CN105326279B - A kind of production method of mint fibers Rachael blanket - Google Patents

A kind of production method of mint fibers Rachael blanket Download PDF

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Publication number
CN105326279B
CN105326279B CN201510721158.2A CN201510721158A CN105326279B CN 105326279 B CN105326279 B CN 105326279B CN 201510721158 A CN201510721158 A CN 201510721158A CN 105326279 B CN105326279 B CN 105326279B
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mint fibers
rachael blanket
finished product
dye
herba menthae
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CN105326279A (en
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陈玉霜
毛森贤
孟波
毛青山
陈金霞
郑其明
韩彬
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Zhejiang Truelove Blanket Industry Technology Co Ltd
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Zhejiang Truelove Blanket Industry Technology Co Ltd
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Abstract

The present invention relates to woollen blanket preparation field, disclose the production method of a kind of mint fibers Rachael blanket, including: 1), weaving: to plush yarn and wire gauze successively warping, weave, cut open floss, prepare mint fibers Rachael blanket semi-finished product;2), prefinishing: by fabric sizing, bristle, hot light, clot;3), dyeing and finishing: by textile dyeing, then to its reduction cleaning, be then passed through acetum and neutralize, wash out cylinder, drying, steaming and color fixing, flexible smooth process, the most again dry;4), Final finishing: fabric drying sizing, front hot light, front bristle, front are scalded cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching;5), product inspection, packaging warehouse-in.The mint fibers Rachael blanket of the present invention has that fine hair is submissive, stands upright, good springiness, fabric skin-friendly, moisture absorption and desorption property, the excellent and antibiotic health care of good permeability, the feature of environmental protection.

Description

A kind of production method of mint fibers Rachael blanket
Technical field
The present invention relates to woollen blanket preparation field, particularly relate to the production method of a kind of mint fibers Rachael blanket.
Background technology
Along with the raising of people's material and culture level, the requirement of textile is also being improved by people, does not require nothing more than warming, attractive in appearance, and more focuses on comfortableness and functional.Functional textile becomes one of following developing trend of textile industry, will collectively form the big tendency of following textile with fine count fiber textile, non-woven fabrics, composite, ep-type material etc..The exploitation developing into functional textile of science and technology now provides guarantee, the most also for textile enterprise's development and product restructuring, serves bigger facilitation and improves the added value of textile.Study and produce the ecological and healthy functional textile product that is beneficial to man, have become as the trend that the world today develops.
In general, the functionalization of textile is mainly realized by two approach: one is that the functional treatment by fabric realizes, and this is also the main path of current functional textile exploitation;Two is the functionalization of textile fabric.Development and the gradually enhancing of people's environmental protection consciousness along with science and technology; the limitation of fabric functional Final finishing processing method is increasingly subject to the concern of people; the functional product obtained by the method processing does not only exist the defect in terms of the durability of function, the comfortableness of use and safety, and inevitable to environment in arranging the course of processing.Then can be overcome many drawbacks of fabric functional Final finishing by functional fiber machining functions textile, be the development trend obtaining functional textile.
Hosiery industry, under the leading of new and high technology, is actively adjusted the product mix, and payes attention to new raw material and the exploitation of the exploitation of new product, particularly fibre in differentiation and functional fiber kind, greatly promotes the development of hosiery industry.In Rachael blanket field, along with exploitation and utilization and the progress of technology of novel material, the most constantly widen its product scope.In addition to conventional Rachael blanket, develop high in technological content Rachael blanket and become an important developing direction.The each big authority's textile mechanism research in the world shows, the development trend in textile product field is to pursue comfortableization and multifunction.
Present consumer does not require nothing more than Rachael blanket and has warmth retention property, have that matte is plentiful, soft comfortable, plain noble quality, slim and graceful feel style and fabric good permeability, moisture absorption and desorption property good, and woollen blanket is had the multifunctionality such as antibiotic health care, environmental protection and has had demand.But at home on market Rachael blanket typically based on acrylon and terylene woollen blanket, also have least a portion of cotton and Pilus Caprae seu Ovis Rachael blanket, quality scale is relatively low or expensive, it is impossible to meet the market demand, and therefore exploitation disclosure satisfy that the Rachael blanket of consumer demand becomes a kind of trend.
Summary of the invention
In order to solve above-mentioned technical problem, the invention provides the production method of a kind of mint fibers Rachael blanket.The mint fibers Rachael blanket of the present invention has that fine hair is submissive, stands upright, good springiness, and fabric skin-friendly, moisture absorption and desorption property, the advantage of good permeability additionally have the feature such as antibiotic health care, environmental protection.
The concrete technical scheme of the present invention is: the production method of a kind of mint fibers Rachael blanket, using mint fibers long filament as plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare mint fibers Rachael blanket semi-finished product.
2), prefinishing: carry out described mint fibers Rachael blanket semi-finished product shaping, bristle, hot light, clot.
3), dyeing and finishing: the mint fibers Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction cleaning liquid, the mint fibers Rachael blanket semi-finished product after dyeing are carried out reduction cleaning, successively neutralize through peracetic acid solution, wash out cylinder, drying, steaming and color fixing after reduction cleaning, use flexible smooth agent that mint fibers Rachael blanket semi-finished product are carried out flexible smooth process after steaming and color fixing, the most again dry.
4), Final finishing: the mint fibers Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching, obtain corn fiber Rachael blanket finished product.
5), product inspection, packaging warehouse-in.
The inventive method, according to the feature of mint fibers long filament, in conjunction with the performance of HDR5DPLM30 raschel machine, designs the upper machine tissue meeting its characteristic.Prefinishing technique is formulated according to mint fibers long filament performance;Grey cloth after cuing open floss first carrying out pre-setting and hot light processes, make the carpet surface fine hair crimpness before dyeing reduce, pieces dissipates pine and is conducive to dyeing, soft treatment and Final finishing processing.
The preparation method of described mint fibers long filament is as follows: carries out spinning by melt spinning machine after polyester slice, Herba Menthae particle, lignocellulose being blended, prepares mint fibers long filament;Wherein said Herba Menthae particle accounts for the 15-25wt% of overall content, and lignocellulose accounts for the 25-35wt% of overall content.
This patent selects natural mint fibers as Rachael blanket plush yarn, Herba Menthae is one of China's conventional Chinese medicine, menthol in Herba Menthae and 8 kinds of tea naphthols acid, it the traditional Chinese medical science is conventional cool property sweating antipyretic medicine, have refrigerant, antipruritic, antiinflammatory, effect of pain relieving, use mint fibers as raw material, mint fibers is by the Main Ingredients and Appearance menthol in Herba Menthae and 8 kinds of tea naphthalene phenolic acid extracts, without adding any chemical substance in extraction process, in conjunction with nano-pulverization technology and microcapsule technology, the menthol of natural plants Herba Menthae and 8 kinds of tea naphthols acid compositions are combined spinning fibroblast with the form of microcapsule with cellulose blending, this fiber is a kind of novel plants antimicrobial fiber.By organizational structure reasonable in design for this raw material, ingenious combination chaining, latitude substrate cloth raw material, by the research and development to key technologies such as warp knit weaving, prefinishing, printing and dyeing and Final finishing productions, thus improve quality and the added value of product, make woollen blanket keep soft, fine and smooth, smooth on the basis of, more have antibiotic health care, the feature such as nice and cool.Product is in use, continuous CONTACT WITH FRICTION along with human body skin Yu fiber, effective component in Herba Menthae is constantly discharged from fiber, and absorbed by human body, the successful development of this project meets the needs of Green Textiles, i.e. ensure that the characteristic of the comfortable softness of Rachael blanket, more outstanding natural, green, healthy concept.
As preferably, tricot machine described in step 1) is HDR5DPLM30 type raschel machine, and braiding speed is 420r/min, L1 Yu L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear;Wherein, the specification of described mint fibers long filament is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
As preferably, step 2) sizing time, mint fibers Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid with the ramp of 2 DEG C/min to 50 DEG C, then 45min it is incubated, after being cooled to room temperature with the speed of 3 DEG C/min, mint fibers Rachael blanket semi-finished product are taken out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
As preferably, before carrying out dyeing and finishing, mint fibers Rachael blanket semi-finished product after prefinishing are carried out pretreatment: mint fibers Rachael blanket semi-finished product submergence is carried out impregnation process in ethanol, wherein mint fibers Rachael blanket semi-finished product are 1:(2-4 with the mass ratio of ethanol), dip time is 20-40min.
Owing to fiber surface has one layer of oil film, therefore when dyeing, due to the obstruct of oil film, dyestuff not easily penetrates into into fibrous inside, causes Color poor.And before dyeing, fabric is carried out in ethanol impregnation process, it is possible to dissolve part oil film so that it is lower thickness, it is simple to dyestuff penetration enters fibrous inside, increase color fastness.However it is necessary that control dip time and ethanol consumption, it is to avoid oil film excessive dissolution and cause fibre-fibre friction, finally affect glossiness and the smoothness of fiber surface.
As preferably, when step 3) dyes, high-temperature and high pressure dyeing process is selected to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls at 5.6-6.8;Then being immersed in dye liquor by mint fibers Rachael blanket semi-finished product, mint fibers Rachael blanket semi-finished product are 1:10 with the mass ratio of dye liquor;Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 DEG C with the speed of 1.5 DEG C/min, then dye liquor is warming up to 125-135 DEG C with the speed of 1 DEG C/min, last fixation 60min;Dye wherein uses during dark product Palanilp nonionic dye;Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
In the present invention, according to mint fibers in morphosis, aggregated structure, physical and mechanical properties, the performances such as the sensitivity of chemical agent, fibrillation are formulated suitable dyeing and finishing technology.Mint fibers is a kind of polyester-based fibers, and molten point is relatively low, and non-refractory is especially sensitive to alkali, it is easy to hydrolysis damage;In acid bath, fiber also can occur significantly to hydrolyze damage, in order to ensure the affinity of mint fibers La Er woollen blanket, dye-uptake, dyeing speed and level-dyeing property, has selected the Colour Difference condition of low temperature, alkali-free, low acid;In dye during dark color, select PalanilP nonionic dye;During dye light-coloured prods, select Mibct keton polyester dispersion dyestuff, dyeed by SYC-300 high-temperature pressure dyeing, it is possible to reduce environmental pollution.
As preferably, reduction cleaning liquid described in step 3) includes synthesis detergent, the tea saponin of 1.0-1.5g/L, 10-15g/L Sargassum powder and the sodium alginate of 1.0-2.0g/L and water, bath raio 1:25, temperature 50-55 DEG C, the scavenging period 25-35min of 1.5-2.5g/L;During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1-2g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 5-10g/L and the nano titanium oxide of 0.3-0.5g/L;After reduction cleaning, the concentration of acetum used is 0.5wt%;When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent;Described flexible smooth agent includes the 2.5-3% that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are water weight, and the weight of smooth agent is the 1.5-2% of water weight, and the weight of tween is the 0.5-1% of water weight.
In the present invention; owing to mint fibers is the most alkaline-resisting; low-temperature neutral bath is used to process time at Rou Ruan; when reduction cleaning soft treatment; after cleanout fluid cleans; make mint fibers Rachael blanket have soft smooth, gloss is beautiful, adding Sargassum powder in reduction cleaning liquid is to make it form a tunic to protect woollen blanket at carpeted surface, having anti-oxidation function;Tea saponin is a kind of nonionic surfactant, therefore, it is possible to use as abluent, tea saponin is compared with common abluent simultaneously, has preferable stability, it is possible to give full play to the surface activity of himself in the water environment of various hardness.In addition tea saponin also has certain color fixative blast, increases the effect of color fastness, when after Woollen blanket printing fixation, it is possible to promote its outward appearance vividness fiber.Na is added when dye is dark3CO3And sodium hydrosulfite, more effectively remove the loose colour of fiber surface;Add tea polyphenols and nano titanium oxide, be then to improve the anti-oxidation function of woollen blanket and anti-microbial property.
Lecithin is oily matter, has good lubricant effect, it is possible to absorbed by fiber, thus promotes toughness and the feel of fiber so that the fine hair of woollen blanket has good anti-pressure ability.In addition lecithin is harmless to health, for green material.Tween has good emulsification, also is able to increase the dissolubility of lecithin simultaneously.
As preferably, described lecithin is through modification: post-heating of being mixed homogeneously with the lactic acid solution that concentration is 50-60wt% by lecithin stirs, the mass ratio of wherein said lecithin and lactic acid solution is 100:(4-6), heating-up temperature is 70-80 DEG C, heat time heating time 40-60min;It is gradually added into, to reactant liquor, the hydrogen peroxide solution that concentration is 30wt% that quality is described lecithin 20-25% during heated and stirred;To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxylating modified lecithin.
The mobility of common lecithin is poor, and viscosity is higher, is unfavorable for being absorbed by fiber and in fiber surface film forming, and the mobility of modified lecithin is therefore greatly increased, and is easier to be absorbed and in fiber surface film forming by fiber.
As preferably, in step 4) Final finishing, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 110-120 DEG C, speed 17-20m/min of shaping;Bristle uses the double roller brushing machine of MB211E type, speed 3-4m/min, enters machine along hair, and bristle spaces 2.5mm;Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120-130 DEG C, speed 7-10m/min;Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out mint fibers Rachael blanket front scalding and cuts, temperature 120-130 DEG C, speed 8-10m/min;Fluffing uses ME331E raising machine, fluffs mint fibers Rachael blanket reverse side, speed 8-10m/min.
As preferably, the preparation method of described Herba Menthae particle is as follows: takes clean mentha leave and pulls an oar it, prepare Herba Menthae serosity, described Herba Menthae serosity is joined in the ethanol solution that concentration is 60-70wt% and carries out microwave radiation exaraction, extract and after filtering, prepare Herba Menthae extracting solution, wherein Herba Menthae serosity and the mass ratio 1:(5-10 of ethanol solution), microwave extraction power 500-600W, extraction time 10-15min, Extracting temperature 60-70 DEG C;In described Herba Menthae extracting solution, add sodium alginate, beta-schardinger dextrin-and stir, preparing Herba Menthae particle after concentrating, being spray-dried again, wherein said Herba Menthae extracting solution, sodium alginate, the mass ratio of beta-schardinger dextrin-are (25-35): 1:1.
Common mint fibers be by spinning after fiber impregnation process in Herba Menthae extracting solution, thus prepare mint fibers, but in this way prepare mint fibers through repeatedly washing after can gradually drop.The mint fibers of the present invention is that with polyester slice and lignin fibre, Herba Menthae particle is together carried out melt spinning.In Herba Menthae particle, the active component in menthe, as carrier, is embedded absorption, thus improves the load stability of mint active composition by sodium alginate, beta-schardinger dextrin-effectively, it is not easy to run off.
It is compared with the prior art, the invention has the beneficial effects as follows: the mint fibers Rachael blanket of the present invention has that fine hair color and luster is good, submissive, stands upright, good springiness, fabric skin-friendly, moisture absorption and desorption property, the advantage of good permeability and antibiotic health care, the feature of environmental protection.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
The production method of a kind of mint fibers Rachael blanket, using mint fibers long filament as plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare mint fibers Rachael blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear;Wherein, the specification of described mint fibers long filament is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
2), prefinishing: carry out described mint fibers Rachael blanket semi-finished product shaping, bristle, hot light, clot.During sizing, mint fibers Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid with the ramp of 2 DEG C/min to 50 DEG C, then 45min it is incubated, after being cooled to room temperature with the speed of 3 DEG C/min, mint fibers Rachael blanket semi-finished product are taken out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: the mint fibers Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction cleaning liquid, the mint fibers Rachael blanket semi-finished product after dyeing are carried out reduction cleaning, successively neutralize through peracetic acid solution, wash out cylinder, drying, steaming and color fixing after reduction cleaning, use flexible smooth agent that mint fibers Rachael blanket semi-finished product are carried out flexible smooth process after steaming and color fixing, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls about 6.2;Then being immersed in dye liquor by mint fibers Rachael blanket semi-finished product, mint fibers Rachael blanket semi-finished product are 1:10 with the mass ratio of dye liquor;Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 DEG C with the speed of 1.5 DEG C/min, then dye liquor is warming up to 130 DEG C with the speed of 1 DEG C/min, last fixation 60min;Dye wherein uses during dark product Palanilp nonionic dye;Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.25g/L, 12.5g/L Sargassum powder and the sodium alginate of 1.5g/L and water, bath raio 1:25, temperature 52 DEG C, the scavenging period 30min of 2g/L;During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1.5g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 7.5g/L and the nano titanium oxide of 0.4g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent;Described flexible smooth agent includes that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are the 2.75% of water weight, and the weight of smooth agent is the 1.75% of water weight, and the weight of tween is the 0.75% of water weight.
4), Final finishing: the mint fibers Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching, obtain corn fiber Rachael blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 115 DEG C, speed 18m/min of shaping;Bristle uses the double roller brushing machine of MB211E type, speed 3.5m/min, enters machine along hair, and bristle spaces 2.5mm;Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 125 DEG C, speed 8m/min;Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out mint fibers Rachael blanket front scalding and cuts, temperature 125 DEG C, speed 9m/min;Fluffing uses ME331E raising machine, fluffs mint fibers Rachael blanket reverse side, speed 9m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described mint fibers long filament is as follows: carries out spinning by melt spinning machine after polyester slice, Herba Menthae particle, lignocellulose being blended, prepares mint fibers long filament;Wherein said Herba Menthae particle accounts for the 20wt% of overall content, and lignocellulose accounts for the 30wt% of overall content.
Embodiment 2
The production method of a kind of mint fibers Rachael blanket, using mint fibers long filament as plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare mint fibers Rachael blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear;Wherein, the specification of described mint fibers long filament is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
2), prefinishing: carry out described mint fibers Rachael blanket semi-finished product shaping, bristle, hot light, clot.During sizing, mint fibers Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid with the ramp of 2 DEG C/min to 50 DEG C, then 45min it is incubated, after being cooled to room temperature with the speed of 3 DEG C/min, mint fibers Rachael blanket semi-finished product are taken out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: before carrying out dyeing and finishing, mint fibers Rachael blanket semi-finished product after prefinishing are carried out pretreatment: mint fibers Rachael blanket semi-finished product submergence is carried out impregnation process in ethanol, wherein mint fibers Rachael blanket semi-finished product are 1:3 with the mass ratio of ethanol, and dip time is 30min.
Pretreated mint fibers Rachael blanket semi-finished product are positioned in dyeing liquor and dye, then with reduction cleaning liquid, the mint fibers Rachael blanket semi-finished product after dyeing are carried out reduction cleaning, successively neutralize through peracetic acid solution, wash out cylinder, drying, steaming and color fixing after reduction cleaning, use flexible smooth agent that mint fibers Rachael blanket semi-finished product are carried out flexible smooth process after steaming and color fixing, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls 6.8;Then being immersed in dye liquor by mint fibers Rachael blanket semi-finished product, mint fibers Rachael blanket semi-finished product are 1:10 with the mass ratio of dye liquor;Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 DEG C with the speed of 1.5 DEG C/min, then dye liquor is warming up to 130 DEG C with the speed of 1 DEG C/min, last fixation 60min;Dye wherein uses during dark product Palanilp nonionic dye;Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.25g/L, 12.5g/L Sargassum powder and the sodium alginate of 1.5g/L and water, bath raio 1:25, temperature 52 DEG C, the scavenging period 30min of 2g/L;During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1.5g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 7.5g/L and the nano titanium oxide of 0.4g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent;Described flexible smooth agent includes that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are the 2.8% of water weight, and the weight of smooth agent is the 1.8% of water weight, and the weight of tween is the 0.7% of water weight.
Wherein said lecithin is through modification: post-heating of being mixed homogeneously with the lactic acid solution that concentration is 55wt% by lecithin stirs, and the mass ratio of wherein said lecithin and lactic acid solution is 100:5, and heating-up temperature is 75 DEG C, heat time heating time 50min;It is gradually added into, to reactant liquor, the hydrogen peroxide solution that concentration is 30wt% that quality is described lecithin 22.5% during heated and stirred;To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxylating modified lecithin.
4), Final finishing: the mint fibers Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching, obtain corn fiber Rachael blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 115 DEG C, speed 19m/min of shaping;Bristle uses the double roller brushing machine of MB211E type, speed 3.5m/min, enters machine along hair, and bristle spaces 2.5mm;Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 125 DEG C, speed 8m/min;Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out mint fibers Rachael blanket front scalding and cuts, temperature 125 DEG C, speed 9m/min;Fluffing uses ME331E raising machine, fluffs mint fibers Rachael blanket reverse side, speed 9m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described mint fibers long filament is as follows: carries out spinning by melt spinning machine after polyester slice, Herba Menthae particle, lignocellulose being blended, prepares mint fibers long filament;Wherein said Herba Menthae particle accounts for the 15wt% of overall content, and lignocellulose accounts for the 25wt% of overall content.
In the present embodiment, the preparation method of described Herba Menthae particle is as follows: takes clean mentha leave and pulls an oar it, prepare Herba Menthae serosity, described Herba Menthae serosity is joined in the ethanol solution that concentration is 65wt% and carries out microwave radiation exaraction, extract and after filtering, prepare Herba Menthae extracting solution, wherein Herba Menthae serosity and the mass ratio 1:7.5, microwave extraction power 550W of ethanol solution, extraction time 12min, Extracting temperature 65 DEG C;Adding sodium alginate, beta-schardinger dextrin-in described Herba Menthae extracting solution and stir, then preparing Herba Menthae particle after concentrating, being spray-dried, wherein said Herba Menthae extracting solution, sodium alginate, the mass ratio of beta-schardinger dextrin-are 30:1:1.
Embodiment 3
The production method of a kind of mint fibers Rachael blanket, using mint fibers long filament as plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare mint fibers Rachael blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear;Wherein, the specification of described mint fibers long filament is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
2), prefinishing: carry out described mint fibers Rachael blanket semi-finished product shaping, bristle, hot light, clot.During sizing, mint fibers Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid with the ramp of 2 DEG C/min to 50 DEG C, then 45min it is incubated, after being cooled to room temperature with the speed of 3 DEG C/min, mint fibers Rachael blanket semi-finished product are taken out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: before carrying out dyeing and finishing, mint fibers Rachael blanket semi-finished product after prefinishing are carried out pretreatment: mint fibers Rachael blanket semi-finished product submergence is carried out impregnation process in ethanol, wherein mint fibers Rachael blanket semi-finished product are 1:2 with the mass ratio of ethanol, and dip time is 40min.
Pretreated mint fibers Rachael blanket semi-finished product are positioned in dyeing liquor and dye, then with reduction cleaning liquid, the mint fibers Rachael blanket semi-finished product after dyeing are carried out reduction cleaning, successively neutralize through peracetic acid solution, wash out cylinder, drying, steaming and color fixing after reduction cleaning, use flexible smooth agent that mint fibers Rachael blanket semi-finished product are carried out flexible smooth process after steaming and color fixing, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls about 5.6;Then being immersed in dye liquor by mint fibers Rachael blanket semi-finished product, mint fibers Rachael blanket semi-finished product are 1:10 with the mass ratio of dye liquor;Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 DEG C with the speed of 1.5 DEG C/min, then dye liquor is warming up to 125 DEG C with the speed of 1 DEG C/min, last fixation 60min;Dye wherein uses during dark product Palanilp nonionic dye;Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.0g/L, 10g/L Sargassum powder and the sodium alginate of 1.0g/L and water, bath raio 1:25, temperature 50 C, the scavenging period 35min of 1.5g/L;During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 5g/L and the nano titanium oxide of 0.3g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent;Described flexible smooth agent includes that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are the 2.5% of water weight, and the weight of smooth agent is the 1.5% of water weight, and the weight of tween is the 0.5% of water weight.
Wherein said lecithin is through modification: post-heating of being mixed homogeneously with the lactic acid solution that concentration is 50wt% by lecithin stirs, and the mass ratio of wherein said lecithin and lactic acid solution is 100:4, and heating-up temperature is 70 DEG C, heat time heating time 60min;It is gradually added into, to reactant liquor, the hydrogen peroxide solution that concentration is 30wt% that quality is described lecithin 20% during heated and stirred;To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxylating modified lecithin.
4), Final finishing: the mint fibers Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching, obtain corn fiber Rachael blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 110 DEG C, speed 17m/min of shaping;Bristle uses the double roller brushing machine of MB211E type, speed 3m/min, enters machine along hair, and bristle spaces 2.5mm;Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120 DEG C, speed 7m/min;Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out mint fibers Rachael blanket front scalding and cuts, temperature 120 DEG C, speed 8m/min;Fluffing uses ME331E raising machine, fluffs mint fibers Rachael blanket reverse side, speed 8m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described mint fibers long filament is as follows: carries out spinning by melt spinning machine after polyester slice, Herba Menthae particle, lignocellulose being blended, prepares mint fibers long filament;Wherein said Herba Menthae particle accounts for the 25wt% of overall content, and lignocellulose accounts for the 35wt% of overall content.
In the present embodiment, the preparation method of described Herba Menthae particle is as follows: takes clean mentha leave and pulls an oar it, prepare Herba Menthae serosity, described Herba Menthae serosity is joined in the ethanol solution that concentration is 60wt% and carries out microwave radiation exaraction, extract and after filtering, prepare Herba Menthae extracting solution, wherein Herba Menthae serosity and the mass ratio 1:5, microwave extraction power 500W of ethanol solution, extraction time 15min, Extracting temperature 60 DEG C;Adding sodium alginate, beta-schardinger dextrin-in described Herba Menthae extracting solution and stir, then preparing Herba Menthae particle after concentrating, being spray-dried, wherein said Herba Menthae extracting solution, sodium alginate, the mass ratio of beta-schardinger dextrin-are 25:1:1.
Embodiment 4
The production method of a kind of mint fibers Rachael blanket, using mint fibers long filament as plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprises the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare mint fibers Rachael blanket semi-finished product.Wherein said tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear;Wherein, the specification of described mint fibers long filament is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
2), prefinishing: carry out described mint fibers Rachael blanket semi-finished product shaping, bristle, hot light, clot.During sizing, mint fibers Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid with the ramp of 2 DEG C/min to 50 DEG C, then 45min it is incubated, after being cooled to room temperature with the speed of 3 DEG C/min, mint fibers Rachael blanket semi-finished product are taken out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
3), dyeing and finishing: before carrying out dyeing and finishing, mint fibers Rachael blanket semi-finished product after prefinishing are carried out pretreatment: mint fibers Rachael blanket semi-finished product submergence is carried out impregnation process in ethanol, wherein mint fibers Rachael blanket semi-finished product are 1:4 with the mass ratio of ethanol, and dip time is 20min.
Pretreated mint fibers Rachael blanket semi-finished product are positioned in dyeing liquor and dye, then with reduction cleaning liquid, the mint fibers Rachael blanket semi-finished product after dyeing are carried out reduction cleaning, successively neutralize through peracetic acid solution, wash out cylinder, drying, steaming and color fixing after reduction cleaning, use flexible smooth agent that mint fibers Rachael blanket semi-finished product are carried out flexible smooth process after steaming and color fixing, the most again dry.
When dyeing, high-temperature and high pressure dyeing process is selected to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls about 6;Then being immersed in dye liquor by mint fibers Rachael blanket semi-finished product, mint fibers Rachael blanket semi-finished product are 1:10 with the mass ratio of dye liquor;Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 DEG C with the speed of 1.5 DEG C/min, then dye liquor is warming up to 135 DEG C with the speed of 1 DEG C/min, last fixation 60min;Dye wherein uses during dark product Palanilp nonionic dye;Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
Described reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.5g/L, 15g/L Sargassum powder and the sodium alginate of 2.0g/L and water, bath raio 1:25, temperature 55 DEG C, the scavenging period 25-35min of 2.5g/L;During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 2g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 10g/L and the nano titanium oxide of 0.5g/L.
After reduction cleaning, the concentration of acetum used is 0.5wt%.
When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent;Described flexible smooth agent includes that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are the 3% of water weight, and the weight of smooth agent is the 2% of water weight, and the weight of tween is the 1% of water weight.
Wherein said lecithin is through modification: post-heating of being mixed homogeneously with the lactic acid solution that concentration is 60wt% by lecithin stirs, and the mass ratio of wherein said lecithin and lactic acid solution is 100:6, and heating-up temperature is 80 DEG C, heat time heating time 60min;It is gradually added into, to reactant liquor, the hydrogen peroxide solution that concentration is 30wt% that quality is described lecithin 25% during heated and stirred;To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxylating modified lecithin.
4), Final finishing: the mint fibers Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching, obtain corn fiber Rachael blanket finished product.Wherein, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 120 DEG C, speed 20m/min of shaping;Bristle uses the double roller brushing machine of MB211E type, speed 4m/min, enters machine along hair, and bristle spaces 2.5mm;Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 130 DEG C, speed 10m/min;Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out mint fibers Rachael blanket front scalding and cuts, temperature 130 DEG C, speed 10m/min;Fluffing uses ME331E raising machine, fluffs mint fibers Rachael blanket reverse side, speed 10m/min.
5), product inspection, packaging warehouse-in.
The preparation method of described mint fibers long filament is as follows: carries out spinning by melt spinning machine after polyester slice, Herba Menthae particle, lignocellulose being blended, prepares mint fibers long filament;Wherein said Herba Menthae particle accounts for the 20wt% of overall content, and lignocellulose accounts for the 35wt% of overall content.
In the present embodiment, the preparation method of described Herba Menthae particle is as follows: takes clean mentha leave and pulls an oar it, prepare Herba Menthae serosity, described Herba Menthae serosity is joined in the ethanol solution that concentration is 70wt% and carries out microwave radiation exaraction, extract and after filtering, prepare Herba Menthae extracting solution, wherein Herba Menthae serosity and the mass ratio 1:10, microwave extraction power 600W of ethanol solution, extraction time 105min, Extracting temperature 70 DEG C;Adding sodium alginate, beta-schardinger dextrin-in described Herba Menthae extracting solution and stir, then preparing Herba Menthae particle after concentrating, being spray-dried, wherein said Herba Menthae extracting solution, sodium alginate, the mass ratio of beta-schardinger dextrin-are 35:1:1.
Raw materials used, equipment in the present invention, unless otherwise noted, is the conventional raw material of this area, equipment;Method therefor in the present invention, unless otherwise noted, is the conventional method of this area.
The above, be only presently preferred embodiments of the present invention, not impose any restrictions the present invention, every any simple modification, change and equivalent transformation made above example according to the technology of the present invention essence, all still falls within the protection domain of technical solution of the present invention.

Claims (8)

1. the production method of a mint fibers Rachael blanket, it is characterised in that using mint fibers long filament as plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprise the steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare mint fibers Rachael blanket semi-finished product;
2), prefinishing: carry out described mint fibers Rachael blanket semi-finished product shaping, bristle, hot light, clot;Wherein, when sizing, mint fibers Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid with the ramp of 2 DEG C/min to 50 DEG C, then 45min it is incubated, after being cooled to room temperature with the speed of 3 DEG C/min, mint fibers Rachael blanket semi-finished product are taken out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20;
3), dyeing and finishing: the mint fibers Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction cleaning liquid, the mint fibers Rachael blanket semi-finished product after dyeing are carried out reduction cleaning, successively neutralize through peracetic acid solution, wash out cylinder, drying, steaming and color fixing after reduction cleaning, use flexible smooth agent that mint fibers Rachael blanket semi-finished product are carried out flexible smooth process after steaming and color fixing, the most again dry;
4), Final finishing: the mint fibers Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching, obtain corn fiber Rachael blanket finished product;
5), product inspection, packaging warehouse-in;
The preparation method of described mint fibers long filament is as follows: carries out spinning by melt spinning machine after polyester slice, Herba Menthae particle, lignocellulose being blended, prepares mint fibers long filament;Wherein said Herba Menthae particle accounts for the 15-25wt% of overall content, and lignocellulose accounts for the 25-35wt% of overall content.
2. the production method of mint fibers Rachael blanket as claimed in claim 1, it is characterized in that, tricot machine described in step 1) is HDR5DPLM30 type raschel machine, braiding speed is 420r/min, L1 Yu L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear;Wherein, the specification of described mint fibers long filament is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
3. the production method of mint fibers Rachael blanket as claimed in claim 1, it is characterized in that, before carrying out dyeing and finishing, mint fibers Rachael blanket semi-finished product after prefinishing are carried out pretreatment: mint fibers Rachael blanket semi-finished product submergence is carried out impregnation process in ethanol, wherein mint fibers Rachael blanket semi-finished product are 1:(2-4 with the mass ratio of ethanol), dip time is 20-40min.
4. the production method of mint fibers Rachael blanket as claimed in claim 1, it is characterised in that when step 3) dyes, selects high-temperature and high pressure dyeing process to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls at 5.6-6.8;Then being immersed in dye liquor by mint fibers Rachael blanket semi-finished product, mint fibers Rachael blanket semi-finished product are 1:10 with the mass ratio of dye liquor;Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 DEG C with the speed of 1.5 DEG C/min, then dye liquor is warming up to 125-135 DEG C with the speed of 1 DEG C/min, last fixation 60min;Dye wherein uses during dark product Palanilp nonionic dye;Mibct is used during dye light-coloured prods Keton polyester dispersion dyestuff.
5. the production method of mint fibers Rachael blanket as claimed in claim 1, it is characterized in that, reduction cleaning liquid described in step 3) includes synthesis detergent, the tea saponin of 1.0-1.5g/L, 10-15g/L Sargassum powder and the sodium alginate of 1.0-2.0g/L and the water of 1.5-2.5g/L; bath raio 1:25; temperature 50-55 DEG C, scavenging period 25-35min;During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1-2g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 5-10g/L and the nano titanium oxide of 0.3-0.5g/L;After reduction cleaning, the concentration of acetum used is 0.5wt%;When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent;Described flexible smooth agent includes the 2.5-3% that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are water weight, and the weight of smooth agent is the 1.5-2% of water weight, and the weight of tween is the 0.5-1% of water weight.
6. the production method of mint fibers Rachael blanket as claimed in claim 5, it is characterized in that, described lecithin is through modification: post-heating of being mixed homogeneously with the lactic acid solution that concentration is 50-60wt% by lecithin stirs, wherein said lecithin is 100:(4-6 with the mass ratio of lactic acid solution), heating-up temperature is 70-80 DEG C, heat time heating time 40-60min;It is gradually added into, to reactant liquor, the hydrogen peroxide solution that concentration is 30wt% that quality is described lecithin 20-25% during heated and stirred;To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxylating modified lecithin.
7. the production method of mint fibers Rachael blanket as claimed in claim 1, it is characterised in that in step 4) Final finishing, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 110-120 DEG C, speed 17-20m/min of shaping;Bristle uses the double roller brushing machine of MB211E type, speed 3-4m/min, enters machine along hair, and bristle spaces 2.5mm;Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120-130 DEG C, speed 7-10m/min;Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out mint fibers Rachael blanket front scalding and cuts, temperature 120-130 DEG C, speed 8-10m/min;Fluffing uses ME331E raising machine, fluffs mint fibers Rachael blanket reverse side, speed 8-10m/min.
8. the production method of mint fibers Rachael blanket as claimed in claim 1, it is characterized in that, the preparation method of described Herba Menthae particle is as follows: takes clean mentha leave and pulls an oar it, prepare Herba Menthae serosity, described Herba Menthae serosity is joined in the ethanol solution that concentration is 60-70wt% and carries out microwave radiation exaraction, extract and after filtering, prepare Herba Menthae extracting solution, wherein Herba Menthae serosity and the mass ratio 1:(5-10 of ethanol solution), microwave extraction power 500-600W, extraction time 10-15min, Extracting temperature 60-70 DEG C;In described Herba Menthae extracting solution, add sodium alginate, beta-schardinger dextrin-and stir, preparing Herba Menthae particle after concentrating, being spray-dried again, wherein said Herba Menthae extracting solution, sodium alginate, the mass ratio of beta-schardinger dextrin-are (25-35): 1:1.
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