CN106367882A - Production technology of ice jade fiber raschel blanket - Google Patents
Production technology of ice jade fiber raschel blanket Download PDFInfo
- Publication number
- CN106367882A CN106367882A CN201610748795.3A CN201610748795A CN106367882A CN 106367882 A CN106367882 A CN 106367882A CN 201610748795 A CN201610748795 A CN 201610748795A CN 106367882 A CN106367882 A CN 106367882A
- Authority
- CN
- China
- Prior art keywords
- ice
- jade fiber
- fiber raschel
- raschel blanket
- finished product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
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Classifications
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- D—TEXTILES; PAPER
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- D06C11/00—Teasing, napping or otherwise roughening or raising pile of textile fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D—TEXTILES; PAPER
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
- D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
- D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
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Abstract
The invention relates to the field of blanket preparation and discloses a production method of an ice jade fiber raschel blanket. The production method comprises the following steps: 1) weaving: performing warping, weaving and velvet cutting of plush yarn and ground yarn to obtain a semi-finished product of the ice jade fiber raschel blanket; 2) pre-finishing: performing setting, brushing, luster finishing and rolling of the fabric; 3) dyeing and finishing: dyeing the fabric, then performing reduction cleaning on the fabric, neutralizing with an acetic acid solution, washing and discharging, drying, performing aging and color fixation and softening and smoothing treatment, and finally, drying again; 4) after-finishing: performing drying and setting, front luster finishing, front brushing, front ironing and shearing, back fluffing, back brushing, back luster finishing, back grabbing and shearing, re-setting, front ironing and shearing, back ironing and shearing and cutting strip sewing of the fabric; and 5) performing finished product inspection, packaging and storing. In the ice jade fiber raschel blanket, the fluff is smooth and upright and has good elasticity, and the fabric has good skin friendliness, moisture absorption and release properties and air permeability; and the ice jade fiber raschel blanket has the characteristics of antibacterial and healthcare properties and environmental friendliness.
Description
Technical field
The invention belongs to woollen blanket preparation field, more particularly, to a kind of fine hair color and luster is good, submissive, stand upright, elasticity is good, fabric parent
Skin, moisture absorption and desorption property, improve blood circulation, enhance metabolism, the advantage of good permeability and ice are felt well jade fiber raschel
The production technology of woollen blanket.
Background technology
With the raising of people's material and culture level, the requirement to textile for the people is also improving, and does not require nothing more than warming, beautiful
See, and more focus on comfortableness and feature.Functional textile becomes one of following developing trend of textile industry, will be with
Fine count fiber textile, non-woven fabrics, composite, ep-type material etc. collectively form the big tendency of following textile.Section now
The exploitation developing into functional textile of skill provides guarantee, also develops and product restructuring for textile enterprise simultaneously, rises
To larger facilitation and improve the added value of textile.Research and the function of producing be beneficial to man ecology and health
Property textile product, have become as the world today development trend.
In general, the functionalization of textile mainly passes through two approach realizations: one is the functional treatment by fabric
To realize, this is also the main path of current functional textile exploitation；Two is the functionalization of textile fabric.With science and technology
Development and people's environmental protection consciousness gradually enhancing, the limitation of fabric functional Final finishing processing method is increasingly subject to people
Concern, do not only exist durability, the comfortableness using and the safety of function by the method functional product of obtaining of processing
Property aspect defect, and in arranging the course of processing inevitable to environment.Work(is processed by functional fiber
Energy property textile then can overcome many drawbacks of fabric functional Final finishing, is the development trend obtaining functional textile.
Hosiery industry, under the leading of new and high technology, is actively adjusted the product mix, and payes attention to the exploitation of new raw material and new product,
The exploitation of particularly fibre in differentiation and functional fiber kind, greatly promotes the development of hosiery industry.In Rachael blanket
Field, along with exploitation and the progress of utilization and technology of novel material, is constantly widening its product scope.Except commonly use
Outside Rachael blanket, developing high in technological content Rachael blanket becomes an important developing direction.The each big authority in the world spins
The research of loom structure shows, the development trend in textile product field is to pursue comfortableization and multifunction.
Present consumer does not require nothing more than Rachael blanket and has warmth retention property, has that matte is plentiful, soft comfortable, plain height
Expensive, slim and graceful feel style and fabric good permeability, moisture absorption and desorption property are good, and have antibiotic health care, green ring to woollen blanket
The multifunctionalities such as guarantor have demand.But Rachael blanket is typically based on acrylon and terylene woollen blanket in the domestic market, also
Least a portion of cotton and Pilus Caprae seu Oviss Rachael blanket, quality scale relatively low or expensive it is impossible to meet the market demand, therefore develop
Disclosure satisfy that the Rachael blanket of consumer demand becomes a kind of trend.
Ice refreshing jade fiber is that natural jade becomes nano-scale particle through attrition process, using nucleocapsid structure two-shipper energy principle skill
Art, with terylene as carrier, in spinning process add nanoscale ice feel well jade through spinning technique process differential new
Fiber.It is slow that this product has a heat absorption, the features such as rapid heat dissipation, based on fiber property itself, when this fabric contacts with skin, more commonly
Fabric is compared temperature and can be reduced 1-2 DEG C.If for a long time according to body, ectonexine can produce 5-6 DEG C of the temperature difference to sunlight, moment feels nice and cool
Function, the clothing being processed into have the features such as Comfortable ice cold boiled water, wet-guide quick-drying.Therefore this project is intended using jade is hair
Floss yarn raw material, jade is to add in spinning process, and determining the product that this product makes will not reduce clearly because of product washing
Cool, smooth effect, has the characteristics that durable wear-resistant compared with similar product Lu by Final finishing.
Content of the invention
It is an object of the invention in order to solve that existing Rachael blanket quality scale is relatively low, expensive defect and carry
For a kind of fine hair color and luster good, submissive, stand upright, elasticity good, fabric skin-friendly, moisture absorption and desorption property, improve blood circulation, promote newly old
The production technology of metabolism, the advantage of good permeability and ice refreshing jade fiber raschel blanket.
To achieve these goals, the present invention employs the following technical solutions:
A kind of production technology of ice refreshing jade fiber raschel blanket, feels well jade fiber as plush yarn raw material using ice, with drafted polyester
Silk and special fibre, as wire gauze raw material, comprise the following steps:
1), weave: on tricot machine, plush yarn and wire gauze priority are carried out by warping, weave, cut open floss, prepared ice refreshing jade fiber draws house
That woollen blanket semi-finished product；
2), prefinishing: by described ice feel well jade fiber raschel blanket semi-finished product carry out shaping, bristle, hot light, clot；
3), dyeing and finishing: the refreshing jade fiber raschel blanket semi-finished product of the ice after prefinishing are positioned in dyeing liquor and are dyeed, then
Jade fiber raschel blanket semi-finished product of ice after dyeing being felt well with reduction cleaning liquid carry out reduction cleaning, warp after elder generation after reduction cleaning
Peracetic acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, using flexible smooth agent, ice refreshing jade fiber is drawn after steaming and color fixing
She Er woollen blanket semi-finished product carry out flexible smooth process, finally dry again；
4), Final finishing: to the ice after dyeing and finishing feel well jade fiber raschel blanket semi-finished product carry out successively drying and shaping, front hot light,
Front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot
Cut, cutting sutures, obtain final product ice refreshing jade fiber raschel blanket finished product；
5), product inspection, packaging and storage；
The preparation method of described wire gauze is as follows: by after special fibre, polyester drawn yarns blending, spinning is carried out by melt spinning machine,
Prepared wire gauze；Wherein said special fibre takes up an area the 6-10% of yarn gross mass.
In the technical program, the inventive method according to ice feel well jade fiber feature, in conjunction with hdr5dplm30 La Sheer warp
The performance of volume machine, designs the upper machine tissue meeting its characteristic.Whole before being formulated according to the plush yarn performance that ice refreshing jade fiber is made
Science and engineering skill；To cuing open, the grey cloth after floss first carries out pre-setting and hot light is processed, and so that the carpet surface fine hair crimpness before dyeing is reduced, hair
Beam spreading pine is conducive to dyeing, soft treatment and Final finishing processing.
The present invention is that natural jade becomes nano-scale particle through attrition process from ice refreshing jade fiber, double using nucleocapsid structure
Function principle art, with terylene as carrier, adds nanoscale ice in spinning process and feels well what jade processed through spinning technique
Differential tencel.It is slow that this product has a heat absorption, and the features such as rapid heat dissipation, based on fiber property itself, this fabric and skin connect
When tactile, more common fabric is compared temperature and can be reduced 1-2 DEG C.If for a long time according to body, ectonexine can produce 5-6 DEG C of temperature to sunlight
Difference, the function that moment feels nice and cool, the clothing being processed into have the features such as Comfortable ice cold boiled water, wet-guide quick-drying.Therefore this project is intended adopting
It is plush yarn raw material with jade, jade is to add in spinning process, and determining the product that this product makes will not be because of product
Wash and reduce refrigerant, smooth effect, compared with similar product Lu by Final finishing, there is durable wear-resistant.
Compared with similar products, this product is keeping the spies such as similar this product gloss nature, good permeability, skin-friendly improvement
On the basis of point, this project adopts ice to feel well jade terylene base dty as the plush yarn raw material of Rachael blanket, because the refreshing jade of ice is to adopt
Natural jade becomes nano-scale particle through attrition process, because jade contains multiple mineral beneficial to human body and trace element,
As zinc, magnesium, ferrum, copper, selenium, chromium, manganese, cobalt etc., prolonged permeation enters in human body cell, can improve microcirculation, and activating cell is organized, and promotees
Enter metabolism, improving the immunologic function of human body, thus reaching the effect of prevention disease, allaying tiredness, being that the mankind are rare
Health substance.Jade fiber feel well with ice as the raw material of Rachael blanket, the Rachael blanket made is maintaining La Sheermao
On the basis of blanket traditional performance, with more the premium properties such as beautiful ice is refreshing, smooth, it is attached to for a long time and is released on the skin of human body
Put, blood circulation can be improved, enhance metabolism, thus reaching the effect of prevention disease, allaying tiredness.
Preferably, step 1) described in tricot machine be hdr5dplm30 type raschel machine, braiding speed is 420r/
Min, l1 and l5 sley bar adopts inlaid thread filling inlaid thread, and l2 adopts inlaid thread filling chaining with l4 sley bar, and l3 wool yarn sley bar is using through flat
Braiding, form of entrying is completely to wear；Wherein, the specification of described plush yarn is 150d/72f, and the specification of polyester drawn yarns is 150d/
36f.
Preferably, step 2) sizing when, ice jade fiber raschel blanket semi-finished product of feeling well are immersed treatment fluid at room temperature
In, treatment fluid to 65 DEG C, is then incubated 50min, is cooled to after room temperature with the speed of 3 DEG C/min with the ramp of 3 DEG C/min
Ice refreshing jade fiber raschel blanket semi-finished product are taken out washing, in treatment fluid, contains following material: sodium silicate 0.2g/l, Matrii Sulfas Exsiccatus
2.5g/l, aluminium silicate 0.36g/l, modified graphene 4.6g/l, chitin 1.5g/l and penetrating agent 0.5g/l, bath raio 1:20.
Preferably, the preparation method of described modified graphene is: Graphene is dissolved in diethylene glycol and obtains reaction system,
It is then slowly added into sodium hydroxide, after stirring 1-3h, is warming up to 140-160 DEG C in 2-2.5h, cool down after reaction 1-3h；Centrifugation
The precipitate obtaining uses ethanol and dichloromethane mixed solution, acetone, the deionized water wash of volume ratio 1:2 successively, and vacuum is done
Dry obtain base nuclear graphite alkene；Then, by base nuclear graphite alkene ultrasonic disperse in dehydrated alcohol, add the phosphoric acid containing mol ratio 1:1
Diester and the ethanol solution of 1,2,3,-thrihydroxy-benzene, Deca strong aqua ammonia, stirring reaction 1-1.5h at 85-95 DEG C, are centrifugally separating to obtain
Precipitate use dehydrated alcohol, deionized water wash successively, cool down after 600-850 DEG C of roasting 30min, attrition grinding obtains modification
Graphene.
Preferably, before carrying out dyeing and finishing, jade fiber raschel blanket semi-finished product that the ice after prefinishing is felt well carry out pre- place
Reason: ice refreshing jade fiber raschel blanket semi-finished product submergence is carried out impregnation process, wherein ice refreshing jade fiber raschel in ethanol
Woollen blanket semi-finished product are 1:10-15 with the mass ratio of ethanol, and dip time is 20-40min.
In the technical program, because fiber surface has one layer of oil film, therefore in dyeing, due to the obstruct of oil film,
Dyestuff not easily penetrates into into fibrous inside, leads to Color poor.And before dyeing, fabric is carried out at dipping in ethanol
Reason, can dissolve part oil film so as to lower thickness, be easy to dyestuff penetration and enter fibrous inside, increase color fastness.However it is necessary that
Control dip time and ethanol consumption, it is to avoid oil film excessive dissolution and cause fibre-fibre friction, the final light affecting fiber surface
Damp degree and smoothness.
Preferably, in step 3) in dyeing when, dyeed from high-temperature and high pressure dyeing process: prepare at normal temperatures
Dye liquor, the ph of described dye liquor controls in 5.6-6.8；Then ice refreshing jade fiber raschel blanket semi-finished product are immersed in dye liquor,
Ice refreshing jade fiber raschel blanket semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out with heat temperature raising: first will
Dye liquor is warming up to 90 DEG C with the speed of 3 DEG C/min, then with the speed of 1.5 DEG C/min, dye liquor is warming up to 125-135 DEG C, finally
Fixation 60min.
Preferably, step 3) described in reduction cleaning liquid include the synthesis detergent of 1.5-2.5g/l, 1.0-1.5g/l
The sodium alginate of tea saponin, 10-15g/l Sargassum powder and 1.0-2.0g/l and water, bath raio 1:25, temperature 50-55 DEG C, during cleaning
Between 25-35min；During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1-2g/l, the sodium hydrosulfite of 2g/l, 5-
The tea polyphenols of 10g/l and the nano titanium oxide of 0.3-0.5g/l；After reduction cleaning, the concentration of acetum used is
0.5wt%；When flexible smooth is processed, with flexible smooth agent, fabric is carried out arranging the 2-3 second；Described flexible smooth agent includes ovum
Phospholipid, smooth agent, tween 80 and water, the weight of wherein said lecithin is the heavy 2.5-3% of water, and the weight of smooth agent is water
The 1.5-2% of weight, the weight of tween is the heavy 0.5-1% of water.
In the technical program, in reduction cleaning soft treatment, after cleanout fluid cleaning, ice refreshing jade fiber is made to draw house
It is beautiful that your woollen blanket has soft smooth, gloss, adds Sargassum powder to be in order that it is in carpeted surface shape in reduction cleaning liquid
Become a tunic to protect woollen blanket, there is anti-oxidation function；Tea saponin is a kind of nonionic surfactant, therefore, it is possible to conduct
Abluent uses, and tea saponin, compared with common abluent, has preferable stability in the water environment of various hardness simultaneously,
The surface activity of its own can be given full play to.In addition tea saponin also has certain color fixative blast, increases color fastness to fiber
Effect, after Woollen blanket printing fixation, its outward appearance vividness can be lifted.Na is added when dye is dark3co3And sodium hydrosulfite, more effectively
Removal fiber surface loose colour；Add tea polyphenols and nano titanium oxide, then be in order to improve the anti-oxidation function of woollen blanket with
Anti-microbial property.
Lecithin is oily matter, has good lubricant effect, can be absorbed by fiber, thus lifting the toughness of fiber
And feel is so that the fine hair of woollen blanket has good anti-pressure ability.In addition lecithin is harmless to the body, is green material.Tell
Temperature has good emulsification, also can increase the dissolubility of lecithin simultaneously.
Preferably, the dyestuff of dyeing, through modified, by weight, 100 parts of dye particles is dispersed in 200-300
In the dimethylbenzene of part, while stirring, add 10 parts of chloropropene acyl chlorides, filtration drying obtains just modified dye particle；Then by 50
At the beginning of part, modified dye particle and 10 parts of isobutyl methacrylates are added in 120 parts of dichloromethane, and evacuation simultaneously keeps shaking
30min, is vacuum dried after filtration and modified dyestuff is obtained.
Preferably, step 4) in Final finishing, drying and shaping adopts fir4 drying and setting machine, and inverse hair enters machine, patent door width
158-162cm, temperature 110-120 DEG C, sizing speed 17-20m/min；Bristle adopts mb211e type double roller brushing machine, speed 3-
4m/min, enters machine, bristle gauge 2.5mm along hair；Hot light adopts the secondary boiling hot shearing machine of sme473h type list roller, hot light temperature 120-130
DEG C, speed 7-10m/min；Scald to cut and shearing machine is scalded using mb322e type high-speed and high-efficiency, jade fiber raschel blanket front that ice is felt well is entered
Row scalds to be cut, temperature 120-130 DEG C, speed 8-10m/min；Fluffing adopts me331e raising machine, jade fiber raschel hair that ice is felt well
Blanket reverse side is fluffed, speed 8-10m/min.
Preferably, the preparation method of described special fibre is as follows: take bamboo powder and add to the concentration of its 8-12 times of quality
For, in the sodium hydroxide solution of 8-12wt%, after being uniformly dispersed, to 110-130 DEG C, 6-8h is discongested in insulation to heating under reduced pressure；After discongesting
It is filtrated to get bamboo powder, then concentration bamboo powder added to its 8-12 times of quality is in the ethanol solution of 70-80wt%, is heated to
It is incubated 3-5h after 80-90 DEG C, is filtered again, precipitate is added water and pulls an oar, pull an oar and be 14-16 ° to slurry beating degree
Sr, then carries out defibrination, defibrination to slurry beating degree be 18-22 ° of sr, wash after making beating and vacuum distillation after obtain fiber
Element；Cellulose is added to the ionic liquid of its 18-22 times of quality, obtains cellulose solution；Add in cellulose solution
The PTT Fiber of its quality 0.4-0.6 times and the nanometer zinc chloride of its quality 0.005-0.01 times, stir
Uniformly obtain mixed solution, in mixed solution, then add the calcium chloride solution that isopyknic concentration is 2-4wt%, in 40-
After crosslinked 1-2h at 50 DEG C, freeze 1-2 days in transfer liquid nitrogen, then take out frost thing, thawed with flowing water, prepared special fibre water
Gel, then carry out solvent displacement with dehydrated alcohol, after eventually passing vacuum drying, prepared special fibre.
In the technical program, in the preparation process of the special fibre of the present invention, first prepare cellulose, the inventive method system
Standby cellulolytic activity is high, easily crosslinked.Then will be common with PTT Fiber and nano zine oxide for cellulose
Mixed, add cross-linking agent calcium chloride solution, make partial cross-linked solidification, be then passed through freezing, make cellulose crosslinked sizing, thaw and molten
After agent displacement, prepare special fibre, it is multiple with cellulose that this special fibre is actually PTT Fiber
The aeroge closing, PTT Fiber and the interlaced crosslinking of cellulose, and cellulose and spinning liquid is compatible
Property preferably, the special fibre intensity that spinning obtains is higher, and the load fastness of active substance is high.Additionally, special fibre have higher
Specific surface area so as to have the advantages that moisture absorption and desorption property, good permeability.
Beneficial effects of the present invention, the ice of the present invention is felt well, and to have fine hair color and luster good, submissive, very for jade fiber raschel blanket
Vertical, elastic good, fabric skin-friendly, the feature of moisture absorption and desorption property, the advantage of good permeability and antibiotic health care, environmental protection, use
Ice feels well jade fiber as the raw material of Rachael blanket, and the Rachael blanket made is maintaining the base of Rachael blanket traditional performance
On plinth, with more the premium properties such as beautiful ice is refreshing, smooth, it is attached to for a long time and is discharged on the skin of human body, blood can be improved
Circulation, enhances metabolism, thus reaching the effect of prevention disease, allaying tiredness.
Specific embodiment
Technical scheme in the embodiment of the present invention will be carried out with clear, complete description below it is clear that described enforcement
Example is only a part of embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, this area is common
All other embodiment that technical staff is obtained under the premise of not making creative work, broadly falls into the model of present invention protection
Enclose.
In the present invention, agents useful for same is all commercially available.
Embodiment 1
A kind of production technology of ice refreshing jade fiber raschel blanket, feels well jade fiber as plush yarn raw material using ice, with drafted polyester
Silk and special fibre, as wire gauze raw material, comprise the following steps:
1), weave: on tricot machine, plush yarn and wire gauze priority are carried out by warping, weave, cut open floss, prepared ice refreshing jade fiber draws house
That woollen blanket semi-finished product；Described tricot machine is hdr5dplm30 type raschel machine, and braiding speed is that 420r/min, l1 and l5 comb
Comb adopts inlaid thread filling inlaid thread, and l2 adopts inlaid thread filling chaining with l4 sley bar, and l3 wool yarn sley bar is knitted using through flat sennit, form of entrying
For completely wearing；Wherein, the specification of described plush yarn is 150d/72f, and the specification of polyester drawn yarns is 150d/36f；
2), prefinishing: by described ice feel well jade fiber raschel blanket semi-finished product carry out shaping, bristle, hot light, clot；During sizing,
Ice refreshing jade fiber raschel blanket semi-finished product are immersed in treatment fluid at room temperature, treatment fluid is with the ramp of 3 DEG C/min extremely
65 DEG C, then it is incubated 50min, be cooled to after room temperature with the speed of 3 DEG C/min and ice refreshing jade fiber raschel blanket semi-finished product are taken
Go out washing, in treatment fluid, contain following material: sodium silicate 0.2g/l, Matrii Sulfas Exsiccatus 2.5g/l, aluminium silicate 0.36g/l, modified graphite
Alkene 4.6g/l, chitin 1.5g/l and penetrating agent 0.5g/l, bath raio 1:20；
The preparation method of modified graphene is: Graphene is dissolved in diethylene glycol and obtains reaction system, be then slowly added into hydroxide
Sodium, is warming up to 140 DEG C after stirring 1h in 2h, cools down after reaction 1h；It is centrifuged the second that the precipitate obtaining uses volume ratio 1:2 successively
Alcohol and dichloromethane mixed solution, acetone, deionized water wash, vacuum drying obtains base nuclear graphite alkene；Then by base nuclear graphite
Alkene ultrasonic disperse, in dehydrated alcohol, adds the ethanol solution of the di-phosphate ester containing mol ratio 1:1 and 1,2,3,-thrihydroxy-benzene, drips
Enriching ammonia, stirring reaction 1h at 85 DEG C, the precipitate being centrifugally separating to obtain successively use dehydrated alcohol, deionized water wash, 600
Cool down after DEG C roasting 30min, attrition grinding obtains modified graphene；
3), dyeing and finishing: the refreshing jade fiber raschel blanket semi-finished product of the ice after prefinishing are positioned in dyeing liquor and are dyeed, then
Jade fiber raschel blanket semi-finished product of ice after dyeing being felt well with reduction cleaning liquid carry out reduction cleaning, warp after elder generation after reduction cleaning
Peracetic acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, using flexible smooth agent, ice refreshing jade fiber is drawn after steaming and color fixing
She Er woollen blanket semi-finished product carry out flexible smooth process, finally dry again；Reduction cleaning liquid include 1.5g/l synthesis detergent,
The sodium alginate of the tea saponin of 1.0g/l, 10g/l Sargassum powder and 1.0g/l and water, bath raio 1:25, temperature 50 C, scavenging period
25min；During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1g/l, the sodium hydrosulfite of 2g/l, the tea polyphenols of 5g/l
Nano titanium oxide with 0.3g/l；After reduction cleaning, the concentration of acetum used is 0.5wt%；Process in flexible smooth
When, with flexible smooth agent, fabric is carried out arranging the 2-3 second；Described flexible smooth agent include lecithin, smooth agent, tween 80 and
Water, the weight of wherein said lecithin is the 2.5% of water weight, and the weight of smooth agent is the 1.5% of water weight, and the weight of tween is water
The 0.5% of weight；
Before carrying out dyeing and finishing, jade fiber raschel blanket semi-finished product that the ice after prefinishing is felt well carry out pretreatment: ice is felt well beautiful fine
Dimension Rachael blanket semi-finished product submergence carries out impregnation process, wherein ice refreshing jade fiber raschel blanket semi-finished product and second in ethanol
The mass ratio of alcohol is 1:10, and dip time is 20min；
During dyeing, dyeed from high-temperature and high pressure dyeing process: prepare dye liquor at normal temperatures, the ph of described dye liquor controls
5.6；Then by ice feel well jade fiber raschel blanket semi-finished product be immersed in dye liquor, ice feel well jade fiber raschel blanket semi-finished product with
The mass ratio of dye liquor is 1:10；Then dye liquor is carried out with heat temperature raising: first dye liquor is warming up to 90 with the speed of 3 DEG C/min
DEG C, then dye liquor is warming up to 125 DEG C with the speed of 1.5 DEG C/min, last fixation 60min；
The dyestuff of dyeing, through modified, by weight, 100 parts of dye particles is dispersed in 200 parts of dimethylbenzene, stirring
While add 10 parts of chloropropene acyl chlorides, filtration drying obtains just modified dye particle；Then by modified dye particle at the beginning of 50 parts
It is added in 120 parts of dichloromethane with 10 parts of isobutyl methacrylates, evacuation simultaneously keeps shaking 30min, vacuum after filtration
It is dried and modified dyestuff is obtained；
4), Final finishing: to the ice after dyeing and finishing feel well jade fiber raschel blanket semi-finished product carry out successively drying and shaping, front hot light,
Front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot
Cut, cutting sutures, obtain final product ice refreshing jade fiber raschel blanket finished product；In Final finishing, drying and shaping adopts fir4 drying and setting machine,
Inverse hair enters machine, patent door width 158cm, 110 DEG C of temperature, sizing speed 17m/min；Bristle adopts mb211e type double roller brushing machine,
Speed 3m/min, enters machine, bristle gauge 2.5mm along hair；Hot light adopts the secondary boiling hot shearing machine of sme473h type list roller, hot light temperature 120
DEG C, speed 7m/min；Scald to cut and shearing machine is scalded using mb322e type high-speed and high-efficiency, jade fiber raschel blanket front that ice is felt well is scalded
Cut, 120 DEG C of temperature, speed 8m/min；Fluffing adopts me331e raising machine, and jade fiber raschel blanket reverse side that ice is felt well has been carried out
Hair, speed 8m/min；
5), product inspection, packaging and storage；
The preparation method of described wire gauze is as follows: by after special fibre, polyester drawn yarns blending, spinning is carried out by melt spinning machine,
Prepared wire gauze；Wherein said special fibre takes up an area the 6% of yarn gross mass.The preparation method of special fibre is as follows: takes bamboo powder and adds
The concentration adding to its 8 times of quality is in the sodium hydroxide solution of 8wt%, and after being uniformly dispersed, heating under reduced pressure to 110 DEG C, dredge by insulation
Solution 6h；It is filtrated to get bamboo powder after discongesting, then concentration bamboo powder added to its 8 times of quality is in the ethanol solution of 70wt%, plus
Heat is incubated 3h to after 80 DEG C, is filtered again, precipitate is added water and pulls an oar, and pulling an oar to slurry beating degree is 14 ° of sr, so
After carry out defibrination, defibrination to slurry beating degree be 18 ° of sr, wash after making beating and vacuum distillation after obtain cellulose；By fibre
Dimension element adds to the ionic liquid of its 18 times of quality, obtains cellulose solution；Add 0.4 times of its quality in cellulose solution
PTT Fiber and 0.005 times of its quality nanometer zinc chloride, be uniformly mixing to obtain mixed solution, then
Add the calcium chloride solution that isopyknic concentration is 2wt% in mixed solution, after crosslinked 1-2h at 40 DEG C, in transfer liquid nitrogen
Frost 1 day, then takes out frost thing, is thawed with flowing water, prepared special fibre hydrogel, then carries out solvent with dehydrated alcohol and put
Change, after eventually passing vacuum drying, prepared special fibre.
Embodiment 2
A kind of production technology of ice refreshing jade fiber raschel blanket, feels well jade fiber as plush yarn raw material using ice, with drafted polyester
Silk and special fibre, as wire gauze raw material, comprise the following steps:
1), weave: on tricot machine, plush yarn and wire gauze priority are carried out by warping, weave, cut open floss, prepared ice refreshing jade fiber draws house
That woollen blanket semi-finished product；Described tricot machine is hdr5dplm30 type raschel machine, and braiding speed is that 420r/min, l1 and l5 comb
Comb adopts inlaid thread filling inlaid thread, and l2 adopts inlaid thread filling chaining with l4 sley bar, and l3 wool yarn sley bar is knitted using through flat sennit, form of entrying
For completely wearing；Wherein, the specification of described plush yarn is 150d/72f, and the specification of polyester drawn yarns is 150d/36f；
2), prefinishing: by described ice feel well jade fiber raschel blanket semi-finished product carry out shaping, bristle, hot light, clot；During sizing,
Ice refreshing jade fiber raschel blanket semi-finished product are immersed in treatment fluid at room temperature, treatment fluid is with the ramp of 3 DEG C/min extremely
65 DEG C, then it is incubated 50min, be cooled to after room temperature with the speed of 3 DEG C/min and ice refreshing jade fiber raschel blanket semi-finished product are taken
Go out washing, in treatment fluid, contain following material: sodium silicate 0.2g/l, Matrii Sulfas Exsiccatus 2.5g/l, aluminium silicate 0.36g/l, modified graphite
Alkene 4.6g/l, chitin 1.5g/l and penetrating agent 0.5g/l, bath raio 1:20；The preparation method of modified graphene is: by Graphene
It is dissolved in diethylene glycol and obtains reaction system, be then slowly added into sodium hydroxide, be warming up to 145 DEG C in 2.2h after stirring 2h, reaction
Cool down after 2h；It is centrifuged ethanol and dichloromethane mixed solution, acetone, the deionization that the precipitate obtaining uses volume ratio 1:2 successively
Water washing, vacuum drying obtains base nuclear graphite alkene；Then, by base nuclear graphite alkene ultrasonic disperse in dehydrated alcohol, add to contain and rub
The ethanol solution of your di-phosphate ester than 1:1 and 1,2,3,-thrihydroxy-benzene, Deca strong aqua ammonia, stirring reaction 1.2h at 88 DEG C, centrifugation
Separate the precipitate obtaining and use dehydrated alcohol, deionized water wash successively, cool down after 750 DEG C of roasting 30min, attrition grinding obtains
Modified graphene；
3), dyeing and finishing: the refreshing jade fiber raschel blanket semi-finished product of the ice after prefinishing are positioned in dyeing liquor and are dyeed, then
Jade fiber raschel blanket semi-finished product of ice after dyeing being felt well with reduction cleaning liquid carry out reduction cleaning, warp after elder generation after reduction cleaning
Peracetic acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, using flexible smooth agent, ice refreshing jade fiber is drawn after steaming and color fixing
She Er woollen blanket semi-finished product carry out flexible smooth process, finally dry again；Reduction cleaning liquid include 2g/l synthesis detergent,
The sodium alginate of the tea saponin of 1.2g/l, 13g/l Sargassum powder and 1.8g/l and water, bath raio 1:25,53 DEG C of temperature, scavenging period
30min；During the dark product of dye, described reduction cleaning liquid also include the sodium carbonate of 1.5g/l, the sodium hydrosulfite of 2g/l, 7g/l tea many
Phenol and the nano titanium oxide of 0.4g/l；After reduction cleaning, the concentration of acetum used is 0.5wt%；Process in flexible smooth
When, with flexible smooth agent, fabric is carried out arranging the 2-3 second；Described flexible smooth agent include lecithin, smooth agent, tween 80 and
Water, the weight of wherein said lecithin is the 2.7% of water weight, and the weight of smooth agent is the 1.65% of water weight, and the weight of tween is
The 0.8% of water weight；
Before carrying out dyeing and finishing, jade fiber raschel blanket semi-finished product that the ice after prefinishing is felt well carry out pretreatment: ice is felt well beautiful fine
Dimension Rachael blanket semi-finished product submergence carries out impregnation process, wherein ice refreshing jade fiber raschel blanket semi-finished product and second in ethanol
The mass ratio of alcohol is 1:13, and dip time is 30min；
During dyeing, dyeed from high-temperature and high pressure dyeing process: prepare dye liquor at normal temperatures, the ph of described dye liquor controls
5.9；Then by ice feel well jade fiber raschel blanket semi-finished product be immersed in dye liquor, ice feel well jade fiber raschel blanket semi-finished product with
The mass ratio of dye liquor is 1:10；Then dye liquor is carried out with heat temperature raising: first dye liquor is warming up to 90 with the speed of 3 DEG C/min
DEG C, then dye liquor is warming up to 130 DEG C with the speed of 1.5 DEG C/min, last fixation 60min；
The dyestuff of dyeing, through modified, by weight, 100 parts of dye particles is dispersed in 260 parts of dimethylbenzene, stirring
While add 10 parts of chloropropene acyl chlorides, filtration drying obtains just modified dye particle；Then by modified dye particle at the beginning of 50 parts
It is added in 120 parts of dichloromethane with 10 parts of isobutyl methacrylates, evacuation simultaneously keeps shaking 30min, vacuum after filtration
It is dried and modified dyestuff is obtained；
4), Final finishing: to the ice after dyeing and finishing feel well jade fiber raschel blanket semi-finished product carry out successively drying and shaping, front hot light,
Front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot
Cut, cutting sutures, obtain final product ice refreshing jade fiber raschel blanket finished product；In Final finishing, drying and shaping adopts fir4 drying and setting machine,
Inverse hair enters machine, patent door width 160cm, 115 DEG C of temperature, sizing speed 18m/min；Bristle adopts mb211e type double roller brushing machine,
Speed 4m/min, enters machine, bristle gauge 2.5mm along hair；Hot light adopts the secondary boiling hot shearing machine of sme473h type list roller, hot light temperature 125
DEG C, speed 8m/min；Scald to cut and shearing machine is scalded using mb322e type high-speed and high-efficiency, jade fiber raschel blanket front that ice is felt well is scalded
Cut, 127 DEG C of temperature, speed 9m/min；Fluffing adopts me331e raising machine, and jade fiber raschel blanket reverse side that ice is felt well has been carried out
Hair, speed 9m/min；
5), product inspection, packaging and storage；
The preparation method of described wire gauze is as follows: by after special fibre, polyester drawn yarns blending, spinning is carried out by melt spinning machine,
Prepared wire gauze；Wherein said special fibre takes up an area the 8% of yarn gross mass.The preparation method of special fibre is as follows: takes bamboo powder and adds
The concentration adding to its 11 times of quality is in the sodium hydroxide solution of 10wt%, and after being uniformly dispersed, heating under reduced pressure, to 122 DEG C, is incubated
Discongest 7h；It is filtrated to get bamboo powder after discongesting, then concentration bamboo powder added to its 10 times of quality is in the ethanol solution of 77wt%,
It is incubated 4h after being heated to 83 DEG C, is filtered again, precipitate is added water and pulls an oar, pulling an oar to slurry beating degree is 15 ° of sr,
Then carry out defibrination, defibrination to slurry beating degree be 20 ° of sr, wash after making beating and vacuum distillation after obtain cellulose；Will
Cellulose adds to the ionic liquid of its 20 times of quality, obtains cellulose solution；Add its quality 0.5 in cellulose solution
PTT Fiber again and the nanometer zinc chloride of 0.008 times of its quality, are uniformly mixing to obtain mixed solution, so
Add, in backward mixed solution, the calcium chloride solution that isopyknic concentration is 3wt%, after crosslinked 2h at 48 DEG C, in transfer liquid nitrogen
Frost 2 days, then takes out frost thing, is thawed with flowing water, prepared special fibre hydrogel, then carries out solvent with dehydrated alcohol and put
Change, after eventually passing vacuum drying, prepared special fibre.
Embodiment 3
A kind of production technology of ice refreshing jade fiber raschel blanket, feels well jade fiber as plush yarn raw material using ice, with drafted polyester
Silk and special fibre, as wire gauze raw material, comprise the following steps:
1), weave: on tricot machine, plush yarn and wire gauze priority are carried out by warping, weave, cut open floss, prepared ice refreshing jade fiber draws house
That woollen blanket semi-finished product；Described tricot machine is hdr5dplm30 type raschel machine, and braiding speed is that 420r/min, l1 and l5 comb
Comb adopts inlaid thread filling inlaid thread, and l2 adopts inlaid thread filling chaining with l4 sley bar, and l3 wool yarn sley bar is knitted using through flat sennit, form of entrying
For completely wearing；Wherein, the specification of described plush yarn is 150d/72f, and the specification of polyester drawn yarns is 150d/36f；
2), prefinishing: by described ice feel well jade fiber raschel blanket semi-finished product carry out shaping, bristle, hot light, clot；During sizing,
Ice refreshing jade fiber raschel blanket semi-finished product are immersed in treatment fluid at room temperature, treatment fluid is with the ramp of 3 DEG C/min extremely
65 DEG C, then it is incubated 50min, be cooled to after room temperature with the speed of 3 DEG C/min and ice refreshing jade fiber raschel blanket semi-finished product are taken
Go out washing, in treatment fluid, contain following material: sodium silicate 0.2g/l, Matrii Sulfas Exsiccatus 2.5g/l, aluminium silicate 0.36g/l, modified graphite
Alkene 4.6g/l, chitin 1.5g/l and penetrating agent 0.5g/l, bath raio 1:20；The preparation method of modified graphene is: by Graphene
It is dissolved in diethylene glycol and obtains reaction system, be then slowly added into sodium hydroxide, be warming up to 160 DEG C in 2.5h after stirring 3h, reaction
Cool down after 3h；It is centrifuged ethanol and dichloromethane mixed solution, acetone, the deionization that the precipitate obtaining uses volume ratio 1:2 successively
Water washing, vacuum drying obtains base nuclear graphite alkene；Then, by base nuclear graphite alkene ultrasonic disperse in dehydrated alcohol, add to contain and rub
The ethanol solution of your di-phosphate ester than 1:1 and 1,2,3,-thrihydroxy-benzene, Deca strong aqua ammonia, stirring reaction 1.5h at 95 DEG C, centrifugation
Separate the precipitate obtaining and use dehydrated alcohol, deionized water wash successively, cool down after 850 DEG C of roasting 30min, attrition grinding obtains
Modified graphene；
3), dyeing and finishing: the refreshing jade fiber raschel blanket semi-finished product of the ice after prefinishing are positioned in dyeing liquor and are dyeed, then
Jade fiber raschel blanket semi-finished product of ice after dyeing being felt well with reduction cleaning liquid carry out reduction cleaning, warp after elder generation after reduction cleaning
Peracetic acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, using flexible smooth agent, ice refreshing jade fiber is drawn after steaming and color fixing
She Er woollen blanket semi-finished product carry out flexible smooth process, finally dry again；Reduction cleaning liquid include 2.5g/l synthesis detergent,
The sodium alginate of the tea saponin of 1.5g/l, 15g/l Sargassum powder and 2.0g/l and water, bath raio 1:25,55 DEG C of temperature, scavenging period
35min；During the dark product of dye, described reduction cleaning liquid also include the sodium carbonate of 2g/l, the sodium hydrosulfite of 2g/l, 10g/l tea many
Phenol and the nano titanium oxide of 0.5g/l；After reduction cleaning, the concentration of acetum used is 0.5wt%；Process in flexible smooth
When, with flexible smooth agent, fabric is carried out arranging the 2-3 second；Described flexible smooth agent include lecithin, smooth agent, tween 80 and
Water, the weight of wherein said lecithin is the 3% of water weight, and the weight of smooth agent is the 2% of water weight, and the weight of tween is water weight
1%；
Before carrying out dyeing and finishing, jade fiber raschel blanket semi-finished product that the ice after prefinishing is felt well carry out pretreatment: ice is felt well beautiful fine
Dimension Rachael blanket semi-finished product submergence carries out impregnation process, wherein ice refreshing jade fiber raschel blanket semi-finished product and second in ethanol
The mass ratio of alcohol is 1:15, and dip time is 40min；
During dyeing, dyeed from high-temperature and high pressure dyeing process: prepare dye liquor at normal temperatures, the ph of described dye liquor controls
5.6-6.8；Then ice refreshing jade fiber raschel blanket semi-finished product are immersed in dye liquor, ice refreshing jade fiber raschel blanket half one-tenth
Product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out with heat temperature raising: first dye liquor is warming up to the speed of 3 DEG C/min
90 DEG C, then dye liquor is warming up to 135 DEG C with the speed of 1.5 DEG C/min, last fixation 60min；
The dyestuff of dyeing, through modified, by weight, 100 parts of dye particles is dispersed in 300 parts of dimethylbenzene, stirring
While add 10 parts of chloropropene acyl chlorides, filtration drying obtains just modified dye particle；Then by modified dye particle at the beginning of 50 parts
It is added in 120 parts of dichloromethane with 10 parts of isobutyl methacrylates, evacuation simultaneously keeps shaking 30min, vacuum after filtration
It is dried and modified dyestuff is obtained；
4), Final finishing: to the ice after dyeing and finishing feel well jade fiber raschel blanket semi-finished product carry out successively drying and shaping, front hot light,
Front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot
Cut, cutting sutures, obtain final product ice refreshing jade fiber raschel blanket finished product；In Final finishing, drying and shaping adopts fir4 drying and setting machine,
Inverse hair enters machine, patent door width 162cm, 120 DEG C of temperature, sizing speed 20m/min；Bristle adopts mb211e type double roller brushing machine,
Speed 4m/min, enters machine, bristle gauge 2.5mm along hair；Hot light adopts the secondary boiling hot shearing machine of sme473h type list roller, hot light temperature 130
DEG C, speed 10m/min；Scald to cut and shearing machine is scalded using mb322e type high-speed and high-efficiency, jade fiber raschel blanket front that ice is felt well is carried out
Scald and cut, 130 DEG C of temperature, speed 10m/min；Fluffing adopts me331e raising machine, and jade fiber raschel blanket reverse side that ice is felt well enters
Row fluffing, speed 10m/min；
5), product inspection, packaging and storage；
The preparation method of described wire gauze is as follows: by after special fibre, polyester drawn yarns blending, spinning is carried out by melt spinning machine,
Prepared wire gauze；Wherein said special fibre takes up an area the 10% of yarn gross mass.The preparation method of special fibre is as follows: takes bamboo powder and adds
The concentration adding to its 12 times of quality is in the sodium hydroxide solution of 12wt%, and after being uniformly dispersed, heating under reduced pressure, to 130 DEG C, is incubated
Discongest 8h；It is filtrated to get bamboo powder after discongesting, then concentration bamboo powder added to its 12 times of quality is in the ethanol solution of 80wt%,
It is incubated 5h after being heated to 90 DEG C, is filtered again, precipitate is added water and pulls an oar, pulling an oar to slurry beating degree is 16 ° of sr,
Then carry out defibrination, defibrination to slurry beating degree be 22 ° of sr, wash after making beating and vacuum distillation after obtain cellulose；Will
Cellulose adds to the ionic liquid of its 22 times of quality, obtains cellulose solution；Add its quality 0.6 in cellulose solution
PTT Fiber again and the nanometer zinc chloride of 0.01 times of its quality, are uniformly mixing to obtain mixed solution, so
Add, in backward mixed solution, the calcium chloride solution that isopyknic concentration is 4wt%, after crosslinked 2h at 50 DEG C, in transfer liquid nitrogen
Frost 2 days, then takes out frost thing, is thawed with flowing water, prepared special fibre hydrogel, then carries out solvent with dehydrated alcohol and put
Change, after eventually passing vacuum drying, prepared special fibre.
Ice jade fiber raschel blanket of feeling well reaches following technical specification:
1st, size changing rate/(%): >=-4.0 are washed；
2nd, color fastness
2.1 color fastness to water/(level): >=3；
2.2 colour fastness to rubbings/(level): >=3
2.3 colour fastness to perspirations/(level): >=3
3rd, heat transfer coefficient/w/ (m2 DEG C): >=10.
Raw materials used in the present invention, equipment, unless otherwise noted, is conventional raw material, the equipment of this area；In the present invention
Method therefor, unless otherwise noted, is the conventional method of this area.
The above, be only presently preferred embodiments of the present invention, not the present invention imposed any restrictions, every according to the present invention
Any simple modification, change and equivalent transformation that technical spirit is made to above example, all still fall within the technology of the present invention side
The protection domain of case.
Claims (10)
1. a kind of ice feel well jade fiber raschel blanket production technology it is characterised in that using ice feel well jade fiber former as plush yarn
Material, using polyester drawn yarns with special fibre as wire gauze raw material, comprises the following steps:
1), weave: on tricot machine, plush yarn and wire gauze priority are carried out by warping, weave, cut open floss, prepared ice refreshing jade fiber draws house
That woollen blanket semi-finished product；
2), prefinishing: by described ice feel well jade fiber raschel blanket semi-finished product carry out shaping, bristle, hot light, clot；
3), dyeing and finishing: the refreshing jade fiber raschel blanket semi-finished product of the ice after prefinishing are positioned in dyeing liquor and are dyeed, then
Jade fiber raschel blanket semi-finished product of ice after dyeing being felt well with reduction cleaning liquid carry out reduction cleaning, warp after elder generation after reduction cleaning
Peracetic acid solution neutralizes, washes out cylinder, drying, steaming and color fixing, using flexible smooth agent, ice refreshing jade fiber is drawn after steaming and color fixing
She Er woollen blanket semi-finished product carry out flexible smooth process, finally dry again；
4), Final finishing: to the ice after dyeing and finishing feel well jade fiber raschel blanket semi-finished product carry out successively drying and shaping, front hot light,
Front bristle, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot
Cut, cutting sutures, obtain final product ice refreshing jade fiber raschel blanket finished product；
5), product inspection, packaging and storage；
The preparation method of described wire gauze is as follows: by after special fibre, polyester drawn yarns blending, spinning is carried out by melt spinning machine,
Prepared wire gauze；Wherein said special fibre takes up an area the 6-10% of yarn gross mass.
2. a kind of ice according to claim 1 feel well jade fiber raschel blanket production technology it is characterised in that step 1)
Described in tricot machine be hdr5dplm30 type raschel machine, braiding speed adopts inlaid thread for 420r/min, l1 and l5 sley bar
Filling inlaid thread, l2 adopts inlaid thread filling chaining with l4 sley bar, and l3 wool yarn sley bar is knitted using through flat sennit, and form of entrying is completely to wear；Its
In, the specification of described plush yarn is 150d/72f, and the specification of polyester drawn yarns is 150d/36f.
3. a kind of ice according to claim 1 feel well jade fiber raschel blanket production technology it is characterised in that step 2)
During sizing, ice refreshing jade fiber raschel blanket semi-finished product are immersed in treatment fluid at room temperature, treatment fluid is with the speed of 3 DEG C/min
It is warming up to 65 DEG C, is then incubated 50min, be cooled to after room temperature with the speed of 3 DEG C/min and ice is felt well jade fiber raschel blanket partly
Finished product takes out washing, contains following material: sodium silicate 0.2g/l, Matrii Sulfas Exsiccatus 2.5g/l, aluminium silicate 0.36g/l, change in treatment fluid
Property Graphene 4.6g/l, chitin 1.5g/l and penetrating agent 0.5g/l, bath raio 1:20.
4. a kind of ice according to claim 3 feel well jade fiber raschel blanket production technology it is characterised in that described
The preparation method of modified graphene is: Graphene is dissolved in diethylene glycol and obtains reaction system, be then slowly added into sodium hydroxide, stir
It is warming up to 140-160 DEG C after mixing 1-3h in 2-2.5h, cool down after reaction 1-3h；It is centrifuged the precipitate obtaining and use volume ratio successively
The ethanol of 1:2 and dichloromethane mixed solution, acetone, deionized water wash, vacuum drying obtains base nuclear graphite alkene；Then by base
Nuclear graphite alkene ultrasonic disperse, in dehydrated alcohol, adds the dehydrated alcohol of the di-phosphate ester containing mol ratio 1:1 and 1,2,3,-thrihydroxy-benzene
Solution, Deca strong aqua ammonia, stirring reaction 1-1.5h at 85-95 DEG C, the precipitate being centrifugally separating to obtain successively with dehydrated alcohol, go
Ion water washing, cools down after 600-850 DEG C of roasting 30min, and attrition grinding obtains modified graphene.
5. a kind of production technology of ice according to claim 1 refreshing jade fiber raschel blanket is it is characterised in that carrying out
Before dyeing and finishing, jade fiber raschel blanket semi-finished product that the ice after prefinishing is felt well carry out pretreatment: by ice refreshing jade fiber raschel hair
Blanket semi-finished product submergence carries out impregnation process, the wherein mass ratio of ice refreshing jade fiber raschel blanket semi-finished product and ethanol in ethanol
For 1:10-15, dip time is 20-40min.
6. a kind of ice according to claim 1 feel well jade fiber raschel blanket production technology it is characterised in that in step
3), during dyeing in, dyeed from high-temperature and high pressure dyeing process: prepare dye liquor at normal temperatures, the ph of described dye liquor controls
5.6-6.8；Then ice refreshing jade fiber raschel blanket semi-finished product are immersed in dye liquor, ice refreshing jade fiber raschel blanket half one-tenth
Product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out with heat temperature raising: first dye liquor is warming up to the speed of 3 DEG C/min
90 DEG C, then dye liquor is warming up to 125-135 DEG C with the speed of 1.5 DEG C/min, last fixation 60min.
7. a kind of ice according to claim 1 feel well jade fiber raschel blanket production technology it is characterised in that step 3)
Described in reduction cleaning liquid include 1.5-2.5g/l synthesis detergent, the tea saponin of 1.0-1.5g/l, 10-15g/l Sargassum powder
With sodium alginate and the water of 1.0-2.0g/l, bath raio 1:25, temperature 50-55 DEG C, scavenging period 25-35min；The dark product of dye
When, described reduction cleaning liquid also includes the sodium carbonate of 1-2g/l, the sodium hydrosulfite of 2g/l, the tea polyphenols of 5-10g/l and 0.3-0.5g/
The nano titanium oxide of l；After reduction cleaning, the concentration of acetum used is 0.5wt%；When flexible smooth is processed, with softness
Smooth agent carries out to fabric arranging the 2-3 second；Described flexible smooth agent includes lecithin, smooth agent, tween 80 and water, wherein institute
State the 2.5-3% for water weight for the weight of lecithin, the weight of smooth agent is the heavy 1.5-2% of water, and the weight of tween is water weight
0.5-1%.
8. a kind of production technology of ice according to claim 6 refreshing jade fiber raschel blanket is it is characterised in that dyeing is used
Dyestuff through modified, by weight, 100 parts of dye particles are dispersed in the dimethylbenzene of 200-300 part, while stirring
Add 10 parts of chloropropene acyl chlorides, filtration drying obtains just modified dye particle；Then by modified dye particle at the beginning of 50 parts and 10 parts
Isobutyl methacrylate is added in 120 parts of dichloromethane, and evacuation simultaneously keeps shaking 30min, vacuum drying system after filtration
Obtain modified dyestuff.
9. a kind of ice according to claim 1 feel well jade fiber raschel blanket production technology it is characterised in that step 4)
In Final finishing, drying and shaping adopts fir4 drying and setting machine, and inverse hair enters machine, patent door width 158-162cm, temperature 110-120 DEG C,
Sizing speed 17-20m/min；Bristle adopts mb211e type double roller brushing machine, speed 3-4m/min, enters machine, bristle gauge along hair
2.5mm；Hot light adopts the secondary boiling hot shearing machine of sme473h type list roller, hot light temperature 120-130 DEG C, speed 7-10m/min；Scald to cut and adopt
Scald shearing machine with mb322e type high-speed and high-efficiency, jade fiber raschel blanket front that ice is felt well carries out scalding cuts, temperature 120-130 DEG C, speed
Degree 8-10m/min；Fluffing adopts me331e raising machine, and jade fiber raschel blanket reverse side that ice is felt well fluffs, speed 8-
10m/min.
10. the production technology of the refreshing jade of a kind of ice according to claim 1 or 2 or 3 or 5 or 9 fiber raschel blanket, it is special
Levy and be, the preparation method of special fibre is as follows: take bamboo powder and add the hydrogen being 8-12wt% to the concentration of its 8-12 times of quality
In sodium hydroxide solution, after being uniformly dispersed, to 110-130 DEG C, 6-8h is discongested in insulation to heating under reduced pressure；It is filtrated to get bamboo powder after discongesting,
Again by bamboo powder add to its 8-12 times of quality concentration be 70-80wt% ethanol solution in, after being heated to 80-90 DEG C be incubated 3-
5h, is filtered again, precipitate is added water and pulls an oar, and pulling an oar to slurry beating degree is 14-16 ° of sr, then carries out defibrination,
Defibrination to slurry beating degree be 18-22 ° of sr, wash after making beating and vacuum distillation after obtain cellulose；Cellulose is added
To the ionic liquid of its 18-22 times of quality, obtain cellulose solution；Add its quality 0.4-0.6 times in cellulose solution
PTT Fiber and its quality 0.005-0.01 times nanometer zinc chloride, be uniformly mixing to obtain mix molten
Liquid, then adds the calcium chloride solution that isopyknic concentration is 2-4wt% in mixed solution, crosslinked 1-2h at 40-50 DEG C
Afterwards, freeze 1-2 days in transfer liquid nitrogen, then take out frost thing, thawed with flowing water, prepared special fibre hydrogel, then with anhydrous
Ethanol carries out solvent displacement, after eventually passing vacuum drying, prepared special fibre.
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Application publication date: 20170201 |