CN105726385A - Stimulation-free skin protection lotion containing essential oil and preparing method thereof - Google Patents

Stimulation-free skin protection lotion containing essential oil and preparing method thereof Download PDF

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Publication number
CN105726385A
CN105726385A CN201610080729.3A CN201610080729A CN105726385A CN 105726385 A CN105726385 A CN 105726385A CN 201610080729 A CN201610080729 A CN 201610080729A CN 105726385 A CN105726385 A CN 105726385A
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CN
China
Prior art keywords
quintessence oil
oil
extract
surfactant
formula
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Granted
Application number
CN201610080729.3A
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Chinese (zh)
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CN105726385B (en
Inventor
郭雷平
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Guangdong Xing Mei cosmetics limited company
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Kingway Cosmetics Technology Guangzhou Co Ltd
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Priority to CN201610080729.3A priority Critical patent/CN105726385B/en
Publication of CN105726385A publication Critical patent/CN105726385A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/484—Glycyrrhiza (licorice)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
    • A61K36/704—Polygonum, e.g. knotweed
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216—Solid or semisolid forms
    • A61K8/0233—Distinct layers, e.g. core/shell sticks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42—Amides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52—Stabilizers
    • A61K2800/524—Preservatives

Abstract

The invention relates to a stimulation-free skin protection lotion containing essential oil.The stimulation-free skin protection lotion comprises, by weight, 0.1%-1% of centella asiatica extract, 0.1%-1% of polygonum cuspidatum extract, 0.1%-1% of licorice extract, 1%-5% of olive oil, 0.01%-0.1% of essential oil, 5%-20% of humectant, 0.1%-1% of preservative and the balance water.According to the skin protection lotion containing the essential oil, plant extract with the stimulation relieving effect and the anti-allergy effect is added, and the skin protection lotion is mild and free of stimulation accordingly.

Description

A kind of containing non-stimulated surfactant of quintessence oil and preparation method thereof
Technical field
The invention belongs to cosmetic field, more particularly to one containing non-stimulated surfactant of quintessence oil and preparation method thereof.
Background technology
Quintessence oil is from the flower of plant, leaf, stem, root or fruit, by steam distillation, squeezing and pressing method, cold-maceration or Solvent extraction method refines the volatile flavor of extraction.Quintessence oil has point (compound essential Oil) and the not diluted of dilution (single Side's quintessence oil).Essence oil volatility is very strong, and once ingress of air will quickly volatilize, it is therefore desirable to use solubilizing agent by It dissolves wherein, to be uniformly dispersed.
Quintessence oil is made up of some the least molecules, these high volatile substances, can be entered body by nasal membrane tissue resorption Body, is directly sent to brain by message, by the limbic system of brain, regulation emotion and the physiological function of health, therefore essence Oil is often used in cosmetics as additive.But quintessence oil has lipotropy, it is easy to be dissolved in oils and fats, because smart The strand of oil is the most comparatively short, and this makes them easily permeate in skin, and by blood capillary abundant under subcutaneous fat Managing and enter internal, being directly entered skin if do not dealt with, skin can be produced bigger stimulation.
On market, the surfactant containing quintessence oil is the most, also gets consumer reception, but is all quintessence oil solubilizing agent solubilising mostly In rear addition water preparation, such way has two problems: 1, due to the more difficult solubilising of quintessence oil, solubilizing agent ratio therefore The highest, bigger to skin irritation and damage；2, the molecular weight of quintessence oil own is smaller, and permeability is stronger, therefore containing essence The surfactant of oil is bigger to the zest of skin.
It is thus desirable to research and development one can add functional quintessence oil, there is the surfactant less to skin irritation.
Summary of the invention
In order to solve the above-mentioned problems in the prior art, the invention provides a kind of interpolation quintessence oil but to skin irritation The least surfactant.
The technical purpose of the present invention is achieved through the following technical solutions:
The present invention containing the non-stimulated surfactant of quintessence oil, its formula contains following components in percentage by weight: Herba Centellae carries Take thing 0.1-1%, Rhizoma Polygoni Cuspidati extract 0.1-1%, Radix Glycyrrhizae extract 0.1-1%, olive oil 1-5%, quintessence oil 0.01-0.1%, Wetting agent 5-20%, preservative 0.1-1%, water surplus.
Further, the formula containing the non-stimulated surfactant of quintessence oil of the present invention, contains following components in percentage by weight: Herba Centellae extract 0.1-0.5%, Rhizoma Polygoni Cuspidati extract 0.1-0.5%, Radix Glycyrrhizae extract 0.1-0.5%, olive oil 1-3%, essence Oil 0.01-0.05%, wetting agent 9-26%, preservative 0.1-0.8%, water surplus.
Specifically, in described formula, preservative is caprylhydroxamic acid.Caprylhydroxamic acid does not list 2017 editions cosmetics healths in Preservative catalogue in specification, using suitably to measure has preferable antisepsis, and as mild as a dove.
Specifically, the quintessence oil in described formula is Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil or Geranium Essential.Required interpolation Quintessence oil is not limited to mentioned kind, can add according to practical use.
Preferably, wetting agent one or two in glycerol, glycine betaine, butanediol, hyaluronate sodium in described formula Plant above material.
It is highly preferred that the kind that in described formula, wetting agent comprises and weight ratio percentage ratio thereof: glycerol 5-10%, glycine betaine 1-5%, butanediol 1-5%, hyaluronate sodium 0.01-0.5%.
On the other hand, present invention also offers and a kind of prepare the above-mentioned method containing the non-stimulated surfactant of quintessence oil, including following Step:
1), each component is weighed according to formula；
2), by water, wetting agent addition emulsifying pot stirring and being warming up to 70～90 DEG C, stir 15～25 minutes；It is cooled to 40～50 DEG C；
3), it is subsequently adding quintessence oil, olive oil, snow grass extract, Rhizoma Polygoni Cuspidati extract, Radix Glycyrrhizae extract, preservative, stirs Mix rear cooling 35～40 DEG C and get final product.
Further, described quintessence oil dissolves in advance with olive oil before being added into emulsifying pot.
It is commercially available, from Korea S for the Herba Centellae extracting solution in above-mentioned formula, Radix Glycyrrhizae extract, Rhizoma Polygoni Cuspidati extracting solution BIOSPECTRUM company, wherein said Herba Centellae extracting solution is processing rheumatic arthritis, calm vasodilation and anti-ageing Old aspect has good effect.Described Radix Glycyrrhizae extract has a good effect at calmness, antiallergic, aspect of releiving, and Rhizoma Polygoni Cuspidati Extracting solution then has good antiphlogistic effects.Above-mentioned three Plant Extracts combinations have thorn of well releiving in surfactant Sharp, hypo-allergenic effect.
Beneficial effects of the present invention:
Compared with prior art, the non-stimulated surfactant containing quintessence oil of the present invention has the advantages that
1, the surfactant containing quintessence oil of the present invention, adds and has stimulation of releiving, the plant extraction liquid of hypo-allergenic effect, gentle Non-stimulated.
2, double-deck surfactant made by monolayer surfactant by the present invention, is dissolved in olive oil by quintessence oil, floats over surfactant upper strata, Lower floor is water preparation, uses, does not the most use solubilizing agent, reduce skin irritation during use after shaking mix homogeneously.
3, being added with natural moisture preserving agent in inventive formulation, skin affinity is preferable, reduces anaphylactogen, as glycine betaine is (high Rieter Perfojet produces) and hyaluronate sodium (production of Shandong Fu Ruida company).
4, preservative mesh during preservative caprylhydroxamic acid of the present invention does not list 2017 editions cosmetics health specifications in Record, simply using suitably to measure has preferable antisepsis, and as mild as a dove.
Accompanying drawing explanation
Fig. 1 is the production technological process containing quintessence oil surfactant preparing the present invention.
Detailed description of the invention
In order to make the object, technical solutions and advantages of the present invention definitely, below the preferred embodiments of the present invention are carried out Detailed description.
Embodiment 1-3 (containing quintessence oil non-stimulated surfactant embodiment)
1, embodiment 1～3 and the formula table of the product containing quintessence oil skin water of comparative example 1～3, the weight hundred of the most each component It is 100% that mark adds up.
The formula table of the table 1 product containing quintessence oil skin water
2, the preparation method containing the non-stimulated surfactant of quintessence oil of embodiment 1～3
1), each component is weighed according to the formula of table 1；
2), water, hyaluronate sodium, butanediol, glycerol, glycine betaine, addition emulsifying pot are stirred and to be warmed up to 80 Celsius Degree, stirs 20 minutes；
3) after, being then cooled to 45 degrees Celsius, by Flos Rosae Rugosae quintessence oil, olive oil, (Flos Rosae Rugosae quintessence oil here needs first to use Fructus Canarii albi oil soluble Add again after solution), snow grass extract, Rhizoma Polygoni Cuspidati extract, Radix Glycyrrhizae extract, caprylhydroxamic acid, addition stirring cool to 38 Degree Celsius and get final product.Check qualified discharging fill.
Comparative example 1～3
Weighing each component in comparative example 1～3 according to the formula table of table 1, the percentage by weight sum of each component materials is 100%.The preparation method of comparative example 1～3 is roughly the same with the preparation method of embodiment 1～3, simply step 3) in rhodamine toner Oil needs to add after Cremophor RH40 solubilising.
Measure of merit
Acute ocular zest/corrosion test
Surfactant prepared by embodiment 1 send Bao Hua inspection center of Guangdong Province do acute ocular zest/corrosion test, real Test result as follows:
Within the observation period, there is not zest in the right eye (surfactant that spray embodiment 1 prepares) of 3 tested new zealand rabbits Reaction.Left eye (comparison eye) occurs without any irritation, and result sees table 2.
Table 1 embodiment 1 acute ocular zest test result
Compare above-mentioned test result, according to " cosmetics health specification " 2007 editions " acute ocular irritative response classification " Grade scale be judged to: new zealand rabbit tested surfactant Eye irritation intensity (30 seconds rinse) is nonirritant.
The surfactant that comparative example 1 prepares has been also carried out acute ocular zest/corrosion test, and its result is as shown in table 3.
The acute ocular zest test result of table 3 comparative example 1
It addition, the surfactant also prepared embodiment 2, embodiment 3 and comparative example 2, comparative example 3 is tried out, point Not having 10 volunteers to participate in trying out, directly surfactant sprayed eyes, 30 seconds afterflush, not find twinge With inflamed eyes as passing judgment on non-irritating standard, find eye after trying out the formulation product of embodiment 2, embodiment 3 Eyeball is non-stimulated, and use comparative example 2, volunteer's eyes of comparative example 3 have slight discomfort.
Experiment conclusion: the surfactant containing quintessence oil of the present invention can be seen that eyes non-stimulated by the test of acute ocular zest Property, there is not hyperemia or edema phenomenon in eye conjunctiva.
Obviously, the above embodiment of the present invention is only for clearly demonstrating example of the present invention, and is not to this The restriction of the embodiment of invention.For those of ordinary skill in the field, the most also may be used To make other changes in different forms.Here cannot all of embodiment be given exhaustive.Every belong to this What the technical scheme of invention was extended out obviously changes or changes the row still in protection scope of the present invention.

Claims (8)

1. a non-stimulated surfactant Han quintessence oil, it is characterised in that its formula contains following group in percentage by weight Point: Herba Centellae extract 0.1-1%, Rhizoma Polygoni Cuspidati extract 0.1-1%, Radix Glycyrrhizae extract 0.1-1%, olive oil 1-5%, essence Oil 0.01-0.1%, wetting agent 5-20%, preservative 0.1-1%, water surplus.
The most according to claim 1 containing the non-stimulated surfactant of quintessence oil, it is characterised in that its formula is according to weight hundred Proportion by subtraction meter contains following components: Herba Centellae extract 0.1-0.5%, Rhizoma Polygoni Cuspidati extract 0.1-0.5%, Radix Glycyrrhizae extract 0.1-0.5%, olive oil 1-3%, quintessence oil 0.01-0.05%, wetting agent 5-20%, preservative 0.1-0.8%, water surplus.
The most according to claim 1 and 2 containing the non-stimulated surfactant of quintessence oil, it is characterised in that in described formula Preservative is caprylhydroxamic acid.
The most according to claim 1 and 2 containing the non-stimulated surfactant of quintessence oil, it is characterised in that in described formula Quintessence oil is Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil or Geranium Essential.
The most according to claim 1 and 2 containing the non-stimulated surfactant of quintessence oil, it is characterised in that described formula is protected Humectant one or more materials in glycerol, glycine betaine, butanediol, hyaluronate sodium.
The most according to claim 5 containing the non-stimulated surfactant of quintessence oil, it is characterised in that wetting agent in described formula The kind comprised and percentage by weight thereof be: glycerol 5-10%, glycine betaine 1-5%, butanediol 1-5%, hyaluronate sodium 0.01～0.5%.
7. preparing the method containing the non-stimulated surfactant of quintessence oil as described in any one in claim 1-6, it is special Levy and be, comprise the following steps:
1), each component is weighed according to formula；
2), by water, wetting agent addition emulsifying pot stirring and being warming up to 70～90 DEG C, stir 15～25 minutes；It is cooled to 40～50 DEG C；
3), it is subsequently adding quintessence oil, olive oil, snow grass extract, Rhizoma Polygoni Cuspidati extract, Radix Glycyrrhizae extract, preservative, stirs Mix rear cooling 35～40 DEG C and get final product.
Method the most according to claim 7, it is characterised in that further comprising the steps of, described quintessence oil is adding Dissolve in advance with olive oil before entering emulsifying pot.
CN201610080729.3A 2016-02-04 2016-02-04 One kind is containing non-stimulated surfactant of essential oil and preparation method thereof Active CN105726385B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106798658A (en) * 2017-03-08 2017-06-06 国东启 A kind of moisture-keeping composition and skin care item
CN109172413A (en) * 2018-10-12 2019-01-11 深圳市仙迪化妆品有限公司 A kind of composite fruit oil surfactant and preparation method thereof
CN110179948A (en) * 2019-05-15 2019-08-30 深圳市植乐家芳香科技有限公司 A kind of application and preparation method thereof ached of releiving

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CN103251531A (en) * 2013-04-28 2013-08-21 福建省梦娇兰日用化学品有限公司 Relief propolis cream
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CN104523493A (en) * 2014-12-11 2015-04-22 罗生芳 Toner with lavender fragrance and preparation method of toner

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CN103251531A (en) * 2013-04-28 2013-08-21 福建省梦娇兰日用化学品有限公司 Relief propolis cream
CN104382784A (en) * 2014-11-12 2015-03-04 孙艺洲 Facial mask emulsion and preparation method thereof
CN104523493A (en) * 2014-12-11 2015-04-22 罗生芳 Toner with lavender fragrance and preparation method of toner

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106798658A (en) * 2017-03-08 2017-06-06 国东启 A kind of moisture-keeping composition and skin care item
CN109172413A (en) * 2018-10-12 2019-01-11 深圳市仙迪化妆品有限公司 A kind of composite fruit oil surfactant and preparation method thereof
CN110179948A (en) * 2019-05-15 2019-08-30 深圳市植乐家芳香科技有限公司 A kind of application and preparation method thereof ached of releiving

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