CN105724440A - Cinnamomum camphora insecticide and preparation method thereof - Google Patents
Cinnamomum camphora insecticide and preparation method thereof Download PDFInfo
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- CN105724440A CN105724440A CN201610263518.3A CN201610263518A CN105724440A CN 105724440 A CN105724440 A CN 105724440A CN 201610263518 A CN201610263518 A CN 201610263518A CN 105724440 A CN105724440 A CN 105724440A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/26—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-nitrogen bonds
- A01N57/28—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-nitrogen bonds containing acyclic or cycloaliphatic radicals
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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Abstract
The invention provides cinnamomum camphora insecticide which is characterized by being prepared from, by weight, 20-40 parts of cyfluthrin, 12-24 parts of acephate, 40-60 parts of sophocarpidine, 25-55 parts of vitex negundo, 10-25 parts of herba verbenae, 5-12 parts of a citric acid/sodium citrate buffer solution, 0.5-5 parts of antioxidant, 5-7.5 parts of ethyl alcohol and 100-150 parts of water. The cinnamomum camphora insecticide is low in cost, simple in preparation method and good in insect damage prevention effect, raw materials are easy to obtain, and the effect of raising the yield is achieved.
Description
Technical field
The present invention relates to a kind of insecticide, particularly relate to a kind of Radix Cinnamomi porrecti insecticide and preparation method.
Background technology
Radix Cinnamomi porrecti is that Perenniporia martius evergreen broadleaf forest represents seeds, adaptable, distributed areas all have distribution on the south Hainan Province to the Changjiang river, the main place of production is Hainan Province of China, Taiwan, Fujian, Jiangxi, Guangdong, Hunan, Hubei, Sichuan, Yunnan, Guizhou, zhejiang and other places, especially most with Taiwan.Vertical distribution is typically in the hills of height above sea level less than 600 meters, low mountain, Plain, but the highest.In Hunan, area, boundary, Guizhou reach height above sea level 1000 meters (height above sea level more than 1000 meters for Cinnamomum porrectum (Roxb.) Kosterm.).Mostly being Artificial Pure the central and north, Taiwan height above sea level less than 1000 meters, 1000-1500 rice is mainly the Natural Mixed Forest of Radix Cinnamomi porrecti and other deciduous species composition.Radix Cinnamomi porrecti occupies critical role in Taiwan Forestry, is listed in economic reproducting tree species, is worth in bigger seeds in existing 200 diversified economies, and Radix Cinnamomi porrecti comes out at the top.In the theropencedrymion chief species of subtropical zone, it is the first that Radix Cinnamomi porrecti occupies it.
Along with the development of urban economy, people are more and more higher to the requirement of quality of life.How considering the benefit that ecological benefits, society are long-range while pursuing economic benefit, the road walking sustainable development becomes the direction that governments at all levels in recent years make great efforts to implement.Radix Cinnamomi porrecti is because its attitude is beautiful, with luxuriant foliage and spreading branches in leafy profusion and the four seasons evergreen two are widely used as street green area, park plaza and forest belt, sheet woods and shade tree.In Shanghai, extension along with Shanghai Urban Area, the integrated general layout of Urban-rural Development creates comprehensive, all standing of Greenbelt Developing, urban afforestation and Suburban Forestry synchronized development, either street green area, park plaza or forest belt, sheet woods, shade tree, Radix Cinnamomi porrecti is widely cultivated, and is the first-selected seeds of District of Shanghai greening aiphyllium.Its overall frequency occurred in the Garden Plant Community of Shanghai Urban is 48.7%, occupies first of five overall garden seeds southern magnolia (25.97%), Metasequoia glyptostroboides Hu et Cheng (20.78%), Cedrus deoclar (Roxb.) G. Don (18.83%), cypress (10.39%).The frequency occurred in park green land, street greens, Yard-greenbelt, factory greenery patches is respectively 27.78%, 42.86%, 58.69%, 56.56%, is respectively positioned on the front side of southern magnolia, Metasequoia glyptostroboides Hu et Cheng, Cedrus deoclar (Roxb.) G. Don, cypress.
But, along with day by day increasing of Radix Cinnamomi porrecti plantation, design density is too high simultaneously, nursery stock source is complicated, Tree Structure is single, causing harm of Lignum cinnamomi camphorae insect pest day by day increases the weight of, Radix Cinnamomi porrecti is produced and the performance of afforestation ecological effect brings threat greatly, such as biological harm caused such as Lignum cinnamomi camphorae louse, Camphor tree nest snout moth's larva, leaf of Lignum cinnamomi camphorae honeybee, sampling techniquc, blue square tumor lepidosaphes.Due to less to Radix Cinnamomi porrecti prevention and control of plant diseases, pest control research, there is no the prophylactico-therapeutic measures of specification, cause a lot of preventing and treating tool to bear the character of much blindness.Accordingly, it would be desirable to strengthen Radix Cinnamomi porrecti Major Pests and integrated control technique thereof are studied.
For solving problems, Chinese patent 201410628860.X, disclose one and the invention discloses a kind of Radix Cinnamomi porrecti insecticide and preparation method thereof, include following component according to mass fraction: cloudy XIANGSHU
30-40 part, Fructus Capsici 20-30 part, Herba Alii fistulosi 18-20 part, Pericarpium Zanthoxyli 15-17 part, anistree 8-12 part, Radix seu Caulis Derridis Trifoliatae 40-50 part, Pericarpium Granati 40-60 part, Herba Houttuyniae 30-50 part, Radix Arnebiae (Radix Lithospermi) 35-45 part, Radix Tripterygii Wilfordii 11-13 part, Herba polygoni hydropiperis 5-7 part, water 1150-1350 part, the present invention is a kind of green plants property insecticide, degradable, noresidue there is no drug-fast environment-protection pesticide.But, a kind of Radix Cinnamomi porrecti insecticide ingredient of this inventive method is of a great variety, and raw material is difficult to obtain, and the Radix Cinnamomi porrecti insecticide insecticidal effect inconspicuous that the method prepares.
Summary of the invention
For solving the problem of above-mentioned existence, it is an object of the invention to provide a kind of Radix Cinnamomi porrecti insecticide and preparation method.
For reaching above-mentioned purpose, the technical scheme is that
A kind of Radix Cinnamomi porrecti insecticide, it is made up of the following raw material according to weight fraction meter: cyfloxylate 20-40 part, orthene 12-24 part, matrine 40-60 part, five-leaved chaste tree 25-55 part, Herba Verbenae 10-25 part, citric acid/sodium citrate buffer solution 5-12 part, antioxidant 0.5-5 part, ethanol 5-7.5 part, water 100-150 part.
Further, it is made up of the following raw material according to weight fraction meter: cyfloxylate 28-37 part, orthene 13-20 part, matrine 45-55 part, five-leaved chaste tree 32-40 part, Herba Verbenae 13-18 part, citric acid/sodium citrate buffer solution 5-8 part, antioxidant 1.2-3.8 part, ethanol 5.5-7 part, water 110-140 part.
Further, it is made up of the following raw material according to weight fraction meter: cyfloxylate 35 parts, orthene 18 parts, matrine 49 parts, five-leaved chaste tree 36 parts, Herba Verbenae 17 parts, 7.5 parts of citric acid/sodium citrate buffer solution, antioxidant 2.5 parts, ethanol 6 parts, 120 parts of water.
Separately, the pH value of described citric acid/sodium citrate buffer solution is 5.8-6.6.
And have, described water is deionized water.
A kind of Radix Cinnamomi porrecti method for producing insecticide, comprises the steps:
(1) matrine, five-leaved chaste tree, Herba Verbenae are cleaned and remove surface impurity, pulverizer is broken into powder, is proportionally added under soaked overnight in ethanol water, stirring condition being heated to reflux 4-10h；
(2) filter, obtain clear liquid, when clear liquid is cooled to 30-40 DEG C, add cyfloxylate and orthene, stir；
(3) add citric acid/sodium citrate buffer solution and antioxidant after continuing cool to room temperature and stir and make insecticide.
Further, described insecticide color is light yellow, pH value is 6.2-7.0.
The beneficial effects of the present invention is:
(1) present invention provides a kind of Radix Cinnamomi porrecti pesticide grade preparation method, and raw material is drawn materials easily, and cost price is cheap, and preparation method is simple；
(2) present invention provides a kind of Radix Cinnamomi porrecti pesticide grade preparation method, obtained insecticide insect-pest is effective, it is possible to effectively kill such as the Cortex cinnamomi camphorae worms such as sampling techniquc, has the effect preferably preventing and treating sampling techniquc insect pest, be conducive to the healthy growth of Cortex cinnamomi camphorae, play the effect increasing yield.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearer, further describe below in conjunction with embodiment.
Embodiment 1
A kind of Radix Cinnamomi porrecti insecticide, is made up of the following raw material according to weight fraction meter: cyfloxylate 35 parts, orthene 18 parts, matrine 49 parts, five-leaved chaste tree 36 parts, Herba Verbenae 17 parts, 7.5 parts of citric acid/sodium citrate buffer solution, antioxidant 2.5 parts, ethanol 6 parts, 120 parts of water.The pH value of described citric acid/sodium citrate buffer solution is 6.2, and described water is deionized water.
A kind of Radix Cinnamomi porrecti method for producing insecticide, comprises the steps:
(1) matrine, five-leaved chaste tree, Herba Verbenae are cleaned and remove surface impurity, pulverizer is broken into powder, is proportionally added under soaked overnight in ethanol water, stirring condition being heated to reflux 8h；
(2) filter, obtain clear liquid, when clear liquid is cooled to 38 DEG C, add cyfloxylate and orthene, stir；
(3) add citric acid/sodium citrate buffer solution and antioxidant after continuing cool to room temperature and stir and make insecticide.
Described insecticide color is light yellow, and pH value is 6.8.
Embodiment 2
A kind of Radix Cinnamomi porrecti insecticide, is made up of the following raw material according to weight fraction meter: cyfloxylate 20 parts, orthene 24 parts, matrine 42 parts, five-leaved chaste tree 53 parts, Herba Verbenae 23 parts, 5 parts of citric acid/sodium citrate buffer solution, antioxidant 1.3 parts, ethanol 5 parts, 140 parts of water.The pH value of described citric acid/sodium citrate buffer solution is 6.5, and described water is deionized water.
A kind of Radix Cinnamomi porrecti method for producing insecticide, comprises the steps:
(1) matrine, five-leaved chaste tree, Herba Verbenae are cleaned and remove surface impurity, pulverizer is broken into powder, is proportionally added under soaked overnight in ethanol water, stirring condition being heated to reflux 4.5h；
(2) filter, obtain clear liquid, when clear liquid is cooled to 30 DEG C, add cyfloxylate and orthene, stir；
(3) add citric acid/sodium citrate buffer solution and antioxidant after continuing cool to room temperature and stir and make insecticide.
Described insecticide color is light yellow, and pH value is 6.9.
Embodiment 3
A kind of Radix Cinnamomi porrecti insecticide, is made up of the following raw material according to weight fraction meter: cyfloxylate 40 parts, orthene 12 parts, matrine 58 parts, five-leaved chaste tree 29 parts, Herba Verbenae 12 parts, 12 parts of citric acid/sodium citrate buffer solution, antioxidant 0.5 part, ethanol 7.5 parts, 108 parts of water.The pH value of described citric acid/sodium citrate buffer solution is 5.8, and described water is deionized water.
A kind of Radix Cinnamomi porrecti method for producing insecticide, comprises the steps:
(1) matrine, five-leaved chaste tree, Herba Verbenae are cleaned and remove surface impurity, pulverizer is broken into powder, is proportionally added under soaked overnight in ethanol water, stirring condition being heated to reflux 10h；
(2) filter, obtain clear liquid, when clear liquid is cooled to 40 DEG C, add cyfloxylate and orthene, stir；
(3) add citric acid/sodium citrate buffer solution and antioxidant after continuing cool to room temperature and stir and make insecticide.
Further, described insecticide color is light yellow, pH value is 6.3.
Above-described embodiment 1-3 carries out preventing and treating sampling techniquc efficacy testing, and test data are shown in Table 1.
Table 1: preventing and treating sampling techniquc efficacy testing result.
As it can be seen from table 1 a kind of Radix Cinnamomi porrecti insecticide of the present invention, having an effect preferably preventing and treating sampling techniquc insect pest, the deinsectization rate after dispenser 10 days is more than 85%.
It should be noted that above example is only in order to illustrate technical scheme and unrestricted.Although the present invention being described in detail with reference to preferred embodiment, it will be understood by those within the art that, can modify the technical scheme of invention or equivalent, without deviating from the scope of technical solution of the present invention, it all should be contained in scope of the presently claimed invention.
Claims (7)
1. a Radix Cinnamomi porrecti insecticide, it is characterized in that, it is made up of the following raw material according to weight fraction meter: cyfloxylate 20-40 part, orthene 12-24 part, matrine 40-60 part, five-leaved chaste tree 25-55 part, Herba Verbenae 10-25 part, citric acid/sodium citrate buffer solution 5-12 part, antioxidant 0.5-5 part, ethanol 5-7.5 part, water 100-150 part.
A kind of Radix Cinnamomi porrecti insecticide the most according to claim 1, it is characterized in that, it is made up of the following raw material according to weight fraction meter: cyfloxylate 28-37 part, orthene 13-20 part, matrine 45-55 part, five-leaved chaste tree 32-40 part, Herba Verbenae 13-18 part, citric acid/sodium citrate buffer solution 5-8 part, antioxidant 1.2-3.8 part, ethanol 5.5-7 part, water 110-140 part.
A kind of Radix Cinnamomi porrecti insecticide the most according to claim 1, it is characterized in that, it is made up of the following raw material according to weight fraction meter: cyfloxylate 35 parts, orthene 18 parts, matrine 49 parts, five-leaved chaste tree 36 parts, Herba Verbenae 17 parts, 7.5 parts of citric acid/sodium citrate buffer solution, antioxidant 2.5 parts, ethanol 6 parts, 120 parts of water.
A kind of Radix Cinnamomi porrecti insecticide the most according to claim 1, it is characterised in that the pH value of described citric acid/sodium citrate buffer solution is 5.8-6.6.
A kind of Radix Cinnamomi porrecti insecticide the most according to claim 1, it is characterised in that described water is deionized water.
6. a Radix Cinnamomi porrecti method for producing insecticide, it is characterised in that comprise the steps:
Matrine, five-leaved chaste tree, Herba Verbenae are cleaned and remove surface impurity, pulverizer is broken into powder, is proportionally added under soaked overnight in ethanol water, stirring condition being heated to reflux 4-10h；
Filter, obtain clear liquid, when clear liquid is cooled to 30-40 DEG C, add cyfloxylate and orthene, stir；
Add citric acid/sodium citrate buffer solution and antioxidant after continuing cool to room temperature and stir and make insecticide.
A kind of Radix Cinnamomi porrecti insecticide preparation method the most according to claim 6, it is characterised in that described insecticide color is light yellow, and pH value is 6.2-7.0.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020161634A1 (en) * | 2019-02-07 | 2020-08-13 | Upl Ltd | Insecticidal compositions resistant to active ingredient degradation and process for preparation thereof |
| CN112674120A (en) * | 2019-10-17 | 2021-04-20 | 南京宿根花卉植物园有限公司 | Insecticide containing garden negundo chastetree seeds |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020161634A1 (en) * | 2019-02-07 | 2020-08-13 | Upl Ltd | Insecticidal compositions resistant to active ingredient degradation and process for preparation thereof |
| CN113473855A (en) * | 2019-02-07 | 2021-10-01 | Upl有限公司 | Insecticidal composition resistant to active ingredient degradation and preparation method thereof |
| CN112674120A (en) * | 2019-10-17 | 2021-04-20 | 南京宿根花卉植物园有限公司 | Insecticide containing garden negundo chastetree seeds |
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