CN105495570B - A kind of manufacturing method of dendrobium candidum suspended gel - Google Patents
A kind of manufacturing method of dendrobium candidum suspended gel Download PDFInfo
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- CN105495570B CN105495570B CN201510859250.5A CN201510859250A CN105495570B CN 105495570 B CN105495570 B CN 105495570B CN 201510859250 A CN201510859250 A CN 201510859250A CN 105495570 B CN105495570 B CN 105495570B
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- 241000026010 Dendrobium candidum Species 0.000 title claims abstract description 221
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- 239000006185 dispersion Substances 0.000 claims abstract description 66
- 239000007788 liquid Substances 0.000 claims abstract description 58
- 238000003756 stirring Methods 0.000 claims abstract description 42
- 239000000839 emulsion Substances 0.000 claims abstract description 37
- 241000196324 Embryophyta Species 0.000 claims abstract description 30
- 239000002002 slurry Substances 0.000 claims abstract description 28
- 238000002156 mixing Methods 0.000 claims abstract description 24
- 238000000034 method Methods 0.000 claims abstract description 23
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 16
- 238000001879 gelation Methods 0.000 claims abstract description 11
- 239000000725 suspension Substances 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims abstract description 6
- 230000001954 sterilising effect Effects 0.000 claims description 51
- 239000002270 dispersing agent Substances 0.000 claims description 50
- 238000004659 sterilization and disinfection Methods 0.000 claims description 41
- 239000000843 powder Substances 0.000 claims description 37
- 239000003995 emulsifying agent Substances 0.000 claims description 35
- 239000003292 glue Substances 0.000 claims description 31
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 28
- 229920001285 xanthan gum Polymers 0.000 claims description 21
- 239000000230 xanthan gum Substances 0.000 claims description 21
- 235000010493 xanthan gum Nutrition 0.000 claims description 21
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- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 17
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 17
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 17
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 239000003795 chemical substances by application Substances 0.000 claims description 16
- -1 alginic acid sodium salt Chemical class 0.000 claims description 15
- 229920002907 Guar gum Polymers 0.000 claims description 14
- 239000000665 guar gum Substances 0.000 claims description 14
- 235000010417 guar gum Nutrition 0.000 claims description 14
- 229960002154 guar gum Drugs 0.000 claims description 14
- 229910052742 iron Inorganic materials 0.000 claims description 14
- 239000000796 flavoring agent Substances 0.000 claims description 13
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- 235000010443 alginic acid Nutrition 0.000 claims description 12
- 239000000783 alginic acid Substances 0.000 claims description 12
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- 235000013355 food flavoring agent Nutrition 0.000 claims description 12
- 235000003599 food sweetener Nutrition 0.000 claims description 12
- 239000003755 preservative agent Substances 0.000 claims description 12
- 230000002335 preservative effect Effects 0.000 claims description 12
- 239000003765 sweetening agent Substances 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 11
- 229920000161 Locust bean gum Polymers 0.000 claims description 10
- 235000010420 locust bean gum Nutrition 0.000 claims description 10
- 239000000711 locust bean gum Substances 0.000 claims description 10
- 229940105329 carboxymethylcellulose Drugs 0.000 claims description 8
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 claims description 6
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 6
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical group CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 6
- 244000247812 Amorphophallus rivieri Species 0.000 claims description 6
- 235000001206 Amorphophallus rivieri Nutrition 0.000 claims description 6
- 229920002581 Glucomannan Polymers 0.000 claims description 6
- 229920002752 Konjac Polymers 0.000 claims description 6
- 229930006000 Sucrose Natural products 0.000 claims description 6
- 235000010418 carrageenan Nutrition 0.000 claims description 6
- 239000000679 carrageenan Substances 0.000 claims description 6
- 229920001525 carrageenan Polymers 0.000 claims description 6
- 229940113118 carrageenan Drugs 0.000 claims description 6
- 229940046240 glucomannan Drugs 0.000 claims description 6
- 239000000252 konjac Substances 0.000 claims description 6
- 235000010485 konjac Nutrition 0.000 claims description 6
- 229940083466 soybean lecithin Drugs 0.000 claims description 6
- 239000005720 sucrose Substances 0.000 claims description 6
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 6
- 229920000881 Modified starch Polymers 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 239000004575 stone Substances 0.000 claims description 5
- 241000894006 Bacteria Species 0.000 claims description 2
- 239000006071 cream Substances 0.000 claims 2
- 238000004945 emulsification Methods 0.000 claims 1
- 238000009461 vacuum packaging Methods 0.000 abstract description 10
- 238000010521 absorption reaction Methods 0.000 abstract description 8
- 239000000470 constituent Substances 0.000 abstract description 5
- 239000004480 active ingredient Substances 0.000 abstract description 2
- 238000012856 packing Methods 0.000 description 9
- 240000004638 Dendrobium nobile Species 0.000 description 8
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- 239000003814 drug Substances 0.000 description 4
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- 238000011068 loading method Methods 0.000 description 4
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- 229920000609 methyl cellulose Polymers 0.000 description 4
- 239000001923 methylcellulose Substances 0.000 description 4
- 235000010981 methylcellulose Nutrition 0.000 description 4
- 150000004781 alginic acids Chemical group 0.000 description 3
- 239000008280 blood Substances 0.000 description 3
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- 230000007547 defect Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 159000000000 sodium salts Chemical class 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 210000000988 bone and bone Anatomy 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- NOESYZHRGYRDHS-UHFFFAOYSA-N insulin Chemical compound N1C(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(NC(=O)CN)C(C)CC)CSSCC(C(NC(CO)C(=O)NC(CC(C)C)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CCC(N)=O)C(=O)NC(CC(C)C)C(=O)NC(CCC(O)=O)C(=O)NC(CC(N)=O)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CSSCC(NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2C=CC(O)=CC=2)NC(=O)C(CC(C)C)NC(=O)C(C)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2NC=NC=2)NC(=O)C(CO)NC(=O)CNC2=O)C(=O)NCC(=O)NC(CCC(O)=O)C(=O)NC(CCCNC(N)=N)C(=O)NCC(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC(O)=CC=3)C(=O)NC(C(C)O)C(=O)N3C(CCC3)C(=O)NC(CCCCN)C(=O)NC(C)C(O)=O)C(=O)NC(CC(N)=O)C(O)=O)=O)NC(=O)C(C(C)CC)NC(=O)C(CO)NC(=O)C(C(C)O)NC(=O)C1CSSCC2NC(=O)C(CC(C)C)NC(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CC(N)=O)NC(=O)C(NC(=O)C(N)CC=1C=CC=CC=1)C(C)C)CC1=CN=CN1 NOESYZHRGYRDHS-UHFFFAOYSA-N 0.000 description 2
- 210000003097 mucus Anatomy 0.000 description 2
- 239000002088 nanocapsule Substances 0.000 description 2
- 238000009928 pasteurization Methods 0.000 description 2
- 210000002784 stomach Anatomy 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 210000001519 tissue Anatomy 0.000 description 2
- 235000015961 tonic Nutrition 0.000 description 2
- 230000001256 tonic effect Effects 0.000 description 2
- 206010010144 Completed suicide Diseases 0.000 description 1
- 244000241257 Cucumis melo Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- RYAHJFGVOCZDEI-UFFNCVEVSA-N Dendrobine Chemical compound C([C@H]1CC[C@@H]2[C@@]31C)N(C)[C@@H]3[C@H]1[C@@H](C(C)C)[C@@H]2C(=O)O1 RYAHJFGVOCZDEI-UFFNCVEVSA-N 0.000 description 1
- 241001523681 Dendrobium Species 0.000 description 1
- 241001076416 Dendrobium tosaense Species 0.000 description 1
- 208000007882 Gastritis Diseases 0.000 description 1
- 241000594394 Hedyotis Species 0.000 description 1
- 102000004877 Insulin Human genes 0.000 description 1
- 108090001061 Insulin Proteins 0.000 description 1
- 241001646834 Mesona Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 241000233855 Orchidaceae Species 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 description 1
- 201000001352 cholecystitis Diseases 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- RYAHJFGVOCZDEI-CZKZLRAZSA-N dendrobine Natural products O=C1O[C@@H]2[C@H](C(C)C)[C@H]1[C@H]1[C@@]3(C)[C@@H]2N(C)C[C@H]3CC1 RYAHJFGVOCZDEI-CZKZLRAZSA-N 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 230000004438 eyesight Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 210000000232 gallbladder Anatomy 0.000 description 1
- 208000006454 hepatitis Diseases 0.000 description 1
- 231100000283 hepatitis Toxicity 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 229940125396 insulin Drugs 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 150000004804 polysaccharides Chemical class 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 235000012976 tarts Nutrition 0.000 description 1
- 229960000716 tonics Drugs 0.000 description 1
- 210000004881 tumor cell Anatomy 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines Containing Plant Substances (AREA)
- Medicinal Preparation (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
A kind of manufacturing method of dendrobium candidum suspended gel, its process flow are as follows: 1) dendrobium candidum Fresh Plants being cleaned the impurity such as removal silt, obtain clean dendrobium candidum Fresh Plants；2) 1. clean dendrobium candidum Fresh Plants cauline leaf is separated, obtains dendrobium candidum stem and leaf；2. mixing after dendrobium candidum stem and leaf are distinguished pulp, dendrobium candidum slurries are obtained；3. dendrobium candidum slurries are dispersed agent dispersion, dendrobium candidum dispersion liquid is obtained；4. dendrobium candidum dispersion liquid is emulsified, dendrobium candidum emulsion is obtained；5. by dendrobium candidum emulsion add formula, stir and evenly mix, sterilize and vacuum dispense, obtain dendrobium candidum emulsifying product；6. adding formula, stirring and evenly mixing, sterilize simultaneously vacuum packing, obtain dendrobium candidum suspended gel product dendrobium candidum emulsion suspension gelation；The suspended gel product of the method for the present invention production almost includes and protects whole active constituents of dendrobium candidum; convenient, absorption easy to digest, human body almost can absorb its all active ingredient; absorption efficiency is significantly higher than other dendrobium candidum products, up to 95% or more.
Description
Technical field
The present invention relates to a kind of dendrobium candidum suspended gel eat dosage form manufacturing method, especially it is a kind of it is convenient,
Effective component is not easy to be oxidized the manufacturing method of the high dendrobium candidum new product of destruction, human consumption's absorption and use efficiency, belongs to
Food, field of health care products.
Background technique
Dendrobium candidum also known as ribbed hedyotis herb belong to micro- specific item, the perennial herbaceous plant that grows nonparasitically upon another plant of orchid family.Stem is upright, cylindrical, long 9-
35cm, thick 2-8mm, sepal and petal yellow green, long round shape lanceolar are about 1.8cm, wide 4-5mm, the month at florescence 3-6.Main point
Cloth is on Anhui, Fujian, Zhejiang, Yunnan and other places.Stem can be used as medicine, and belong to the yin tonics in tonic.
The medicinal component of dendrobium candidum mainly has dendrobium polysaccharide, dendrobine and total amino acid etc..Its main function has: one
It is to nourish yin jin, there is the gas-liquid for growing lung stomach, moisten body internal organs, brains bone, inhibits the effect of sun Kang Huodong；Second is that enhancing
Constitution has nourishing yin and nourishing blood, enhances the effect of immune function；Third is that strengthening the spleen and stomach, protecting gallbladder benefit liver, by force through bone strengthening, has and nourish
Liver-yin helps to treat the effect of hepatitis, cholecystitis, some gastritis；Fourth is that reducing blood glucose, there is enhancing insulin active and show
Write the effect for reducing blood glucose level；Fifth is that inhibiting tumour, have the function of killing certain tumour cells；Sixth is that the bright eye of improving eyesight, taste
It supports skin, promote longevity, have the function of that enriching yin is supported mesh, moisturized the skin, macrobiosis of making light of one's life by commiting suicide.
Currently, the major product of Tiepi Fengdou has in the market: first is that the fresh item of dendrobium candidum, major defect is without place
Reason is not easy transport and preservation；Second is that iron and bor on compound, its major defect is that edible crowd is limited, vegetarian, certain religions
Personage's inedibility because its capsule shells animal glue multi-purpose greatly is made, and will cause the loss of part effective ingredient in process；Three
It is dendrobium officinale powder, major defect is that the big effective component of surface area is oxidized easily, and packing instructions are stringent.
Dendrobium candidum is a kind of rare traditional Chinese medicine, is acknowledged as the diamond health superfine product of most significant end, and many critical
The help mesona that patient dreams of.It therefore, is efficiently the highest of dendrobium candidum product using the effective ingredient contained by it comprehensively
It pursues.A kind of manufacturing method for dendrobium candidum suspended gel that this patent provides, the dendrobium candidum suspended gel of this method production
It almost include all compositions of dendrobium candidum, meanwhile, it can be well protected effective component therein, human body is bright to its absorption efficiency
It is aobvious to be higher than other products, up to 95% or more.
Summary of the invention
It is using modern biochemistry the purpose of the present invention is to provide a kind of manufacturing method of dendrobium candidum suspended gel
Technology and food drug forward position processing technology principle, form nanoscale and micron order capsule, effective protection iron sheet stone using emulsifying technology
The active constituent of dry measure used in former times, reapplies gel technique, and nanoscale and micron order capsule are protected, finally again using suspended gel technology
Secondary protection nanocapsule and micron capsule, and form suspended gel liquid similar with human body inner tissue mucus.The suspension of this method production
Gel products not only almost include and protect whole active constituents of dendrobium candidum, meanwhile, convenient, absorption easy to digest,
Human body almost can absorb its all active ingredient, and absorption efficiency is significantly higher than other dendrobium candidum products, up to 95% or more.
To achieve the goals above, the technical scheme adopted by the invention is that: a kind of manufacture of dendrobium candidum suspended gel
Method, which is characterized in that it includes the following steps:
1) dendrobium candidum Fresh Plants are cleaned into the impurity such as removal silt, obtains clean dendrobium candidum Fresh Plants；
2) clean dendrobium candidum Fresh Plants point two ways is handled；
Processing one: 1. separating clean dendrobium candidum Fresh Plants cauline leaf, obtains dendrobium candidum stem and leaf；2. by iron sheet stone
Dry measure used in former times stem and leaf mix after distinguishing pulp, obtain dendrobium candidum slurries；3. dendrobium candidum slurries are dispersed agent dispersion, iron sheet is obtained
Dendrobium nobile dispersion liquid；4. dendrobium candidum dispersion liquid is emulsified, dendrobium candidum emulsion is obtained；Match 5. dendrobium candidum emulsion is added
Side stirs and evenly mixs, sterilizes simultaneously vacuum packing, obtains dendrobium candidum emulsifying product；6. by dendrobium candidum emulsion suspension gelation,
Add formula, stir and evenly mix, sterilize simultaneously vacuum packing, obtains dendrobium candidum suspended gel product；
Processing two: clean dendrobium candidum Fresh Plants are 1. obtained into dendrobium candidum hay through frozen drying；2. by iron
Skin dendrobium nobile hay is crushed to 80-500 mesh, obtains dendrobium candidum dry powder；3. dendrobium candidum dry powder is dispersed agent dispersion, iron is obtained
Skin dendrobium nobile dry powder dispersion liquid；4. dendrobium candidum dry powder dispersion liquid is emulsified, dendrobium candidum dry powder emulsion is obtained；5. by iron sheet stone
Dry measure used in former times emulsion adds formula, stirs and evenly mixs, sterilizes simultaneously vacuum packing, obtains dendrobium candidum emulsifying product；6. by dendrobium candidum dry powder
Glue suspension gelation is added in emulsion, adds formula, stirs and evenly mixs, sterilizes simultaneously vacuum packing, obtains dendrobium candidum dry powder and suspend
Gel products.
The step 3. in, dispersing agent weigh in proportion it is good after, need preprocessed, mix, add water and stir to being completely dissolved,
Obtain dispersant solution；The pretreatment refers to sterilizing, disinfection and crushing to dispersing agent；The dispersing agent sterilization
Method includes but is not limited to: ultraviolet sterilization, high-temperature sterilization, microwave sterilization；It is molten that the dendrobium candidum slurries are added to dispersing agent
In liquid, or dispersant solution is added in dendrobium candidum slurries, Stirring, speed is 500-15000 revs/min, no
Disconnected stirring 5-30 minutes to get dendrobium candidum dispersion liquid.
The step 4. in, the dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, emulsifier need to carry out pretreatment goes out
Bacterium, method include but is not limited to high-temperature sterilization, microwave sterilization, ultraviolet sterilization；Then plus water is stirred continuously, until be completely dissolved,
Obtain emulsifier solution；The emulsifier solution is added in dendrobium candidum dispersion liquid, stirring rate be 500-20000 turn/
Minute, mixing time is 5-30 minutes, obtains dendrobium candidum emulsion.
The step 5. in, the glue preparation is guar gum, carboxymethyl cellulose, xanthan gum, locust bean gum with glue
One or more of combinations；Total colloidality is 0.05-0.8%.
The glue is to be formulated by glue or carboxymethyl cellulose with water, the glue preparation with glue be guar gum,
The mixed glue solutions of the one or more of carboxymethyl cellulose, xanthan gum, locust bean gum being composed, the ratio between them are
0.1-10:0.1-15:0.2-40:0.2-20；After the dendrobium candidum emulsion is added to glue, stirred with blender equal
It is even, blender be it is rotary, rotation adds down convertible or rotation plus backflow-type, revolving speed is 500-3000 revs/min, when stirring
Between be 5-30 minute, acquisition dendrobium candidum suspended gel.
The dispersing agent includes but is not limited to: alginic acid sodium salt, carrageenan, guar gum, locust bean gum, carboxymethyl cellulose,
One or more of combinations of xanthan gum, konjac glucomannan, modified corn starch；Concentration of the dispersing agent in dispersion liquid is
0.01-0.2%.
The dispersing agent is alginic acid sodium salt, carrageenan, guar gum, carboxymethyl cellulose, xanthan gum, modified corn shallow lake
The combination of powder, konjac glucomannan, their ratio are as follows: 0.1-10:0.1-5:0.3-20:0.2-50:1-30:0.2-15:0.2-20.
The emulsifier includes but is not limited to: soybean lecithin, monoglyceride, sucrose ester, xanthan gum, alginic acid sodium salt, carboxylic
One or more of combinations of methylcellulose；The addition total concentration of the emulsifier is 0.1-2%.
The emulsifier is soybean lecithin, monoglyceride, sucrose ester, xanthan gum, alginic acid sodium salt, carboxymethyl cellulose
Combination, ratio between them is 0.1-10:0.01-30:0.1-20:0.5-30:0.1-10:1-20.
The step 6. in, dendrobium candidum suspended gel need to be added formula, and the formula is by sweetener, flavouring agent, tart flavour
Agent and preservative composition.
The dendrobium candidum suspended gel for having added formula will be dispensed on demand, and single dispensed loading amount is 100-
5000ml。
The packing material can be vial, PET bottle, PET barrels, pop can or Composite paper box.
The dendrobium candidum suspended gel that the packing finishes need to sterilize, and sterilizing methods include but is not limited to: Pasteur
Sterilization, microwave sterilization method.After sterilizing, dendrobium candidum suspended gel product is obtained.
The beneficial effects of the present invention are: the present invention is former using modern biochemistry technology and food drug forward position processing technology
Reason forms nanoscale using emulsifying technology and micron order capsule, the active constituent of effective protection dendrobium candidum reapplies gel skill
Nanoscale and micron order capsule is protected in art, finally protects nanocapsule and micron capsule, and shape again using suspended gel technology
At suspended gel liquid similar with human body inner tissue mucus.The suspended gel product of this method production not only almost includes and protects
Whole active constituents of dendrobium candidum, meanwhile, convenient, absorption easy to digest, human body almost can absorb its institute it is active at
Part, absorption efficiency is significantly higher than other dendrobium candidum products, up to 95% or more.
Specific embodiment
The embodiment of the present invention is further described below.Following embodiment only carries out furtherly the application
It is bright, it should not be construed as the limitation to the application.
Embodiment 1, as shown in Figure 1:
A kind of manufacturing method of dendrobium candidum suspended gel, it includes the following steps:
1) dendrobium candidum Fresh Plants are cleaned into the impurity such as removal silt, obtains clean dendrobium candidum Fresh Plants；
2) clean dendrobium candidum Fresh Plants point two ways is handled；
Processing one:
1. clean dendrobium candidum Fresh Plants cauline leaf is separated, dendrobium candidum stem and leaf are obtained；
2. mixing after dendrobium candidum stem and leaf are distinguished pulp, dendrobium candidum slurries are obtained；
3. dendrobium candidum slurries are dispersed agent dispersion, dendrobium candidum dispersion liquid is obtained；Here dispersing agent is alginic acid
The combination of sodium salt, carrageenan, guar gum, carboxymethyl cellulose, xanthan gum, modified corn starch, konjac glucomannan, their ratio
Are as follows: 0.1:0.1:0.3:0.2:1:0.2:0.2.Concentration of the dispersing agent in dispersion liquid is 0.01%.Dispersing agent is in proportion
After weighing well, preprocessed, mixing is needed, adds water and stirs to being completely dissolved, obtains dispersant solution；The pretreatment refers to pair
Sterilizing (ultraviolet sterilization), disinfection and the crushing of dispersing agent；The dendrobium candidum slurries are added in dispersant solution, or will be divided
Dispersant solution is added in dendrobium candidum slurries, Stirring, speed be 1000 revs/min, be stirred continuously 5 minutes to get
Dendrobium candidum dispersion liquid.
4. dendrobium candidum dispersion liquid is emulsified, dendrobium candidum emulsion is obtained；
Here emulsifier is soybean lecithin, monoglyceride, sucrose ester, xanthan gum, alginic acid sodium salt, carboxymethyl cellulose
Combination, ratio between them is 0.1:0.01:0.1:0.5:0.1:1.The addition total concentration of the emulsifier is 0.1%.
The dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, and emulsifier need to carry out pretreatment sterilizing (high-temperature sterilization)；
Then plus water is stirred continuously, until being completely dissolved, obtains emulsifier solution；The emulsifier solution is added to dendrobium candidum dispersion
In liquid, stirring rate is 1000 revs/min, and mixing time is 5 minutes, obtains dendrobium candidum emulsion.
5. dendrobium candidum emulsion is added formula (sweetener, flavouring agent, acid and preservative), stirs and evenly mixs, sterilize
And vacuum dispenses, and obtains dendrobium candidum emulsifying product；
6. adding formula (sweetener, flavouring agent, acid and preservative), stirring dendrobium candidum emulsion suspension gelation
Mixing, disinfection and vacuum packing are mixed, dendrobium candidum suspended gel product is obtained；The glue preparation is guar gum, carboxylic with glue
One or more of combinations of methylcellulose, xanthan gum, locust bean gum；Total colloidality is 0.05%.
Processing two:
1. clean dendrobium candidum Fresh Plants are obtained dendrobium candidum hay through frozen drying；
2. dendrobium candidum hay is crushed to 80 mesh, dendrobium candidum dry powder is obtained；
3. dendrobium candidum dry powder is dispersed agent dispersion, dendrobium candidum dry powder dispersion liquid is obtained；Dispersing agent weighs in proportion
After good, preprocessed, mixing is needed, adds water and stirs to being completely dissolved, obtains dispersant solution；The pretreatment refers to dispersion
Sterilizing, disinfection and the crushing of agent；The method (ultraviolet sterilization) of the dispersing agent sterilization；The dendrobium candidum slurries are added
It is added in dendrobium candidum slurries into dispersant solution, or by dispersant solution, Stirring, speed is 1000 revs/min
Clock is stirred continuously 5 minutes to get dendrobium candidum dispersion liquid.
4. dendrobium candidum dry powder dispersion liquid is emulsified, dendrobium candidum dry powder emulsion is obtained；
The dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, and emulsifier need to carry out pretreatment sterilizing (high-temperature sterilization)；
Then plus water is stirred continuously, until being completely dissolved, obtains emulsifier solution；The emulsifier solution is added to dendrobium candidum dispersion
In liquid, stirring rate is 1000 revs/min, and mixing time is 5 minutes, obtains dendrobium candidum emulsion.
5. glue suspension gelation is added in dendrobium candidum dry powder emulsion, add formula (sweetener, flavouring agent, acid
And preservative), stirred evenly with blender, blender be it is rotary, revolving speed is 500 revs/min, and mixing time is 5 minutes, disappears
Poison and vacuum packing, obtain dendrobium candidum dry powder suspended gel product.The glue preparation is guar gum, carboxymethyl fibre with glue
Tie up the combination of element, xanthan gum, locust bean gum；Ratio between them is 0.1:0.1:0.2:0.2；Total colloidality is 0.05%.Finally,
The dendrobium candidum suspended gel for having added formula will be dispensed on demand, and single dispensed loading amount is 100ml.The packing
Material is pop can.The dendrobium candidum suspended gel that the packing finishes need to sterilize, and sterilizing methods use pasteurization
Method.After sterilizing, dendrobium candidum suspended gel product is obtained.
Embodiment 2:
A kind of manufacturing method of dendrobium candidum suspended gel, it includes the following steps:
1) dendrobium candidum Fresh Plants are cleaned into the impurity such as removal silt, obtains clean dendrobium candidum Fresh Plants；
2) clean dendrobium candidum Fresh Plants point two ways is handled；
Processing one:
1. clean dendrobium candidum Fresh Plants cauline leaf is separated, dendrobium candidum stem and leaf are obtained；
2. mixing after dendrobium candidum stem and leaf are distinguished pulp, dendrobium candidum slurries are obtained；
3. dendrobium candidum slurries are dispersed agent dispersion, dendrobium candidum dispersion liquid is obtained；Here dispersing agent is alginic acid
The combination of sodium salt, carrageenan, guar gum, carboxymethyl cellulose, xanthan gum, modified corn starch, konjac glucomannan, their ratio
Are as follows: 5:3:10:25:15:8:10.Concentration of the dispersing agent in dispersion liquid is 0.1%.After dispersing agent weighs well in proportion,
Preprocessed, mixing is needed, adds water and stirs to being completely dissolved, obtains dispersant solution；The pretreatment refers to dispersing agent
It sterilizes (ultraviolet sterilization), sterilize and crushes；The dendrobium candidum slurries are added in dispersant solution, or by dispersant solution
It is added in dendrobium candidum slurries, Stirring, speed is 8000 revs/min, is stirred continuously 15 minutes to get dendrobium candidum
Dispersion liquid.
4. dendrobium candidum dispersion liquid is emulsified, dendrobium candidum emulsion is obtained；
Here emulsifier is soybean lecithin, monoglyceride, sucrose ester, xanthan gum, alginic acid sodium salt, carboxymethyl cellulose
Combination, ratio between them is 5:15:10:15:5:10.The addition total concentration of the emulsifier is 1%.
The dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, and emulsifier need to carry out pretreatment sterilizing (microwave sterilization)；
Then plus water is stirred continuously, until being completely dissolved, obtains emulsifier solution；The emulsifier solution is added to dendrobium candidum dispersion
In liquid, stirring rate is 2000 revs/min, and mixing time is 15 minutes, obtains dendrobium candidum emulsion.
5. dendrobium candidum emulsion is added formula (sweetener, flavouring agent, acid and preservative), stirs and evenly mixs, sterilize
And vacuum dispenses, and obtains dendrobium candidum emulsifying product；
6. adding formula (sweetener, flavouring agent, acid and preservative), stirring dendrobium candidum emulsion suspension gelation
Mixing, disinfection and vacuum packing are mixed, dendrobium candidum suspended gel product is obtained；The glue preparation is guar gum, carboxylic with glue
One or more of combinations of methylcellulose, xanthan gum, locust bean gum；Total colloidality is 0.3%.
Processing two:
1. clean dendrobium candidum Fresh Plants are obtained dendrobium candidum hay through frozen drying；
2. dendrobium candidum hay is crushed to 300 mesh, dendrobium candidum dry powder is obtained；
3. dendrobium candidum dry powder is dispersed agent dispersion, dendrobium candidum dry powder dispersion liquid is obtained；Dispersing agent weighs in proportion
After good, preprocessed, mixing is needed, adds water and stirs to being completely dissolved, obtains dispersant solution；The pretreatment refers to dispersion
Sterilizing (high-temperature sterilization), disinfection and the crushing of agent；The dendrobium candidum slurries are added in dispersant solution, or by dispersing agent
Solution is added in dendrobium candidum slurries, Stirring, and speed is 8000 revs/min, is stirred continuously 15 minutes to get iron sheet
Dendrobium nobile dispersion liquid.
4. dendrobium candidum dry powder dispersion liquid is emulsified, dendrobium candidum dry powder emulsion is obtained；
The dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, and emulsifier need to carry out pretreatment sterilizing (microwave sterilization)；
Then plus water is stirred continuously, until being completely dissolved, obtains emulsifier solution；The emulsifier solution is added to dendrobium candidum dispersion
In liquid, stirring rate is 10000 revs/min, and mixing time is 15 minutes, obtains dendrobium candidum emulsion.
5. glue suspension gelation is added in dendrobium candidum dry powder emulsion, add formula (sweetener, flavouring agent, acid
And preservative), stirred evenly with blender, it is convertible that blender is that rotation adds down, and revolving speed is 1500 revs/min, when stirring
Between for 15 minutes, disinfection and vacuum packing, obtain dendrobium candidum dry powder suspended gel product.The glue preparation is melon with glue
The combination of your glue, carboxymethyl cellulose, xanthan gum, locust bean gum；Ratio between them is 5:8:20:10；Always colloidality is
0.4%.Finally, the dendrobium candidum suspended gel for having added formula will be dispensed on demand, single dispensed loading amount is
2500ml.The packing material is PET bottle.The dendrobium candidum suspended gel that the packing finishes need to sterilize, sterilizing
Method uses microwave sterilization method.After sterilizing, dendrobium candidum suspended gel product is obtained.
Embodiment 3:
A kind of manufacturing method of dendrobium candidum suspended gel, it includes the following steps:
1) dendrobium candidum Fresh Plants are cleaned into the impurity such as removal silt, obtains clean dendrobium candidum Fresh Plants；
2) clean dendrobium candidum Fresh Plants point two ways is handled；
Processing one:
1. clean dendrobium candidum Fresh Plants cauline leaf is separated, dendrobium candidum stem and leaf are obtained；
2. mixing after dendrobium candidum stem and leaf are distinguished pulp, dendrobium candidum slurries are obtained；
3. dendrobium candidum slurries are dispersed agent dispersion, dendrobium candidum dispersion liquid is obtained；Here dispersing agent is alginic acid
The combination of sodium salt, carrageenan, guar gum, carboxymethyl cellulose, xanthan gum, modified corn starch, konjac glucomannan, their ratio
Are as follows: 10:5:20:50:30:15:20.Concentration of the dispersing agent in dispersion liquid is 0.2%.Dispersing agent weighs in proportion
Afterwards, preprocessed, mixing is needed, adds water and stirs to being completely dissolved, obtains dispersant solution；The pretreatment refers to dispersing agent
Sterilizing (microwave sterilization), disinfection and crush；The dendrobium candidum slurries are added in dispersant solution, or dispersing agent is molten
Liquid is added in dendrobium candidum slurries, Stirring, and speed is 15000 revs/min, is stirred continuously 30 minutes to get iron sheet
Dendrobium nobile dispersion liquid.
4. dendrobium candidum dispersion liquid is emulsified, dendrobium candidum emulsion is obtained；
Here emulsifier is soybean lecithin, monoglyceride, sucrose ester, xanthan gum, alginic acid sodium salt, carboxymethyl cellulose
Combination, ratio between them is 10:30:20:30:10:20.The addition total concentration of the emulsifier is 2%.
The dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, and emulsifier need to carry out pretreatment sterilizing, and method is high
Temperature sterilizing；Then plus water is stirred continuously, until being completely dissolved, obtains emulsifier solution；The emulsifier solution is added to iron sheet
In dendrobium nobile dispersion liquid, stirring rate is 1000 revs/min, and mixing time is 5 minutes, obtains dendrobium candidum emulsion.
5. dendrobium candidum emulsion is added formula (sweetener, flavouring agent, acid and preservative), stirs and evenly mixs, sterilize
And vacuum dispenses, and obtains dendrobium candidum emulsifying product；
6. adding formula (sweetener, flavouring agent, acid and preservative), stirring dendrobium candidum emulsion suspension gelation
Mixing, disinfection and vacuum packing are mixed, dendrobium candidum suspended gel product is obtained；The glue preparation is guar gum, carboxylic with glue
One or more of combinations of methylcellulose, xanthan gum, locust bean gum；Total colloidality is 0.05%.
Processing two:
1. clean dendrobium candidum Fresh Plants are obtained dendrobium candidum hay through frozen drying；
2. dendrobium candidum hay is crushed to 80 mesh, dendrobium candidum dry powder is obtained；
3. dendrobium candidum dry powder is dispersed agent dispersion, dendrobium candidum dry powder dispersion liquid is obtained；Dispersing agent weighs in proportion
After good, preprocessed, mixing is needed, adds water and stirs to being completely dissolved, obtains dispersant solution；The pretreatment refers to dispersion
Sterilizing (high-temperature sterilization), disinfection and the crushing of agent；The dendrobium candidum slurries are added in dispersant solution, or by dispersing agent
Solution is added in dendrobium candidum slurries, Stirring, and speed is 1000 revs/min, is stirred continuously 5 minutes to get iron sheet
Dendrobium nobile dispersion liquid.
4. dendrobium candidum dry powder dispersion liquid is emulsified, dendrobium candidum dry powder emulsion is obtained；
The dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, and emulsifier need to carry out pretreatment sterilizing, and method uses
Microwave sterilization；Then plus water is stirred continuously, until being completely dissolved, obtains emulsifier solution；The emulsifier solution is added to iron
In skin dendrobium nobile dispersion liquid, stirring rate is 3000 revs/min, and mixing time is 30 minutes, obtains dendrobium candidum emulsion.
5. glue suspension gelation is added in dendrobium candidum dry powder emulsion, add formula (sweetener, flavouring agent, acid
And preservative), stirred evenly with blender, blender be it is rotary, rotation adds down convertible or rotation plus backflow-type, revolving speed
It is 3000 revs/min, mixing time is 30 minutes, disinfection and vacuum dispense, and obtains dendrobium candidum dry powder suspended gel product.Institute
The glue preparation stated is the combination of guar gum, carboxymethyl cellulose, xanthan gum, locust bean gum with glue；Ratio between them is 10:
15:40:20；Total colloidality is 0.4%.Finally, the dendrobium candidum suspended gel for having added formula will be dispensed on demand,
Single dispensed loading amount is 5000ml.The packing material is vial.The dendrobium candidum suspended gel that the packing finishes needs
It sterilizes, sterilizing methods use pasteurization.After sterilizing, dendrobium candidum suspended gel product is obtained.
Claims (3)
1. a kind of manufacturing method of dendrobium candidum suspended gel, which is characterized in that it includes the following steps:
1) dendrobium candidum Fresh Plants are cleaned into removal silt impurity, obtains clean dendrobium candidum Fresh Plants；
2) clean dendrobium candidum Fresh Plants point two ways is handled；
Processing one: 1. separating clean dendrobium candidum Fresh Plants cauline leaf, obtains dendrobium candidum stem and leaf；2. by dendrobium candidum stem
It is mixed after distinguishing pulp with leaf, obtains dendrobium candidum slurries；3. dendrobium candidum slurries are dispersed agent dispersion, dendrobium candidum is obtained
Dispersion liquid；4. dendrobium candidum dispersion liquid is emulsified, dendrobium candidum emulsion is obtained；5. dendrobium candidum emulsion addition glue is hanged
Floating gelation, adds sweetener, flavouring agent, acid and preservative, stirs and evenly mixs, sterilizes and vacuum dispenses, obtains dendrobium candidum
Suspended gel product；
Processing two: clean dendrobium candidum Fresh Plants are 1. obtained into dendrobium candidum hay through frozen drying；2. by iron sheet stone
Dry measure used in former times hay is crushed to 80-500 mesh, obtains dendrobium candidum dry powder；3. dendrobium candidum dry powder is dispersed agent dispersion, iron sheet stone is obtained
Dry measure used in former times dry powder dispersion liquid；Concentration of the dispersing agent in dispersion liquid is 0.01-0.2%；4. by dendrobium candidum dry powder dispersion liquid cream
Change, obtains dendrobium candidum dry powder emulsion；5. by dendrobium candidum dry powder emulsion be added glue suspension gelation, add sweetener,
Flavouring agent, acid and preservative, stir and evenly mix, sterilize and vacuum dispenses, and obtain dendrobium candidum dry powder suspended gel product；Always
Colloidality is 0.05-0.8%；
Processing one and processing two the step of 5. described in glue be by guar gum, carboxymethyl cellulose, xanthan gum, locust bean gum group
Mixed glue solution made of conjunction, the ratio between them are 0.1-10:0.1-15:0.2-40:0.2-20；The dendrobium candidum cream
It after change liquid is added to glue, is stirred evenly with blender, blender adds down convertible or rotation for rotary, rotation and adds refluence
Formula, revolving speed are 500-3000 revs/min, and mixing time is 5-30 minutes, obtain dendrobium candidum suspended gel；
Processing one and processing two described in dispersing agent be alginic acid sodium salt, carrageenan, guar gum, carboxymethyl cellulose, xanthan gum,
The combination of modified corn starch, konjac glucomannan, their ratio are as follows: 0.1-10:0.1-5:0.3-20:0.2-50:1-30:0.2-
15:0.2-20；
Emulsifier is used when the emulsification of dendrobium candidum dispersion liquid in processing one and processing two；The addition total concentration of the emulsifier is
0.1-2%；The emulsifier is soybean lecithin, monoglyceride, sucrose ester, xanthan gum, alginic acid sodium salt, carboxymethyl cellulose
Combination, ratio between them is 0.1-10:0.01-30:0.1-20:0.5-30:0.1-10:1-20.
2. a kind of manufacturing method of dendrobium candidum suspended gel described in accordance with the claim 1, which is characterized in that the processing one
In step 3. in, dispersing agent weigh in proportion it is good after, need preprocessed, mix, add water and stir to being completely dissolved, dispersed
Agent solution；The pretreatment refers to sterilizing, disinfection and crushing to dispersing agent；The method packet of the dispersing agent sterilization
It includes: ultraviolet sterilization, high-temperature sterilization, microwave sterilization；The dendrobium candidum slurries are added in dispersant solution, or by dispersing agent
Solution is added in dendrobium candidum slurries, Stirring, and speed is 500-15000 revs/min, is stirred continuously 5-30 points
Clock is to get dendrobium candidum dispersion liquid.
3. a kind of manufacturing method of dendrobium candidum suspended gel described in accordance with the claim 1, which is characterized in that the processing
One, processing two in step 4. in, the dendrobium candidum dispersion liquid emulsifies in emulsifying kettle, emulsifier need to carry out pretreatment goes out
Bacterium, method include: high-temperature sterilization, microwave sterilization, ultraviolet sterilization；Then plus water is stirred continuously, until being completely dissolved, is emulsified
Agent solution；The emulsifier solution is added in dendrobium candidum dispersion liquid, and stirring rate is 500-20000 revs/min, stirring
Time is 5-30 minutes, obtains dendrobium candidum emulsion.
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