CN105517975A - 陶瓷的快速烧制方法 - Google Patents
陶瓷的快速烧制方法 Download PDFInfo
- Publication number
- CN105517975A CN105517975A CN201480025700.4A CN201480025700A CN105517975A CN 105517975 A CN105517975 A CN 105517975A CN 201480025700 A CN201480025700 A CN 201480025700A CN 105517975 A CN105517975 A CN 105517975A
- Authority
- CN
- China
- Prior art keywords
- honeycomb ceramic
- ceramic body
- heating rate
- temperature
- inches
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000919 ceramic Substances 0.000 title claims abstract description 206
- 238000000034 method Methods 0.000 title claims abstract description 81
- 238000010304 firing Methods 0.000 title claims abstract description 21
- 238000010438 heat treatment Methods 0.000 claims abstract description 184
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 22
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 53
- 229910052760 oxygen Inorganic materials 0.000 claims description 53
- 239000001301 oxygen Substances 0.000 claims description 53
- 239000007789 gas Substances 0.000 claims description 37
- 238000012423 maintenance Methods 0.000 claims description 16
- 229910052878 cordierite Inorganic materials 0.000 claims description 12
- JSKIRARMQDRGJZ-UHFFFAOYSA-N dimagnesium dioxido-bis[(1-oxido-3-oxo-2,4,6,8,9-pentaoxa-1,3-disila-5,7-dialuminabicyclo[3.3.1]nonan-7-yl)oxy]silane Chemical compound [Mg++].[Mg++].[O-][Si]([O-])(O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2)O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2 JSKIRARMQDRGJZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000010439 graphite Substances 0.000 claims description 5
- 229910002804 graphite Inorganic materials 0.000 claims description 5
- 239000004927 clay Substances 0.000 claims description 4
- 239000000454 talc Substances 0.000 claims description 4
- 229910052623 talc Inorganic materials 0.000 claims description 4
- 235000012222 talc Nutrition 0.000 claims description 4
- 229910052570 clay Inorganic materials 0.000 claims description 3
- 241000264877 Hippospongia communis Species 0.000 description 155
- 238000005336 cracking Methods 0.000 description 32
- 238000010411 cooking Methods 0.000 description 16
- 230000008859 change Effects 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- 239000000203 mixture Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- 238000005245 sintering Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 230000004048 modification Effects 0.000 description 5
- 238000012986 modification Methods 0.000 description 5
- 239000011148 porous material Substances 0.000 description 5
- 230000008569 process Effects 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 238000009770 conventional sintering Methods 0.000 description 3
- 239000011368 organic material Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000008602 contraction Effects 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000012855 volatile organic compound Substances 0.000 description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 238000010793 Steam injection (oil industry) Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000036284 oxygen consumption Effects 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/0006—Honeycomb structures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
- C04B35/195—Alkaline earth aluminosilicates, e.g. cordierite or anorthite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/0038—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by superficial sintering or bonding of particulate matter
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/34—Non-shrinking or non-cracking materials
- C04B2111/343—Crack resistant materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
- C04B2235/6583—Oxygen containing atmosphere, e.g. with changing oxygen pressures
- C04B2235/6584—Oxygen containing atmosphere, e.g. with changing oxygen pressures at an oxygen percentage below that of air
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/658—Atmosphere during thermal treatment
- C04B2235/6588—Water vapor containing atmospheres
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9607—Thermal properties, e.g. thermal expansion coefficient
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Filtering Materials (AREA)
- Porous Artificial Stone Or Porous Ceramic Products (AREA)
- Compositions Of Oxide Ceramics (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361775027P | 2013-03-08 | 2013-03-08 | |
| US61/775,027 | 2013-03-08 | ||
| PCT/US2014/020202 WO2014138015A1 (en) | 2013-03-08 | 2014-03-04 | Fast firing method for ceramics |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105517975A true CN105517975A (zh) | 2016-04-20 |
Family
ID=50288343
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201480025700.4A Pending CN105517975A (zh) | 2013-03-08 | 2014-03-04 | 陶瓷的快速烧制方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US10000424B2 (https=) |
| EP (1) | EP2964587B1 (https=) |
| JP (3) | JP2016513615A (https=) |
| CN (1) | CN105517975A (https=) |
| PL (1) | PL2964587T3 (https=) |
| WO (1) | WO2014138015A1 (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115867519A (zh) * | 2020-08-31 | 2023-03-28 | 康宁股份有限公司 | 用于陶瓷制造的高氧快速烧制方法 |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105517975A (zh) | 2013-03-08 | 2016-04-20 | 康宁股份有限公司 | 陶瓷的快速烧制方法 |
| US9452578B2 (en) | 2013-07-26 | 2016-09-27 | Corning Incorporated | Fast firing method for high porosity ceramics |
| US9446560B2 (en) * | 2013-07-26 | 2016-09-20 | Corning Incorporated | Fast firing method for high porosity ceramics |
| JP2018520970A (ja) * | 2015-05-07 | 2018-08-02 | コーニング インコーポレイテッド | セラミックハニカム体を焼成する方法 |
| JP6691493B2 (ja) * | 2017-02-24 | 2020-04-28 | 日本碍子株式会社 | セラミック体の製造方法 |
| US11661379B2 (en) | 2017-07-21 | 2023-05-30 | Corning Incorporated | Methods of extracting volatiles from ceramic green bodies |
| JP7022593B2 (ja) * | 2018-01-15 | 2022-02-18 | 日本碍子株式会社 | セラミックス焼成体の製造方法、及びセラミックス成形体の焼成方法 |
| CN117776761B (zh) * | 2023-12-27 | 2026-01-27 | 云南菲尔特环保科技股份有限公司 | 一种弱氧化低温烧结碳化硅蜂窝陶瓷载体的方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1272833A (zh) * | 1997-10-03 | 2000-11-08 | 康宁股份有限公司 | 陶瓷蜂窝体的烧制方法 |
| CN1431978A (zh) * | 2000-06-05 | 2003-07-23 | 普莱克斯技术有限公司 | 脱出陶瓷坯件中有机粘结剂的方法 |
| WO2012074944A1 (en) * | 2010-11-30 | 2012-06-07 | Corning Incorporated | Ceramic processing firing |
| CN102639459A (zh) * | 2009-11-30 | 2012-08-15 | 康宁股份有限公司 | 控制烧制陶瓷制品中孔尺寸分布的方法 |
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|---|---|---|---|---|
| JPH0745348B2 (ja) * | 1988-02-10 | 1995-05-17 | 日本碍子株式会社 | セラミックハニカム構造体の焼成法 |
| US6225733B1 (en) | 1997-11-18 | 2001-05-01 | Corning Incorporated | Activated carbon electrodes for electrical double layer capacitors |
| DE69841628D1 (de) * | 1997-12-02 | 2010-06-02 | Corning Inc | Verfahren zum brennen von keramischen honigwabenstrukturen |
| EP1042250A4 (en) | 1997-12-02 | 2004-04-28 | Corning Inc | METHOD FOR BURNING CERAMIC HONEYCOMB BODIES |
| MXPA02011870A (es) * | 2000-06-01 | 2003-04-10 | Corning Inc | Cuerpo de cordierita. |
| JP2002160976A (ja) | 2000-11-21 | 2002-06-04 | Hitachi Metals Ltd | セラミックハニカム構造体の製造方法 |
| DE60222225T2 (de) * | 2001-12-03 | 2008-06-12 | Hitachi Metals, Ltd. | Keramischer Wabenfilter |
| US6849181B2 (en) | 2002-07-31 | 2005-02-01 | Corning Incorporated | Mullite-aluminum titanate diesel exhaust filter |
| JP2004292292A (ja) * | 2003-03-28 | 2004-10-21 | Hitachi Metals Ltd | セラミックハニカム構造体の焼成方法 |
| EP2444766B1 (en) * | 2003-07-15 | 2014-04-09 | NGK Insulators, Ltd. | Firing furnace and method for firing |
| EP3087949B1 (en) | 2004-06-14 | 2018-07-25 | Boston Scientific Limited | System relating to implantable supportive slings |
| EP1816101B1 (en) * | 2004-10-26 | 2012-08-22 | NGK Insulators, Ltd. | Industrial furnace with steam reforming apparatus and method for steam reforming using the same |
| JP2008545612A (ja) * | 2005-05-31 | 2008-12-18 | コーニング インコーポレイテッド | 細孔形成剤の組合せを含有するチタン酸アルミニウムセラミック形成バッチ混合物および未焼成体、および同混合物および未焼成体の製造および焼成方法 |
| US20070254798A1 (en) | 2006-03-31 | 2007-11-01 | Addiego William P | Peroxide containing compounds as pore formers in the manufacture of ceramic articles |
| US7883563B2 (en) * | 2006-04-25 | 2011-02-08 | Sharp Kabushiki Kaisha | Honeycomb structure and manufacturing method thereof, and air cleaner and water purifier containing the honeycomb structure |
| US20070265161A1 (en) | 2006-05-11 | 2007-11-15 | Gadkaree Kishor P | Activated carbon honeycomb catalyst beds and methods for the manufacture of same |
| US8093351B2 (en) | 2006-08-24 | 2012-01-10 | Cornell Research Foundation, Inc. | Copolymerization of propylene oxide and carbon dioxide and homopolymerization of propylene oxide |
| JP2010501467A (ja) * | 2006-08-25 | 2010-01-21 | コーニング インコーポレイテッド | 低背圧の多孔質コージエライトセラミックハニカム物品およびその製造方法 |
| EP2078553B1 (en) * | 2006-09-29 | 2013-02-27 | Hitachi Metals, Ltd. | Process for producing cordierite ceramic honeycomb filter |
| EP2083000B1 (en) * | 2006-10-31 | 2019-12-04 | NGK Insulators, Ltd. | Method for pretreating honeycomb formed article before firing |
| EP2030957A1 (en) | 2007-08-28 | 2009-03-04 | Corning Incorporated | Fugitive pore former for porous ceramic articles |
| US20090298670A1 (en) | 2008-05-27 | 2009-12-03 | Martin Joseph Murtagh | Method for removing graphite from cordierite bodies |
| US8101117B2 (en) | 2008-05-30 | 2012-01-24 | Corning, Incorporated | Controlled gas pore formers in extruded ware |
| US20100052197A1 (en) * | 2008-08-27 | 2010-03-04 | Thomas James Deneka | Method for Manufacturing Ceramic Honeycombs |
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| JP5443723B2 (ja) | 2008-10-02 | 2014-03-19 | Dowaエレクトロニクス株式会社 | 磁性粒子、キャリア芯材およびその製造法並びにキャリアおよび現像剤 |
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| WO2011064854A1 (ja) * | 2009-11-25 | 2011-06-03 | イビデン株式会社 | セラミック焼成体の製造方法及びハニカム構造体の製造方法 |
| US9393752B2 (en) | 2010-10-29 | 2016-07-19 | Sumitomo Chemical Company, Limited | Method for producing fired body and firing furnace used therefor |
| US20130269303A1 (en) | 2010-12-17 | 2013-10-17 | Sumitomo Chemical Company, Limited | Green formed body, and process for production of honeycomb structure |
| CN103459655B (zh) * | 2011-03-24 | 2016-02-03 | 出光兴产株式会社 | 烧结体及其制造方法 |
| CN103517885B (zh) * | 2012-01-06 | 2016-09-28 | 康宁股份有限公司 | 陶瓷加工烧制 |
| CN103145439B (zh) * | 2013-02-21 | 2014-09-17 | 安徽中鼎美达环保科技有限公司 | 一种高热导率、超低膨胀系数的蜂窝多孔陶瓷 |
| CN105517975A (zh) | 2013-03-08 | 2016-04-20 | 康宁股份有限公司 | 陶瓷的快速烧制方法 |
-
2014
- 2014-03-04 CN CN201480025700.4A patent/CN105517975A/zh active Pending
- 2014-03-04 US US14/196,163 patent/US10000424B2/en active Active
- 2014-03-04 PL PL14710764T patent/PL2964587T3/pl unknown
- 2014-03-04 JP JP2015561527A patent/JP2016513615A/ja active Pending
- 2014-03-04 EP EP14710764.3A patent/EP2964587B1/en active Active
- 2014-03-04 WO PCT/US2014/020202 patent/WO2014138015A1/en not_active Ceased
-
2018
- 2018-06-20 JP JP2018116929A patent/JP2018184342A/ja active Pending
- 2018-06-20 JP JP2018116932A patent/JP2018184343A/ja active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1272833A (zh) * | 1997-10-03 | 2000-11-08 | 康宁股份有限公司 | 陶瓷蜂窝体的烧制方法 |
| CN1431978A (zh) * | 2000-06-05 | 2003-07-23 | 普莱克斯技术有限公司 | 脱出陶瓷坯件中有机粘结剂的方法 |
| CN102639459A (zh) * | 2009-11-30 | 2012-08-15 | 康宁股份有限公司 | 控制烧制陶瓷制品中孔尺寸分布的方法 |
| WO2012074944A1 (en) * | 2010-11-30 | 2012-06-07 | Corning Incorporated | Ceramic processing firing |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115867519A (zh) * | 2020-08-31 | 2023-03-28 | 康宁股份有限公司 | 用于陶瓷制造的高氧快速烧制方法 |
| US12281046B2 (en) | 2020-08-31 | 2025-04-22 | Corning Incorporated | High oxygen fast firing methods for ceramics manufacture |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2964587B1 (en) | 2019-06-19 |
| PL2964587T3 (pl) | 2019-12-31 |
| EP2964587A1 (en) | 2016-01-13 |
| WO2014138015A1 (en) | 2014-09-12 |
| US20140252695A1 (en) | 2014-09-11 |
| JP2016513615A (ja) | 2016-05-16 |
| US10000424B2 (en) | 2018-06-19 |
| JP2018184342A (ja) | 2018-11-22 |
| JP2018184343A (ja) | 2018-11-22 |
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