CN105769940A - Making method for honey ganoderma lucidum spore powder - Google Patents
Making method for honey ganoderma lucidum spore powder Download PDFInfo
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- CN105769940A CN105769940A CN201610133633.9A CN201610133633A CN105769940A CN 105769940 A CN105769940 A CN 105769940A CN 201610133633 A CN201610133633 A CN 201610133633A CN 105769940 A CN105769940 A CN 105769940A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
- A61K36/074—Ganoderma
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/141—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers
- A61K9/148—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers with compounds of unknown constitution, e.g. material from plants or animals
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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Abstract
The invention discloses a making method for honey ganoderma lucidum spore powder. The making method comprises the following steps: carrying out ultrasonic treatment, liquid nitrogen quenching and thawing on ganoderma lucidum spore powder in sequence, mixing, extruding and grinding the ganoderma lucidum spore powder and honey powder by a funnel type grinder, finally grinding the ganoderma lucidum spore powder and the honey powder again by a vibration mill, so as to enable the sporoderm-broken rate of ganoderma lucidum spores to be 99.9% or above and enable the ganoderma lucidum spore powder to be fully mixed with the honey powder.
Description
Technical field
The invention belongs to the processing technique of Ganoderma spore powder, be specifically related to the manufacture method of a kind of honey glossy ganoderma spore powder.
Background technology
Ganoderma is Chinese traditional medicine rarity, and China is Ganoderma application and the cradle of Ganoderma culture.Shennong's Herbal is recorded, Ganoderma is listed in safely and effectively, have no adverse reaction top grade, it is described as Herba mesonae chinensis, Ganoderma and Herba Reineckeae Carneae, the Compendium of Material Medica of Ming Dynasty's Li Shizhen (1518-1593 A.D.) is thought and Ganoderma is made that Ganoderma " main deafness, profit joint, protect vital essence refreshing, beneficial, hard muscles and bones, good color, for a long time clothes are not prolonged life always " significantly high evaluation.Ganoderma by the whole world generally acknowledge a kind of can strengthening by means of tonics, strengthening the body resistance Chinese medicine.
Ganoderma spore powder be Ganoderma in the growth and maturity phase, the seed of be hit by a bullet from Ganoderma the lamella extremely small avette sexual cell shot out and Ganoderma.Each Ganoderma spore only has 4-6 micron, is living organisms, double-walled construction, outer is surrounded by hard chitin fiber element, and human body is difficult to fully absorb.It is more suitable for human body the intestines and stomach after breaking cellular wall directly to absorb.It has condensed is the elite of Ganoderma, has whole hereditary materials and the health-care effect of Ganoderma.The breaking cellular wall of Ganoderma spore powder refers to it with cellulosic shell, the material that should not directly assimilate for human body, by artificial machinery, physico-chemical process, biologic enzymolysis method, after broken for its cellulose outer wall or elimination so that it is be more prone to the nutrient substance digesting and assimilating in cellulose wall.
Summary of the invention
The technical problem to be solved is to provide the manufacture method of a kind of honey glossy ganoderma spore powder, it is possible to Simplified flowsheet, improves the extraction ratio of effective ingredient.
In order to solve above-mentioned technical problem, the present invention adopts the following technical scheme that:
The manufacture method of a kind of honey glossy ganoderma spore powder, comprises the steps:
A. Mel is prepared: honey raw material allotment uniformly and is preheating to 20 DEG C-35 DEG C, and with Mel described in microwave vacuum drying, temperature is maintained at 35 DEG C-50 DEG C, makes water content reach 2%-8%, pulverizes stand-by；
B. Ganoderma spore powder is mixed mutually with solvent, utilize ultrasound wave that mixture is carried out pretreatment；
C. put into after the Ganoderma spore powder of upper step process being dried and normal pressure liquid nitrogen carries out quenching process；
D. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step c-d and be dried after for several times again；
E. a funneling pulverizer being vertically arranged is prepared, the central shaft of described funneling pulverizer is provided with spiral, the Ganoderma spore powder of upper step process and Mel powder are injected the entrance of described funneling pulverizer by a pipeline pressurization, described Ganoderma spore powder and Mel powder are carried out mixing extruding and pulverize by the described mode being threaded through rotating, and the outlet that its from top to down pushes to described funneling pulverizer is discharged；
F. vibromill is adopted again above-mentioned Ganoderma spore powder and Mel powder to be pulverized so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9% and is sufficiently mixed with Mel powder.
In described step b, described solvent is alcoholic solution or the water of 50%, and the time of described ultrasonic pretreatment is 10-15min.
In described step c, described liquid nitrogen temperature is less than-196 DEG C.
Funneling pulverizer in described step e, its diameter installing spiral on center shaft reduces along with reducing of funnel space from the inlet to the outlet successively, the diameter of the central shaft of described funneling pulverizer increases along with reducing of funnel space from import successively to outlet, to realize described spiral when rotated at radial and axial extruding crush force that described Ganoderma spore powder and Mel powder kept.
In described step f, the rotating speed of described vibromill is 800-1200r/min, and power is 1000-1500w, and frequency of vibration is 800-1000Hz, and amplitude is 2-4cm.
Adopt the manufacture method of a kind of honey glossy ganoderma spore powder of the present invention, have the advantage that
1, heat extremely low according to the heat conductivity of Ganoderma spore wall transmits slow feature, Ganoderma spore powder after drying is carried out quenching process in normal pressure liquid nitrogen, produce thermal stress cause that breaking cellular wall phenomenon occurs by the temperature difference more than 200 DEG C inside and outside wall, put into again in hot water and thaw, repeatedly for several times, it is achieved the sporoderm-broken rate of more than 90%；
2, mixed further and breaking cellular wall by funneling pulverizer and vibromill, to realize the sporoderm-broken rate of more than 99.9% and to mix fully；
3, technique is simple, yield is high, be effectively split into extraction ratio height.
Accompanying drawing
Fig. 1 is the flow chart of one embodiment of the invention；
Fig. 2 is the funneling pulverizer schematic diagram described in one embodiment of the invention.
Detailed description of the invention
The manufacture method of a kind of honey glossy ganoderma spore powder of the present invention comprises the steps:
A. Mel is prepared: honey raw material allotment uniformly and is preheating to 20 DEG C-35 DEG C, and with Mel described in microwave vacuum drying, temperature is maintained at 35 DEG C-50 DEG C, makes water content reach 2%-8%, pulverizes stand-by；
B. Ganoderma spore powder is mixed mutually with solvent, utilize ultrasound wave that mixture is carried out pretreatment；
C. put into after the Ganoderma spore powder of upper step process being dried and normal pressure liquid nitrogen carries out quenching process；
D. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step c-d and be dried after for several times again；
E. a funneling pulverizer being vertically arranged is prepared, the central shaft of described funneling pulverizer is provided with spiral, the Ganoderma spore powder of upper step process and Mel powder are injected the entrance of described funneling pulverizer by a pipeline pressurization, described Ganoderma spore powder and Mel powder are carried out mixing extruding and pulverize by the described mode being threaded through rotating, and the outlet that its from top to down pushes to described funneling pulverizer is discharged；
F. vibromill is adopted again above-mentioned Ganoderma spore powder and Mel powder to be pulverized so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9% and is sufficiently mixed with Mel powder.
In described step b, described solvent is alcoholic solution or the water of 50%, and the time of described ultrasonic pretreatment is 10-15min.
In described step c, described liquid nitrogen temperature is less than-196 DEG C.
Funneling pulverizer in described step e, its diameter installing spiral on center shaft reduces along with reducing of funnel space from the inlet to the outlet successively, the diameter of the central shaft of described funneling pulverizer increases along with reducing of funnel space from import successively to outlet, to realize described spiral when rotated at radial and axial extruding crush force that described Ganoderma spore powder and Mel powder kept.
In described step f, the rotating speed of described vibromill is 800-1200r/min, and power is 1000-1500w, and frequency of vibration is 800-1000Hz, and amplitude is 2-4cm.
In step e, the percentage by weight of each component is: Ganoderma spore powder 90%, Mel powder 10%.
Embodiment 1
A. Mel is prepared: honey raw material allotment uniformly and is preheating to 20 DEG C-35 DEG C, and with Mel described in microwave vacuum drying, temperature is maintained at 35 DEG C-50 DEG C, makes water content reach 2%-8%, pulverizes stand-by.
B. mixing with Ganoderma spore powder as solvent with the alcoholic solution of 50%, after the ultrasonic pretreatment of 10min, at room temperature, employing pressure is 380MPa, dwell time is that 5min carries out HIGH PRESSURE TREATMENT.
C. the Ganoderma spore powder after drying is put in the liquid nitrogen of normal pressure-196 DEG C and carry out quenching process；
D. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and is dried after repeating step c-d twice again, makes wall breaking rate of ganoderma lucidum spores reach more than 90%；
E. referring to Fig. 2, prepare a funneling pulverizer 100 being vertically arranged, the central shaft 130 of described funneling pulverizer 100 is provided with spiral 120, the Ganoderma spore powder of upper step process and Mel powder being pressurizeed by a pipeline 200 and inject the entrance 110 of described funneling pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funneling pulverizer 100.Described Ganoderma spore powder and Mel powder are carried out extruding by the mode rotated and pulverize by described spiral 120, and the outlet 140 that described Ganoderma spore powder and Mel powder from top to down push to described funneling pulverizer 100 is discharged.The diameter of the spiral 120 being arranged on central shaft 130 reduces along with reducing of funnel space from entrance 110 successively to outlet 140, the diameter of the central shaft 130 of described funneling pulverizer 100 140 increases along with reducing of funnel space from import 110 successively to outlet, radial and axial, described Ganoderma spore powder and Mel powder is kept extruding crush force when rotated realizing described spiral 120.
F. vibromill is adopted again above-mentioned Ganoderma spore powder and Mel powder to be pulverized so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9% and is sufficiently mixed with Mel powder.Vibromill rotating speed is 800r/min, and power is 1000w, and frequency of vibration is 800Hz, and amplitude is 2cm so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
Embodiment 2
A. Mel is prepared: honey raw material allotment uniformly and is preheating to 20 DEG C-35 DEG C, and with Mel described in microwave vacuum drying, temperature is maintained at 35 DEG C-50 DEG C, makes water content reach 2%-8%, pulverizes stand-by.
B. mixing with Ganoderma spore powder as solvent with the alcoholic solution of 50%, after the ultrasonic pretreatment of 15min, at room temperature, employing pressure is 420MPa, dwell time is that 15min carries out HIGH PRESSURE TREATMENT.
C. the Ganoderma spore powder after drying is put in the liquid nitrogen of normal pressure-196 DEG C and carry out quenching process；
D. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and is dried after repeating step c-d twice again, makes wall breaking rate of ganoderma lucidum spores reach more than 90%；
E. referring to Fig. 2, prepare a funneling pulverizer 100 being vertically arranged, the central shaft 130 of described funneling pulverizer 100 is provided with spiral 120, the Ganoderma spore powder of upper step process and Mel powder being pressurizeed by a pipeline 200 and inject the entrance 110 of described funneling pulverizer 100, described pipeline 200 is connected with the entrance 110 of described funneling pulverizer 100.Described Ganoderma spore powder and Mel powder are carried out extruding by the mode rotated and pulverize by described spiral 120, and the outlet 140 that described Ganoderma spore powder and Mel powder from top to down push to described funneling pulverizer 100 is discharged.The diameter of the spiral 120 being arranged on central shaft 130 reduces along with reducing of funnel space from entrance 110 successively to outlet 140, the diameter of the central shaft 130 of described funneling pulverizer 100 140 increases along with reducing of funnel space from import 110 successively to outlet, radial and axial, described Ganoderma spore powder and Mel powder is kept extruding crush force when rotated realizing described spiral 120.
F. vibromill is adopted again above-mentioned Ganoderma spore powder and Mel powder to be pulverized so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9% and is sufficiently mixed with Mel powder.Vibromill rotating speed is 1000r/min, and power is 1200w, and frequency of vibration is 900Hz, and amplitude is 3cm so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9%.
Identify after testing, the final sporoderm-broken rate of spore powder with crushed sporoderm after above example 1-2 processes is all up to more than 99.9% (laboratory adopts the sporoderm-broken rate of wall-breaking method of the present invention to be 100%), yield >=96%, its mixing with Mel powder and fully.
In sum, the method adopting the present invention, have that epigranular, yield is high, the effective ingredient release rate advantages of higher of spore powder, thoroughly solve and existing Ganoderma spore powder is processed the complex process existed, the problem that effective component extraction rate is low.
But, those of ordinary skill in the art will be appreciated that, above embodiments is intended merely to the explanation present invention, and it is not used as limitation of the invention, as long as in the spirit of the present invention, to the change of embodiment described above, modification all by the Claims scope dropping on the present invention.
Claims (5)
1. the manufacture method of a honey glossy ganoderma spore powder, it is characterised in that comprise the steps:
A. Mel is prepared: honey raw material allotment uniformly and is preheating to 20 DEG C-35 DEG C, and with Mel described in microwave vacuum drying, temperature is maintained at 35 DEG C-50 DEG C, makes water content reach 2%-8%, pulverizes stand-by；
B. Ganoderma spore powder is mixed mutually with solvent, utilize ultrasound wave that mixture is carried out pretreatment；
C. put into after the Ganoderma spore powder of upper step process being dried and normal pressure liquid nitrogen carries out quenching process；
D. the Ganoderma spore powder after being processed by quenching quickly puts in hot water and thaws, and repeats step c-d and be dried after for several times again；
E. a funneling pulverizer being vertically arranged is prepared, the central shaft of described funneling pulverizer is provided with spiral, the Ganoderma spore powder of upper step process and Mel powder are injected the entrance of described funneling pulverizer by a pipeline pressurization, described Ganoderma spore powder and Mel powder are carried out mixing extruding and pulverize by the described mode being threaded through rotating, and the outlet that its from top to down pushes to described funneling pulverizer is discharged；
F. vibromill is adopted again above-mentioned Ganoderma spore powder and Mel powder to be pulverized so that wall breaking rate of ganoderma lucidum spores reaches more than 99.9% and is sufficiently mixed with Mel powder.
2. the manufacture method of honey glossy ganoderma spore powder according to claim 1, it is characterised in that in described step b, described solvent is alcoholic solution or the water of 50%, and the time of described ultrasonic pretreatment is 10-15min.
3. the manufacture method of honey glossy ganoderma spore powder according to claim 1, it is characterised in that in described step c, described liquid nitrogen temperature is less than-196 DEG C.
4. the manufacture method of honey glossy ganoderma spore powder according to claim 1, it is characterized in that, funneling pulverizer in described step e, its diameter installing spiral on center shaft reduces along with reducing of funnel space from the inlet to the outlet successively, the diameter of the central shaft of described funneling pulverizer increases along with reducing of funnel space from import successively to outlet, to realize described spiral when rotated at radial and axial extruding crush force that described Ganoderma spore powder and Mel powder kept.
5. the manufacture method of honey glossy ganoderma spore powder according to claim 1, it is characterised in that in described step f, the rotating speed of described vibromill is 800-1200r/min, and power is 1000-1500w, and frequency of vibration is 800-1000Hz, and amplitude is 2-4cm.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610133633.9A CN105769940A (en) | 2016-03-09 | 2016-03-09 | Making method for honey ganoderma lucidum spore powder |
| AU2016201962A AU2016201962A1 (en) | 2016-03-09 | 2016-03-30 | Preparation method of honey ganoderma lucidum spore powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610133633.9A CN105769940A (en) | 2016-03-09 | 2016-03-09 | Making method for honey ganoderma lucidum spore powder |
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| CN105769940A true CN105769940A (en) | 2016-07-20 |
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| CN201610133633.9A Pending CN105769940A (en) | 2016-03-09 | 2016-03-09 | Making method for honey ganoderma lucidum spore powder |
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| AU (1) | AU2016201962A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111686156A (en) * | 2020-05-20 | 2020-09-22 | 安徽利民生物科技股份有限公司 | Throat-moistening agent containing ganoderma lucidum spore powder and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1378791A (en) * | 2002-01-25 | 2002-11-13 | 上海理工大学 | Process for breaking wall of pollen and ganoderma spore |
| CN1401331A (en) * | 2002-10-08 | 2003-03-12 | 吉林大学 | Method for wall-breaking leaching ganoderma spore powder |
| CN1820629A (en) * | 2006-03-02 | 2006-08-23 | 陈西喆 | Method for producing solid honey |
| CN101524376A (en) * | 2009-04-10 | 2009-09-09 | 南京师范大学 | Extrusion wall breaking method of lucidum spore powder |
| CN102726735A (en) * | 2012-07-19 | 2012-10-17 | 福建省健神生物工程有限公司 | Ganoderma lucidum spore honey and preparation method thereof |
| CN103190605A (en) * | 2013-04-24 | 2013-07-10 | 东北大学 | Method for preparing ganodorma wall-broken spore powder |
| CN105125595A (en) * | 2015-08-07 | 2015-12-09 | 重庆市生物技术研究所有限责任公司 | Ganoderma lucidum spore powder wall breaking method |
-
2016
- 2016-03-09 CN CN201610133633.9A patent/CN105769940A/en active Pending
- 2016-03-30 AU AU2016201962A patent/AU2016201962A1/en not_active Abandoned
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1378791A (en) * | 2002-01-25 | 2002-11-13 | 上海理工大学 | Process for breaking wall of pollen and ganoderma spore |
| CN1401331A (en) * | 2002-10-08 | 2003-03-12 | 吉林大学 | Method for wall-breaking leaching ganoderma spore powder |
| CN1820629A (en) * | 2006-03-02 | 2006-08-23 | 陈西喆 | Method for producing solid honey |
| CN101524376A (en) * | 2009-04-10 | 2009-09-09 | 南京师范大学 | Extrusion wall breaking method of lucidum spore powder |
| CN102726735A (en) * | 2012-07-19 | 2012-10-17 | 福建省健神生物工程有限公司 | Ganoderma lucidum spore honey and preparation method thereof |
| CN103190605A (en) * | 2013-04-24 | 2013-07-10 | 东北大学 | Method for preparing ganodorma wall-broken spore powder |
| CN105125595A (en) * | 2015-08-07 | 2015-12-09 | 重庆市生物技术研究所有限责任公司 | Ganoderma lucidum spore powder wall breaking method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111686156A (en) * | 2020-05-20 | 2020-09-22 | 安徽利民生物科技股份有限公司 | Throat-moistening agent containing ganoderma lucidum spore powder and preparation method thereof |
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| AU2016201962A1 (en) | 2017-09-28 |
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