CN108992508A - Four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof - Google Patents
Four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof Download PDFInfo
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Abstract
A kind of four taste lanatechead saussurea herb with flower particles and preparation method thereof, composition of raw materials includes the raw material of following parts by weight: the root of kirilow rhodiola of 18-22 parts by weight, the lanatechead saussurea herb with flower of 4-6 parts by weight, the rheum officinale of 4-6 parts by weight, the fern fiber crops of 8-12 parts by weight, 45-55 parts by weight cane sugar powder.Preparation method includes the preparation of the preparation of root of kirilow rhodiola and fern fiber crops extracting solution, the preparation of rheum officinale ethanol extract, the preparation of lanatechead saussurea herb with flower ethyl alcohol soak and four taste lanatechead saussurea herb with flower particles.Preparation method simple process of the invention, convenient for operation.
Description
Technical field
The present invention relates to a kind of four taste lanatechead saussurea herb with flower particles and preparation method thereof, belong to Tibetan medicine preparation technical field.
Background technique
Root of kirilow rhodiola is herbaceos perennial, is grown in 1800-2500 meters of height above sea level of high and cold contamination-freely band more.Root of kirilow rhodiola
With tonifying Qi clearing lung-heat, intelligence development nourishing heart, controlling of bleeding with astringents, eliminating stasis to subdue swelling and other effects, it is to act on extensive Chinese medicine simply, cures mainly deficiency of vital energy body
Weak, illnesss such as chilly, shortness of breath and fatigue, cough with lung heat, hemoptysis, leukorrhea diarrhea, traumatic injury after being ill.
Lanatechead saussurea herb with flower is herbaceos perennial, is similar to lotus flower because it is pushed up, therefore lanatechead saussurea herb with flower of gaining the name, abbreviation saussurea involucrata；It is grown on more
In rock seam, cliff and ice sulphur ruckle near high mountain snow line, generally at 2400-4000 meters of height above sea level.Lanatechead saussurea herb with flower contain protein,
Amino acid, flavone compound, alkaloid etc. have clearing and activating the channels and collaterals, dispelling cold and removing dampness, hemostasia and detumescence, isostere endotoxin and other effects.
Rheum officinale is being collectively referred to as the perennial plant of a variety of polygonaceae Rheums.In China, rheum officinale is used mainly as Chinese medicine.
Annual autumn end cauline leaf is withered to the germination of spring next year, and the root of rheum officinale plant is excavated, and removes radicula, scrapes off crust, valve cutting or
Chinese medicine " rheum officinale " is made after dry in section.Chinese medicine rheum officinale, which has, attacks the function such as stagnant, clearing away damp-heat, purging intense heat, cool blood, dissolving stasis, removing toxic substances
Effect.
Fern fiber crops also known as life fruit, rosaceae Potentilla herbaceos perennial.The root swelling of fern fiber crops, rich in starch,
Tanning material etc., can be used as medicine eliminate-poverty blood and malnutritive illness.
Summary of the invention
The purpose of the present invention is to provide a kind of four taste lanatechead saussurea herb with flower particles and preparation method thereof.
In order to achieve the above objects and other related objects, present invention provide the technical scheme that a kind of four taste lanatechead saussurea herb with flower
Grain, composition of raw materials includes the raw material of following parts by weight: the root of kirilow rhodiola of 18-22 parts by weight, the lanatechead saussurea herb with flower of 4-6 parts by weight, 4-6 weight
Part rheum officinale, 8-12 parts by weight fern fiber crops, 45-55 parts by weight cane sugar powder.
Preferred technical solution are as follows: the root of kirilow rhodiola, lanatechead saussurea herb with flower, rheum officinale, fern fiber crops are dried product.
Preferred technical solution are as follows: its fineness of the cane sugar powder is 100-120 mesh.
In order to achieve the above objects and other related objects, present invention provide the technical scheme that a kind of four taste lanatechead saussurea herb with flower
The preparation method of grain, for composition of raw materials using any composition of raw materials of claim 1-3, preparation method includes root of kirilow rhodiola and fern
The preparation of numb extracting solution, the preparation of rheum officinale ethanol extract, the preparation of lanatechead saussurea herb with flower ethyl alcohol soak and four taste lanatechead saussurea herb with flower particles
Preparation:
The preparation of the root of kirilow rhodiola and fern fiber crops extracting solution includes: by the root of kirilow rhodiola after broken wall treatment, the fern after Steam explosion treatment
Numb cortical granule, fern fiber crops core material particles are mixed to get mixed material, then mixed material is mixed with water 1:4-7 in mass ratio, leaching
5-6h is steeped, is then placed into the thermal extraction device with steam condensate collection device, 5-6h is extracted in boiling, right after the completion of extraction
Extracting solution is filtered；Collecting obtained filtrate is root of kirilow rhodiola and fern fiber crops extracting solution, spare；
The preparation method of root of kirilow rhodiola after the broken wall treatment: root of kirilow rhodiola is broken into the root of kirilow rhodiola particle of 10-12 mesh；By red scape
Its particle 2-3 freeze thawing treatment of progress is spare to get the root of kirilow rhodiola after broken wall treatment；The freeze thawing treatment is by root of kirilow rhodiola
Grain is placed in 2-3min in liquid nitrogen, then takes out 2-3min in the hot wind environment for be placed in 85-95 DEG C；
The preparation of fern fiber crops cortical granule after the Steam explosion treatment includes: that fern fiber crops are broken into the fern that fineness is 10-12 mesh
Numb particle；Then fern fiber crops particle is separated, obtains fern fiber crops cortical granule and fern hemp core layer particle；Then by fern hemp skin layer
Grain impregnates 60-120min with 5-30 DEG C of water, then by the fern fiber crops cortical granule after immersion be placed in steam blasting equipment into
Row Steam explosion treatment；Fern fiber crops cortical granule after obtaining Steam explosion treatment, it is spare；
The preparation of the rheum officinale ethanol extract includes: that rheum officinale is crushed to 40-60 mesh, obtains Rhubarb Powder, by Rhubarb Powder and second
Alcohol 1:4 in mass ratio ~ 8 mixing, is subsequently placed in ultrasonic equipment and handles 20-30min, ultrasonic frequency 25-35KHz, function
Rate density is 0.4-0.5W/cm2；By after ultrasonication Rhubarb Powder and alcohol mixture be placed into refluxing extraction device,
Heating and refluxing extraction 2-4h；Extracting solution is filtered after the completion of extraction, the filtrate collected is rheum officinale ethanol extract；
The preparation of the lanatechead saussurea herb with flower ethyl alcohol soak includes: the second for being 55-65% with volume fraction by the lanatechead saussurea herb with flower after broken wall treatment
Alcohol 1:2-6 in mass ratio mixing, impregnates 3-5d, pours out to obtain the first leachate, then add the volume fraction of same quality again
For the ethyl alcohol of 8-12%, 2-4d is impregnated, pours out to obtain the second leachate；Receipts are filtered after merging the first leachate and the second leachate
Collect filtrate, obtains lanatechead saussurea herb with flower ethyl alcohol soak, it is spare；
The preparation of lanatechead saussurea herb with flower after the broken wall treatment includes: the lanatechead saussurea herb with flower particle that lanatechead saussurea herb with flower is broken into 10-12 mesh；By saussurea involucrata
Flower particle 2-3 freeze thawing treatment of progress is spare to get the lanatechead saussurea herb with flower after broken wall treatment；The freeze thawing treatment is by lanatechead saussurea herb with flower
Grain is placed in 2-3min in liquid nitrogen, then takes out 2-3min in the hot wind environment for be placed in 85-95 DEG C；
The preparation of the four tastes lanatechead saussurea herb with flower particle includes: root of kirilow rhodiola and fern fiber crops extracting solution, rheum officinale ethanol extract and lanatechead saussurea herb with flower second
The mixing of alcohol soak, then stores 24-30h under the conditions of -2-5 DEG C for mixed liquor；Then to mixed liquor 50-55 DEG C of condition into
Row vacuum concentration, obtaining relative density under the conditions of 30-40 DEG C is 1.20-1.25g/cm3Clear cream；It is added into the clear cream
Particle is made after mixing evenly in cane sugar powder；60-70 DEG C of heated-air drying is used, less than 8%, to be let cool to moisture content to room particle
Four taste lanatechead saussurea herb with flower grain products are obtained after temperature.
Preferred technical solution are as follows: the ethyl alcohol is the ethyl alcohol that volume fraction is 60-80%.
Preferred technical solution are as follows: the technological parameter of the Steam explosion treatment are as follows: ratio of water to material 1:5-6, dimension pressure time
120-180s, steam pressure 1.8-2.0Mpa.
Since above-mentioned technical proposal is used, the present invention has the advantage, that compared with prior art
Preparation method simple process of the invention, convenient for operation.
Specific embodiment
Embodiments of the present invention are illustrated by particular specific embodiment below, those skilled in the art can be by this implementation
Content disclosed by example is understood other advantages and efficacy of the present invention easily.
The purpose of term used herein, which is only that, illustrates particular embodiment, it is not intended to be limited to the present invention.It removes
Non- context is explicitly shown, otherwise singular " one " used herein, "one" also include plural form.
When illustrating preferred embodiment, it is potentially based on clear purpose and uses special term；However, this specification institute
Revealer is not intended to be limited in the selected special term；And it is to be understood that each particular element includes having
Identical function, all equivalence techniques for operating in a similar manner and reaching similar effects.
Embodiment one: four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof
Four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof, which is characterized in that include the following steps.
(1) raw material preparation
By mass, prepare the root of kirilow rhodiola of 20 parts by weight, the lanatechead saussurea herb with flower of 5 parts by weight, the rheum officinales of 5 parts by weight, 10 parts by weight
Fern fiber crops, 50 parts by weight cane sugar powder.
The root of kirilow rhodiola, lanatechead saussurea herb with flower, rheum officinale, fern fiber crops are dried product.
The cane sugar powder, fineness are 110 mesh.
(2) root of kirilow rhodiola, lanatechead saussurea herb with flower broken wall treatment
The root of kirilow rhodiola got ready is broken into the single-size of 11 mesh；Particle is subjected to 2 fast freeze-thaw broken wall treatments, i.e., by particle
It is placed in 2.5min in liquid nitrogen, takes out be placed in 2.5min in 90 DEG C of hot wind environment rapidly；Then it is first placed on liquid nitrogen and heat again
It is handled in wind environment, so circulation 2 times, obtains the root of kirilow rhodiola particle of broken wall treatment, it is spare.
Ibid, lanatechead saussurea herb with flower is handled using identical method, obtains the lanatechead saussurea herb with flower particle of broken wall treatment, it is spare.
(3) fern fiber crops pre-process
Fern fiber crops are placed in crushing plant, the single-size that fineness is 11 mesh is broken into；Then simultaneously using the separation of CCD color-selection apparatus
The relatively deep and shallower particle of color is collected respectively；The deeper particle of color is mainly the cortex of fern fiber crops, the shallower particle master of color
It to be the core material of fern fiber crops.
By the cortical granule of fern fiber crops, 90min is impregnated at a temperature of 17 DEG C using enough distilled water；By the cortex after immersion
Particle is placed in steam blasting equipment, and the parameter of time 150s, steam pressure 1.9MPa are pressed using ratio of water to material 1:6, dimension, into
Row Steam explosion treatment；Fern fiber crops cortical granule after obtaining steam blasting, it is spare.
(4) root of kirilow rhodiola, fern fiber crops extracting solution are prepared
By the root of kirilow rhodiola after broken wall treatment, the fern fiber crops cortical granule after steam blasting, fern fiber crops core material particles mix, then by material with
Distilled water 1:5 in mass ratio mixing, is placed into the thermal extraction device with steam condensate collection device, impregnates 5.5h；Then
It is heated to fluidized state and keeps, extract 5.5h.After the completion of extraction, extracting solution is passed through into 100 mesh net filtrations；Filtrate is collected,
Root of kirilow rhodiola, fern fiber crops extracting solution are obtained, it is spare.
(5) rheum officinale ethanol extract is prepared
The rheum officinale got ready is crushed to 50 mesh, obtains Rhubarb Powder.Rhubarb Powder and 70% ethyl alcohol of volume fraction 1:5 in mass ratio are mixed
It closes, is placed in ultrasonic equipment and handles 25min, ultrasonic frequency 30KHz, power density 0.5W/cm2；At ultrasonic wave
Rhubarb Powder, 70% alcohol mixture of volume fraction after reason are placed into refluxing extraction device, heating and refluxing extraction 3h；It has extracted
Extracting solution is passed through 100 mesh net filtrations by Cheng Hou；Filtrate is collected, rheum officinale ethanol extract is obtained, it is spare.
(6) lanatechead saussurea herb with flower ethyl alcohol soak is prepared
It by the lanatechead saussurea herb with flower after broken wall treatment, is mixed with 60% ethyl alcohol of volume fraction 1:3 in mass ratio, impregnates 3d, immersion liquid is poured out；
And then, then 10% ethyl alcohol of volume fraction of same quality is added, impregnates 2d, immersion liquid is poured out；Merge immersion liquid twice, by 100
Mesh net filtration；Filtrate is collected, lanatechead saussurea herb with flower ethyl alcohol soak is obtained, it is spare.The additive amount and volume point of 10% ethyl alcohol of volume fraction
The additive amount of several 60% ethyl alcohol is equal
(7) four taste lanatechead saussurea herb with flower particles are prepared
By root of kirilow rhodiola, fern fiber crops extracting solution, rheum officinale ethanol extract, the mixing of lanatechead saussurea herb with flower ethyl alcohol soak, 0 DEG C of stored refrigerated 28h；It will
Mixed liquor is concentrated in vacuo to 52 DEG C, and relative density is 1.22 under the conditions of 35 DEG C, obtains clear cream；The sugarcane got ready is added into clear cream
Icing Sugar is crushed to uniform particle after mixing evenly；65 DEG C of heated-air dryings are used for 7%, to let cool to moisture content particle
To room temperature to get to four taste lanatechead saussurea herb with flower grain products.
Four taste lanatechead saussurea herb with flower particles are formed with root of kirilow rhodiola, lanatechead saussurea herb with flower, rheum officinale, potentilla anserina extract compatibility, are had promoting blood circulation Wen Jing, are changed
Turbid grease removal and other effects can be used for treating hyperlipidemia caused by phlegm-turbidity and blood stasis hinders, and has and improve the shortness of breath uncomfortable in chest occurred by anoxic, tired
The illnesss such as powerless, while can be used for treating habitual constipation.
Embodiment two: four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof
A kind of four taste lanatechead saussurea herb with flower particles, composition of raw materials includes the raw material of following parts by weight: the root of kirilow rhodiola of 18 parts by weight, 4 parts by weight
Lanatechead saussurea herb with flower, the rheum officinales of 4 parts by weight, the fern fiber crops of 8 parts by weight, 45 parts by weight cane sugar powder.
Preferred embodiment are as follows: the root of kirilow rhodiola, lanatechead saussurea herb with flower, rheum officinale, fern fiber crops are dried product.
Preferred embodiment are as follows: its fineness of the cane sugar powder is 100 mesh.
Preparation method includes the preparation of root of kirilow rhodiola and fern fiber crops extracting solution, the preparation of rheum officinale ethanol extract, lanatechead saussurea herb with flower ethyl alcohol
The preparation of soak and the preparation of four taste lanatechead saussurea herb with flower particles:
The preparation of the root of kirilow rhodiola and fern fiber crops extracting solution includes: by the root of kirilow rhodiola after broken wall treatment, the fern after Steam explosion treatment
Numb cortical granule, fern fiber crops core material particles are mixed to get mixed material, then mixed material is mixed with water 1:4 in mass ratio, impregnate
5h is then placed into the thermal extraction device with steam condensate collection device, and 5h is extracted in boiling, to extracting solution after the completion of extraction
It is filtered；Collecting obtained filtrate is root of kirilow rhodiola and fern fiber crops extracting solution, spare；
The preparation method of root of kirilow rhodiola after the broken wall treatment: root of kirilow rhodiola is broken into the root of kirilow rhodiola particle of 10 mesh；By root of kirilow rhodiola
Particle 2 freeze thawing treatments of progress are spare to get the root of kirilow rhodiola after broken wall treatment；The freeze thawing treatment is to set root of kirilow rhodiola particle
The 2min in liquid nitrogen then takes out 2min in the hot wind environment for be placed in 85 DEG C；
The preparation of fern fiber crops cortical granule after the Steam explosion treatment includes: that fern fiber crops are broken into the fern fiber crops that fineness is 10 mesh
Grain；Then fern fiber crops particle is separated, obtains fern fiber crops cortical granule and fern hemp core layer particle；Then fern fiber crops cortical granule is used
5 DEG C of water impregnates 60min, and then the fern fiber crops cortical granule after immersion is placed in steam blasting equipment and is carried out at steam blasting
Reason；Fern fiber crops cortical granule after obtaining Steam explosion treatment, it is spare；
The preparation of the rheum officinale ethanol extract includes: that rheum officinale is crushed to 40 mesh, obtains Rhubarb Powder, Rhubarb Powder and ethyl alcohol are pressed
Mass ratio 1:4 mixing, is subsequently placed in ultrasonic equipment and handles 20min, ultrasonic frequency 25KHz, power density 0.4W/
cm2；By after ultrasonication Rhubarb Powder and alcohol mixture be placed into refluxing extraction device, heating and refluxing extraction 2h；It mentions
Extracting solution is filtered after the completion of taking, the filtrate collected is rheum officinale ethanol extract；
The preparation of the lanatechead saussurea herb with flower ethyl alcohol soak includes: the ethyl alcohol for being 55% with volume fraction by the lanatechead saussurea herb with flower after broken wall treatment
The mixing of 1:2 in mass ratio, impregnates 3d, pours out to obtain the first leachate, and the volume fraction for then adding same quality again is 8%
Ethyl alcohol impregnates 2d, pours out to obtain the second leachate；Filtrate is collected by filtration after merging the first leachate and the second leachate, obtains
Lanatechead saussurea herb with flower ethyl alcohol soak, it is spare；
The preparation of lanatechead saussurea herb with flower after the broken wall treatment includes: the lanatechead saussurea herb with flower particle that lanatechead saussurea herb with flower is broken into 10 mesh；By lanatechead saussurea herb with flower
Particle 2 freeze thawing treatments of progress are spare to get the lanatechead saussurea herb with flower after broken wall treatment；The freeze thawing treatment is to set lanatechead saussurea herb with flower particle
The 2min in liquid nitrogen then takes out 2min in the hot wind environment for be placed in 85 DEG C；
The preparation of the four tastes lanatechead saussurea herb with flower particle includes: root of kirilow rhodiola and fern fiber crops extracting solution, rheum officinale ethanol extract and lanatechead saussurea herb with flower second
The mixing of alcohol soak, then stores mixed liquor for 24 hours under the conditions of -2 DEG C；Then it is dense vacuum to be carried out in 50 DEG C of conditions to mixed liquor
Contracting, obtaining relative density under the conditions of 30 DEG C is 1.20g/cm3Clear cream；Cane sugar powder is added into the clear cream, is stirred evenly
Afterwards, particle is made；Use 60 DEG C of heated-air dryings that for 7.5%, four taste saussurea involucrata are obtained after letting cool to room temperature to moisture content particle
Flower grain products.
Preferred embodiment: the ethyl alcohol is the ethyl alcohol that volume fraction is 60%.
Preferred embodiment: the technological parameter of the Steam explosion treatment are as follows: ratio of water to material 1:5, dimension pressure time 120s, steam
Vapor pressure 1.8Mpa.
Embodiment three: four taste lanatechead saussurea herb with flower particles of one kind and preparation method thereof
A kind of four taste lanatechead saussurea herb with flower particles, composition of raw materials includes the raw material of following parts by weight: the root of kirilow rhodiola of 22 parts by weight, 6 parts by weight
Lanatechead saussurea herb with flower, the rheum officinales of 6 parts by weight, the fern fiber crops of 12 parts by weight, 55 parts by weight cane sugar powder.
Preferred embodiment: the root of kirilow rhodiola, lanatechead saussurea herb with flower, rheum officinale, fern fiber crops are dried product.
Preferred embodiment: its fineness of the cane sugar powder is 120 mesh.
Preparation method includes the preparation of root of kirilow rhodiola and fern fiber crops extracting solution, the preparation of rheum officinale ethanol extract, lanatechead saussurea herb with flower ethyl alcohol
The preparation of soak and the preparation of four taste lanatechead saussurea herb with flower particles:
The preparation of the root of kirilow rhodiola and fern fiber crops extracting solution includes: by the root of kirilow rhodiola after broken wall treatment, the fern after Steam explosion treatment
Numb cortical granule, fern fiber crops core material particles are mixed to get mixed material, then mixed material is mixed with water 1:7 in mass ratio, impregnate
6h is then placed into the thermal extraction device with steam condensate collection device, and 6h is extracted in boiling, to extracting solution after the completion of extraction
It is filtered；Collecting obtained filtrate is root of kirilow rhodiola and fern fiber crops extracting solution, spare；
The preparation method of root of kirilow rhodiola after the broken wall treatment: root of kirilow rhodiola is broken into the root of kirilow rhodiola particle of 12 mesh；By root of kirilow rhodiola
Particle 3 freeze thawing treatments of progress are spare to get the root of kirilow rhodiola after broken wall treatment；The freeze thawing treatment is to set root of kirilow rhodiola particle
The 3min in liquid nitrogen then takes out 3min in the hot wind environment for be placed in 95 DEG C；
The preparation of fern fiber crops cortical granule after the Steam explosion treatment includes: that fern fiber crops are broken into the fern fiber crops that fineness is 12 mesh
Grain；Then fern fiber crops particle is separated, obtains fern fiber crops cortical granule and fern hemp core layer particle；Then fern fiber crops cortical granule is used
30 DEG C of water impregnates 120min, and then the fern fiber crops cortical granule after immersion is placed in steam blasting equipment and carries out steam blasting
Processing；Fern fiber crops cortical granule after obtaining Steam explosion treatment, it is spare；
The preparation of the rheum officinale ethanol extract includes: that rheum officinale is crushed to 60 mesh, obtains Rhubarb Powder, Rhubarb Powder and ethyl alcohol are pressed
Mass ratio 1:8 mixing, is subsequently placed in ultrasonic equipment and handles 30min, ultrasonic frequency 35KHz, and power density is
0.5W/cm2；By after ultrasonication Rhubarb Powder and alcohol mixture be placed into refluxing extraction device, heating and refluxing extraction
4h；Extracting solution is filtered after the completion of extraction, the filtrate collected is rheum officinale ethanol extract；
The preparation of the lanatechead saussurea herb with flower ethyl alcohol soak includes: the ethyl alcohol for being 65% with volume fraction by the lanatechead saussurea herb with flower after broken wall treatment
The mixing of 1:6 in mass ratio, impregnates 5d, pours out to obtain the first leachate, and the volume fraction for then adding same quality again is 12%
Ethyl alcohol impregnates 4d, pours out to obtain the second leachate；Filtrate is collected by filtration after merging the first leachate and the second leachate, obtains
Lanatechead saussurea herb with flower ethyl alcohol soak, it is spare；
The preparation of lanatechead saussurea herb with flower after the broken wall treatment includes: the lanatechead saussurea herb with flower particle that lanatechead saussurea herb with flower is broken into 12 mesh；By lanatechead saussurea herb with flower
Particle 3 freeze thawing treatments of progress are spare to get the lanatechead saussurea herb with flower after broken wall treatment；The freeze thawing treatment is to set lanatechead saussurea herb with flower particle
The 3min in liquid nitrogen then takes out 3min in the hot wind environment for be placed in 95 DEG C；
The preparation of the four tastes lanatechead saussurea herb with flower particle includes: root of kirilow rhodiola and fern fiber crops extracting solution, rheum officinale ethanol extract and lanatechead saussurea herb with flower second
The mixing of alcohol soak, then stores 30h under the conditions of 5 DEG C for mixed liquor；Then it is dense vacuum to be carried out in 55 DEG C of conditions to mixed liquor
Contracting, obtaining relative density under the conditions of 40 DEG C is 1.25g/cm3Clear cream；Cane sugar powder is added into the clear cream, is stirred evenly
Afterwards, particle is made；Use 70 DEG C of heated-air dryings that for 6%, four taste lanatechead saussurea herb with flower are obtained after letting cool to room temperature to moisture content particle
Grain products.
Preferred embodiment: the ethyl alcohol is the ethyl alcohol that volume fraction is 80%.
Preferred embodiment: the technological parameter of the Steam explosion treatment are as follows: ratio of water to material 1:6, dimension pressure time 180s, steam
Vapor pressure 2.0Mpa.
As described above is only to be not intended to tool to explain the preferred embodiments of the invention to do any shape to the present invention
Limitation in formula should all wrap therefore all have any modification or change for making the related present invention under identical spirit
It includes in the scope that the invention is intended to protect.
Claims (6)
1. a kind of four taste lanatechead saussurea herb with flower particles, it is characterised in that: composition of raw materials includes the raw material of following parts by weight: 18-22 parts by weight
Root of kirilow rhodiola, the lanatechead saussurea herb with flower of 4-6 parts by weight, the rheum officinale of 4-6 parts by weight, 8-12 parts by weight fern fiber crops, 45-55 parts by weight sucrose
Powder.
2. four tastes lanatechead saussurea herb with flower particle according to claim 1, it is characterised in that: the root of kirilow rhodiola, lanatechead saussurea herb with flower, rheum officinale, fern
Fiber crops are dried product.
3. four tastes lanatechead saussurea herb with flower particle according to claim 1, it is characterised in that: its fineness of the cane sugar powder is 100-
120 mesh.
4. a kind of preparation method of four taste lanatechead saussurea herb with flower particles, it is characterised in that: composition of raw materials is any described using claim 1-3
Composition of raw materials, preparation method includes the preparation of root of kirilow rhodiola and fern fiber crops extracting solution, the preparation of rheum officinale ethanol extract, lanatechead saussurea herb with flower second
The preparation of alcohol soak and the preparation of four taste lanatechead saussurea herb with flower particles:
The preparation of the root of kirilow rhodiola and fern fiber crops extracting solution includes: by the root of kirilow rhodiola after broken wall treatment, the fern after Steam explosion treatment
Numb cortical granule, fern fiber crops core material particles are mixed to get mixed material, then mixed material is mixed with water 1:4-7 in mass ratio, leaching
5-6h is steeped, is then placed into the thermal extraction device with steam condensate collection device, 5-6h is extracted in boiling, right after the completion of extraction
Extracting solution is filtered；Collecting obtained filtrate is root of kirilow rhodiola and fern fiber crops extracting solution, spare；
The preparation method of root of kirilow rhodiola after the broken wall treatment: root of kirilow rhodiola is broken into the root of kirilow rhodiola particle of 10-12 mesh；By red scape
Its particle 2-3 freeze thawing treatment of progress is spare to get the root of kirilow rhodiola after broken wall treatment；The freeze thawing treatment is by root of kirilow rhodiola
Grain is placed in 2-3min in liquid nitrogen, then takes out 2-3min in the hot wind environment for be placed in 85-95 DEG C；
The preparation of fern fiber crops cortical granule after the Steam explosion treatment includes: that fern fiber crops are broken into the fern that fineness is 10-12 mesh
Numb particle；Then fern fiber crops particle is separated, obtains fern fiber crops cortical granule and fern hemp core layer particle；Then by fern hemp skin layer
Grain impregnates 60-120min with 5-30 DEG C of water, then by the fern fiber crops cortical granule after immersion be placed in steam blasting equipment into
Row Steam explosion treatment；Fern fiber crops cortical granule after obtaining Steam explosion treatment, it is spare；
The preparation of the rheum officinale ethanol extract includes: that rheum officinale is crushed to 40-60 mesh, obtains Rhubarb Powder, by Rhubarb Powder and second
Alcohol 1:4 in mass ratio ~ 8 mixing, is subsequently placed in ultrasonic equipment and handles 20-30min, ultrasonic frequency 25-35KHz, function
Rate density is 0.4-0.5W/cm2；By after ultrasonication Rhubarb Powder and alcohol mixture be placed into refluxing extraction device,
Heating and refluxing extraction 2-4h；Extracting solution is filtered after the completion of extraction, the filtrate collected is rheum officinale ethanol extract；
The preparation of the lanatechead saussurea herb with flower ethyl alcohol soak includes: the second for being 55-65% with volume fraction by the lanatechead saussurea herb with flower after broken wall treatment
Alcohol 1:2-6 in mass ratio mixing, impregnates 3-5d, pours out to obtain the first leachate, then add the volume fraction of same quality again
For the ethyl alcohol of 8-12%, 2-4d is impregnated, pours out to obtain the second leachate；Receipts are filtered after merging the first leachate and the second leachate
Collect filtrate, obtains lanatechead saussurea herb with flower ethyl alcohol soak, it is spare；
The preparation of lanatechead saussurea herb with flower after the broken wall treatment includes: the lanatechead saussurea herb with flower particle that lanatechead saussurea herb with flower is broken into 10-12 mesh；By saussurea involucrata
Flower particle 2-3 freeze thawing treatment of progress is spare to get the lanatechead saussurea herb with flower after broken wall treatment；The freeze thawing treatment is by lanatechead saussurea herb with flower
Grain is placed in 2-3min in liquid nitrogen, then takes out 2-3min in the hot wind environment for be placed in 85-95 DEG C；
The preparation of the four tastes lanatechead saussurea herb with flower particle includes: root of kirilow rhodiola and fern fiber crops extracting solution, rheum officinale ethanol extract and lanatechead saussurea herb with flower second
The mixing of alcohol soak, then stores 24-30h under the conditions of -2-5 DEG C for mixed liquor；Then to mixed liquor 50-55 DEG C of condition into
Row vacuum concentration, obtaining relative density under the conditions of 30-40 DEG C is 1.20-1.25g/cm3Clear cream；It is added into the clear cream
Particle is made after mixing evenly in cane sugar powder；60-70 DEG C of heated-air drying is used, less than 8%, to be let cool to moisture content to room particle
Four taste lanatechead saussurea herb with flower grain products are obtained after temperature.
5. the preparation method of four tastes lanatechead saussurea herb with flower particle according to claim 4, it is characterised in that: the ethyl alcohol is volume point
Number is the ethyl alcohol of 60-80%.
6. the preparation method of four tastes lanatechead saussurea herb with flower particle according to claim 4, it is characterised in that: the Steam explosion treatment
Technological parameter are as follows: ratio of water to material 1:5-6, dimension pressure time 120-180s, steam pressure 1.8-2.0Mpa.
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796609A (en) * | 2016-03-09 | 2016-07-27 | 孙继勇 | Quenching treatment based ganoderma spore powder wall breaking method |
-
2018
- 2018-10-26 CN CN201811256885.6A patent/CN108992508A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105796609A (en) * | 2016-03-09 | 2016-07-27 | 孙继勇 | Quenching treatment based ganoderma spore powder wall breaking method |
Non-Patent Citations (2)
| Title |
|---|
| 国家药品监督管理局: "《国家中成药标准汇编.中成药地方标准上升国家标准部分.内科.心系分册》", 31 December 2002 * |
| 易军鹏；等: "蒸汽爆破提取牛膝多糖工艺优化及抗氧化性研究", 《食品与机械》 * |
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Application publication date: 20181214 |