CN105380831A - Mild nursing hair oil treatment and care composition containing no silicone oil and preparation method of mild nursing hair oil treatment and care composition - Google Patents

Mild nursing hair oil treatment and care composition containing no silicone oil and preparation method of mild nursing hair oil treatment and care composition Download PDF

Info

Publication number
CN105380831A
CN105380831A CN201510945249.4A CN201510945249A CN105380831A CN 105380831 A CN105380831 A CN 105380831A CN 201510945249 A CN201510945249 A CN 201510945249A CN 105380831 A CN105380831 A CN 105380831A
Authority
CN
China
Prior art keywords
oil
hair
silicone oil
tiao
gentle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510945249.4A
Other languages
Chinese (zh)
Other versions
CN105380831B (en
Inventor
麦捷骅
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUANGZHOU YOUNGRACE COSMETICS CO Ltd
Original Assignee
GUANGZHOU YOUNGRACE COSMETICS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GUANGZHOU YOUNGRACE COSMETICS CO Ltd filed Critical GUANGZHOU YOUNGRACE COSMETICS CO Ltd
Priority to CN201510945249.4A priority Critical patent/CN105380831B/en
Publication of CN105380831A publication Critical patent/CN105380831A/en
Application granted granted Critical
Publication of CN105380831B publication Critical patent/CN105380831B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • A61K8/416Quaternary ammonium compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/85Polyesters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • A61K2800/34Free of silicones

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to a mild nursing hair oil treatment and care composition containing no silicone oil and a preparation method of the mild nursing hair oil treatment and care composition. The hair care composition is prepared from the following components in percentage by weight: 2-7% of a cation conditioner, 1-4% of an emulsifier, 2-10% of higher aliphatic alcohol, 1-10% of non-silicone oil-type oil or a derivative thereof, 0.1-8% of an additive, and the balance of water, wherein the cation conditioner is composed of behentrimonium chloride, oilseed rape oleamidopropyl dimethylamine, aspartic acid and polyester-11. According to the hair care composition, no silicone oil is added, so that the defects that after silicone oil products are used for a long term, the conditioning property and the smoothness of hair are reduced, and the hair is dry, bifurcate, broken and free of luster are overcome, the hair care composition achieves the effects of moistening and caring hair in the real sense, preserves moisture and provides nutrition from the deep position of the hair, obviously improves the combing property of the wet hair, the combing property of the dry hair, the limpness of the wet hair, and the limpness of the dry hair, and obviously improves the tenacity, the elasticity and the luster of the hair.

Description

Without silicone oil gentle Tiao Li treatment oil Haircare composition and preparation method thereof
Technical field
The present invention relates to Haircare composition, particularly relate to a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition and preparation method thereof.
Background technology
Along with improving constantly of people's living standard, almost every day, people were at use conditioner hair conditioning.But current hair products on the market, major part is containing silicone oil (silicone oil alkane product) composition.Silicone oil component is widely used as conditioner conventional in hair conditioning, silicone oil can make hair hair scale sheet more level and smooth, effectively can reduce between hair and rub, make hair more smooth, be easy to combing, but silicone oil has water-insoluble simultaneously, permanent use can produce excessive buildup on hair, reduces the hair conditioning of hair and submissive sense.
Possessor cooks conditioner use with oils and fats in hair products to the greatest extent, but its conditioning effect still compared with silicone oil, and cannot exist many uses limitation, such as result of use, stability problem etc.How while not using silicone oil (silicone product), realizing preferably conditioning effect, is at present without silicone oil hair products research problem demanding prompt solution.
Summary of the invention
Based on this, be necessary to provide a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition.
The invention provides a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprise following component:
Described cation opsonizing agent is made up of mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, polyester-11 and aspartic acid.
Wherein in an embodiment, by weight percentage, comprise following component:
Wherein in an embodiment, in described cation opsonizing agent, the weight ratio of described rapeseed oil amido propyl dimethylamine and aspartic acid is 1:(0.2-0.3).
Wherein in an embodiment, described cation opsonizing agent is weight ratio is (2-4): (0.5-2): (0.115-0.46): the mountain Yu base trimethyl ammonium chloride of (0.3-1), rapeseed oil amido propyl dimethylamine, aspartic acid and polyester-11, wherein, the weight ratio of described rapeseed oil amido propyl dimethylamine and aspartic acid is 1:0.23.
Wherein in an embodiment, described cation opsonizing agent is weight ratio is (2-4): (1-2): (0.23-0.46): the mountain Yu base trimethyl ammonium chloride of (0.3-1), rapeseed oil amido propyl dimethylamine, aspartic acid and polyester-11.
Wherein in an embodiment, described cation opsonizing agent is weight ratio is (3-4): (1-2): (0.23-0.46): the mountain Yu base trimethyl ammonium chloride of (0.6-1), rapeseed oil amido propyl dimethylamine, aspartic acid and polyester-11.
Wherein in an embodiment, the oils and fats of described non-silicone oil or oils and fats derivant are weight ratio is (1-2): the synthetic ester oil of the non-silicone oil of 1 and Vegetable oil lipoprotein, wherein, the synthetic ester oil of described non-silicone oil is one or more in C10-12 alkane/cycloalkanes, synthesis Jojoba oil; Described Vegetable oil lipoprotein is one or more in olive oil, American Avocado Tree oil.
Wherein in an embodiment, described emulsifying agent comprise in glyceryl stearate, glyceryl stearate/PEG-100 stearate, cetearyl alcohol/PEG-20 stearate, ceteareth-20, cocamido propyl betaine one or more; Described high fatty alcohol is one or more in cetearyl alcohol, stearyl alcohol, isooctadecanol, behenyl alcohol; Described additive is one or more in viscosity modifier, nutrient, wetting agent, anti-dandruff agent, antiseptic, essence.
Wherein in an embodiment, described viscosity modifier is one or more in hydroxyethyl-cellulose, hydroxypropyl cellulose, hydroxypropyl emthylcellulose, further preferred hydroxypropyl emthylcellulose; Nutrient is one or more in D-panthenol, hydrolysis of keratin, further selective hydrolysis keratin; Wetting agent is one or more in trimethyl glycine, levan, glycerol, further preferably glycerine; Anti-dandruff agent is one or more in climbazole, octopirox (octopirox), pyrithione slaine (as Zinc Pyrithione ZPT), further preferred octopirox (octopirox); Described antiseptic is one or more in potassium sorbate, phenoxyethanol; Essence be in vanillin, Herba Menthae, Oleum Rosae Rugosae one or more.All components meets the regulation of hygienic standards for cosmetics, selects safe raw material.
The present invention also provides the preparation method of described Haircare composition for the treatment of with oil without the gentle Tiao Li of silicone oil, comprises the steps:
(1) add suitable quantity of water and described cation opsonizing agent in a kettle., dispersed with stirring, be heated to 75 DEG C-85 DEG C;
(2) will be added in described reactor after the oils and fats of described emulsifying agent, high fatty alcohol and non-silicone oil or oils and fats derivant heat fused, emulsifying also, after being incubated 10-20 minute, cools;
(3) when temperature is down to 45 DEG C-50 DEG C, add described additive, continue to stir;
(4) finally add remaining water, filter discharging, to obtain final product.
Principle of the present invention and advantage as follows:
Of the present invention without silicone oil gentle Tiao Li treatment oil Haircare composition, with rational percentage by weight by cation opsonizing agent, emulsifying agent, oils and fats or the oils and fats derivant of high fatty alcohol and non-silicone oil are prepared, wherein, the cation opsonizing agent stability of combination to Haircare composition is embodied in the nursing role of hair key and the absorption stability to other component plays an important role, particularly adopt mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, aspartic acid and polyester-11 are as cation opsonizing agent, make this Haircare composition correct flourishing in required conditioning, effect of moisturizing and water retention.Do not adding under silicon oil condition, deep layer can nourish hair, obviously improving wet Comb rationality, hair drying comb rationality, wetting and send out flexibility, the dry problem sending out flexibility, hair is moistened, strong, and make user more acceptant.In addition, the oils and fats of abundant non-silicone oil or oils and fats derivant (as synthetic ester oil, Vegetable oil lipoprotein, animal oil), obviously improve silicone oil and produce excessive buildup on hair, really moistens hair, give moisture-keeping nutrient from depths, strengthen toughness and the elastic force of hair; Add high fatty alcohol, hair can be made to keep fit, light, and high resilience.
By the concrete composition and ratio of further conservative control cation opsonizing agent, can be in harmonious proportion to this Haircare composition integral formulation, strengthen the protective action of oils and fats, make that hair epidermis is level and smooth, lubrication, soft, reduce hair and move swiftly and improve the cardability of hair, obtain more excellent hair care effect.
Compared with prior art, the present invention has following beneficial effect:
Of the present invention without silicone oil gentle Tiao Li treatment oil Haircare composition, add without silicone oil, avoid silicone oil product life-time service and reduce the hair conditioning of hair and submissive sense, hair is withered, bifurcated, fracture, lusterless defect, really play moist hair care effect, give moisture-keeping nutrient from hair depths, obviously improve wet Comb rationality, hair drying comb rationality, a wet flexibility, the dry problem sending out flexibility, obviously improve the toughness of hair, elastic force and gloss.
This Haircare composition also can coordinate Jia Re treatment oil to use, and deep layer nourishes hair thus, after hair nutrition maintenance effect, makes hair moist, strong, makes the hair color and luster after dyeing distincter, strengthen the endurance of hair-waving.
Detailed description of the invention
Be described in further detail without silicone oil gentle Tiao Li treatment oil Haircare composition and preparation method thereof of the present invention below in conjunction with specific embodiment.
Rapeseed oil amido propyl dimethylamine purchased from American Inolex company of the present invention;
Described polyester-11 purchased from American Inolex company.
Embodiment 1
The present embodiment is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, aspartic acid, polyester-11, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by cetearyl alcohol and PEG-20 stearate, cetearyl alcohol, C10-12 alkane/cycloalkanes and American Avocado Tree oil heat fused, and be added to described reactor, emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, phenoxyethanol, vanillin continues to stir, mix homogeneously;
(4) finally add remaining deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Embodiment 2
The present embodiment is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, aspartic acid, polyester-11, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by ceteareth-20, cetearyl alcohol, isooctadecanol, C10-12 alkane/cycloalkanes, American Avocado Tree oil heat fused, is added to described reactor, and emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, phenoxyethanol, Herba Menthae continues to stir, mix homogeneously;
(4) finally add residue deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Embodiment 3
The present embodiment is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, aspartic acid, polyester-11, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by glyceryl stearate/PEG-100 stearate, behenyl alcohol, C10-12 alkane/cycloalkanes, American Avocado Tree oil heat fused, is added in described reactor, and emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, phenoxyethanol, Oleum Rosae Rugosae continues to stir, mix homogeneously;
(4) finally add residue deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Embodiment 4
The present embodiment is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, aspartic acid, polyester-11, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by cetearyl alcohol/PEG-20 stearate, cetearyl alcohol, isooctadecanol, synthesis Jojoba oil, olive oil heat fused, is added to described reactor, and emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, potassium sorbate, Oleum Rosae Rugosae continues to stir, mix homogeneously;
(4) finally add residue deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Embodiment 5
The present embodiment is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, aspartic acid, polyester-11, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by glyceryl stearate, stearyl alcohol, synthesis Jojoba oil, olive oil heat fused is added in described reactor, and emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, potassium sorbate, Herba Menthae continues to stir, mix homogeneously;
(4) finally add residue deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Adjust reason treatment oil Haircare composition to be white bright cream shape product without silicone oil gentleness described in embodiment 1-5, pH value is 5.0-5.5 (under 25 DEG C of conditions, being the pH value of the aqueous solution of the Haircare composition of 10% containing percentage by weight).
Using method is: after hair washing by its uniform application on hair, softly massage 2 ~ 3 minutes, use heating cap Huo to treat with oil after machine heating 15 ~ 20 minutes hair conditionings, rinse well with clear water.
Comparative example 1
This comparative example is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add mountain Yu base trimethyl ammonium chloride, polyester-11, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by cetearyl alcohol and PEG-20 stearate, cetearyl alcohol, C10-12 alkane/cycloalkanes and American Avocado Tree oil heat fused, and be added to described reactor, emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, phenoxyethanol, vanillin continues to stir, mix homogeneously;
(4) finally add remaining deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Comparative example 2
This comparative example is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, aspartic acid, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by ceteareth-20, cetearyl alcohol, isooctadecanol, C10-12 alkane/cycloalkanes, American Avocado Tree oil heat fused, is added to described reactor, and emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, phenoxyethanol, Herba Menthae continues to stir, mix homogeneously;
(4) finally add residue deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Comparative example 3
This comparative example is a kind of without silicone oil gentle Tiao Li treatment oil Haircare composition, by weight percentage, comprises following component:
Its preparation method comprises the following steps:
(1) add appropriate amount of deionized water in a kettle., add rapeseed oil amido propyl dimethylamine, aspartic acid, polyester-11, slowly stir, be uniformly dispersed, be heated to 75 DEG C ~ 85 DEG C;
(2) by glyceryl stearate/PEG-100 stearate, behenyl alcohol, C10-12 alkane/cycloalkanes, American Avocado Tree oil heat fused, is added in described reactor, and emulsifying also, after being incubated 10 ~ 20 minutes, cools;
(3), when temperature is down to 45 DEG C ~ 50 DEG C, add in advance respectively with hydroxypropyl emthylcellulose, hydrolysis of keratin that appropriate amount of deionized water is dissolved, glycerol, octopirox octopirox, phenoxyethanol, Oleum Rosae Rugosae continues to stir, mix homogeneously;
(4) finally add residue deionized water and complement to scheduled volume filtration discharging, shut down, sampling detects to be analyzed.It is qualified to detect, quantitative package.
Adopt sensory evaluation method to embodiment 1-5 and comparative example 1-5 Haircare composition, detailed description of the invention is as follows:
Test use to respectively 100 experimenters by described in the embodiment 1-5 of preparation and comparative example 1-5 without silicone oil gentle Tiao Li treatment oil Haircare composition.Experimenter takes care of hair according to above-mentioned using method, often kind of Haircare composition uses two weeks continuously, experimenter marks to Haircare composition according to the sensation of oneself, scoring employing 5 points system, 1 is divided into the poorest, and 3 points are moderate, 5 be divided into best, the higher effect of score is better, and before 100 experimenters use, scoring is 1-2 and divides, and uses rear effect evaluation result as follows:
Wet Comb rationality Hair drying comb rationality A wet flexibility A dry flexibility
Embodiment 1 4.3 4.3 4.5 4.3
Embodiment 2 4.5 4.2 4.4 4.3
Embodiment 3 4.2 4.2 4.4 4.5
Embodiment 4 4.3 4.3 4.5 4.2
Embodiment 5 4.4 4.2 4.4 4.3
Comparative example 1 2.9 3.0 2.9 3.0
Comparative example 2 3.0 3.1 3.0 3.0
Comparative example 3 3.0 2.9 3.0 3.0
Shown by the test result in table, use of the present invention without after silicone oil gentle Tiao Li treatment oil Haircare composition, the cardability of wet or dry and flexibility problem obtain obviously to be improved, and all experimenters represent the sensation liking using Haircare composition for the treatment of with oil without the gentle Tiao Li of silicone oil of the present invention, and the experimenter of 98% can continue regularly to use after the research phase of 14 days.
From comparative example 1-3 effect assessment result, delete one of them or two cation opsonizing agents on hair wet Comb rationality, wetly send out a flexibility effect, hair drying comb rationality, a dry flexibility effect of sending out all have and comparatively significantly affect.
Each technical characteristic of the above embodiment can combine arbitrarily, for making description succinct, the all possible combination of each technical characteristic in above-described embodiment is not all described, but, as long as the combination of these technical characteristics does not exist contradiction, be all considered to be the scope that this description is recorded.
The above embodiment only have expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be construed as limiting the scope of the patent.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.

Claims (10)

1. adjust a reason treatment oil Haircare composition without silicone oil gentleness, it is characterized in that, by weight percentage, comprise following component:
Described cation opsonizing agent is made up of mountain Yu base trimethyl ammonium chloride, rapeseed oil amido propyl dimethylamine, polyester-11 and aspartic acid.
2. according to claim 1 without silicone oil gentle Tiao Li treatment oil Haircare composition, it is characterized in that, by weight percentage, comprise following component:
3. according to claim 1 without silicone oil gentle Tiao Li treatment oil Haircare composition, it is characterized in that, in described cation opsonizing agent, the weight ratio of described rapeseed oil amido propyl dimethylamine and aspartic acid is 1:(0.2-0.3).
4. according to claim 3 without silicone oil gentle Tiao Li treatment oil Haircare composition, it is characterized in that, described cation opsonizing agent is weight ratio is (2-4): (0.5-2): (0.115-0.46): the mountain Yu base trimethyl ammonium chloride of (0.3-1), rapeseed oil amido propyl dimethylamine, aspartic acid and polyester-11, wherein, the weight ratio of described rapeseed oil amido propyl dimethylamine and aspartic acid is 1:0.23.
5. according to claim 4 without silicone oil gentle Tiao Li treatment oil Haircare composition, it is characterized in that, described cation opsonizing agent is weight ratio is (2-4): (1-2): (0.23-0.46): the mountain Yu base trimethyl ammonium chloride of (0.3-1), rapeseed oil amido propyl dimethylamine, aspartic acid and polyester-11.
6. according to claim 5 without silicone oil gentle Tiao Li treatment oil Haircare composition, it is characterized in that, described cation opsonizing agent is weight ratio is (3-4): (1-2): (0.23-0.46): the mountain Yu base trimethyl ammonium chloride of (0.6-1), rapeseed oil amido propyl dimethylamine, aspartic acid and polyester-11.
7. according to claim 1 without silicone oil gentle Tiao Li treatment oil Haircare composition, it is characterized in that, the oils and fats of described non-silicone oil or oils and fats derivant are weight ratio is (1-2): the synthetic ester oil of the non-silicone oil of 1 and Vegetable oil lipoprotein, wherein, the synthetic ester oil of described non-silicone oil is one or more in C10-12 alkane/cycloalkanes, synthesis Jojoba oil; Described Vegetable oil lipoprotein is one or more in olive oil, American Avocado Tree oil.
8. to treat with oil Haircare composition without the gentle Tiao Li of silicone oil according to any one of claim 1-7, it is characterized in that, described emulsifying agent comprise in glyceryl stearate, glyceryl stearate/PEG-100 stearate, cetearyl alcohol/PEG-20 stearate, ceteareth-20, cocamido propyl betaine one or more; Described high fatty alcohol is one or more in cetearyl alcohol, stearyl alcohol, isooctadecanol, behenyl alcohol; Described additive is one or more in viscosity modifier, nutrient, wetting agent, anti-dandruff agent, antiseptic, essence.
9. according to claim 8ly to treat with oil Haircare composition without the gentle Tiao Li of silicone oil, it is characterized in that, described viscosity modifier is one or more in hydroxyethyl-cellulose, hydroxypropyl cellulose, hydroxypropyl emthylcellulose; Described nutrient is one or more in D-panthenol, hydrolysis of keratin; Described wetting agent is one or more in trimethyl glycine, levan, glycerol; Described anti-dandruff agent is one or more in climbazole, octopirox, pyrithione slaine; Described antiseptic is one or more in potassium sorbate, phenoxyethanol; Described essence be in vanillin, Herba Menthae, Oleum Rosae Rugosae one or more.
10. the preparation method of the Haircare composition for the treatment of with oil without the gentle Tiao Li of silicone oil described in any one of claim 1-9, is characterized in that, comprise the steps:
(1) add suitable quantity of water and described cation opsonizing agent in a kettle., dispersed with stirring, be heated to 75 DEG C-85 DEG C;
(2) will be added in described reactor after the oils and fats of described emulsifying agent, high fatty alcohol and non-silicone oil or oils and fats derivant heat fused, emulsifying also, after being incubated 10-20 minute, cools;
(3) when temperature is down to 45 DEG C-50 DEG C, add described additive, continue to stir;
(4) finally add remaining water, filter discharging, to obtain final product.
CN201510945249.4A 2015-12-15 2015-12-15 No mild Tiao Li treatment oil Haircare composition of silicone oil and preparation method thereof Expired - Fee Related CN105380831B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510945249.4A CN105380831B (en) 2015-12-15 2015-12-15 No mild Tiao Li treatment oil Haircare composition of silicone oil and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510945249.4A CN105380831B (en) 2015-12-15 2015-12-15 No mild Tiao Li treatment oil Haircare composition of silicone oil and preparation method thereof

Publications (2)

Publication Number Publication Date
CN105380831A true CN105380831A (en) 2016-03-09
CN105380831B CN105380831B (en) 2018-09-21

Family

ID=55414014

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510945249.4A Expired - Fee Related CN105380831B (en) 2015-12-15 2015-12-15 No mild Tiao Li treatment oil Haircare composition of silicone oil and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105380831B (en)

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106580858A (en) * 2016-12-30 2017-04-26 广州市科能化妆品科研有限公司 Silicon-free hydrotherapy essence hair care composition
CN106974846A (en) * 2017-04-07 2017-07-25 美晨集团股份有限公司 A kind of moist shampoo and preparation method thereof
CN107440940A (en) * 2017-08-04 2017-12-08 澳宝化妆品(惠州)有限公司 It is a kind of containing house oil without silicone oil hair care composition
CN107569408A (en) * 2017-09-08 2018-01-12 新时代健康产业(集团)有限公司 A kind of hair-care essence liquid for increasing hair brightness and preparation method thereof
CN107789212A (en) * 2017-09-30 2018-03-13 朱耀灯 A kind of water moistens glossy Haircare composition
CN108125814A (en) * 2018-02-08 2018-06-08 花安堂生物科技集团有限公司 A kind of hair care and skin care compositions of cation form work composition
CN109125097A (en) * 2018-07-10 2019-01-04 广州温雅日用化妆品有限公司 A kind of shampooing process of foaming agent shampoo
WO2019127214A1 (en) * 2017-12-28 2019-07-04 L'oreal Composition for conditioning keratin fibers
CN111888270A (en) * 2020-09-09 2020-11-06 广州博氏化妆品有限公司 Hair care composition and preparation method and application thereof
CN115369648A (en) * 2021-10-21 2022-11-22 青岛融美发制品集团有限公司 Silicone-oil-free wig post-treatment agent and preparation method thereof
CN117100729A (en) * 2023-10-18 2023-11-24 露乐健康科技股份有限公司 Private part antibacterial composition, private part nursing product, and preparation methods and applications thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102138879A (en) * 2010-01-29 2011-08-03 上海华银日用品有限公司 Nutrient hair conditioner containing silk peptide essence and preparation method thereof
CN102552088A (en) * 2012-01-16 2012-07-11 澳宝化妆品(惠州)有限公司 Rapid-nourishing hair-care combination
CN104997661A (en) * 2015-06-15 2015-10-28 上海媚兰生物科技发展有限公司 Mild silicone-oil-free shampoo in cation system and preparing method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102138879A (en) * 2010-01-29 2011-08-03 上海华银日用品有限公司 Nutrient hair conditioner containing silk peptide essence and preparation method thereof
CN102552088A (en) * 2012-01-16 2012-07-11 澳宝化妆品(惠州)有限公司 Rapid-nourishing hair-care combination
CN104997661A (en) * 2015-06-15 2015-10-28 上海媚兰生物科技发展有限公司 Mild silicone-oil-free shampoo in cation system and preparing method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
INOLEX公司: "《化妆品安全技术规格书MSDS/SDS》", 《HTTPS://WWW.ULPROSPECTOR.COM/ZH-CN/ASIA/PERSONALCARE/DETAIL/759/75577/KERABASE?ST=1》 *

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106580858B (en) * 2016-12-30 2019-11-15 广州市科能化妆品科研有限公司 A kind of no silicon hydrotherapy element hair care composition
CN106580858A (en) * 2016-12-30 2017-04-26 广州市科能化妆品科研有限公司 Silicon-free hydrotherapy essence hair care composition
CN106974846A (en) * 2017-04-07 2017-07-25 美晨集团股份有限公司 A kind of moist shampoo and preparation method thereof
CN106974846B (en) * 2017-04-07 2020-09-29 美晨集团股份有限公司 Moisturizing shampoo and preparation method thereof
CN107440940A (en) * 2017-08-04 2017-12-08 澳宝化妆品(惠州)有限公司 It is a kind of containing house oil without silicone oil hair care composition
CN107569408A (en) * 2017-09-08 2018-01-12 新时代健康产业(集团)有限公司 A kind of hair-care essence liquid for increasing hair brightness and preparation method thereof
CN107789212A (en) * 2017-09-30 2018-03-13 朱耀灯 A kind of water moistens glossy Haircare composition
WO2019127214A1 (en) * 2017-12-28 2019-07-04 L'oreal Composition for conditioning keratin fibers
US11975089B2 (en) 2017-12-28 2024-05-07 L'oreal Composition for conditioning keratin fibers
CN108125814A (en) * 2018-02-08 2018-06-08 花安堂生物科技集团有限公司 A kind of hair care and skin care compositions of cation form work composition
CN109125097A (en) * 2018-07-10 2019-01-04 广州温雅日用化妆品有限公司 A kind of shampooing process of foaming agent shampoo
CN109125097B (en) * 2018-07-10 2021-07-13 广州温雅日用化妆品有限公司 Hair washing method of bubble shampoo
CN111888270A (en) * 2020-09-09 2020-11-06 广州博氏化妆品有限公司 Hair care composition and preparation method and application thereof
CN115369648A (en) * 2021-10-21 2022-11-22 青岛融美发制品集团有限公司 Silicone-oil-free wig post-treatment agent and preparation method thereof
CN115369648B (en) * 2021-10-21 2024-03-08 青岛海森林发制品集团股份有限公司 Silicone oil-free wig post-treatment agent and preparation method thereof
CN117100729A (en) * 2023-10-18 2023-11-24 露乐健康科技股份有限公司 Private part antibacterial composition, private part nursing product, and preparation methods and applications thereof
CN117100729B (en) * 2023-10-18 2024-01-26 露乐健康科技股份有限公司 Private part antibacterial composition, private part nursing product, and preparation methods and applications thereof

Also Published As

Publication number Publication date
CN105380831B (en) 2018-09-21

Similar Documents

Publication Publication Date Title
CN105380831A (en) Mild nursing hair oil treatment and care composition containing no silicone oil and preparation method of mild nursing hair oil treatment and care composition
CN102552088B (en) Rapid-nourishing hair-care combination
CN105769599B (en) A kind of low molecular weight cationic albumen hair care conditioning frost
CN108078796B (en) Silicone-oil-free moistening and smoothing hair mask and preparation method thereof
CN102727410B (en) Hair conditioner comprising olive oil and derivatives of olive oil and preparation method of hair conditioner
CN111671677A (en) Softening and repairing plant hair care composition
CN106344434A (en) Nutritious supple shampoo without silicon oil and preparation method thereof
CN105997560A (en) Camellia seed protein hair conditioner and preparation method
CN105326655A (en) Silicone-oil-free folic acid shampoo and preparation method thereof
CN104940078A (en) Liquid shampoo containing Chinese herbal medicinal ingredients
CN110403882A (en) A kind of shampoo with hair-growing and hair care effect
CN107184406A (en) One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof
CN113081935A (en) Amino acid oil-control fluffy moisturizing hair conditioner and preparation process thereof
CN102716046B (en) Liquid shampoo containing natural olive oil and derivative of natural olive oil and preparation method for liquid shampoo
CN107308057A (en) A kind of submissive nourishing hair and nontoxic soft hair cream and preparation method thereof
CN104434698A (en) Anti-static and anti-radiation shampoo paste and preparation method thereof
CN107854403A (en) A kind of clean moisture surge treatment formula
CN107375053A (en) A kind of ginseng and Chinese angelica root is without silicone oil shampoo and preparation method thereof
CN107184413A (en) It is a kind of to repair moist hair film of root of hair and preparation method thereof without anti-corrosion depth
CN104146931B (en) A kind of natural nourishing maintenance type hair conditioner and preparation method thereof
CN109431895A (en) A kind of scalp care compositions of Anti-hair loss and its preparation method and application
CN103040671A (en) Skin beautifying cosmetic
CN111821220A (en) Hair care composition, repairing hair film and preparation method thereof
JP4716476B2 (en) Hair rinse
CN104147103B (en) A kind of Chinese medicine composition and preparation method thereof of anti-dandruff sterilizing and itch-relieving, piliation

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180921

Termination date: 20191215