015-12-02 | 2016-02-17 | 青岛市中心医院 | Traditional Chinese medicine preparation for treating thyroid cancer |
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| CN106511694A (en) * | 2016-11-14 | 2017-03-22 | 吉林大学 | Preparation with function of resisting thyroid cancer in ultrasound department and preparation method |
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