CN105754768A - Natural camellia saponin-containing baby care handmade soap and preparation method thereof - Google Patents
Natural camellia saponin-containing baby care handmade soap and preparation method thereof Download PDFInfo
- Publication number
- CN105754768A CN105754768A CN201610100337.9A CN201610100337A CN105754768A CN 105754768 A CN105754768 A CN 105754768A CN 201610100337 A CN201610100337 A CN 201610100337A CN 105754768 A CN105754768 A CN 105754768A
- Authority
- CN
- China
- Prior art keywords
- parts
- extract
- preparation
- filter
- feed liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a natural camellia saponin-containing baby care handmade soap and a preparation method thereof; the natural camellia saponin-containing baby care handmade soap is prepared from the following raw materials in parts by weight: 10-30 parts of wild camellia oil, 10-20 parts of oil-tea camellia cakes, 5-10 parts of Chinese honeylocust fruit, 5-15 parts of porcine pancreas, 5-10 parts of fir wood ash, 5-10 parts of hibiscus syriacus, 1-5 parts of aloe, 3-5 parts of cortex mori, 5-10 parts of radix lithospermi, 2-5 parts of fructus lycii, 1-3 parts of bombyx batryticatus, 3-5 parts of peach flowers, 3-5 parts of orchid, 3-8 parts of KOH and 1 part of rock candies. The natural camellia saponin-containing baby care handmade soap is a natural handmade soap developed by taking multiple animal and plant degreasing components as main components and compounding natural plant components with functions of protection skin and beautifying; the baby care handmade soap has multiple functions of washing hair, cleansing face, washing body, cleaning and the like, and has higher cleaning ability and good safety, thus being suitable for babies.
Description
Technical field
The invention belongs to cosmetics of everyday use technical field, be specifically related to a kind of Baby Care handmade soap containing natural oil theasaponin and preparation method thereof.
Background technology
Fancy soap is the daily articles for washing for deterging skin; along with the quick more new development of scientific level and improving constantly of people's living standard; people are no longer only limitted to most basic washing cleaning action for the requirement of fancy soap effect; and start to repel the fancy soap prepared by chemical composition; simultaneously as fancy soap neutral and alkali is crossed can wash away by force a large amount of sebum of skin surface, make that skin is excessively dry, allergy is even red and swollen; the protective effect making skin declines, and is susceptible to suffer from dermatosis.Therefore, by natural animal-plant be development of raw materials not only have very strong cleaning function and there is better skin care effect, Manual perfumed soap safe to use becomes the new pursuit of people, and its degradability is better than synthetic detergent, more becomes soap and make the research and development focus in field.
Summary of the invention
It is an object of the invention to provide a kind of Baby Care handmade soap containing natural oil theasaponin and preparation method thereof, it is mixed with oils and fats by organic base, inorganic base and prepares soap base, composite with vegetalitas soil release component such as Sasanguasaponin, Fructus Gleditsia, Hibiscus syriacus L., the shortcoming overcoming the hard water resistance difference of soap base greatly, attach natural plant component again well to reach skin protection water retention, gained Manual perfumed soap has hair washing, has a bath, washs the multiple functions such as medicated clothing, has the multiple prominent effects such as beauty treatment, health care, sterilization, sterilization concurrently.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of Baby Care handmade soap containing natural oil theasaponin, it is raw materials used includes by weight: wild Oleum Camelliae 10 ~ 30 parts, Oil-tea-cake 10 ~ 20 parts, 5 ~ 10 parts of Fructus Gleditsia, Pancreas Sus domestica 5 ~ 15 parts, Lignum seu Ramulus Cunninghamiae Lanceolatae ash 5 ~ 10 parts, Flos Hibisci and 5 ~ 10 parts of leaf, Aloe 1 ~ 5 part, Cortex Mori 3 ~ 5 parts, Radix Arnebiae (Radix Lithospermi) 5 ~ 10 parts, Fructus Lycii 2 ~ 5 parts, Bombyx Batryticatus 1 ~ 3 part, 3 ~ 5 parts of Flos persicae, 3 ~ 5 parts of Cymbidium ensifolium (L.) Sw., KOH3 ~ 8 part, 1 part of crystal sugar.
Described Lignum seu Ramulus Cunninghamiae Lanceolatae ash is to pulverize after fully being burnt by dry Folium Cunninghamiae lanceolatae to prepare.
The preparation method of the described Baby Care handmade soap containing natural oil theasaponin comprises the following steps:
1) preparation of Bombyx Batryticatus powder: roast the wheat bran of Bombyx Batryticatus weight 0.5-1 times to 50% carbonization in pot, be subsequently adding Bombyx Batryticatus, roasts to Bombyx Batryticatus flavescence brown, screens out wheat bran after cooling, by abundant for Bombyx Batryticatus crushed after being dried to 300 ~ 400 orders, obtains Bombyx Batryticatus powder；
2) preparation of Sasanguasaponin: be divided into two parts after complete for Oil-tea-cake defat, pulverizing, by the hot water adding 95 ~ 100 DEG C in feed liquid weight ratio 1:15 wherein a Oil-tea-cake ground product, lixiviate 38min, filters residue；Gained filtrate adds another part of Oil-tea-cake ground product, adds the hot water of ground product weight 3 times, continue lixiviate 38min, filter；Filtrate to paste, obtains Sasanguasaponin through disk centrifugal, ultrafiltration, rotary evaporation；
3) preparation of Fructus Gleditsia extract: Fructus Gleditsia is dried, pulverize after be divided into two parts, by a copy of it Fructus Gleditsia ground product in Ultrasound Instrument with 85 ~ 95 DEG C, feed liquid weight ratio 1:12 when hot water extraction 25min, filter, remove residue；Gained filtrate adds another part of Fructus Gleditsia ground product, 85 ~ 95 DEG C, feed liquid weight ratio 1:6 when hot water extraction 15min, filter；Filtrate to paste, obtains Fructus Gleditsia extract through disk centrifugal, ultrafiltration, rotary evaporation；
4) preparation of Pancreas Sus domestica stamping: fresh pig pancreas is washed away blood and slime, is cut into small pieces, adds finely ground crystal sugar, adds the purified water mixing weighed with crystal sugar etc., obtain Pancreas Sus domestica stamping after fully smashing to pieces；
5) preparation of Aloe extract: take fresh Aloe, washes away surface dirt impurity, adds water by feed liquid weight ratio 1:1, fully smashs to pieces in juice extractor, and drop goes out fresh juice；It is the alcoholic solution of 45% that filtering residue adds mass concentration by feed liquid weight ratio 1:6, in 75 ~ 80 DEG C of lixiviate 35min, filters, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 25 ~ 30Brix after, mix with the fresh juice of first time gained, obtain Aloe extract；
6) preparation of Hibiscus syriacus L. extract: Flos Hibisci and leaf are washed away surface dirt impurity respectively, adds water by feed liquid weight ratio 1:1, fully smashs to pieces, gone out by juice drop in juice extractor；After filtering residue adds water by feed liquid weight ratio 1:8, in 65 ~ 70 DEG C of lixiviate 24h, filter；Filtrate mixes with first time gained juice to paste through disk centrifugal, rotary evaporation, obtains Hibiscus syriacus L. extract；
7) preparation of Flos persicae extract or Cymbidium ensifolium (L.) Sw. extract: add water in Flos persicae or Cymbidium ensifolium (L.) Sw., juice extractor is squeezed the juice, then add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 65 ~ 70 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 25 ~ 30Brix, obtain Flos persicae extract or Cymbidium ensifolium (L.) Sw. extract；
8) preparation of Cortex Mori-wolfberry fruit extract: Cortex Mori is dried, is crushed to after 10 ~ 20 orders and adds Fructus Lycii, 95 ~ 100 DEG C, feed liquid weight ratio be 1:25 when hot water extraction 75min, filter；Filtering residue 95 ~ 100 DEG C, feed liquid weight ratio 1:10 when reheating flooding 15min, filter；Merge twice filter liquor, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain Cortex Mori-wolfberry fruit extract；
9) preparation of Oleum Radix Arnebiae (Oleum Radix Lithospermi): be immersed in by Radix Arnebiae (Radix Lithospermi) in the wild Oleum Camelliae of its 1-2 times of weight, soaks 21d in room temperature darkness when, filters；The filtering residue wild Oleum Camelliae of residue soaks 1.5h, then heating extraction 25min, stands percolation 12h and makes it fully filter, merge twice filtrate, obtain Oleum Radix Arnebiae (Oleum Radix Lithospermi) after cooling；
10) preparation of Manual perfumed soap: KOH is configured to the KOH solution that mass concentration is 30%, is then added into heating to the mixture of the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 60 DEG C and Sasanguasaponin, is stirred continuously to paste as A phase using 500r/min；It is slowly added in Pancreas Sus domestica stamping using Lignum seu Ramulus Cunninghamiae Lanceolatae ash constantly to stir evenly as B phase；Fructus Gleditsia extract and Hibiscus syriacus L. extract are mixed and mixes thoroughly as C phase；Cortex Mori-wolfberry fruit extract, Bombyx Batryticatus powder, Aloe extract are mixed and mix thoroughly as D phase；Flos persicae extract and Cymbidium ensifolium (L.) Sw. extract are mixed and mixes thoroughly as E phase；By A heat phase to 60 DEG C, add B phase, C phase and constantly stir evenly, treating that temperature is reduced to 55 DEG C of addition D phases and stirs evenly, be finally cooled to 50 DEG C of addition E phases and mix thoroughly and casting, deposit after 28 ~ 31d and get final product.
Sasanguasaponin is pentacyclic triterpene saponins, and HLB value is 16, has good emulsifying, dispersion and foamability, has good bactericidal properties simultaneously, so there being very strong degreasing bactericidal action, and skin is not had zest；Flos persicae contains the main components such as kaempferol, Trifolin, naringenin, vitamin, blood capillary can be expanded, improve blood circulation, thus promoting skin-nourishing and the supply of oxygen, skin care, preventing melanic deposition in skin, it is with the composite effect with emotion of refreshing oneself, regulate of Cymbidium ensifolium (L.) Sw.；Fructus Lycii contains the compositions such as glycine betaine, multivitamin (VB1, VB2 etc.), nicotinic acid, has the effects such as good defying age, skin nutrition, preventing and treating alopecia and white hair；Radix Arnebiae (Radix Lithospermi) is mainly composed of shikonin, has antipruritic, antipyretic, antiinflammatory, convergence, antibacterial function, can conditioning skin and hair, the dermatosis such as pachylosis, cicatrix is had good curative effect；Aloe contains the compositions such as aloin, Aloe polysaccharide, aminoacid, organic acid, enzyme, the effects such as skin is nutritious, moist moisturizing, speckle dispelling, crease-resistant, antibacterial (being mainly fungus), anti-ultraviolet, promotion Growth of Cells, being conducive to tissue repair and wound healing, it has good hair growth promoting, black hair effect simultaneously；The similar fat of Pancreas Sus domestica, possibly together with compositions such as pancreas fat digestive enzyme, elastoser, polypeptide, Lignum seu Ramulus Cunninghamiae Lanceolatae ash mainly contains potassium carbonate composition, Pancreas Sus domestica and Lignum seu Ramulus Cunninghamiae Lanceolatae ash are constituted the main component of fancy soap, can form exquisite quality, gentle to skin, ability of cleaning greasy dirt strong, and can prevent xerosis cutis, chap, and has and moistens the Natural toilet soap supporting the effects such as skin, if also have the effect of removing scurf and relieving itching for hair, and Lignum seu Ramulus Cunninghamiae Lanceolatae ash also has the effect of good soil pick-up decontamination；Cortex Mori contains the compositions such as abundant flavonoid, Mulberrofuran, polysaccharide, and skin has the effect of very strong antiinflammatory, antibacterial, repair tissue cell, desalination cicatrix etc., and its fancy soap made has effect anti-dandruff, Anti-hair loss, hair color when hair washing；Bombyx Batryticatus contains the compositions such as rich in protein, esterase, protease, hydrolytic enzyme, ammonium oxalate, use in fancy soap have good nutrition skin to send out, antiinflammatory, antibacterial (especially for pathomycete), whitening, the effect such as speckle dispelling；The effects such as Flos Hibisci and Folium Hibisci contain the important component such as protein, reducing sugar, saponarin, inositol, phlegmatic temperament, its antibacterial, clearing away heat and cooling blood, removing toxic substances and promoting subsidence of swelling of having can make fancy soap have the effect washing decontamination, skin care, anti-dandruff, soft of hair color and treatment dermatosis (tinea, scald) etc. preferably；Fructus Gleditsia, containing compositions such as triterpene saponin, tannin, ceryl alcohols, has stronger washing ability of cleaning greasy dirt, and its antibacterial action is possible to prevent the generation of scurf, has the effect of Anti-hair loss and black hair simultaneously.
The present invention has the great advantage that gained Baby Care handmade soap of the present invention has the effect of skin protection, nourishes rough skin, skin ulcer antipruritic, freeze proof, fatigue taking away of refreshing oneself, adjustment emotion, anti-drying desquamation, preventing and treating alopecia, hair color, anti-harm ray etc..Its component is both from the extract of natural animal-plant, without any hormone, have no side effect, there is higher safety in utilization, do not only have stronger cleaning function, also have skin care effect, even can treat part dermatosis, and its alkalescence is little, the natural fragrance of a flower of its delicate fragrance can refresh oneself after allowing people use, regulate emotion.
Detailed description of the invention
In order to make content of the present invention easily facilitate understanding, below in conjunction with detailed description of the invention, technical solutions according to the invention are described further, but the present invention is not limited only to this.
Pulverize after dry Folium Cunninghamiae lanceolatae is fully burnt and prepare required Lignum seu Ramulus Cunninghamiae Lanceolatae ash.
Embodiment 1
The preparation method of the Baby Care handmade soap containing natural oil theasaponin, comprises the following steps:
1) preparation of Bombyx Batryticatus powder: roast 1 weight portion wheat bran to 50% carbonization in pot, is subsequently adding 1 weight portion Bombyx Batryticatus, roasts to Bombyx Batryticatus flavescence brown, screens out wheat bran after cooling, by abundant for Bombyx Batryticatus crushed after being dried to 400 orders, obtains Bombyx Batryticatus powder；
2) preparation of Sasanguasaponin: be divided into two parts after the 20 complete defats of weight portion Oil-tea-cake, pulverizing, by the hot water adding 95 DEG C in feed liquid weight ratio 1:15 wherein a Oil-tea-cake ground product, lixiviate 38min, filters residue；Gained filtrate adds another part of Oil-tea-cake ground product, adds the hot water of ground product weight 3 times, continue lixiviate 38min, filter；Filtrate to paste, obtains Sasanguasaponin through disk centrifugal, ultrafiltration, rotary evaporation；
3) preparation of Fructus Gleditsia extract: be divided into two parts after 10 weight portion Fructus Gleditsias are dried, pulverized, by a copy of it Fructus Gleditsia ground product in Ultrasound Instrument with 95 DEG C, feed liquid weight ratio 1:12 when hot water extraction 25min, filter, remove residue；Gained filtrate adds another part of Fructus Gleditsia ground product, 85 DEG C, feed liquid weight ratio 1:6 when hot water extraction 15min, filter；Filtrate to paste, obtains Fructus Gleditsia extract through disk centrifugal, ultrafiltration, rotary evaporation；
4) preparation of Pancreas Sus domestica stamping: 10 weight portion fresh pig pancreases are washed away blood and slime, is cut into small pieces, adds the crystal sugar that 1 weight portion is finely ground, adds 1 weight portion purified water mixing, obtains Pancreas Sus domestica stamping after fully smashing to pieces；
5) preparation of Aloe extract: take fresh Aloe 2 weight portion, wash away surface dirt impurity, adds water by feed liquid weight ratio 1:1, fully smashs to pieces in juice extractor, and drop goes out fresh juice；It is the alcoholic solution of 45% that filtering residue adds mass concentration by feed liquid weight ratio 1:6, in 78 DEG C of lixiviate 35min, filters, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 26Brix after, mix with the fresh juice of first time gained, obtain Aloe extract；
6) preparation of Hibiscus syriacus L. extract: 5 weight portion Flos Hibisci and leaf are washed away surface dirt impurity respectively, adds water by feed liquid weight ratio 1:1, fully smashs to pieces, gone out by juice drop in juice extractor；After filtering residue adds water by feed liquid weight ratio 1:8, in 70 DEG C of lixiviate 24h, filter；Filtrate mixes with first time gained juice to paste through disk centrifugal, rotary evaporation, obtains Hibiscus syriacus L. extract；
7) preparation of Flos persicae extract: add 1 weight parts water in 3 weight portion Flos persicaes, juice extractor is squeezed the juice, then add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 65 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 25Brix, obtain Flos persicae extract；
8) preparation of Cymbidium ensifolium (L.) Sw. extract: add 1 weight parts water in 5 weight portion Cymbidium ensifolium (L.) Sw.s, juice extractor is squeezed the juice, then add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 68 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 28Brix, obtain Cymbidium ensifolium (L.) Sw. extract；
9) preparation of Cortex Mori-wolfberry fruit extract: add 2 weight portion Fructus Lyciis after being dried, be crushed to 10 orders by 3 weight portion Cortex Mori, 95 DEG C, feed liquid weight ratio be 1:25 when hot water extraction 75min, filter；Filtering residue 95 DEG C, feed liquid weight ratio 1:10 when reheating flooding 15min, filter；Merge twice filter liquor, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain Cortex Mori-wolfberry fruit extract；
10) preparation of Oleum Radix Arnebiae (Oleum Radix Lithospermi): be immersed in by 5 weight portion Radix Arnebiae (Radix Lithospermi)s in 5 weight portion open country Oleum Camelliae, soaks 21d in room temperature darkness when, filters；Filtering residue soaks 1.5h, then heating extraction 25min with 5 weight portion open country Oleum Camelliae again, stands percolation 12h and makes it fully filter, merge twice filtrate, obtain Oleum Radix Arnebiae (Oleum Radix Lithospermi) after cooling；
11) preparation of Manual perfumed soap: 3 weight portion KOH are configured to the KOH solution that mass concentration is 30%, is then added into heating to the mixture of the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 60 DEG C and Sasanguasaponin, is stirred continuously to paste as A phase using 500r/min；10 weight portion Lignum seu Ramulus Cunninghamiae Lanceolatae ashes are slowly added in Pancreas Sus domestica stamping and constantly stir evenly as B phase；Fructus Gleditsia extract and Hibiscus syriacus L. extract are mixed and mixes thoroughly as C phase；Cortex Mori-wolfberry fruit extract, Bombyx Batryticatus powder, Aloe extract are mixed and mix thoroughly as D phase；Flos persicae extract and Cymbidium ensifolium (L.) Sw. extract are mixed and mixes thoroughly as E phase；By A heat phase to 60 DEG C, add B phase, C phase and constantly stir evenly, treating that temperature is reduced to 55 DEG C of addition D phases and stirs evenly, be finally cooled to 50 DEG C of addition E phases and mix thoroughly and casting, deposit after 28d and get final product.
Embodiment 2
The preparation method of the Baby Care handmade soap containing natural oil theasaponin, comprises the following steps:
1) preparation of Bombyx Batryticatus powder: roast 1 weight portion wheat bran to 50% carbonization in pot, is subsequently adding 2 weight portion Bombyx Batryticatus, roasts to Bombyx Batryticatus flavescence brown, screens out wheat bran after cooling, by abundant for Bombyx Batryticatus crushed after being dried to 300 orders, obtains Bombyx Batryticatus powder；
2) preparation of Sasanguasaponin: be divided into two parts after the 15 complete defats of weight portion Oil-tea-cake, pulverizing, by the hot water adding 98 DEG C in feed liquid weight ratio 1:15 wherein a Oil-tea-cake ground product, lixiviate 38min, filters residue；Gained filtrate adds another part of Oil-tea-cake ground product, adds the hot water of ground product weight 3 times, continue lixiviate 38min, filter；Filtrate to paste, obtains Sasanguasaponin through disk centrifugal, ultrafiltration, rotary evaporation；
3) preparation of Fructus Gleditsia extract: be divided into two parts after 8 weight portion Fructus Gleditsias are dried, pulverized, by a copy of it Fructus Gleditsia ground product in Ultrasound Instrument with 90 DEG C, feed liquid weight ratio 1:6 when hot water extraction 25min, filter, remove residue；Gained filtrate adds another part of Fructus Gleditsia ground product, 90 DEG C, feed liquid weight ratio 1:6 when hot water extraction 15min, filter；Filtrate to paste, obtains Fructus Gleditsia extract through disk centrifugal, ultrafiltration, rotary evaporation；
4) preparation of Pancreas Sus domestica stamping: 5 weight portion fresh pig pancreases are washed away blood and slime, is cut into small pieces, adds the crystal sugar that 1 weight portion is finely ground, adds 1 weight portion purified water mixing, obtains Pancreas Sus domestica stamping after fully smashing to pieces；
5) preparation of Aloe extract: take fresh Aloe 1 weight portion, wash away surface dirt impurity, adds water by feed liquid weight ratio 1:1, fully smashs to pieces in juice extractor, and drop goes out fresh juice；It is the alcoholic solution of 45% that filtering residue adds mass concentration by feed liquid weight ratio 1:6, in 75 DEG C of lixiviate 35min, filters, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 25Brix after, mix with the fresh juice of first time gained, obtain Aloe extract；
6) preparation of Hibiscus syriacus L. extract: 8 weight portion Flos Hibisci and leaf are washed away surface dirt impurity respectively, adds water by feed liquid weight ratio 1:1, fully smashs to pieces, gone out by juice drop in juice extractor；After filtering residue adds water by feed liquid weight ratio 1:8, in 68 DEG C of lixiviate 24h, filter；Filtrate mixes with first time gained juice to paste through disk centrifugal, rotary evaporation, obtains Hibiscus syriacus L. extract；
7) preparation of Flos persicae extract: add 1 weight parts water in 4 weight portion Flos persicaes, juice extractor is squeezed the juice, then add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 68 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 28Brix, obtain Flos persicae extract；
8) preparation of Cymbidium ensifolium (L.) Sw. extract: add 1 weight parts water in 3 weight portion Cymbidium ensifolium (L.) Sw.s, juice extractor is squeezed the juice, then add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 65 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 25Brix, obtain Cymbidium ensifolium (L.) Sw. extract；
9) preparation of Cortex Mori-wolfberry fruit extract: add 3 weight portion Fructus Lyciis after being dried, be crushed to 10 orders by 4 weight portion Cortex Mori, 98 DEG C, feed liquid weight ratio be 1:25 when hot water extraction 75min, filter；Filtering residue 98 DEG C, feed liquid weight ratio 1:10 when reheating flooding 15min, filter；Merge twice filter liquor, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain Cortex Mori-wolfberry fruit extract；
10) preparation of Oleum Radix Arnebiae (Oleum Radix Lithospermi): be immersed in the wild Oleum Camelliae of its 2 times of weight by 8 weight portion Radix Arnebiae (Radix Lithospermi)s, soaks 21d in room temperature darkness when, filters；Filtering residue soaks 1.5h, then heating extraction 25min with 6 weight portion open country Oleum Camelliae again, stands percolation 12h and makes it fully filter, merge twice filtrate, obtain Oleum Radix Arnebiae (Oleum Radix Lithospermi) after cooling；
11) preparation of Manual perfumed soap: 4 weight portion KOH are configured to the KOH solution that mass concentration is 30%, is then added into heating to the mixture of the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 60 DEG C and Sasanguasaponin, is stirred continuously to paste as A phase using 500r/min；8 weight portion Lignum seu Ramulus Cunninghamiae Lanceolatae ashes are slowly added in Pancreas Sus domestica stamping and constantly stir evenly as B phase；Fructus Gleditsia extract and Hibiscus syriacus L. extract are mixed and mixes thoroughly as C phase；Cortex Mori-wolfberry fruit extract, Bombyx Batryticatus powder, Aloe extract are mixed and mix thoroughly as D phase；Flos persicae extract and Cymbidium ensifolium (L.) Sw. extract are mixed and mixes thoroughly as E phase；By A heat phase to 60 DEG C, add B phase, C phase and constantly stir evenly, treating that temperature is reduced to 55 DEG C of addition D phases and stirs evenly, be finally cooled to 50 DEG C of addition E phases and mix thoroughly and casting, deposit after 30d and get final product.
Embodiment 3
The preparation method of the Baby Care handmade soap containing natural oil theasaponin, comprises the following steps:
1) preparation of Bombyx Batryticatus powder: roast 3 weight portion wheat brans to 50% carbonization in pot, is subsequently adding 3 weight portion Bombyx Batryticatus, roasts to Bombyx Batryticatus flavescence brown, screens out wheat bran after cooling, by abundant for Bombyx Batryticatus crushed after being dried to 300 orders, obtains Bombyx Batryticatus powder；
2) preparation of Sasanguasaponin: be divided into two parts after the 10 complete defats of weight portion Oil-tea-cake, pulverizing, by the hot water adding 95 DEG C in feed liquid weight ratio 1:15 wherein a Oil-tea-cake ground product, lixiviate 38min, filters residue；Gained filtrate adds another part of Oil-tea-cake ground product, adds the hot water of ground product weight 3 times, continue lixiviate 38min, filter；Filtrate to paste, obtains Sasanguasaponin through disk centrifugal, ultrafiltration, rotary evaporation；
3) preparation of Fructus Gleditsia extract: be divided into two parts after 5 weight portion Fructus Gleditsias are dried, pulverized, by a copy of it Fructus Gleditsia ground product in Ultrasound Instrument with 85 DEG C, feed liquid weight ratio 1:12 when hot water extraction 25min, filter, remove residue；Gained filtrate adds another part of Fructus Gleditsia ground product, 95 DEG C, feed liquid weight ratio 1:6 when hot water extraction 15min, filter；Filtrate to paste, obtains Fructus Gleditsia extract through disk centrifugal, ultrafiltration, rotary evaporation；
4) preparation of Pancreas Sus domestica stamping: 15 weight portion fresh pig pancreases are washed away blood and slime, is cut into small pieces, adds the crystal sugar that 1 weight portion is finely ground, adds 1 weight portion purified water mixing, obtains Pancreas Sus domestica stamping after fully smashing to pieces；
5) preparation of Aloe extract: take fresh Aloe 5 weight portion, wash away surface dirt impurity, adds water by feed liquid weight ratio 1:1, fully smashs to pieces in juice extractor, and drop goes out fresh juice；It is the alcoholic solution of 45% that filtering residue adds mass concentration by feed liquid weight ratio 1:6, in 80 DEG C of lixiviate 35min, filters, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 30Brix after, mix with the fresh juice of first time gained, obtain Aloe extract；
6) preparation of Hibiscus syriacus L. extract: 10 weight portion Flos Hibisci and leaf are washed away surface dirt impurity respectively, adds water by feed liquid weight ratio 1:1, fully smashs to pieces, gone out by juice drop in juice extractor；After filtering residue adds water by feed liquid weight ratio 1:8, in 65 DEG C of lixiviate 24h, filter；Filtrate mixes with first time gained juice to paste through disk centrifugal, rotary evaporation, obtains Hibiscus syriacus L. extract；
7) preparation of Flos persicae extract: add 1 weight parts water in 5 weight portion Flos persicaes, juice extractor is squeezed the juice, then add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 70 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 30Brix, obtain Flos persicae extract；
8) preparation of Cymbidium ensifolium (L.) Sw. extract: add 1 weight parts water in 4 weight portion Cymbidium ensifolium (L.) Sw.s, juice extractor is squeezed the juice, then add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 70 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 30Brix, obtain Cymbidium ensifolium (L.) Sw. extract；
9) preparation of Cortex Mori-wolfberry fruit extract: add 5 weight portion Fructus Lyciis after being dried, be crushed to 20 orders by 5 weight portion Cortex Mori, 100 DEG C, feed liquid weight ratio be 1:25 when hot water extraction 75min, filter；Filtering residue 100 DEG C, feed liquid weight ratio 1:10 when reheating flooding 15min, filter；Merge twice filter liquor, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain Cortex Mori-wolfberry fruit extract；
10) preparation of Oleum Radix Arnebiae (Oleum Radix Lithospermi): be immersed in the wild Oleum Camelliae of its 2 times of weight by 10 weight portion Radix Arnebiae (Radix Lithospermi)s, soaks 21d in room temperature darkness when, filters；Filtering residue soaks 1.5h, then heating extraction 25min with 10 weight portion open country Oleum Camelliae again, stands percolation 12h and makes it fully filter, merge twice filtrate, obtain Oleum Radix Arnebiae (Oleum Radix Lithospermi) after cooling；
11) preparation of Manual perfumed soap: 8 weight portion KOH are configured to the KOH solution that mass concentration is 30%, is then added into heating to the mixture of the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 60 DEG C and Sasanguasaponin, is stirred continuously to paste as A phase using 500r/min；5 weight portion Lignum seu Ramulus Cunninghamiae Lanceolatae ashes are slowly added in Pancreas Sus domestica stamping and constantly stir evenly as B phase；Fructus Gleditsia extract and Hibiscus syriacus L. extract are mixed and mixes thoroughly as C phase；Cortex Mori-wolfberry fruit extract, Bombyx Batryticatus powder, Aloe extract are mixed and mix thoroughly as D phase；Flos persicae extract and Cymbidium ensifolium (L.) Sw. extract are mixed and mixes thoroughly as E phase；By A heat phase to 60 DEG C, add B phase, C phase and constantly stir evenly, treating that temperature is reduced to 55 DEG C of addition D phases and stirs evenly, be finally cooled to 50 DEG C of addition E phases and mix thoroughly and casting, deposit after 31d and get final product.
One, Manual perfumed soap is of different nature measures according to QB/T2485-2008
1, physicochemical property: the natural Manual perfumed soap of the present invention belongs to compound fancy soap, total effective content and dry soap content are 75% ~ 85%(QB/T2487-2008), moisture and volatile matter are 5% ~ 25%(QB/T2623.4-2003), total free alkali is 0.2%(QB/T2623.2-2003), free caustic alkali is 0.05%(QB/T2623.1-2003), all meet the requirements of the standard.
2, soap body outward appearance: soap body is rectified, uniform color, do not seen cracking, smooth exquisiteness, it does not have macroscopic impurity and stain.
3, abnormal smells from the patient: have the Flos persicae fragrance that stable Cymbidium ensifolium (L.) Sw. is fragrant and indistinct, it does not have wild Oleum Camelliae becomes sour and other obvious abnormal flavour.
4, resistance to hard water: resistance to hard water respectively 4.1ml, 3.9ml, 4.0ml of 3 embodiment gained Manual perfumed soaps, illustrates stronger resistance to hard water (QB/T2487-2008).
5, dissolubility: the dissolubility respectively 0.8341mg/cm of 3 embodiment gained Manual perfumed soaps2、0.8581mg/cm2、0.8434mg/cm2, show that it is respectively provided with higher dissolubility, it is easy to use.
6, stability: fancy soap is respectively placed in 42 DEG C of 7d ,-4 DEG C of 7d, uses water logging 1d, result display fancy soap soap body is without substantially melting, ftracture, stick with paste the bad phenomenon that the conventional toilet soaps such as rotten under equal conditions easily occurs.
Two, result of use
3 embodiment gained Manual perfumed soaps are tried out, all display has the foam of certain richness, and wherein the foaming power of embodiment 1 is the strongest, and the people being suitable for liking foam many uses, there is extraordinary cleaning effect, and will not produce stimulate and tighten sense to skin after using.
Overall result of use compares with commercially available magic soap prevailing, and result is table 1 such as.
Table 1 evil spirit soap uses result with fancy soap of the present invention
Result shows, gained Manual perfumed soap of the present invention can compare favourably with evil spirit soap in part, even more than the effect of evil spirit soap, can bring to user and well wash with effect and enjoyment.Wherein, the Manual perfumed soap of embodiment 1 lays particular emphasis on moisturizing, moist effect, and embodiment 2,3 lays particular emphasis on sterilization, the effect such as antipruritic.
Three, bactericidal assay
nullThe present invention adopts Sasanguasaponin、Radix Arnebiae (Radix Lithospermi)、Aloe、Bombyx Batryticatus、Hibiscus syriacus L.、Manual perfumed soap prepared by the natural plant formulas such as Fructus Gleditsia has stronger sterilization (particularly skin pathomycete)、Antibacterial and skin care effect，With commercially available evil spirit soap for matched group，Manual perfumed soap prepared by embodiment 1-3 is test group，Adopt several child common skin pathomycete for test strain，Measure evil spirit soap with cup-plate method and skin is cured the disease the inactivation inhibition of fungus by Manual perfumed soap of the present invention，Its method particularly includes: is by peptone 5g、Extracted beef powder 3g、Agar 15g、Buffer 3g is diluted to 1L bacterium culture medium，Sterilizing，60 dish it are classified as when being cooled to 35 DEG C-45 DEG C，Every dish 20mL，It is separately added into the mixing of equivalent different strain，Every kind of strain repeats 3 dish，Every dish adds four Oxford cups，Separately take four kinds of each 1g of fancy soap，Fully dissolve with 100mL60 DEG C of warm water，200 μ L drawn by every kind of fancy soap，It is added drop-wise to respectively in four Oxford cups of every dish，Cultivate under 37 DEG C of conditions，Observe and measure the size of inhibition zone，Result is in Table 2.
Test result (unit: the cm of the different fancy soap bactericidal effect of table 22)
Being shown by table 2 result, Manual perfumed soap of the present invention skin is cured the disease fungus has stronger inhibitory action, it is possible to prevent the generation of some dermatosis, thus reaching better skin effect.
The foregoing is only presently preferred embodiments of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to the covering scope of the present invention.
Claims (3)
1. the Baby Care handmade soap containing natural oil theasaponin, it is characterised in that: it is raw materials used includes by weight: wild Oleum Camelliae 10 ~ 30 parts, Oil-tea-cake 10 ~ 20 parts, 5 ~ 10 parts of Fructus Gleditsia, Pancreas Sus domestica 5 ~ 15 parts, Lignum seu Ramulus Cunninghamiae Lanceolatae ash 5 ~ 10 parts, Flos Hibisci and 5 ~ 10 parts of leaf, Aloe 1 ~ 5 part, Cortex Mori 3 ~ 5 parts, Radix Arnebiae (Radix Lithospermi) 5 ~ 10 parts, Fructus Lycii 2 ~ 5 parts, Bombyx Batryticatus 1 ~ 3 part, 3 ~ 5 parts of Flos persicae, 3 ~ 5 parts of Cymbidium ensifolium (L.) Sw., KOH3 ~ 8 part, 1 part of crystal sugar.
2. Baby Care handmade soap containing natural oil theasaponin according to claim 1, it is characterised in that: described Lignum seu Ramulus Cunninghamiae Lanceolatae ash is to pulverize after fully being burnt by dry Folium Cunninghamiae lanceolatae to prepare.
3. the preparation method of the Baby Care handmade soap containing natural oil theasaponin as claimed in claim 1, it is characterised in that: comprise the following steps:
1) preparation of Bombyx Batryticatus powder: roast the wheat bran of Bombyx Batryticatus weight 0.5-1 times to 50% carbonization in pot, be subsequently adding Bombyx Batryticatus, roasts to Bombyx Batryticatus flavescence brown, screens out wheat bran after cooling, by abundant for Bombyx Batryticatus crushed after being dried to 300 ~ 400 orders, obtains Bombyx Batryticatus powder；
2) preparation of Sasanguasaponin: be divided into two parts after complete for Oil-tea-cake defat, pulverizing, by the hot water adding 95 ~ 100 DEG C in feed liquid weight ratio 1:15 wherein a Oil-tea-cake ground product, lixiviate 38min, filters residue；Gained filtrate adds another part of Oil-tea-cake ground product, adds the hot water of ground product weight 3 times, continue lixiviate 38min, filter；Filtrate to paste, obtains Sasanguasaponin through disk centrifugal, ultrafiltration, rotary evaporation；
3) preparation of Fructus Gleditsia extract: Fructus Gleditsia is dried, pulverize after be divided into two parts, by a copy of it Fructus Gleditsia ground product in Ultrasound Instrument with 85 ~ 95 DEG C, feed liquid weight ratio 1:12 when hot water extraction 25min, filter, remove residue；Gained filtrate adds another part of Fructus Gleditsia ground product, 85 ~ 95 DEG C, feed liquid weight ratio 1:6 when hot water extraction 15min, filter；Filtrate to paste, obtains Fructus Gleditsia extract through disk centrifugal, ultrafiltration, rotary evaporation；
4) preparation of Pancreas Sus domestica stamping: fresh pig pancreas is washed away blood and slime, is cut into small pieces, adds finely ground crystal sugar, adds the purified water mixing weighed with crystal sugar etc., obtain Pancreas Sus domestica stamping after fully smashing to pieces；
5) preparation of Aloe extract: take fresh Aloe, washes away surface dirt impurity, adds water by feed liquid weight ratio 1:1, fully smashs rear drop to pieces and go out fresh juice；It is the alcoholic solution of 45% that filtering residue adds mass concentration by feed liquid weight ratio 1:6, in 75 ~ 80 DEG C of lixiviate 35min, filters, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 25 ~ 30Brix after, mix with the fresh juice of first time gained, obtain Aloe extract；
6) preparation of Hibiscus syriacus L. extract: Flos Hibisci and leaf are washed away surface dirt impurity respectively, adds water by feed liquid weight ratio 1:1, is gone out by juice drop after fully smashing to pieces；After filtering residue adds water by feed liquid weight ratio 1:8, in 65 ~ 70 DEG C of lixiviate 24h, filter；Filtrate mixes with first time gained juice to paste through disk centrifugal, rotary evaporation, obtains Hibiscus syriacus L. extract；
7) preparation of Flos persicae extract or Cymbidium ensifolium (L.) Sw. extract: add water after squeezing the juice in Flos persicae or Cymbidium ensifolium (L.) Sw., add water weight 5 times used in juice, mass concentration is the alcoholic solution of 65%, lixiviate 25min under 65 ~ 70 DEG C of conditions, filter, filtrate through disk centrifugal, ultrafiltration, reverse osmosis concentrated be reduced to 25 ~ 30Brix, obtain Flos persicae extract or Cymbidium ensifolium (L.) Sw. extract；
8) preparation of Cortex Mori-wolfberry fruit extract: Cortex Mori is dried, is crushed to after 10 ~ 20 orders and adds Fructus Lycii, 95 ~ 100 DEG C, feed liquid weight ratio be 1:25 when hot water extraction 75min, filter；Filtering residue 95 ~ 100 DEG C, feed liquid weight ratio 1:10 when reheating flooding 15min, filter；Merge twice filter liquor, through disk centrifugal, ultrafiltration, rotary evaporation to paste, obtain Cortex Mori-wolfberry fruit extract；
9) preparation of Oleum Radix Arnebiae (Oleum Radix Lithospermi): be immersed in by Radix Arnebiae (Radix Lithospermi) in the wild Oleum Camelliae of its 1-2 times of weight, soaks 21d in room temperature darkness when, filters；The filtering residue wild Oleum Camelliae of residue soaks 1.5h, then heating extraction 25min, stands percolation 12h and makes it fully filter, merge twice filtrate, obtain Oleum Radix Arnebiae (Oleum Radix Lithospermi) after cooling；
10) preparation of Manual perfumed soap: KOH is configured to the KOH solution that mass concentration is 30%, is then added into heating to the mixture of the Oleum Radix Arnebiae (Oleum Radix Lithospermi) of 60 DEG C and Sasanguasaponin, is stirred continuously to paste as A phase using 500r/min；It is slowly added in Pancreas Sus domestica stamping using Lignum seu Ramulus Cunninghamiae Lanceolatae ash constantly to stir evenly as B phase；Fructus Gleditsia extract and Hibiscus syriacus L. extract are mixed and mixes thoroughly as C phase；Cortex Mori-wolfberry fruit extract, Bombyx Batryticatus powder, Aloe extract are mixed and mix thoroughly as D phase；Flos persicae extract and Cymbidium ensifolium (L.) Sw. extract are mixed and mixes thoroughly as E phase；By A heat phase to 60 DEG C, add B phase, C phase and constantly stir evenly, treating that temperature is reduced to 55 DEG C of addition D phases and stirs evenly, be finally cooled to 50 DEG C of addition E phases and mix thoroughly and casting, deposit after 28 ~ 31d and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610100337.9A CN105754768B (en) | 2016-02-24 | 2016-02-24 | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610100337.9A CN105754768B (en) | 2016-02-24 | 2016-02-24 | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105754768A true CN105754768A (en) | 2016-07-13 |
| CN105754768B CN105754768B (en) | 2018-03-23 |
Family
ID=56329746
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610100337.9A Active CN105754768B (en) | 2016-02-24 | 2016-02-24 | A kind of Baby Care handmade soap containing natural Sasanguasaponin and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105754768B (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106038421A (en) * | 2016-07-27 | 2016-10-26 | 福建春辉生物工程有限公司 | Antipruritic skin cream containing well-aged wild tea oil and its preparation method |
| CN106214734A (en) * | 2016-07-27 | 2016-12-14 | 南京正宽医药科技有限公司 | The extracting method of a kind of Fructus Gleditsia extract and bar soap |
| CN106318715A (en) * | 2016-08-03 | 2017-01-11 | 南安辰光日用化工品有限公司 | Sterilization soap with antibacterial activity |
| CN106833973A (en) * | 2017-01-18 | 2017-06-13 | 广西南宁博智生物科技有限公司 | A kind of cold process soap for acne of dispelling and preparation method thereof |
| CN107213081A (en) * | 2017-05-22 | 2017-09-29 | 邵洁明 | It is a kind of to improve hair washing gel of oily hair and preparation method thereof |
| CN107354038A (en) * | 2017-07-13 | 2017-11-17 | 罗平县腊峰蜂业科技有限公司 | A kind of honey nourishes soap and preparation method thereof |
| CN108839165A (en) * | 2018-06-08 | 2018-11-20 | 阜南县星光工艺品有限公司 | A method of reducing wood color difference before and after highland hook leaf rattan thermal softening |
| CN109568182A (en) * | 2018-12-14 | 2019-04-05 | 江西绿海油脂有限公司 | A kind of tea oil children Shu Run cream |
| CN111378540A (en) * | 2020-03-30 | 2020-07-07 | 山西大学 | Preparation method of novel pig pancreas soap |
| CN112111342A (en) * | 2020-09-08 | 2020-12-22 | 杭州耕欣农林科技开发有限公司 | Handmade soap and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1534087A (en) * | 2003-04-01 | 2004-10-06 | 王保迎 | Skin protection soap and its making method |
| CN103333752A (en) * | 2013-07-10 | 2013-10-02 | 福建农林大学 | Preparation method of camellia oil skin care soap |
| WO2014179305A1 (en) * | 2013-04-29 | 2014-11-06 | IINN, Inc. | Soap composition |
| CN105296232A (en) * | 2015-11-25 | 2016-02-03 | 王晓伟 | Arnebia root handmade soap and production method thereof |
-
2016
- 2016-02-24 CN CN201610100337.9A patent/CN105754768B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1534087A (en) * | 2003-04-01 | 2004-10-06 | 王保迎 | Skin protection soap and its making method |
| WO2014179305A1 (en) * | 2013-04-29 | 2014-11-06 | IINN, Inc. | Soap composition |
| CN103333752A (en) * | 2013-07-10 | 2013-10-02 | 福建农林大学 | Preparation method of camellia oil skin care soap |
| CN105296232A (en) * | 2015-11-25 | 2016-02-03 | 王晓伟 | Arnebia root handmade soap and production method thereof |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106038421A (en) * | 2016-07-27 | 2016-10-26 | 福建春辉生物工程有限公司 | Antipruritic skin cream containing well-aged wild tea oil and its preparation method |
| CN106214734A (en) * | 2016-07-27 | 2016-12-14 | 南京正宽医药科技有限公司 | The extracting method of a kind of Fructus Gleditsia extract and bar soap |
| CN106038421B (en) * | 2016-07-27 | 2019-03-12 | 福建春辉生物工程有限公司 | A kind of itching-relieving lotion and preparation method thereof containing old wild tea oil |
| CN106318715A (en) * | 2016-08-03 | 2017-01-11 | 南安辰光日用化工品有限公司 | Sterilization soap with antibacterial activity |
| CN106833973A (en) * | 2017-01-18 | 2017-06-13 | 广西南宁博智生物科技有限公司 | A kind of cold process soap for acne of dispelling and preparation method thereof |
| CN107213081A (en) * | 2017-05-22 | 2017-09-29 | 邵洁明 | It is a kind of to improve hair washing gel of oily hair and preparation method thereof |
| CN107354038A (en) * | 2017-07-13 | 2017-11-17 | 罗平县腊峰蜂业科技有限公司 | A kind of honey nourishes soap and preparation method thereof |
| CN108839165A (en) * | 2018-06-08 | 2018-11-20 | 阜南县星光工艺品有限公司 | A method of reducing wood color difference before and after highland hook leaf rattan thermal softening |
| CN109568182A (en) * | 2018-12-14 | 2019-04-05 | 江西绿海油脂有限公司 | A kind of tea oil children Shu Run cream |
| CN111378540A (en) * | 2020-03-30 | 2020-07-07 | 山西大学 | Preparation method of novel pig pancreas soap |
| CN112111342A (en) * | 2020-09-08 | 2020-12-22 | 杭州耕欣农林科技开发有限公司 | Handmade soap and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105754768B (en) | 2018-03-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105754768A (en) | Natural camellia saponin-containing baby care handmade soap and preparation method thereof | |
| CN103756808B (en) | A kind of natural washing liquid of preservative free and preparation method thereof | |
| CN104825351B (en) | A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof | |
| CN105997836A (en) | Ferment liquid shampoo and preparation method thereof | |
| KR101054378B1 (en) | Herbal soap composition and its manufacturing method | |
| CN102670447B (en) | Natural plant extract for hair care and preparation method and application thereof | |
| CN105078850A (en) | Liquid shampoo and preparation method thereof | |
| KR100634816B1 (en) | Oriental facial cleanser and manufacturing process thereof | |
| CN104434731B (en) | Nutritional nourishing hand cream and preparation method thereof | |
| JP7315985B2 (en) | Soap composition using mountain ginseng and soap containing the same | |
| CN105012224A (en) | Natural shampoo and preparation method thereof | |
| CN102846503A (en) | Refreshing, anti-dandruff, nourishing and healthful shampoo and preparation method thereof | |
| CN106473996A (en) | A kind of shining skin anti-acne of oil-control repairs mildy wash and preparation method thereof | |
| CN105997827A (en) | Compound camellia oil moisturizer and preparation method thereof | |
| CN107802547A (en) | A kind of rosemary shampoo | |
| CN109010178B (en) | Shower gel and production process thereof | |
| US20110293760A1 (en) | Method for extracting substances from soapberry fruit and seed and products made therefrom | |
| CN107375087A (en) | A kind of shower cream and preparation method thereof | |
| CN106974858A (en) | A kind of acne-removing composition of Sage Extract and its application | |
| KR101926080B1 (en) | Soap composition and soap comprising the same | |
| CN105963240A (en) | Avocado fruit shampoo shower gel applied to infants | |
| KR101554598B1 (en) | Manufacturing method of body cleanser using herb and body cleanser made by that manufacturing method | |
| CN106265266A (en) | A kind of containing chlorophyllous Shu Min bath gel | |
| CN105395444A (en) | Method for preparing oyster facial mask | |
| CN105441230A (en) | Camellia oil cold processed soap |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |