CN105660740A - 一种田间大豆种植早期除草剂及其制备方法 - Google Patents

一种田间大豆种植早期除草剂及其制备方法 Download PDF

Info

Publication number
CN105660740A
CN105660740A CN201610148309.4A CN201610148309A CN105660740A CN 105660740 A CN105660740 A CN 105660740A CN 201610148309 A CN201610148309 A CN 201610148309A CN 105660740 A CN105660740 A CN 105660740A
Authority
CN
China
Prior art keywords
parts
herbicide
soybeans
heating
early period
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610148309.4A
Other languages
English (en)
Inventor
刘兴武
徐飞
傅昌群
林友军
王玉贵
李霞
蔡昌武
吴春喜
李信
戴仕明
江磊
赵忠
张妙松
邵二凯
徐文斐
李平
赵龙凯
尤墩亚
娄功君
高建华
肖尚华
臧启军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Huaxing Chemical Co Ltd
Original Assignee
Anhui Huaxing Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Huaxing Chemical Co Ltd filed Critical Anhui Huaxing Chemical Co Ltd
Priority to CN201610148309.4A priority Critical patent/CN105660740A/zh
Publication of CN105660740A publication Critical patent/CN105660740A/zh
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • A01N37/26—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof containing the group; Thio analogues thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/58—1,2-Diazines; Hydrogenated 1,2-diazines
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/66—1,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms
    • A01N43/68—1,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms with two or three nitrogen atoms directly attached to ring carbon atoms
    • A01N43/70—Diamino—1,3,5—triazines with only one oxygen, sulfur or halogen atom or only one cyano, thiocyano (—SCN), cyanato (—OCN) or azido (—N3) group directly attached to a ring carbon atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/24—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing the groups, or; Thio analogues thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/30—Derivatives containing the group >N—CO—N aryl or >N—CS—N—aryl
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10—Animals; Substances produced thereby or obtained therefrom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D1/00—Fertilisers containing potassium
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
    • C05F5/006—Waste from chemical processing of material, e.g. diestillation, roasting, cooking
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F9/00—Fertilisers from household or town refuse
    • C05F9/04—Biological compost
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • Environmental Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Virology (AREA)
  • Molecular Biology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

一种田间大豆种植早期除草剂，其各组分含量重量份为：乙草胺35-45份、莠去津35-45份、炙款冬花15-19份、炒桔梗6-9份、炙僵蚕15-18份、川贝母12-14份、炙罂粟壳5-7份、梨皮9-14份、罗汉果30-50份、醋50-60份、花生50-60份、麦芽糖50-60份、绿茶1000-1200份、橙汁70-80份、番茄汁50-70份、玉竹5-10份、黄豆200-220份、秸秆50-56份、草木灰10-15份、糖厂滤泥10-20份、1份-2份益生菌、丁醚脲10-15份、灭多威10-15份、哒螨灵10-15份、麦宝素10-15份。本发明的有益效果是：本法制备的除草剂专业用于除去田间大豆早期的杂草，不影响大豆涨势，同时除草剂溶于水后渗入地下，还可对早期大豆起到营养供给，本方法减少病虫害，优质高产，大幅提高大豆的产量，本方法所产的大豆颗粒饱满，营养丰富，适于推广。

Description

一种田间大豆种植早期除草剂及其制备方法
技术领域：
本发明设计一种田间除草剂，具体涉及一种田间大豆种植早期除草剂及其制备方法。
背景技术：
化学除草是现代农业的发展趋势，我国农田目前大部分已经广泛使用化学除草剂，产生了很大的经济效益，但是，通过对河南、河北、山东等农田化学除草的调查，发现在防除效果和除草剂品种上存在缺点，经过多年的除草剂的使用，大部分杂草均已经出现不同程度的抗性，同时现有的除草剂并非由针对初期，中期，晚期农作物长势进行相对应的除草，除草效果一般。
发明内容：
本发明所要解决的技术问题在于克服现有技术的缺陷，提供一种田间大豆种植早期除草剂及其制备方法。
本发明所要解决的技术问题采用以下技术方案来实现。
一种田间大豆种植早期除草剂，其特征在于：其各组分含量重量份为：乙草胺35-45份、莠去津35-45份、炙款冬花15-19份、炒桔梗6-9份、炙僵蚕15-18份、川贝母12-14份、炙罂粟壳5-7份、梨皮9-14份、罗汉果30-50份、醋50-60份、花生50-60份、麦芽糖50-60份、绿茶1000-1200份、橙汁70-80份、番茄汁50-70份、玉竹5-10份、黄豆200-220份、秸秆50-56份、草木灰10-15份、糖厂滤泥10-20份、1份-2份益生菌、丁醚脲10-15份、灭多威10-15份、哒螨灵10-15份、麦宝素10-15份。
其制备方法包括：
1)选取优质黄豆，脱皮；
2)取脱皮的黄豆浸泡在橙汁内，浸泡时长1-2小时，其中浸泡过程分为三段，前段浸泡温度50℃，中段浸泡温度为30℃，后段浸泡温度为50℃，且在三步浸泡过程中分别加入1/5、3/5、1/5番茄汁；
3)去浸泡后的黄豆与花生磨成浆；
4)经过100目筛过滤，得到豆浆；
5)将豆浆加热到100℃，保持20分钟，然后把豆浆放入到盛满绿茶的起皮锅内，保持温度80-90℃，加入玉竹、麦芽糖，每隔2-5分钟器豆腐皮一张，直至豆浆取完为止；
6)取步骤1)中的黄豆皮磨成粉，
7)将步骤5)中的豆腐皮放置在冰块上，冷却1-2分钟，冷却至60℃，在冷却的同时将6)中粉洒在豆腐皮上；
8)将秸秆粉碎，长度1-3厘米，与草木灰和益生菌液翻到混合，堆成宽2米，高1米，长度不限的条形锥，用塑料布盖好，经过2-3星期高温发酵，至秸秆变成褐色或黑褐色即可，然后捣碎过筛，加入糖厂滤泥混合搅拌，干燥，过筛；
9)将炙款冬花、炒桔梗、炙僵蚕、川贝母、炙罂粟壳、梨皮放置在醋中，加温浸泡30分钟，醋温度控制在80℃以上；
10)捞出浸泡后的药材，烘干，研磨；
11)放入蒸馏器中，加入500ml水进行蒸馏，收集水蒸气，得到药液；
12)将药液置于加热罐中，利用超声波加热罐体，加热，加热过程中收集水蒸气，将药液浓缩至加热罐中的药液蒸发殆尽；
13)选取新鲜的罗汉果，压榨成汁，与收集的水蒸气混合；
14)微波加热10分钟得到液体；
15)取步骤7中的豆腐皮浸泡在上步骤中的液体中，蒸馏，收集蒸馏的气体，与步骤8)中的搅拌物混合，混合静止1天；
16)将步骤15)静止后的混合料至于压榨机中，压榨出水，取水与丁醚脲、灭多威、哒螨灵、麦宝素混合；
17)加热至75℃，加入乙草胺、莠去津，搅拌10分钟，冷却，即得到除草剂。
本发明的有益效果是：本法制备的除草剂专业用于除去田间大豆早期的杂草，不影响大豆涨势，同时除草剂溶于水后渗入地下，还可对早期大豆起到营养供给，本方法减少病虫害，优质高产，大幅提高大豆的产量，本方法所产的大豆颗粒饱满，营养丰富，适于推广。
具体实施方式：
为了使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施例，进一步阐述本发明。
具体实施例1：一种田间大豆种植早期除草剂，其各组分含量重量份为：乙草胺35份、莠去津35份、炙款冬花15份、炒桔梗6份、炙僵蚕15份、川贝母12份、炙罂粟壳5份、梨皮9份、罗汉果30份、醋50份、花生50份、麦芽糖50份、绿茶1000份、橙汁70份、番茄汁50份、玉竹5份、黄豆200份、秸秆50份、草木灰10份、糖厂滤泥10份、1份益生菌、丁醚脲10份、灭多威10份、哒螨灵10份、麦宝素10份。
具体实施例2：一种田间大豆种植早期除草剂，其各组分含量重量份为：乙草胺45份、莠去津45份、炙款冬花19份、炒桔梗9份、炙僵蚕18份、川贝母14份、炙罂粟壳7份、梨皮14份、罗汉果50份、醋60份、花生60份、麦芽糖60份、绿茶1200份、橙汁80份、番茄汁70份、玉竹10份、黄豆220份、秸秆56份、草木灰15份、糖厂滤泥20份、2份益生菌、丁醚脲15份、灭多威15份、哒螨灵15份、麦宝素15份。
其制备方法包括：
1)选取优质黄豆，脱皮；
2)取脱皮的黄豆浸泡在橙汁内，浸泡时长1-2小时，其中浸泡过程分为三段，前段浸泡温度50℃，中段浸泡温度为30℃，后段浸泡温度为50℃，且在三步浸泡过程中分别加入1/5、3/5、1/5番茄汁；
3)去浸泡后的黄豆与花生磨成浆；
4)经过100目筛过滤，得到豆浆；
5)将豆浆加热到100℃，保持20分钟，然后把豆浆放入到盛满绿茶的起皮锅内，保持温度80-90℃，加入玉竹、麦芽糖，每隔2-5分钟器豆腐皮一张，直至豆浆取完为止；
6)取步骤1)中的黄豆皮磨成粉，
7)将步骤5)中的豆腐皮放置在冰块上，冷却1-2分钟，冷却至60℃，在冷却的同时将6)中粉洒在豆腐皮上；
8)将秸秆粉碎，长度1-3厘米，与草木灰和益生菌液翻到混合，堆成宽2米，高1米，长度不限的条形锥，用塑料布盖好，经过2-3星期高温发酵，至秸秆变成褐色或黑褐色即可，然后捣碎过筛，加入糖厂滤泥混合搅拌，干燥，过筛；
9)将炙款冬花、炒桔梗、炙僵蚕、川贝母、炙罂粟壳、梨皮放置在醋中，加温浸泡30分钟，醋温度控制在80℃以上；
10)捞出浸泡后的药材，烘干，研磨；
11)放入蒸馏器中，加入500ml水进行蒸馏，收集水蒸气，得到药液；
12)将药液置于加热罐中，利用超声波加热罐体，加热，加热过程中收集水蒸气，将药液浓缩至加热罐中的药液蒸发殆尽；
13)选取新鲜的罗汉果，压榨成汁，与收集的水蒸气混合；
14)微波加热10分钟得到液体；
15)取步骤7中的豆腐皮浸泡在上步骤中的液体中，蒸馏，收集蒸馏的气体，与步骤8)中的搅拌物混合，混合静止1天；
16)将步骤15)静止后的混合料至于压榨机中，压榨出水，取水与丁醚脲、灭多威、哒螨灵、麦宝素混合；
17)加热至75℃，加入乙草胺、莠去津，搅拌10分钟，冷却，即得到除草剂。
以上显示和描述了本发明的基本原理、主要特征和本发明的优点。本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。

Claims (2)

1.一种田间大豆种植早期除草剂，其特征在于：其各组分含量重量份为：乙草胺35-45份、莠去津35-45份、炙款冬花15-19份、炒桔梗6-9份、炙僵蚕15-18份、川贝母12-14份、炙罂粟壳5-7份、梨皮9-14份、罗汉果30-50份、醋50-60份、花生50-60份、麦芽糖50-60份、绿茶1000-1200份、橙汁70-80份、番茄汁50-70份、玉竹5-10份、黄豆200-220份、秸秆50-56份、草木灰10-15份、糖厂滤泥10-20份、1份-2份益生菌、丁醚脲10-15份、灭多威10-15份、哒螨灵10-15份、麦宝素10-15份。
2.根据权利要求1所述的一种田间大豆种植早期除草剂，其特征在于：其制备方法包括：
1)选取优质黄豆，脱皮；
2)取脱皮的黄豆浸泡在橙汁内，浸泡时长1-2小时，其中浸泡过程分为三段，前段浸泡温度50℃，中段浸泡温度为30℃，后段浸泡温度为50℃，且在三步浸泡过程中分别加入1/5、3/5、1/5番茄汁；
3)去浸泡后的黄豆与花生磨成浆；
4)经过100目筛过滤，得到豆浆；
5)将豆浆加热到100℃，保持20分钟，然后把豆浆放入到盛满绿茶的起皮锅内，保持温度80-90℃，加入玉竹、麦芽糖，每隔2-5分钟器豆腐皮一张，直至豆浆取完为止；
6)取步骤1)中的黄豆皮磨成粉，
7)将步骤5)中的豆腐皮放置在冰块上，冷却1-2分钟，冷却至60℃，在冷却的同时将6)中粉洒在豆腐皮上；
8)将秸秆粉碎，长度1-3厘米，与草木灰和益生菌液翻到混合，堆成宽2米，高1米，长度不限的条形锥，用塑料布盖好，经过2-3星期高温发酵，至秸秆变成褐色或黑褐色即可，然后捣碎过筛，加入糖厂滤泥混合搅拌，干燥，过筛；
9)将炙款冬花、炒桔梗、炙僵蚕、川贝母、炙罂粟壳、梨皮放置在醋中，加温浸泡30分钟，醋温度控制在80℃以上；
10)捞出浸泡后的药材，烘干，研磨；
11)放入蒸馏器中，加入500ml水进行蒸馏，收集水蒸气，得到药液；
12)将药液置于加热罐中，利用超声波加热罐体，加热，加热过程中收集水蒸气，将药液浓缩至加热罐中的药液蒸发殆尽；
13)选取新鲜的罗汉果，压榨成汁，与收集的水蒸气混合；
14)微波加热10分钟得到液体；
15)取步骤7中的豆腐皮浸泡在上步骤中的液体中，蒸馏，收集蒸馏的气体，与步骤8)中的搅拌物混合，混合静止1天；
16)将步骤15)静止后的混合料至于压榨机中，压榨出水，取水与丁醚脲、灭多威、哒螨灵、麦宝素混合；
17)加热至75℃，加入乙草胺、莠去津，搅拌10分钟，冷却，即得到除草剂。
CN201610148309.4A 2016-03-15 2016-03-15 一种田间大豆种植早期除草剂及其制备方法 Pending CN105660740A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610148309.4A CN105660740A (zh) 2016-03-15 2016-03-15 一种田间大豆种植早期除草剂及其制备方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610148309.4A CN105660740A (zh) 2016-03-15 2016-03-15 一种田间大豆种植早期除草剂及其制备方法

Publications (1)

Publication Number Publication Date
CN105660740A true CN105660740A (zh) 2016-06-15

Family

ID=56311145

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610148309.4A Pending CN105660740A (zh) 2016-03-15 2016-03-15 一种田间大豆种植早期除草剂及其制备方法

Country Status (1)

Country Link
CN (1) CN105660740A (zh)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103999719A (zh) * 2014-05-05 2014-08-27 郎溪县十字镇林华粮食种植家庭农场 一种高产水稻种植技术
CN104160898A (zh) * 2014-06-19 2014-11-26 蚌埠市禹会天河联众水产养殖农民专业合作社 集约化黄鳝饲养与水稻种植套养技术
CN104381066A (zh) * 2014-10-20 2015-03-04 郎溪县十字镇林华粮食种植家庭农场 一种高产水稻种植技术
CN104855198A (zh) * 2015-06-14 2015-08-26 安徽徽大农业有限公司 一种高产水稻种植技术

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103999719A (zh) * 2014-05-05 2014-08-27 郎溪县十字镇林华粮食种植家庭农场 一种高产水稻种植技术
CN104160898A (zh) * 2014-06-19 2014-11-26 蚌埠市禹会天河联众水产养殖农民专业合作社 集约化黄鳝饲养与水稻种植套养技术
CN104381066A (zh) * 2014-10-20 2015-03-04 郎溪县十字镇林华粮食种植家庭农场 一种高产水稻种植技术
CN104855198A (zh) * 2015-06-14 2015-08-26 安徽徽大农业有限公司 一种高产水稻种植技术

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王江柱主编，: "《农民欢迎的200种农药》", 30 April 2015 *

Similar Documents

Publication Publication Date Title
CN105613889A (zh) 柿蒂葛花保健茶精的制作方法
CN104082603A (zh) 一种配方鹅饲料及其制备方法
CN106069113A (zh) 一种高产高品质冬瓜的种植方法
CN107242492A (zh) 一种利用油莎豆粕制造油莎豆粕精粉的方法
CN103300322B (zh) 一种疙瘩丝酱菜的制备方法
CN104187566A (zh) 一种山慈菇酱的制备方法
CN107307175A (zh) 一种综合利用油莎豆粕的方法
CN105660739A (zh) 一种田间小麦种植早期除草剂及其制备方法
KR101190329B1 (ko) 꾸지뽕을 이용한 고추장 제조방법
CN105602809A (zh) 一种虎刺酒的酿造方法
CN105660746A (zh) 一种田间水稻种植早期除草剂及其制备方法
CN107410977A (zh) 一种以红薯茎叶为原料的富硒食品含片及制备方法
CN106071448A (zh) 一种地草果苣荬菜果蔬饮料的加工工艺
CN106036659A (zh) 一种辣椒叶的腌制方法
CN105660740A (zh) 一种田间大豆种植早期除草剂及其制备方法
CN105613626A (zh) 一种田间水稻种植中期除草剂及其制备方法
CN105660737A (zh) 一种田间玉米种植中期除草剂及其制备方法
CN107259474A (zh) 柠檬香辣沙蟹汁的制备方法
CN105638781A (zh) 一种田间玉米种植早期除草剂及其制备方法
CN103205342B (zh) 一种蛤蚧太白茶米酒及其制备方法
CN105981820A (zh) 一种润燥助眠蜂蜜羊奶及其制备方法
CN106367282A (zh) 一种米兰风味糯米酒的酿制方法
CN105613629A (zh) 一种田间高粱种植早期除草剂及其制备方法
CN105660738A (zh) 一种田间小麦种植中期除草剂及其制备方法
CN104187159A (zh) 一种适口膨化猪饲料及其制备方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20160615

RJ01 Rejection of invention patent application after publication