CN105350280A - 羟乙基纤维素纤维的制备方法 - Google Patents
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Abstract
本发明公开了一种羟乙基纤维素纤维的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：1）在30质量份去离子水中投入1～2质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。本发明羟乙基纤维素纤维的制备方法，包括纤维整理步骤，整理后的羟乙基纤维素纤维具有优异的抗菌、阻燃、抗静电性能。
Description
技术领域
本发明涉及羟乙基纤维素纤维的制备方法。
背景技术
现有羟乙基纤维素纤维的抗菌、阻燃、抗静电性能都有待提高。
发明内容
本发明的目的在于提供一种羟乙基纤维素纤维的制备方法，包括纤维整理步骤，整理后的羟乙基纤维素纤维具有优异的抗菌、阻燃、抗静电性能。
为实现上述目的，本发明的技术方案是设计一种羟乙基纤维素纤维的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入1～2质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
优选的，羟乙基纤维素纤维的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入1质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
优选的，羟乙基纤维素纤维的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入2质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
本发明的优点和有益效果在于：提供一种羟乙基纤维素纤维的制备方法，包括纤维整理步骤，整理后的羟乙基纤维素纤维具有优异的抗菌、阻燃、抗静电性能。
具体实施方式
下面结合实施例，对本发明的具体实施方式作进一步描述。以下实施例仅用于更加清楚地说明本发明的技术方案，而不能以此来限制本发明的保护范围。
本发明具体实施的技术方案是：
实施例1
一种羟乙基纤维素纤维的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入1～2质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
实施例2
羟乙基纤维素纤维的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入1质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
实施例3
羟乙基纤维素纤维的制备方法，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入2质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明技术原理的前提下，还可以做出若干改进和润饰，这些改进和润饰也应视为本发明的保护范围。
Claims (3)
1.羟乙基纤维素纤维的制备方法，其特征在于，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入1～2质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
2.根据权利要求1所述的羟乙基纤维素纤维的制备方法，其特征在于，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入1质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
3.根据权利要求1所述的羟乙基纤维素纤维的制备方法，其特征在于，包括纤维整理步骤，所述纤维整理包括如下步骤：
1）在30质量份去离子水中投入2质量份γ-环氧丙基醚基三甲氧基硅烷、3.3质量份1-(4-氟苯基)双胍盐酸盐、2.4质量份异噻唑啉酮、1.3质量份纳米级氢氧化铝混合，搅拌均匀；
2）再同时缓慢加入2.6质量份木质素磺酸盐、3.6质量份琥珀酸十八烷基二酯磺酸钠、1.7质量份金刚藤提取物、2.1质量份α-烯烃磺酸钠，继续搅拌，至充分混合均匀，制得整理液；
3）将羟乙基纤维素纤维在整理液中浸轧处理，取出后恒温烘干。
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106283631A (zh) * | 2016-08-19 | 2017-01-04 | 常熟市龙飞针纺织有限公司 | 不倒绒面料的后整理工艺 |
| CN106283596A (zh) * | 2016-08-30 | 2017-01-04 | 苏州紫澜实业有限公司 | 天鹅绒织物的退浆处理方法 |
| CN112900103A (zh) * | 2021-01-27 | 2021-06-04 | 宁波润禾高新材料科技股份有限公司 | 一种抗菌柔软组合物及其制备方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102191684A (zh) * | 2010-03-11 | 2011-09-21 | 北京服装学院 | 一种用于纺织品抗菌整理的反应型抗菌剂 |
| CN104233801A (zh) * | 2014-09-15 | 2014-12-24 | 河南工程学院 | 一种阻燃和拒水双功能棉织物的制备方法 |
| CN104790218A (zh) * | 2015-05-14 | 2015-07-22 | 宣海成 | 一种耐久型织物防霉抗静电整理剂 |
| CN105133308A (zh) * | 2015-09-14 | 2015-12-09 | 合肥学院 | 一种浸渍法制备阻燃抗菌无纺纸的方法 |
-
2015
- 2015-12-16 CN CN201510938483.4A patent/CN105350280A/zh active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102191684A (zh) * | 2010-03-11 | 2011-09-21 | 北京服装学院 | 一种用于纺织品抗菌整理的反应型抗菌剂 |
| CN104233801A (zh) * | 2014-09-15 | 2014-12-24 | 河南工程学院 | 一种阻燃和拒水双功能棉织物的制备方法 |
| CN104790218A (zh) * | 2015-05-14 | 2015-07-22 | 宣海成 | 一种耐久型织物防霉抗静电整理剂 |
| CN105133308A (zh) * | 2015-09-14 | 2015-12-09 | 合肥学院 | 一种浸渍法制备阻燃抗菌无纺纸的方法 |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106283631A (zh) * | 2016-08-19 | 2017-01-04 | 常熟市龙飞针纺织有限公司 | 不倒绒面料的后整理工艺 |
| CN106283596A (zh) * | 2016-08-30 | 2017-01-04 | 苏州紫澜实业有限公司 | 天鹅绒织物的退浆处理方法 |
| CN112900103A (zh) * | 2021-01-27 | 2021-06-04 | 宁波润禾高新材料科技股份有限公司 | 一种抗菌柔软组合物及其制备方法 |
| CN112900103B (zh) * | 2021-01-27 | 2023-03-14 | 宁波润禾高新材料科技股份有限公司 | 一种抗菌柔软组合物及其制备方法 |
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