CN105603255A - 一种3d打印制备医用钛合金材料 - Google Patents
一种3d打印制备医用钛合金材料 Download PDFInfo
- Publication number
- CN105603255A CN105603255A CN201610033846.4A CN201610033846A CN105603255A CN 105603255 A CN105603255 A CN 105603255A CN 201610033846 A CN201610033846 A CN 201610033846A CN 105603255 A CN105603255 A CN 105603255A
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- titanium alloy
- powder
- annealing
- temperature
- laser
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- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 44
- 239000000956 alloy Substances 0.000 title claims abstract description 31
- 238000007639 printing Methods 0.000 title abstract description 3
- 239000000843 powder Substances 0.000 claims abstract description 45
- 238000005245 sintering Methods 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 229910045601 alloy Inorganic materials 0.000 claims abstract description 10
- 238000002360 preparation method Methods 0.000 claims abstract description 10
- 239000010936 titanium Substances 0.000 claims abstract description 8
- 229910025794 LaB6 Inorganic materials 0.000 claims abstract description 7
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 claims abstract description 7
- 238000000137 annealing Methods 0.000 claims description 43
- 238000000034 method Methods 0.000 claims description 24
- 238000001816 cooling Methods 0.000 claims description 19
- 238000010146 3D printing Methods 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 16
- 238000012545 processing Methods 0.000 claims description 13
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 12
- 238000000498 ball milling Methods 0.000 claims description 12
- 229910052593 corundum Inorganic materials 0.000 claims description 12
- 239000010431 corundum Substances 0.000 claims description 12
- 239000011812 mixed powder Substances 0.000 claims description 8
- 238000000465 moulding Methods 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 8
- 239000000919 ceramic Substances 0.000 claims description 7
- 229910052779 Neodymium Inorganic materials 0.000 claims description 6
- 229910052786 argon Inorganic materials 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 6
- 229910052802 copper Inorganic materials 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 6
- 238000007648 laser printing Methods 0.000 claims description 6
- 229910052750 molybdenum Inorganic materials 0.000 claims description 6
- 238000007493 shaping process Methods 0.000 claims description 6
- 229910052709 silver Inorganic materials 0.000 claims description 6
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 6
- 238000001291 vacuum drying Methods 0.000 claims description 6
- 229910052720 vanadium Inorganic materials 0.000 claims description 6
- 229910052727 yttrium Inorganic materials 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 4
- 238000000713 high-energy ball milling Methods 0.000 claims description 4
- 230000014759 maintenance of location Effects 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 238000012805 post-processing Methods 0.000 claims description 4
- 239000011265 semifinished product Substances 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 230000003746 surface roughness Effects 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 238000013461 design Methods 0.000 abstract description 4
- 238000005275 alloying Methods 0.000 abstract description 3
- 238000005551 mechanical alloying Methods 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 210000001519 tissue Anatomy 0.000 description 3
- 210000000988 bone and bone Anatomy 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 230000006835 compression Effects 0.000 description 2
- 238000007906 compression Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000007769 metal material Substances 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- 210000000056 organ Anatomy 0.000 description 2
- 101000911772 Homo sapiens Hsc70-interacting protein Proteins 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000003519 biomedical and dental material Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 239000007943 implant Substances 0.000 description 1
- 210000000629 knee joint Anatomy 0.000 description 1
- 239000012567 medical material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 210000003625 skull Anatomy 0.000 description 1
- 210000004872 soft tissue Anatomy 0.000 description 1
- 238000001356 surgical procedure Methods 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/60—Treatment of workpieces or articles after build-up
- B22F10/64—Treatment of workpieces or articles after build-up by thermal means
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C14/00—Alloys based on titanium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/20—Direct sintering or melting
- B22F10/25—Direct deposition of metal particles, e.g. direct metal deposition [DMD] or laser engineered net shaping [LENS]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/30—Process control
- B22F10/32—Process control of the atmosphere, e.g. composition or pressure in a building chamber
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/30—Process control
- B22F10/36—Process control of energy beam parameters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/60—Treatment of workpieces or articles after build-up
- B22F10/62—Treatment of workpieces or articles after build-up by chemical means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/60—Treatment of workpieces or articles after build-up
- B22F10/68—Cleaning or washing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/24—After-treatment of workpieces or articles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
- B33Y10/00—Processes of additive manufacturing
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/04—Making non-ferrous alloys by powder metallurgy
- C22C1/05—Mixtures of metal powder with non-metallic powder
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C32/00—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ
- C22C32/001—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with only oxides
- C22C32/0015—Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with only oxides with only single oxides as main non-metallic constituents
- C22C32/0031—Matrix based on refractory metals, W, Mo, Nb, Hf, Ta, Zr, Ti, V or alloys thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/24—After-treatment of workpieces or articles
- B22F2003/247—Removing material: carving, cleaning, grinding, hobbing, honing, lapping, polishing, milling, shaving, skiving, turning the surface
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/24—After-treatment of workpieces or articles
- B22F2003/248—Thermal after-treatment
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
Abstract
Description
Claims (6)
Priority Applications (1)
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CN201610033846.4A CN105603255B (zh) | 2016-01-19 | 2016-01-19 | 一种3d打印制备医用钛合金材料 |
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CN201610033846.4A CN105603255B (zh) | 2016-01-19 | 2016-01-19 | 一种3d打印制备医用钛合金材料 |
Publications (2)
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CN105603255A true CN105603255A (zh) | 2016-05-25 |
CN105603255B CN105603255B (zh) | 2017-12-12 |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107058799A (zh) * | 2017-01-22 | 2017-08-18 | 康硕电气集团有限公司 | 一种含铼3d打印用钛基合金材料及其制备方法 |
CN107802886A (zh) * | 2017-12-12 | 2018-03-16 | 成都育芽科技有限公司 | 一种3d打印用钛合金人工骨骼材料及制备方法 |
CN109079147A (zh) * | 2018-10-11 | 2018-12-25 | 宝鸡文理学院 | 一种钛基生物合金材料的制备方法 |
PL423273A1 (pl) * | 2017-10-25 | 2019-05-06 | Politechnika Poznanska | Sposób wytwarzania bionanomateriału na bazie tytanu i molibdenu o strukturze jednofazowej β |
CN110499438A (zh) * | 2019-09-30 | 2019-11-26 | 广东省航空航天装备技术研究所 | 材料组合物、钛合金制品及其制备方法 |
CN110863125A (zh) * | 2019-11-28 | 2020-03-06 | 江阴市万里锻件有限公司 | 一种精密加工车床车刀用合金及其制备方法 |
CN114762895A (zh) * | 2022-05-12 | 2022-07-19 | 黑龙江省科学院高技术研究院 | 一种稀土氧化物增强钛基复合材料的制备方法 |
CN115094270A (zh) * | 2022-07-12 | 2022-09-23 | 承德石油高等专科学校 | 一种含Ni、Co、Sc的高强增材制造Ti-Al-V合金其制备方法 |
Citations (7)
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JPH03219035A (ja) * | 1989-10-13 | 1991-09-26 | Honda Motor Co Ltd | 高強度構造部材用チタン基合金、高強度構造部材用チタン基合金の製造方法およびチタン基合金製高強度構造部材の製造方法 |
CN101962721A (zh) * | 2010-11-02 | 2011-02-02 | 中南大学 | 一种粉末冶金钛合金及其制备方法 |
WO2011133132A1 (en) * | 2010-03-29 | 2011-10-27 | Lee Robert G | Composite system |
CN104831119A (zh) * | 2015-04-15 | 2015-08-12 | 苏州维泰生物技术有限公司 | 一种关节用钛合金材料及其制备方法 |
CN104928513A (zh) * | 2015-07-09 | 2015-09-23 | 哈尔滨工业大学 | 一种钛合金激光3d打印改进方法 |
CN105002395A (zh) * | 2015-07-15 | 2015-10-28 | 大连理工大学 | Ti基Ti-Fe-Zr-Y生物医用合金及其制备方法 |
CN105014073A (zh) * | 2015-08-18 | 2015-11-04 | 上海航天精密机械研究所 | 一种tc4钛合金激光选区熔化增材制造及热处理方法 |
-
2016
- 2016-01-19 CN CN201610033846.4A patent/CN105603255B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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JPH03219035A (ja) * | 1989-10-13 | 1991-09-26 | Honda Motor Co Ltd | 高強度構造部材用チタン基合金、高強度構造部材用チタン基合金の製造方法およびチタン基合金製高強度構造部材の製造方法 |
WO2011133132A1 (en) * | 2010-03-29 | 2011-10-27 | Lee Robert G | Composite system |
CN101962721A (zh) * | 2010-11-02 | 2011-02-02 | 中南大学 | 一种粉末冶金钛合金及其制备方法 |
CN104831119A (zh) * | 2015-04-15 | 2015-08-12 | 苏州维泰生物技术有限公司 | 一种关节用钛合金材料及其制备方法 |
CN104928513A (zh) * | 2015-07-09 | 2015-09-23 | 哈尔滨工业大学 | 一种钛合金激光3d打印改进方法 |
CN105002395A (zh) * | 2015-07-15 | 2015-10-28 | 大连理工大学 | Ti基Ti-Fe-Zr-Y生物医用合金及其制备方法 |
CN105014073A (zh) * | 2015-08-18 | 2015-11-04 | 上海航天精密机械研究所 | 一种tc4钛合金激光选区熔化增材制造及热处理方法 |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107058799A (zh) * | 2017-01-22 | 2017-08-18 | 康硕电气集团有限公司 | 一种含铼3d打印用钛基合金材料及其制备方法 |
CN107058799B (zh) * | 2017-01-22 | 2019-09-20 | 康硕电气集团有限公司 | 一种含铼3d打印用钛基合金材料及其制备方法 |
PL423273A1 (pl) * | 2017-10-25 | 2019-05-06 | Politechnika Poznanska | Sposób wytwarzania bionanomateriału na bazie tytanu i molibdenu o strukturze jednofazowej β |
CN107802886A (zh) * | 2017-12-12 | 2018-03-16 | 成都育芽科技有限公司 | 一种3d打印用钛合金人工骨骼材料及制备方法 |
CN109079147A (zh) * | 2018-10-11 | 2018-12-25 | 宝鸡文理学院 | 一种钛基生物合金材料的制备方法 |
CN109079147B (zh) * | 2018-10-11 | 2021-09-24 | 宝鸡文理学院 | 一种钛基生物合金材料的制备方法 |
CN110499438A (zh) * | 2019-09-30 | 2019-11-26 | 广东省航空航天装备技术研究所 | 材料组合物、钛合金制品及其制备方法 |
CN110863125A (zh) * | 2019-11-28 | 2020-03-06 | 江阴市万里锻件有限公司 | 一种精密加工车床车刀用合金及其制备方法 |
CN114762895A (zh) * | 2022-05-12 | 2022-07-19 | 黑龙江省科学院高技术研究院 | 一种稀土氧化物增强钛基复合材料的制备方法 |
CN115094270A (zh) * | 2022-07-12 | 2022-09-23 | 承德石油高等专科学校 | 一种含Ni、Co、Sc的高强增材制造Ti-Al-V合金其制备方法 |
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