CN105647809A - Wall breaking method for ganoderma lucidum spore powder - Google Patents
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Abstract
The invention discloses a wall breaking method for ganoderma lucidum spore powder. The method includes: mixing the ganoderma lucidum spore powder with a solvent; ultrasonically pretreating the mixture; performing high-pressure treatment at the room temperature to realize wall breaking and extraction of the ganoderma lucidum spore powder; using a funnel type grinder for grinding; using supersonic airflow for material impacting and smashing to realize wall breaking again, and carrying out vacuum drying to realize that a room-temperature wall breaking rate of the ganoderma lucidum spore powder is larger than or equal to 99%, the yield is larger than or equal to 95%, and the product particle size is smaller than or equal to 3 micrometers. The wall breaking method for the ganoderma lucidum spore powder has the advantages of uniform particle size, high yield, high release rate of effective ingredients of the spore powder and the like, and the problems of low effective ingredient extraction rate and technical complexity in current treatment of the ganoderma lucidum spore powder are thoroughly solved.
Description
Technical field
The invention belongs to the complete processing of Ganoderma spore powder, it be specifically related to the wall-breaking method of a kind of Ganoderma spore powder.
Background technology
Glossy ganoderma is Chinese traditional medicine rarity, and China is the source region of glossy ganoderma application and glossy ganoderma culture. " Shennong Bencaojing " is recorded, glossy ganoderma be listed in safe and effective, have no adverse reaction top grade, it is described as celestial grass, auspicious grass and Pink Reineckea Herb, the Compendium of Material Medica of Ming Dynasty's LI Shi-Zhen think glossy ganoderma " main deafness, profit joint, protect god, beneficial vital essence, hard muscles and bones, good color, for a long time take always do not prolong life ", glossy ganoderma has been made very high evaluation. Glossy ganoderma by the whole world generally acknowledge a kind of can strengthening by means of tonics, the traditional Chinese medicine strengthened the body resistance to consolidate the constitution.
Ganoderma spore powder be glossy ganoderma in the growth and maturity phase, the seed of be hit by a bullet from glossy ganoderma the lamella extremely small avette sexual cell shot out and glossy ganoderma. Each Ganoderma spore only 4-6 micron is living body biological body, double-walled construction, outer is surrounded by hard chitin fiber element, and human body is difficult to fully absorption. It is more suitable for human body stomach after broken wall directly to absorb. It has condensed is the elite of glossy ganoderma, has whole genetic material and the health-care effect of glossy ganoderma. The broken wall of Ganoderma spore powder refers to that it is with cellulosic shell, should not be directly material that human body is assimilated, by artificial machinery, physico-chemical process, biologic enzymolysis method, after broken for its Mierocrystalline cellulose outer wall or elimination so that it is be more prone to the nutritive substance digested and assimilated in Mierocrystalline cellulose wall.
Summary of the invention
Technical problem to be solved by this invention is to provide the wall-breaking method of a kind of Ganoderma spore powder, it is possible to Simplified flowsheet, it is to increase the extraction yield of effective constituent.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme:
A wall-breaking method for Ganoderma spore powder, comprises the steps:
A. Ganoderma spore powder is mixed mutually with solvent;
B. utilize ultrasonic wave that mixture is carried out pre-treatment in advance;
C. autoclaving is at room temperature carried out, to realize broken wall and the leaching of Ganoderma spore powder;
D. a funnel formula pulverizer vertically arranged is prepared, the central shaft of described funnel formula pulverizer is provided with spiral, the Ganoderma spore powder of upper step process is injected by a pipeline pressurization entrance of described funnel formula pulverizer, described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral, and the outlet that described Ganoderma spore powder from top to down pushes to described funnel formula pulverizer is discharged;
E. utilize supersonic airstream that the Ganoderma spore powder of upper step process carries out shock to break up to realize broken wall again, after vacuum-drying, make Ganoderma spore powder normal temperature sporoderm-broken rate >=99%, receipts rate >=95%, product cut size��3 ��m.
Funnel formula pulverizer in described steps d, its diameter installing spiral on center shaft reducing and reduce along with funnel space successively from the inlet to the outlet, described Ganoderma spore powder, from import to outlet successively reducing and increase along with funnel space, is kept extruding crush force radial and axial when rotated by the diameter of the central shaft of described funnel formula pulverizer to realize described spiral.
In step a, described solvent is spirituous solution or the water of 50%.
In stepb, the time of described ultrasonic pretreatment is 10-15min.
In step c, the pressure of described autoclaving is 250-550MPa, dwell time is 5-20min.
The Selecting parameter principle of described autoclaving is: ensureing to select lower pressure and shorter dwell time under the prerequisite that the sporoderm-broken rate of Ganoderma spore powder reaches more than 70%.
Described step e comprises the steps:
E1. air-flow grinding machine is adopted to be that 5-10 ��m of Ganoderma spore powders spray in the crushiing chamber of air-flow grinding machine with each straying quatity 4.1-4.5g, interval 30s by 20kg granularity, the supersonic airstream that the mouth ejection flow velocity that feed pressure is 0.4-0.8Mpa, sprayed by air-flow grinding machine is 420-470m/s carries out broken wall, and broken wall temperature is 30-35 DEG C;
E2. adopt grading machine that the Ganoderma spore powder after supersonic speed broken wall is carried out thickness separation, sorting, and the spore powder with crushed sporoderm of��3 ��m is collected;
E3. the spore powder with crushed sporoderm collected being carried out vacuum-drying, pressure is 0.4-0.6MPa, and temperature is 30 DEG C;
E4. by the spore powder with crushed sporoderm Returning flow grinding machine repeating step d2-d3 of > 3 ��m;
E5. by dried spore powder with crushed sporoderm sterilizing, packaging.
Adopting the wall-breaking method of a kind of Ganoderma spore powder of the present invention, tool has the following advantages:
1, by, after ultrasonic pretreatment and autoclaving, sporoderm-broken rate can reach more than 70%, then by supersonic speed broken wall, sporoderm-broken rate can reach more than 99%, receipts rate >=95%, product cut size��3 ��m.
2, technique is simple, output height, be effectively divided into extraction yield height.
Accompanying drawing
Fig. 1 is the schema of one embodiment of the invention;
Fig. 2 is the funnel formula pulverizer schematic diagram described in one embodiment of the invention.
Embodiment
See Fig. 1, the wall-breaking method of a kind of Ganoderma spore powder of the present invention, comprises the steps:
A. Ganoderma spore powder is mixed mutually with solvent;
B. utilize ultrasonic wave that mixture is carried out pre-treatment in advance;
C. autoclaving is at room temperature carried out, to realize broken wall and the leaching of Ganoderma spore powder;
D. a funnel formula pulverizer vertically arranged is prepared, the central shaft of described funnel formula pulverizer is provided with spiral, the Ganoderma spore powder of upper step process is injected by a pipeline pressurization entrance of described funnel formula pulverizer, described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral, and the outlet that described Ganoderma spore powder from top to down pushes to described funnel formula pulverizer is discharged;
E. utilize supersonic airstream that the Ganoderma spore powder of upper step process carries out shock to break up to realize broken wall again, after vacuum-drying, make Ganoderma spore powder normal temperature sporoderm-broken rate >=99%, receipts rate >=95%, product cut size��3 ��m.
Funnel formula pulverizer in described steps d, its diameter installing spiral on center shaft reducing and reduce along with funnel space successively from the inlet to the outlet, described Ganoderma spore powder, from import to outlet successively reducing and increase along with funnel space, is kept extruding crush force radial and axial when rotated by the diameter of the central shaft of described funnel formula pulverizer to realize described spiral.
In step a, described solvent is spirituous solution or the water of 50%.
In stepb, the time of described ultrasonic pretreatment is 10-15min.
In step c, the pressure of described autoclaving is 250-550MPa, dwell time is 5-20min.
The Selecting parameter principle of described autoclaving is: ensureing to select lower pressure and shorter dwell time, to boost productivity, to reduce energy consumption under the prerequisite that the sporoderm-broken rate of Ganoderma spore powder reaches more than 70%. Experimentally, when pressure is less than 250MPa, its shell-broken effect is very micro-; When pressure is greater than 550MPa, sporoderm-broken rate is no significant difference then; Under suitable pressure, the dwell time, then sporoderm-broken rate was also without the effect significantly improved more than 20min.
Described step e comprises the steps:
E1. air-flow grinding machine is adopted to be that 5-10 ��m of Ganoderma spore powders spray in the crushiing chamber of air-flow grinding machine with each straying quatity 4.1-4.5g, interval 30s by 20kg granularity, the supersonic airstream that the mouth ejection flow velocity that feed pressure is 0.4-0.8Mpa, sprayed by air-flow grinding machine is 420-470m/s carries out broken wall, and broken wall temperature is 30-35 DEG C;
E2. adopt grading machine that the Ganoderma spore powder after supersonic speed broken wall is carried out thickness separation, sorting, and the spore powder with crushed sporoderm of��3 ��m is collected;
E3. the spore powder with crushed sporoderm collected being carried out vacuum-drying, pressure is 0.4-0.6MPa, and temperature is 30 DEG C;
E4. by the spore powder with crushed sporoderm Returning flow grinding machine repeating step d2-d3 of > 3 ��m;
E5. by dried spore powder with crushed sporoderm sterilizing, packaging.
Carry out below specifically illustrating:
Embodiment 1
Mix with Ganoderma spore powder as solvent with the spirituous solution of 50%, after the ultrasonic pretreatment of 10min, at room temperature, employing pressure is 380MPa, dwell time is that 5min carries out autoclaving. see Fig. 2, prepare a funnel formula pulverizer 100 vertically arranged, the central shaft 130 of described funnel formula pulverizer 100 is provided with spiral 120, being pressurizeed by a pipeline 200 by the Ganoderma spore powder of upper step process and inject the entrance 110 of described funnel formula pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funnel formula pulverizer 100. Described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral 120, and the outlet 140 that described Ganoderma spore powder from top to down pushes to described funnel formula pulverizer 100 is discharged. The diameter of the spiral 120 being arranged on central shaft 130 is from entrance 110 to outlet 140 successively reducing and reduce along with funnel space, described Ganoderma spore powder, from import 110 to outlet 140 successively reducing and increase along with funnel space, is kept extruding crush force radial and axial when rotated by the diameter of the central shaft 130 of described funnel formula pulverizer 100 to realize described spiral 120.
Start air-flow grinding machine and grading machine, it is that 5 ��m of Ganoderma spore powders spray in the crushiing chamber of air-flow grinding machine with each straying quatity 4.1g, interval 30s by the granularity after 20kg autoclaving, the supersonic airstream that the mouth ejection flow velocity that feed pressure is 0.4Mpa, sprayed by air-flow grinding machine is 420m/s makes the particle of two bursts of move toward one another collision mutually occur, clash into, carrying out broken wall, broken wall temperature is 30 DEG C; The material reaching spore powder granularity requirements enters grading machine, and thickness powder is separated, and sorting, collects the spore powder with crushed sporoderm of particle diameter��3 ��m, then carries out broken wall vacuum-drying, and pressure is 0.4MPa, and temperature is 30 ��, sterilizing and packaging. The meal Returning flow grinding machine of particle diameter > 3 ��m is pulverized again, then classification, drying, process 40h through iterative cycles complete.
Embodiment 2
Mixing with Ganoderma spore powder as solvent with the spirituous solution of 50%, after the ultrasonic pretreatment of 15min, at room temperature, employing pressure is 420MPa, dwell time is that 15min carries out autoclaving. See Fig. 2, prepare a funnel formula pulverizer 100 vertically arranged, the central shaft 130 of described funnel formula pulverizer 100 is provided with spiral 120, being pressurizeed by a pipeline 200 by the Ganoderma spore powder of upper step process and inject the entrance 110 of described funnel formula pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funnel formula pulverizer 100. Described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral 120, and the outlet 140 that described Ganoderma spore powder from top to down pushes to described funnel formula pulverizer 100 is discharged. The diameter of the spiral 120 being arranged on central shaft 130 is from entrance 110 to outlet 140 successively reducing and reduce along with funnel space, described Ganoderma spore powder, from import 110 to outlet 140 successively reducing and increase along with funnel space, is kept extruding crush force radial and axial when rotated by the diameter of the central shaft 130 of described funnel formula pulverizer 100 to realize described spiral 120.
Start air-flow grinding machine and grading machine, it is that 10 ��m of Ganoderma spore powders spray in the crushiing chamber of air-flow grinding machine with each straying quatity 4.5g, interval 30s by the granularity after 20kg autoclaving, the supersonic airstream that the mouth ejection flow velocity that feed pressure is 0.8Mpa, sprayed by air-flow grinding machine is 470m/s makes the particle of two bursts of move toward one another collision mutually occur, clash into, carrying out broken wall, broken wall temperature is 30 DEG C; The material reaching spore powder granularity requirements enters grading machine, and thickness powder is separated, and sorting, collects the spore powder with crushed sporoderm of particle diameter��3 ��m, then carries out broken wall vacuum-drying, and pressure is 0.6MPa, and temperature is 30 ��, sterilizing and packaging. The meal Returning flow grinding machine of particle diameter > 3 ��m is pulverized again, then classification, drying, process 40h through iterative cycles complete.
Embodiment 3
Using water as solvent mixes with Ganoderma spore powder, after the ultrasonic pretreatment of 12min, at room temperature, employing pressure is 400MPa, dwell time is that 20min carries out autoclaving. See Fig. 2, prepare a funnel formula pulverizer 100 vertically arranged, the central shaft 130 of described funnel formula pulverizer 100 is provided with spiral 120, being pressurizeed by a pipeline 200 by the Ganoderma spore powder of upper step process and inject the entrance 110 of described funnel formula pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funnel formula pulverizer 100. Described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral 120, and the outlet 140 that described Ganoderma spore powder from top to down pushes to described funnel formula pulverizer 100 is discharged. The diameter of the spiral 120 being arranged on central shaft 130 is from entrance 110 to outlet 140 successively reducing and reduce along with funnel space, described Ganoderma spore powder, from import 110 to outlet 140 successively reducing and increase along with funnel space, is kept extruding crush force radial and axial when rotated by the diameter of the central shaft 130 of described funnel formula pulverizer 100 to realize described spiral 120.
Start air-flow grinding machine and grading machine, it is that 8 ��m of Ganoderma spore powders spray in the crushiing chamber of air-flow grinding machine with each straying quatity 4.3g, interval 30s by the granularity after 20kg autoclaving, the supersonic airstream that the mouth ejection flow velocity that feed pressure is 0.6Mpa, sprayed by air-flow grinding machine is 450m/s makes the particle of two bursts of move toward one another collision mutually occur, clash into, carrying out broken wall, broken wall temperature is 30 DEG C; The material reaching spore powder granularity requirements enters grading machine, and thickness powder is separated, and sorting, collects the spore powder with crushed sporoderm of particle diameter��3 ��m, then carries out broken wall vacuum-drying, and pressure is 0.5MPa, and temperature is 30 ��, sterilizing and packaging. The meal Returning flow grinding machine of particle diameter > 3 ��m is pulverized again, then classification, drying, process 40h through iterative cycles complete.
Identifying after testing, the final sporoderm-broken rate of spore powder with crushed sporoderm after above embodiment 1-3 processes all can reach more than 99%, receipts rate >=95%, product cut size��3 ��m.
In sum, adopt the wall-breaking method of the present invention, have granularity evenly, the effective constituent release rate advantages of higher of output height, spore powder, thoroughly solve existing Ganoderma spore powder process is existed complex process, problem that effective component extraction rate is low.
But, those of ordinary skill in the art will be appreciated that, above embodiment is only used to the present invention is described, and not it is used as limitation of the invention, as long as in the spirit of the present invention, to the change of the above embodiment, modification all by the Claims scope dropping on the present invention.
Claims (7)
1. the wall-breaking method of a Ganoderma spore powder, it is characterised in that, comprise the steps:
A. Ganoderma spore powder is mixed mutually with solvent;
B. utilize ultrasonic wave that mixture is carried out pre-treatment in advance;
C. autoclaving is at room temperature carried out, to realize broken wall and the leaching of Ganoderma spore powder;
D. a funnel formula pulverizer vertically arranged is prepared, the central shaft of described funnel formula pulverizer is provided with spiral, the Ganoderma spore powder of upper step process is injected by a pipeline pressurization entrance of described funnel formula pulverizer, described Ganoderma spore powder is carried out extruding by the mode rotated and pulverizes by described spiral, and the outlet that described Ganoderma spore powder from top to down pushes to described funnel formula pulverizer is discharged;
E. utilize supersonic airstream that the Ganoderma spore powder of upper step process carries out shock to break up to realize broken wall again, after vacuum-drying, make Ganoderma spore powder normal temperature sporoderm-broken rate >=99%, receipts rate >=95%, product cut size��3 ��m.
2. the wall-breaking method of a kind of Ganoderma spore powder according to claim 1, it is characterized in that, funnel formula pulverizer in described steps d, its diameter installing spiral on center shaft reducing and reduce along with funnel space successively from the inlet to the outlet, described Ganoderma spore powder, from import to outlet successively reducing and increase along with funnel space, is kept extruding crush force radial and axial when rotated by the diameter of the central shaft of described funnel formula pulverizer to realize described spiral.
3. the wall-breaking method of a kind of Ganoderma spore powder according to claim 1, it is characterised in that: in step a, described solvent is spirituous solution or the water of 50%.
4. the wall-breaking method of a kind of Ganoderma spore powder according to claim 1, it is characterised in that: in stepb, the time of described ultrasonic pretreatment is 10-15min.
5. the wall-breaking method of a kind of Ganoderma spore powder according to claim 1, it is characterised in that: in step c, the pressure of described autoclaving is 250-550MPa, dwell time is 5-20min.
6. the wall-breaking method of a kind of Ganoderma spore powder according to claim 5, it is characterized in that, the Selecting parameter principle of described autoclaving is: ensureing to select lower pressure and shorter dwell time under the prerequisite that the sporoderm-broken rate of Ganoderma spore powder reaches more than 70%.
7. the wall-breaking method of a kind of Ganoderma spore powder according to claim 1, it is characterised in that, described step e comprises the steps:
E1. air-flow grinding machine is adopted to be that 5-10 ��m of Ganoderma spore powder sprays in the crushiing chamber of air-flow grinding machine with each straying quatity 4.1-4.5g, interval 30s by 20kg granularity, the supersonic airstream that the mouth ejection flow velocity that feed pressure is 0.4-0.8Mpa, sprayed by air-flow grinding machine is 420-470m/s carries out broken wall, and broken wall temperature is 30-35 DEG C;
E2. adopt grading machine that the Ganoderma spore powder after supersonic speed broken wall is carried out thickness separation, sorting, and the spore powder with crushed sporoderm of��3 ��m is collected;
E3. the spore powder with crushed sporoderm collected being carried out vacuum-drying, pressure is 0.4-0.6MPa, and temperature is 30 DEG C;
E4. by the spore powder with crushed sporoderm Returning flow grinding machine repeating step d2-d3 of > 3 ��m;
E5. by dried spore powder with crushed sporoderm sterilizing, packaging.
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| CN106109507A (en) * | 2016-08-08 | 2016-11-16 | 孙继勇 | A kind of manufacture method of ultra micro nanometer Ganoderma spore powder with cellular wall broken |
| CN106418399A (en) * | 2016-09-21 | 2017-02-22 | 端木至冬 | Wall-breaking method for blackberry seeds |
| CN107320503A (en) * | 2017-07-04 | 2017-11-07 | 孙继勇 | The preparation method of ganoderma spove powder |
| CN110813478A (en) * | 2019-11-15 | 2020-02-21 | 苏州鹰皇药业有限公司 | Plasma screening method for processing ganoderma lucidum spore powder |
| CN111642669A (en) * | 2020-06-28 | 2020-09-11 | 武汉绿时代创新科技有限公司 | Bamboo salt ganoderma lucidum spore powder composite solid beverage and preparation method thereof |
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| CN106109507A (en) * | 2016-08-08 | 2016-11-16 | 孙继勇 | A kind of manufacture method of ultra micro nanometer Ganoderma spore powder with cellular wall broken |
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| CN107320503A (en) * | 2017-07-04 | 2017-11-07 | 孙继勇 | The preparation method of ganoderma spove powder |
| CN110813478A (en) * | 2019-11-15 | 2020-02-21 | 苏州鹰皇药业有限公司 | Plasma screening method for processing ganoderma lucidum spore powder |
| CN111642669A (en) * | 2020-06-28 | 2020-09-11 | 武汉绿时代创新科技有限公司 | Bamboo salt ganoderma lucidum spore powder composite solid beverage and preparation method thereof |
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