CN111378540A - Preparation method of novel pig pancreas soap - Google Patents

Preparation method of novel pig pancreas soap Download PDF

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Publication number
CN111378540A
CN111378540A CN202010237913.0A CN202010237913A CN111378540A CN 111378540 A CN111378540 A CN 111378540A CN 202010237913 A CN202010237913 A CN 202010237913A CN 111378540 A CN111378540 A CN 111378540A
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China
Prior art keywords
pancreas
sodium hydroxide
soap
mass
oil
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CN202010237913.0A
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Chinese (zh)
Inventor
王英特
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Shanxi University
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Shanxi University
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Priority to CN202010237913.0A priority Critical patent/CN111378540A/en
Publication of CN111378540A publication Critical patent/CN111378540A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/045Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention provides a preparation method of a novel pig pancreas soap, belongs to the field of daily chemical products, and aims to solve the problems that the existing pig pancreas soap is difficult to form, smells unpleasant and is easy to soften and become smelly along with the rise of temperature. The method comprises the following steps: drying fresh pancreas Sus Domestica in the sun, and pulverizing into fine powder; or cleaning fresh pancreas Sus Domestica, grinding, and pulverizing into paste; taking animal oil and vegetable oil, wherein the proportion of the animal oil to the vegetable oil is that the hardness of the soap is 120-170; determining the using amount of sodium hydroxide, and dissolving the sodium hydroxide in water according to the mass ratio of the water to the sodium hydroxide of 2.6-3.2: 1; adding 5-10% of fructus Gleditsiae Abnormalis powder, 1-3% of crystal sugar and 0.5-2% of essence into sodium hydroxide solution; heating and dissolving animal oil, and mixing the pancreas Sus Domestica with the animal oil and vegetable oil; slowly adding the alkali mixed solution into the grease mixed solution, and stirring until the liquid is viscous; pouring the thick liquid into a mould for natural air drying, drying and forming, then demoulding, and standing for 1-2 months at room temperature.

Description

Preparation method of novel pig pancreas soap
Technical Field
The invention relates to the technical field of daily chemical products, in particular to a preparation method of novel pig pancreas soap.
Background
The porcine pancreas soap has a long history of use in northern areas of China, is a common bathing, decontaminating and cleaning product for royal families and people in ancient times, and has related records on the porcine pancreas soap in the book Qianjin essentials and the book Qianjin pterides of Sun Simiao in Tang Dynasty. The pig pancreas soap not only can wash away stains on the surface of the skin, but also has the functions of preventing freezing, preventing cracking and moistening the skin, and can improve rough skin and make the skin tender after long-term use. Modern researches show that the pancreas of the pig contains rich digestive enzymes such as protease, lipase, amylase and the like, and can promote the decomposition of macromolecules such as protein, fat, starch and the like; the pig pancreas also contains saponin, lecithin, protein, fat, calcium, phosphorus, iron, vitamin B1 and B2, nicotinic acid, insulin and other components, so that the pig pancreas has strong dirt-removing capacity, can effectively prevent hand frost cracking and dry skin, and can whiten, protect and moisten skin. The functions of decontamination, fat dissolving and skin care of the pancreas of the pig have attracted attention of modern science. The pig pancreas soap is fine and smooth in texture, mild and free of damage to skin, is a pure natural, green and environment-friendly skin-nourishing fine product created by ancient workers in practice, and is an intelligent crystal.
The traditional pig pancreas soap is prepared by the following steps: manually smashing cleaned pig pancreas, adding fried edible soda ash while smashing for saponification, smashing the raw materials to a certain degree, adding decocted cane sugar, lard oil and Chinese honeylocust water, adding rice, brown sugar, Chinese herbal medicines and the like according to different effects, and then rubbing on a stone slab, wherein the process is similar to kneading dough, so that the soap product is more smooth; and finally, performing compression molding.
Although the soap of pig pancreas has many advantages, the soap of pig pancreas has low use rate in modern society life because of the following reasons: 1. the appearance of the soap does not conform to the aesthetic feeling of modern people, and the traditional pancreatin soap is made of minced pork after being smashed by pancreas, so the soap is soft and loose, is difficult to form and is difficult to design into a more beautiful appearance; 2. because the peculiar smell of the pancreas Sus Domestica is heavy, the traditional pancreas Sus Domestica soap made is big in peculiar smell and bad in smell, and the taste of skin after use is bad, thus not easy to be accepted by people; 3. the traditional pig pancreas soap is saponified by using soda ash, the soda ash is not strong in alkalinity, the saponification is incomplete, and the pig pancreas minced meat is not completely destroyed and decomposed into small molecular compounds, so that the influence of temperature is large, and the pig pancreas soap is easy to soften and become smelly along with the rise of temperature.
Disclosure of Invention
The invention provides a preparation method of a novel porcine pancreatic soap, which aims to solve the technical problems that the prior porcine pancreatic soap is soft and loose, is difficult to form, smells unpleasant and is easy to become soft and smelly along with the rise of temperature.
In order to solve the technical problems, the invention adopts the technical scheme that:
a preparation method of a novel pig pancreas soap comprises the following steps:
s1, selecting pig pancreas: taking fresh pancreas Sus Domestica, sun drying, and pulverizing into fine powder; or cleaning fresh pancreas Sus Domestica, grinding, and pulverizing into paste;
s2, selecting animal oil and vegetable oil: taking animal oil and vegetable oil with the total mass 10-12 times of the mass of the dried porcine pancreas, or taking animal oil and vegetable oil with the total mass 5-7 times of the mass of the pasty porcine pancreas; the proportion of the animal oil and the vegetable oil is that the hardness (INS value) of the soap is between 120 and 170;
s3, preparing and preparing an alkali solution: determining the using amount of sodium hydroxide according to the using amounts of the animal oil and the vegetable oil and the saponification value corresponding to the grease; dissolving sodium hydroxide in water according to the mass ratio of the water to the sodium hydroxide of 2.6-3.2:1, and stirring to completely dissolve the sodium hydroxide to form a sodium hydroxide solution; after the temperature of the sodium hydroxide solution is reduced to room temperature, adding 5-10% by mass of saponin powder, 1-3% by mass of rock candy and 0.5-2% by mass of essence into the sodium hydroxide solution to form an alkali mixture solution;
s4, saponification: heating and dissolving the animal oil, and uniformly mixing the porcine pancreas taken in the step S1 and the animal oil and vegetable oil taken in the step S2 to form a grease mixed solution; slowly adding the alkali mixed solution prepared in the step S3 into the grease mixed solution, and stirring for 10-40 minutes by using a stirrer until the liquid is viscous, and stopping stirring to obtain a pancreas Sus Domestica viscous liquid;
s5, drying and demolding: pouring the viscous liquid of the soap of pancreas Sus Domestica into a mold, naturally air drying, molding, demolding, and standing at room temperature for 1-2 months to obtain the final product.
Optionally, the mass of the mixture of animal oil and vegetable oil is 10 times of the mass of the sun-dried porcine pancreas; or the mass of the mixture of the animal oil and the vegetable oil is 5 times of that of the paste-shaped porcine pancreas.
The invention has the beneficial effects that:
the saponification reaction is more thorough by using strong alkali, so that the pancreas Sus Domestica can be completely decomposed into small molecular compounds, thereby not only removing peculiar smell in the pancreas Sus Domestica, but also preventing the pancreas Sus Domestica from becoming stink at high temperature; the hardness of the soap is adjusted by doping animal oil and vegetable oil, so that the hardness of the soap is between 120 and 170, the plasticity can be increased, and the porcine pancreatic soap is easy to form; the soap of pancreas Sus Domestica has certain fragrance by adding essence etc. Therefore, compared with the background art, the invention has certain hardness, strong plasticity and easy forming, and is beneficial to the appearance design; the smell is fragrant; the influence of temperature is small; not easy to deform and the like. The pancreas Sus Domestica soap prepared by the invention is more in line with the modern social life requirement from the aspect of aesthetic appearance and texture on the basis of keeping the advantages of the traditional pancreas Sus Domestica soap, and has promotion effect on the pancreas Sus Domestica soap entering the modern life.
Detailed Description
The present invention will be described in further detail with reference to examples.
Example 1
A preparation method of a novel pig pancreas soap comprises the following steps:
s1, selecting pig pancreas: taking fresh pancreas Sus Domestica, sun drying, and pulverizing into fine powder; or cleaning fresh pancreas Sus Domestica, grinding, and pulverizing into paste.
S2, selecting animal oil and vegetable oil: taking animal oil and vegetable oil with the total mass 10-12 times of the mass of the dried porcine pancreas, or taking animal oil and vegetable oil with the total mass 5-7 times of the mass of the pasty porcine pancreas; the ratio of the animal oil to the vegetable oil is such that the soap hardness (INS value) is between 120 and 170.
Wherein the animal oil can be lard, mutton fat, chicken fat, beef tallow and the like, and the vegetable oil can be grape seed oil, castor oil, almond oil, corn oil, linseed oil, peanut oil and the like. The INS value is 120-170, so that the hardness of the soap is relatively ideal. Each grease has a fixed INS value.
Hardness of soap is the ratio of INS value × a of fat a to fat mixture + INS value × B of fat B to fat mixture + INS value × C of fat C to fat mixture … …
Preferably, the mass of the mixture of the animal oil and the vegetable oil is 10 times of that of the dried porcine pancreas; or the mass of the mixture of the animal oil and the vegetable oil is 5 times of that of the paste-shaped porcine pancreas. Tests show that when the mass of the mixture of the animal oil and the vegetable oil and the mass of the dried porcine pancreas or the mass of the pasty porcine pancreas are in the multiple relation, the porcine pancreas can be well dissolved in the mixture of the animal oil and the vegetable oil.
S3, preparing and preparing an alkali solution: determining the using amount of sodium hydroxide according to the using amounts of the animal oil and the vegetable oil and the saponification value corresponding to the grease; dissolving sodium hydroxide in water according to the mass ratio of the water to the sodium hydroxide of 2.6-3.2:1, and stirring to completely dissolve the sodium hydroxide to form a sodium hydroxide solution; after the temperature of the sodium hydroxide solution is reduced to room temperature, adding 5-10% by mass of saponin powder, 1-3% by mass of crystal sugar and 0.5-2% by mass of essence into the sodium hydroxide solution to form an alkali mixture solution.
Wherein the amount (mass) of sodium hydroxide is equivalent to the weight of fat A × A, the saponification number of fat B × B, the saponification number of fat C × C, and … …
S4, saponification: heating and dissolving the animal oil, and uniformly mixing the porcine pancreas taken in the step S1 and the mixture of the animal oil and the vegetable oil taken in the step S2 to form a grease mixed solution; and (4) slowly adding the alkali mixed solution prepared in the step (S3) into the grease mixed solution, and stirring for 10-40 minutes by using a stirrer until the liquid is viscous, and stopping stirring to obtain the pancreas soap viscous liquid.
S5, drying and demolding: pouring the viscous liquid of the soap of pancreas Sus Domestica into a mold, naturally air drying, molding, demolding, and standing at room temperature for 1-2 months to obtain the final product.
Example 2
The preparation method of the novel pancreas Sus Domestica soap in the embodiment comprises the following steps:
a preparation method of a novel pig pancreas soap comprises the following steps:
s1, selecting pig pancreas: taking 50g of dried powdery pig pancreas.
S2, selecting animal oil and vegetable oil: 400g of lard oil and 100g of grape seed oil are taken.
S3, preparing and preparing an alkali solution: weighing 68g of sodium hydroxide, dissolving the sodium hydroxide in 200g of water, and stirring to completely dissolve the sodium hydroxide to form a sodium hydroxide solution; after the temperature of the sodium hydroxide solution is reduced to room temperature, 14g of saponin powder, 4g of rock candy and 1g of vanilla are added into the sodium hydroxide solution to form an alkali mixture solution.
S4, saponification: heating and dissolving 400g of lard, and uniformly mixing 50g of powdery pig pancreas and 100g of grape seed oil to form a grease mixed solution; and (4) slowly adding the alkali mixed solution prepared in the step (S3) into the grease mixed solution, and stirring for 15 minutes by using a stirrer until the liquid is viscous, and stopping stirring to obtain the pancreas soap viscous liquid.
S5, drying and demolding: pouring the viscous liquid of the soap of pancreas Sus Domestica into a mold, naturally air drying, molding, demolding, and standing at room temperature for 1-2 months to obtain the final product.
Example 3
A preparation method of a novel pig pancreas soap comprises the following steps:
s1, selecting pig pancreas: 100g of fresh pig pancreas is taken, channels and collaterals are removed, and the pig pancreas is ground and crushed into paste.
S2, selecting animal oil and vegetable oil: 400g of lard oil and 100g of grape seed oil are taken.
S3, preparing and preparing an alkali solution: weighing 68g of sodium hydroxide, dissolving the sodium hydroxide in 200g of water, and stirring to completely dissolve the sodium hydroxide to form a sodium hydroxide solution; after the temperature of the sodium hydroxide solution is reduced to room temperature, 14g of saponin powder, 4g of rock candy and 1g of vanilla are added into the sodium hydroxide solution to form an alkali mixture solution.
S4, saponification: heating and dissolving 400g of lard, and uniformly mixing 100g of pasty pig pancreas and 100g of grape seed oil to form a grease mixed solution; and (4) slowly adding the alkali mixed solution prepared in the step (S3) into the grease mixed solution, and stirring for 30 minutes by using a stirrer until the liquid is viscous, and stopping stirring to obtain the pancreas soap viscous liquid.
S5, drying and demolding: pouring the viscous liquid of the soap of pancreas Sus Domestica into a mold, naturally air drying, molding, demolding, and standing at room temperature for 1-2 months to obtain the final product.
Example 4
A preparation method of a novel pig pancreas soap comprises the following steps:
s1, selecting pig pancreas: taking 50g of dried powdery pig pancreas.
S2, selecting animal oil and vegetable oil: taking 250g of beef tallow and 250g of grape seed oil.
S3, preparing and preparing an alkali solution: weighing 72g of sodium hydroxide, dissolving the sodium hydroxide in 216g of water, and stirring to completely dissolve the sodium hydroxide to form a sodium hydroxide solution; after the temperature of the sodium hydroxide solution is reduced to room temperature, 15g of saponin powder, 5g of rock candy and 2g of vanilla essence are added into the sodium hydroxide solution to form an alkali mixture solution.
S4, saponification: heating and dissolving 250g of beef tallow, and uniformly mixing 50g of powdery pig pancreas and 250g of grape seed oil to form a grease mixed solution; and (4) slowly adding the alkali mixed solution prepared in the step (S3) into the grease mixed solution, and stirring for 20 minutes by using a stirrer until the liquid is viscous, and stopping stirring to obtain the pancreas soap viscous liquid.
S5, drying and demolding: pouring the viscous liquid of the soap of pancreas Sus Domestica into a mold, naturally air drying, molding, demolding, and standing at room temperature for 1-2 months to obtain the final product.
It will be understood that the above embodiments are merely exemplary embodiments taken to illustrate the principles of the present invention, which is not limited thereto. It will be apparent to those skilled in the art that various modifications and improvements can be made without departing from the spirit and substance of the invention, and these modifications and improvements are also considered to be within the scope of the invention.

Claims (2)

1. The preparation method of the novel pig pancreas soap is characterized by comprising the following steps:
s1, selecting pig pancreas: taking fresh pancreas Sus Domestica, sun drying, and pulverizing into fine powder; or cleaning fresh pancreas Sus Domestica, grinding, and pulverizing into paste;
s2, selecting animal oil and vegetable oil: taking animal oil and vegetable oil with the total mass 10-12 times of the mass of the dried porcine pancreas, or taking animal oil and vegetable oil with the total mass 5-7 times of the mass of the pasty porcine pancreas; the proportion of the animal oil and the vegetable oil is that the hardness of the soap is 120-170;
s3, preparing and preparing an alkali solution: determining the using amount of sodium hydroxide according to the using amounts of the animal oil and the vegetable oil and the saponification value corresponding to the grease; dissolving sodium hydroxide in water according to the mass ratio of the water to the sodium hydroxide of 2.6-3.2:1, and stirring to completely dissolve the sodium hydroxide to form a sodium hydroxide solution; after the temperature of the sodium hydroxide solution is reduced to room temperature, adding 5-10% by mass of saponin powder, 1-3% by mass of rock candy and 0.5-2% by mass of essence into the sodium hydroxide solution to form an alkali mixture solution;
s4, saponification: heating and dissolving the animal oil, and uniformly mixing the porcine pancreas taken in the step S1 and the animal oil and vegetable oil taken in the step S2 to form a grease mixed solution; slowly adding the alkali mixed solution prepared in the step S3 into the grease mixed solution, and stirring for 10-40 minutes by using a stirrer until the liquid is viscous, and stopping stirring to obtain a pancreas Sus Domestica viscous liquid;
s5, drying and demolding: pouring the viscous liquid of the soap of pancreas Sus Domestica into a mold, naturally air drying, molding, demolding, and standing at room temperature for 1-2 months to obtain the final product.
2. The method for preparing novel porcine pancreatic soap according to claim 1, wherein the mass of the mixture of the animal oil and the vegetable oil is 10 times of the mass of the sun-dried porcine pancreas; or the mass of the mixture of the animal oil and the vegetable oil is 5 times of that of the paste-shaped porcine pancreas.
CN202010237913.0A 2020-03-30 2020-03-30 Preparation method of novel pig pancreas soap Pending CN111378540A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103194334A (en) * 2013-04-02 2013-07-10 朱海文 Cold process soap added with fresh fig protoplasm
CN103756817A (en) * 2014-01-26 2014-04-30 夏程 Preparation method for manually ground soap
CN105238590A (en) * 2015-09-30 2016-01-13 河南科技大学 Natural anti-dandruff soap and preparation method thereof
CN105754768A (en) * 2016-02-24 2016-07-13 福建春辉生物工程有限公司 Natural camellia saponin-containing baby care handmade soap and preparation method thereof
CN106675859A (en) * 2016-11-21 2017-05-17 袁艳君 Traditional Chinese medicinal soap
CN106947642A (en) * 2017-02-23 2017-07-14 甘肃有色冶金职业技术学院 One boar pancreas plants essential oil handmade soap and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103194334A (en) * 2013-04-02 2013-07-10 朱海文 Cold process soap added with fresh fig protoplasm
CN103756817A (en) * 2014-01-26 2014-04-30 夏程 Preparation method for manually ground soap
CN105238590A (en) * 2015-09-30 2016-01-13 河南科技大学 Natural anti-dandruff soap and preparation method thereof
CN105754768A (en) * 2016-02-24 2016-07-13 福建春辉生物工程有限公司 Natural camellia saponin-containing baby care handmade soap and preparation method thereof
CN106675859A (en) * 2016-11-21 2017-05-17 袁艳君 Traditional Chinese medicinal soap
CN106947642A (en) * 2017-02-23 2017-07-14 甘肃有色冶金职业技术学院 One boar pancreas plants essential oil handmade soap and preparation method thereof

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Application publication date: 20200707

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