CN105796609A - Quenching treatment based ganoderma spore powder wall breaking method - Google Patents
Quenching treatment based ganoderma spore powder wall breaking method Download PDFInfo
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- CN105796609A CN105796609A CN201610133085.XA CN201610133085A CN105796609A CN 105796609 A CN105796609 A CN 105796609A CN 201610133085 A CN201610133085 A CN 201610133085A CN 105796609 A CN105796609 A CN 105796609A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
- A61K36/074—Ganoderma
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/16—Mills provided with vibrators
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/18—Use of auxiliary physical effects, e.g. ultrasonics, irradiation, for disintegrating
- B02C19/186—Use of cold or heat for disintegrating
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/22—Crushing mills with screw-shaped crushing means
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C21/00—Disintegrating plant with or without drying of the material
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Abstract
The invention discloses a quenching treatment based ganoderma spore powder wall breaking method. The method has the advantages that according to the characteristics that ganoderma spore walls have extremely low heat conductivity and are slow in heat transfer, the dried ganoderma spore powder is subjected to quenching treatment in atmospheric liquid nitrogen, the wall breaking phenomenon is caused by the heat stress generated due to the temperature differences exceeding 200 DEG C inside and outside the walls, then the ganoderma spore powder is put in the hot water to be unfrozen and the steps are repeated several times, thus achieving more than or equal to 90% of wall breaking rate; a funnel type pulverizer is used for pulverizing and wall breaking and then a vibromill is used for further wall breaking to achieve more than or equal to 99.9% of wall breaking rate.
Description
Technical field
The invention belongs to the processing technique of Ganoderma spore powder, be specifically related to the wall-breaking method of a kind of Ganoderma spore powder processed based on quenching.
Background technology
Ganoderma is Chinese traditional medicine rarity, and China is Ganoderma application and the cradle of Ganoderma culture.Shennong's Herbal is recorded, Ganoderma is listed in safely and effectively, have no adverse reaction top grade, it is described as Herba mesonae chinensis, Ganoderma and Herba Reineckeae Carneae, the Compendium of Material Medica of Ming Dynasty's Li Shizhen (1518-1593 A.D.) is thought and Ganoderma is made that Ganoderma " main deafness, profit joint, protect vital essence refreshing, beneficial, hard muscles and bones, good color, for a long time clothes are not prolonged life always " significantly high evaluation.Ganoderma by the whole world generally acknowledge a kind of can strengthening by means of tonics, strengthening the body resistance Chinese medicine.
Ganoderma spore powder be Ganoderma in the growth and maturity phase, the seed of be hit by a bullet from Ganoderma the lamella extremely small avette sexual cell shot out and Ganoderma.Each Ganoderma spore only has 4-6 micron, is living organisms, double-walled construction, outer is surrounded by hard chitin fiber element, and human body is difficult to fully absorb.It is more suitable for human body the intestines and stomach after breaking cellular wall directly to absorb.It has condensed is the elite of Ganoderma, has whole hereditary materials and the health-care effect of Ganoderma.The breaking cellular wall of Ganoderma spore powder refers to it with cellulosic shell, the material that should not directly assimilate for human body, by artificial machinery, physico-chemical process, biologic enzymolysis method, after broken for its cellulose outer wall or elimination so that it is be more prone to the nutrient substance digesting and assimilating in cellulose wall.
Summary of the invention
The technical problem to be solved is to provide the wall-breaking method of a kind of Ganoderma spore powder processed based on quenching, it is possible to Simplified flowsheet, improves the extraction ratio of effective ingredient.
In order to solve above-mentioned technical problem, the present invention adopts the following technical scheme that:
The wall-breaking method of a kind of Ganoderma spore powder processed based on quenching, comprises the steps:
A. Ganoderma spore powder is carried out coarse pulverization by pulverizer；
B. adopt screen cloth that Ganoderma spore is pulverized granule to sieve；
C. the Ganoderma spore powder after sieving is put in hot air drying baking oven and dry；
D. the Ganoderma spore powder after drying is put into and normal pressure liquid nitrogen carries out quenching process；
E. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step d-e for several times, makes wall breaking rate of ganoderma lucidum spores reach more than 90%；
F. a funneling pulverizer being vertically arranged is prepared, the central shaft of described funneling pulverizer is provided with spiral, the Ganoderma spore powder of upper step process is injected by a pipeline pressurization entrance of described funneling pulverizer, described Ganoderma spore powder is carried out extruding and pulverizes by the described mode being threaded through rotating, and the outlet that described Ganoderma spore powder from top to down pushes to described funneling pulverizer is discharged；
G. vibromill breaking cellular wall again is adopted so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
Funneling pulverizer in described step f, its diameter installing spiral on center shaft reduces along with reducing of funnel space from the inlet to the outlet successively, the diameter of the central shaft of described funneling pulverizer from import to outlet increase along with reducing of funnel space successively, with realize described spiral when rotated radial and axial to described Ganoderma spore powder keep extruding crush force.
In step d, described liquid nitrogen temperature is less than-196 DEG C.
In step e, d-e number of described repetition step is more than twice.
In described step f, the rotating speed of described vibromill is 800-1200r/min, and power is 1000-1500w, and frequency of vibration is 800-1000Hz, and amplitude is 2-4cm.
Adopt the wall-breaking method of a kind of Ganoderma spore powder processed based on quenching of the present invention, have the advantage that
1, heat extremely low according to the heat conductivity of Ganoderma spore wall transmits slow feature, Ganoderma spore powder after drying is carried out quenching process in normal pressure liquid nitrogen, produce thermal stress cause that breaking cellular wall phenomenon occurs by the temperature difference more than 200 DEG C inside and outside wall, put into again in hot water and thaw, repeatedly for several times, it is achieved the sporoderm-broken rate of more than 90%；
2, by the further breaking cellular wall of vibromill, to realize the sporoderm-broken rate of more than 99.9%；
3, technique is simple, yield is high, be effectively split into extraction ratio height.
Accompanying drawing
Fig. 1 is the flow chart of one embodiment of the invention；
Fig. 2 is the funneling pulverizer schematic diagram described in one embodiment of the invention.
Detailed description of the invention
A kind of wall-breaking method based on the Ganoderma spore powder of quenching process of the present invention comprises the steps:
A. Ganoderma spore powder is carried out coarse pulverization by pulverizer；
B. adopt screen cloth that Ganoderma spore is pulverized granule to sieve；
C. the Ganoderma spore powder after sieving is put in hot air drying baking oven and dry；
D. the Ganoderma spore powder after drying is put into and normal pressure liquid nitrogen carries out quenching process；
E. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step d-e for several times, makes wall breaking rate of ganoderma lucidum spores reach more than 90%；
F. a funneling pulverizer being vertically arranged is prepared, the central shaft of described funneling pulverizer is provided with spiral, the Ganoderma spore powder of upper step process is injected by a pipeline pressurization entrance of described funneling pulverizer, described Ganoderma spore powder is carried out extruding and pulverizes by the described mode being threaded through rotating, and the outlet that described Ganoderma spore powder from top to down pushes to described funneling pulverizer is discharged；
G. vibromill breaking cellular wall again is adopted so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
Funneling pulverizer in described step f, its diameter installing spiral on center shaft reduces along with reducing of funnel space from the inlet to the outlet successively, the diameter of the central shaft of described funneling pulverizer from import to outlet increase along with reducing of funnel space successively, with realize described spiral when rotated radial and axial to described Ganoderma spore powder keep extruding crush force.
In step d, described liquid nitrogen temperature is less than-196 DEG C.
In step e, d-e number of described repetition step is more than twice.
In described step f, the rotating speed of described vibromill is 800-1200r/min, and power is 1000-1500w, and frequency of vibration is 800-1000Hz, and amplitude is 2-4cm.
Embodiment 1
A. Ganoderma spore powder is carried out coarse pulverization by pulverizer；
B. adopt screen cloth that Ganoderma spore is pulverized granule to sieve；
C. the Ganoderma spore powder after sieving is put in hot air drying baking oven and dry；
D. the Ganoderma spore powder after drying is put in the liquid nitrogen of normal pressure-196 DEG C and carry out quenching process；
E. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step d-e twice, makes wall breaking rate of ganoderma lucidum spores reach more than 90%；
F. referring to Fig. 2, prepare a funneling pulverizer 100 being vertically arranged, the central shaft 130 of described funneling pulverizer 100 is provided with spiral 120, being pressurizeed by a pipeline 200 by the Ganoderma spore powder of upper step process and inject the entrance 110 of described funneling pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funneling pulverizer 100.Described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral 120, and the outlet 140 that described Ganoderma spore powder from top to down pushes to described funneling pulverizer 100 is discharged.The diameter of the spiral 120 being arranged on central shaft 130 reduces along with reducing of funnel space from entrance 110 successively to outlet 140, the diameter of the central shaft 130 of described funneling pulverizer 100 140 increases along with reducing of funnel space from import 110 successively to outlet, to realize described spiral 120 when rotated at radial and axial extruding crush force that described Ganoderma spore powder kept.
G. adopting vibromill breaking cellular wall again, vibromill rotating speed is 800r/min, and power is 1000w, and frequency of vibration is 800Hz, and amplitude is 2cm so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
Embodiment 2
A. Ganoderma spore powder is carried out coarse pulverization by pulverizer；
B. adopt screen cloth that Ganoderma spore is pulverized granule to sieve；
C. the Ganoderma spore powder after sieving is put in hot air drying baking oven and dry；
D. the Ganoderma spore powder after drying is put in the liquid nitrogen of normal pressure-198 DEG C and carry out quenching process；
E. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step d-e bis-times, makes wall breaking rate of ganoderma lucidum spores reach more than 92%；
F. referring to Fig. 2, prepare a funneling pulverizer 100 being vertically arranged, the central shaft 130 of described funneling pulverizer 100 is provided with spiral 120, being pressurizeed by a pipeline 200 by the Ganoderma spore powder of upper step process and inject the entrance 110 of described funneling pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funneling pulverizer 100.Described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral 120, and the outlet 140 that described Ganoderma spore powder from top to down pushes to described funneling pulverizer 100 is discharged.The diameter of the spiral 120 being arranged on central shaft 130 reduces along with reducing of funnel space from entrance 110 successively to outlet 140, the diameter of the central shaft 130 of described funneling pulverizer 100 140 increases along with reducing of funnel space from import 110 successively to outlet, to realize described spiral 120 when rotated at radial and axial extruding crush force that described Ganoderma spore powder kept.
G. adopting vibromill breaking cellular wall again, vibromill rotating speed is 1000r/min, and power is 1200w, and frequency of vibration is 900Hz, and amplitude is 3cm so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
Embodiment 3
A. Ganoderma spore powder is carried out coarse pulverization by pulverizer；
B. adopt screen cloth that Ganoderma spore is pulverized granule to sieve；
C. the Ganoderma spore powder after sieving is put in hot air drying baking oven and dry；
D. the Ganoderma spore powder after drying is put in the liquid nitrogen of normal pressure-197 DEG C and carry out quenching process；
E. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step d-e bis-times, makes wall breaking rate of ganoderma lucidum spores reach more than 91%；
F. referring to Fig. 2, prepare a funneling pulverizer 100 being vertically arranged, the central shaft 130 of described funneling pulverizer 100 is provided with spiral 120, being pressurizeed by a pipeline 200 by the Ganoderma spore powder of upper step process and inject the entrance 110 of described funneling pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funneling pulverizer 100.Described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral 120, and the outlet 140 that described Ganoderma spore powder from top to down pushes to described funneling pulverizer 100 is discharged.The diameter of the spiral 120 being arranged on central shaft 130 reduces along with reducing of funnel space from entrance 110 successively to outlet 140, the diameter of the central shaft 130 of described funneling pulverizer 100 140 increases along with reducing of funnel space from import 110 successively to outlet, to realize described spiral 120 when rotated at radial and axial extruding crush force that described Ganoderma spore powder kept.
G. adopting vibromill breaking cellular wall again, vibromill rotating speed is 1200r/min, and power is 1500w, and frequency of vibration is 1000Hz, and amplitude is 4cm so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
Identifying after testing, the final sporoderm-broken rate of spore powder with crushed sporoderm after above example 1-3 processes is (laboratory adopts the sporoderm-broken rate of wall-breaking method of the present invention to be 100%), yield >=96% up to more than 99.9% all.
In sum, adopt the wall-breaking method of the present invention, have that epigranular, yield is high, the effective ingredient release rate advantages of higher of spore powder, thoroughly solve and existing Ganoderma spore powder is processed the complex process existed, the problem that effective component extraction rate is low.
But, those of ordinary skill in the art will be appreciated that, above embodiments is intended merely to the explanation present invention, and it is not used as limitation of the invention, as long as in the spirit of the present invention, to the change of embodiment described above, modification all by the Claims scope dropping on the present invention.
Claims (5)
1. the wall-breaking method of the Ganoderma spore powder processed based on quenching, it is characterised in that comprise the steps:
A. Ganoderma spore powder is carried out coarse pulverization by pulverizer；
B. adopt screen cloth that Ganoderma spore is pulverized granule to sieve；
C. the Ganoderma spore powder after sieving is put in hot air drying baking oven and dry；
D. the Ganoderma spore powder after drying is put into and normal pressure liquid nitrogen carries out quenching process；
E. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step d-e for several times, makes wall breaking rate of ganoderma lucidum spores reach more than 90%；
F. a funneling pulverizer being vertically arranged is prepared, the central shaft of described funneling pulverizer is provided with spiral, the Ganoderma spore powder of upper step process is injected by a pipeline pressurization entrance of described funneling pulverizer, described Ganoderma spore powder is carried out extruding and pulverizes by the described mode being threaded through rotating, and the outlet that described Ganoderma spore powder from top to down pushes to described funneling pulverizer is discharged；
G. vibromill breaking cellular wall again is adopted so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
2. the wall-breaking method of a kind of Ganoderma spore powder processed based on quenching according to claim 1, it is characterized in that: the funneling pulverizer in described step f, its diameter installing spiral on center shaft reduces along with reducing of funnel space from the inlet to the outlet successively, the diameter of the central shaft of described funneling pulverizer from import to outlet increase along with reducing of funnel space successively, with realize described spiral when rotated radial and axial to described Ganoderma spore powder keep extruding crush force.
3. the wall-breaking method of a kind of Ganoderma spore powder processed based on quenching according to claim 2, it is characterised in that: in step d, described liquid nitrogen temperature is less than-196 DEG C.
4. the wall-breaking method of a kind of Ganoderma spore powder processed based on quenching according to claim 3, it is characterised in that in step e, d-e number of described repetition step is more than twice.
5. the wall-breaking method of a kind of Ganoderma spore powder processed based on quenching according to claim 4, it is characterised in that in described step f, the rotating speed of described vibromill is 800-1200r/min, power is 1000-1500w, and frequency of vibration is 800-1000Hz, and amplitude is 2-4cm.
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106109507A (en) * | 2016-08-08 | 2016-11-16 | 孙继勇 | A kind of manufacture method of ultra micro nanometer Ganoderma spore powder with cellular wall broken |
| CN106861865A (en) * | 2017-04-19 | 2017-06-20 | 长葛市怀瑞蜂产品有限公司 | A kind of means for breaking walls of pollen |
| CN108030050A (en) * | 2017-12-19 | 2018-05-15 | 安徽强旺调味食品有限公司 | A kind of Islamic compound seasoner for extrusion and puffing food |
| CN108654811A (en) * | 2018-03-16 | 2018-10-16 | 中国水产科学研究院东海水产研究所 | A kind of method that laboratory quickly prepares the micro- plastics of micron order |
| CN108992511A (en) * | 2018-10-26 | 2018-12-14 | 青海未来格萨尔王药业有限公司 | A kind of stomach strengthening and digestion promoting water-bindered pill and preparation method thereof |
| CN108992508A (en) * | 2018-10-26 | 2018-12-14 | 青海未来格萨尔王药业有限公司 | Four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof |
| CN108992492A (en) * | 2018-10-26 | 2018-12-14 | 青海未来格萨尔王药业有限公司 | A kind of preparation method of yellow fragrant particle |
| CN109224018A (en) * | 2018-10-29 | 2019-01-18 | 青海未来格萨尔王药业有限公司 | A kind of perfume chrysanthemum promoting blood circulation water-bindered pill and preparation method thereof |
| CN110693922A (en) * | 2019-11-22 | 2020-01-17 | 福建拓天生物科技有限公司 | Hericium erinaceus spore powder wall breaking process |
| CN111282695A (en) * | 2020-01-15 | 2020-06-16 | 好牧人干细胞生物科技有限公司 | Separation method of non-medium nanometer differential |
| CN112442419A (en) * | 2020-12-04 | 2021-03-05 | 江苏滋补堂药业有限公司 | Preparation method of ganoderma lucidum spore oil |
| CN112457991A (en) * | 2020-11-27 | 2021-03-09 | 江苏滋补堂药业有限公司 | A method for breaking cell wall of Ganoderma spore powder |
| CN113210105A (en) * | 2021-05-08 | 2021-08-06 | 江西仙客来生物科技有限公司 | Ganoderma lucidum spore powder wall breaking process |
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Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106109507A (en) * | 2016-08-08 | 2016-11-16 | 孙继勇 | A kind of manufacture method of ultra micro nanometer Ganoderma spore powder with cellular wall broken |
| CN106861865A (en) * | 2017-04-19 | 2017-06-20 | 长葛市怀瑞蜂产品有限公司 | A kind of means for breaking walls of pollen |
| CN108030050A (en) * | 2017-12-19 | 2018-05-15 | 安徽强旺调味食品有限公司 | A kind of Islamic compound seasoner for extrusion and puffing food |
| CN108654811A (en) * | 2018-03-16 | 2018-10-16 | 中国水产科学研究院东海水产研究所 | A kind of method that laboratory quickly prepares the micro- plastics of micron order |
| CN108992492A (en) * | 2018-10-26 | 2018-12-14 | 青海未来格萨尔王药业有限公司 | A kind of preparation method of yellow fragrant particle |
| CN108992508A (en) * | 2018-10-26 | 2018-12-14 | 青海未来格萨尔王药业有限公司 | Four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof |
| CN108992511A (en) * | 2018-10-26 | 2018-12-14 | 青海未来格萨尔王药业有限公司 | A kind of stomach strengthening and digestion promoting water-bindered pill and preparation method thereof |
| CN109224018A (en) * | 2018-10-29 | 2019-01-18 | 青海未来格萨尔王药业有限公司 | A kind of perfume chrysanthemum promoting blood circulation water-bindered pill and preparation method thereof |
| CN110693922A (en) * | 2019-11-22 | 2020-01-17 | 福建拓天生物科技有限公司 | Hericium erinaceus spore powder wall breaking process |
| CN110693922B (en) * | 2019-11-22 | 2022-01-14 | 福建拓天生物科技有限公司 | Hericium erinaceus spore powder wall breaking process |
| CN111282695A (en) * | 2020-01-15 | 2020-06-16 | 好牧人干细胞生物科技有限公司 | Separation method of non-medium nanometer differential |
| CN112457991A (en) * | 2020-11-27 | 2021-03-09 | 江苏滋补堂药业有限公司 | A method for breaking cell wall of Ganoderma spore powder |
| CN112442419A (en) * | 2020-12-04 | 2021-03-05 | 江苏滋补堂药业有限公司 | Preparation method of ganoderma lucidum spore oil |
| CN113210105A (en) * | 2021-05-08 | 2021-08-06 | 江西仙客来生物科技有限公司 | Ganoderma lucidum spore powder wall breaking process |
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Application publication date: 20160727 |