CN105693482B - 纯化方法 - Google Patents

纯化方法 Download PDF

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Publication number
CN105693482B
CN105693482B CN201510915419.4A CN201510915419A CN105693482B CN 105693482 B CN105693482 B CN 105693482B CN 201510915419 A CN201510915419 A CN 201510915419A CN 105693482 B CN105693482 B CN 105693482B
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CN
China
Prior art keywords
alcohol compound
primary alcohol
acylated
mixture
secondary alcohol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201510915419.4A
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English (en)
Chinese (zh)
Other versions
CN105693482A (zh
Inventor
C·D·吉尔摩
C－W·李
P·特雷福纳斯三世
W·威廉姆斯三世
Q·谢
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DuPont Electronic Materials International LLC
Original Assignee
Rohm and Haas Electronic Materials LLC
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Publication date
Application filed by Rohm and Haas Electronic Materials LLC filed Critical Rohm and Haas Electronic Materials LLC
Publication of CN105693482A publication Critical patent/CN105693482A/zh
Application granted granted Critical
Publication of CN105693482B publication Critical patent/CN105693482B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/44—Separation; Purification; Stabilisation; Use of additives by treatments giving rise to a chemical modification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C07C43/13—Saturated ethers containing hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/20—Ethers having an ether-oxygen atom bound to a carbon atom of a six-membered aromatic ring
    • C07C43/23—Ethers having an ether-oxygen atom bound to a carbon atom of a six-membered aromatic ring containing hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/39—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • C07C67/40—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester by oxidation of primary alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
    • C07C69/12—Acetic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/02—Ortho- or ortho- and peri-condensed systems
    • C07C2603/40—Ortho- or ortho- and peri-condensed systems containing four condensed rings
    • C07C2603/42—Ortho- or ortho- and peri-condensed systems containing four condensed rings containing only six-membered rings
    • C07C2603/50—Pyrenes; Hydrogenated pyrenes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201510915419.4A 2014-12-15 2015-12-10 纯化方法 Expired - Fee Related CN105693482B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14/569,813 US9440899B2 (en) 2014-12-15 2014-12-15 Purification method
US14/569813 2014-12-15

Publications (2)

Publication Number Publication Date
CN105693482A CN105693482A (zh) 2016-06-22
CN105693482B true CN105693482B (zh) 2020-05-15

Family

ID=56110499

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510915419.4A Expired - Fee Related CN105693482B (zh) 2014-12-15 2015-12-10 纯化方法

Country Status (5)

Country Link
US (1) US9440899B2 (enExample)
JP (1) JP6246781B2 (enExample)
KR (1) KR101805632B1 (enExample)
CN (1) CN105693482B (enExample)
TW (1) TWI631102B (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018061416A1 (ja) 2016-09-27 2018-04-05 ソニー株式会社 センサ、電子機器、ウエアラブル端末および制御方法
WO2020043518A1 (en) * 2018-08-30 2020-03-05 Basf Se Process to produce a mono vinyl ether
JPWO2021106536A1 (enExample) * 2019-11-29 2021-06-03
WO2021106537A1 (ja) * 2019-11-29 2021-06-03 富士フイルム株式会社 レジスト下層膜形成用組成物、パターン形成方法、及び、電子デバイスの製造方法
JP7309907B2 (ja) * 2019-11-29 2023-07-18 富士フイルム株式会社 感活性光線性又は感放射線性樹脂組成物、パターン形成方法、及び、電子デバイスの製造方法
KR102154356B1 (ko) * 2020-03-10 2020-09-09 주식회사 켐트로닉스 일차 알코올과 이차 알코올의 혼합물로부터 이차 알코올을 분리하여 얻는 방법
JPWO2023054004A1 (enExample) * 2021-09-29 2023-04-06
KR102498772B1 (ko) * 2021-11-29 2023-02-10 주식회사 켐트로닉스 초고순도 pgmea의 제조방법

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2923733A (en) * 1957-03-28 1960-02-02 Pan American Petroleum Corp Process for separating primary from secondary alcohols
CN101250094A (zh) * 2007-02-23 2008-08-27 大赛璐化学工业株式会社 1-甲氧基-2-丙醇的制备方法
CN101985418A (zh) * 2010-08-16 2011-03-16 江苏天音化工有限公司 一种制备2－甲氧基－1－丙醇醋酸酯的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2072806A (en) * 1933-01-06 1937-03-02 Du Pont Process for the separation of primary from secondary alcohols
US2476053A (en) * 1947-01-02 1949-07-12 Standard Oil Dev Co Process for producing esters
US2872478A (en) * 1956-11-06 1959-02-03 Borden Company A Corp Of New J Separation of alcohols from esters
SE8305596D0 (sv) 1983-10-12 1983-10-12 Leo Ab A selective acylation method
US5723024A (en) 1996-08-26 1998-03-03 Berg; Lloyd Separation of 2-methyl-1-propanol from 1-butanol by extractive distillation
DE60238218D1 (de) 2001-09-12 2010-12-16 Anormed Inc Synthese von enantiomerenreinen, aminosubstituierten kondensierten bicyclischen ringen
DE10164348A1 (de) * 2001-12-28 2003-07-17 Basf Ag Verfahren zur Herstellung von 1-Methoypropanol-2
JP2003292471A (ja) * 2002-04-03 2003-10-15 Japan Science & Technology Corp エステル縮合物の製造方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2923733A (en) * 1957-03-28 1960-02-02 Pan American Petroleum Corp Process for separating primary from secondary alcohols
CN101250094A (zh) * 2007-02-23 2008-08-27 大赛璐化学工业株式会社 1-甲氧基-2-丙醇的制备方法
CN101985418A (zh) * 2010-08-16 2011-03-16 江苏天音化工有限公司 一种制备2－甲氧基－1－丙醇醋酸酯的方法

Also Published As

Publication number Publication date
JP6246781B2 (ja) 2017-12-13
JP2016135756A (ja) 2016-07-28
TWI631102B (zh) 2018-08-01
US9440899B2 (en) 2016-09-13
US20160168064A1 (en) 2016-06-16
KR20160072788A (ko) 2016-06-23
CN105693482A (zh) 2016-06-22
TW201638062A (zh) 2016-11-01
KR101805632B1 (ko) 2017-12-08

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