CN105296275B - A kind of fire fiber crops health-care spirit and its brewing method - Google Patents

A kind of fire fiber crops health-care spirit and its brewing method Download PDF

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CN105296275B
CN105296275B CN201510611949.XA CN201510611949A CN105296275B CN 105296275 B CN105296275 B CN 105296275B CN 201510611949 A CN201510611949 A CN 201510611949A CN 105296275 B CN105296275 B CN 105296275B
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numb
fire
fiery
fructus cannabis
acid
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CN105296275A (en
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张兴
郭春景
赵立涛
赵鲁元
孙宇峰
张冬青
唐焕伟
刘新杰
杨雪冰
常存
赵金海
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Heilongjiang Academy of Sciences
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Abstract

The invention belongs to beverage brewing field, and in particular to a kind of fire fiber crops health-care spirit and its brewing method.The present invention includes:Fiery numb seed screening is removed into impurity;Fiery numb seed is subjected to rice huller and grinds shelling, obtains fructus cannabis;Low temperature drying;It will carry out extrusion after fructus cannabis coarse crushing, then by milling to obtain by the numb edible raw material of fire based on fiery sesame oil fat and the numb albumen of fire;The pure water for adding 2~4 times of weight soaks 24~36 hours;0.2~0.5g/L of dry ferment is added, is fermented 3~5 days;Fermented wine is obtained after filter residue.The numb health-care spirit of fire being prepared by the present invention can not introduce high temperature, chemical reagent and enzyme, the structure of original nutriment, grease and protein in can preferably keeping fire numb.

Description

A kind of fire fiber crops health-care spirit and its brewing method
Technical field
The invention belongs to beverage brewing field, and in particular to a kind of fire fiber crops health-care spirit and its brewing method.
Background technology
Fructus cannabis is called cannabis,fructus, Chinese edestan or edestan, is the dry mature fruit of moraceae plants hemp --- fire fiber crops seed By the product of shelling.Modern research shows that fructus cannabis fat content 43%~48%, beyond oil removing, also containing 30% or so Protein, 5% or so sugared and abundant calcium, phosphorus, iron, zinc, manganese.In addition, fructus cannabis is also rich in fat oil, and fat oil In be up to 89.2% containing unrighted acid, its content such as a large amount of oleic acid, linoleic acid, leukotrienes again, particularly wherein flax Acid content reaches more than 20%, these nutriments are highly beneficial to human body.Wherein, linoleic acid plus linolenic acid ratio (ω- 6):(ω -3) is close to 3:1, meet internationally recognized nutritive proportion standard;Fructus cannabis oil can improve the enzyme activity such as SOD/GSH-Px Power, the ability for removing DPPH free radicals have exceeded olive oil, have been suitable as a kind of oxidation resistant dietary sources.Fructus cannabis matter Primary amino acid be arginine, histidine, sulfur-containing amino acid, the effect of arginine, histidine in human body is extremely important, contains Methionine and cysteine in sulphur amino acid be produce biology enzyme necessary to, fructus cannabis be quality plant albumen source it One.There is presently no technology to disclose using fructus cannabis as auxiliary material brewing spirit.
The content of the invention
It is an object of the invention to provide a kind of numb health-care spirit of fire full of nutrition, the present invention also aims to provide A kind of brewing method of the numb health-care spirit of fire.
The object of the present invention is achieved like this:
A kind of numb health-care spirit of fire, per 500mL white wine in contain palmitic acid 50-72mg, stearic acid 10-21mg, oleic acid 5- The numb protein 157-200mg of 11mg, linoleic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fire, choline 150mg.
A kind of brewing method of the numb health-care spirit of fire, includes the following steps:
(1) fiery numb seed screening is removed into impurity;
(2) fiery numb seed is subjected to rice huller and grinds shelling, obtain fructus cannabis;
(3) low temperature drying:Fructus cannabis material bed is paved into by being dissipated by the fructus cannabis of screening, in 30 DEG C of -45 DEG C of progress low temperature bakings It is dry, when drying time is 24-72 small, make fiery numb seed moisture≤5%;
(4) extrusion will be carried out after fructus cannabis coarse crushing, then is by fiery sesame oil fat and the numb albumen of fire by milling to obtain The numb edible raw material of main fire;
(5) pure water for adding 2~4 times of weight soaks 24~36 hours;
(6) 0.2~0.5g/L of dry ferment is added, is fermented 3~5 days;
(7) fermented wine is obtained after filter residue, then adds the white wine brewed and contains palmitic acid 50- into every 500mL white wine The numb protein of 72mg, stearic acid 10-21mg, oleic acid 5-11mg, linoleic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fire 157-200mg, choline 150mg.
The numb edible raw material of fire in the step (4) is carried out at deodorization the fructus cannabis after coarse crushing after extrusion The weight ratio of reason, the fermented wine and white wine is 1:10~1:4.
The beneficial effects of the present invention are:
The numb health-care spirit of fire being prepared by the present invention can not introduce high temperature, chemical reagent and enzyme, can be more preferable Holding fire fiber crops in original nutriment, the structure of grease and protein.
Brief description of the drawings
Drying time different temperatures protein storage schematic diagram when Fig. 1 is 40 small.
Fig. 2 is schematic diagram of the temperature for 37 degrees Celsius of different time protein contents.
It is the contrast schematic diagram that every numb edible raw material of 30 parts of fire adds matrimony vine sub-number and poisonous fungus alkali content shown in Fig. 3.
It is the contrast schematic diagram that every numb edible raw material of 30 parts of fire adds matrimony vine sub-number and poisonous fungus alkali content shown in Fig. 4.
Fig. 5 is the proportionate relationship and anticancer effect figure of blueberry anthocyanin extract and garlic extract.
Embodiment
The present invention is described further below in conjunction with the accompanying drawings.
Embodiment 1
Contain palmitic acid 50-72mg, stearic acid 10-21mg, oleic acid 5-11mg, linoleic acid 30- in per 500mL white wine The numb protein 157-200mg of 56.3mg, alpha-linolenic acid 10-21.2mg, fire, choline 150mg.
Embodiment 2
A kind of brewing method of the numb health-care spirit of fire, includes the following steps:
(1) fiery numb seed screening is removed into impurity;
(2) fiery numb seed is subjected to rice huller and grinds shelling, obtain fructus cannabis;
(3) low temperature drying:Fructus cannabis material bed is paved into by being dissipated by the fructus cannabis of screening, in 30 DEG C of -45 DEG C of progress low temperature bakings It is dry, when drying time is 24-72 small, make fiery numb seed moisture≤5%;
(4) extrusion will be carried out after fructus cannabis coarse crushing, then is by fiery sesame oil fat and the numb albumen of fire by milling to obtain The numb edible raw material of main fire;
(5) pure water for adding 2~4 times of weight soaks 24~36 hours;
(6) 0.2~0.5g/L of dry ferment is added, is fermented 3~5 days;
(7) fermented wine is obtained after filter residue, then adds the white wine brewed and contains palmitic acid 50- into every 500mL white wine The numb protein of 72mg, stearic acid 10-21mg, oleic acid 5-11mg, linoleic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fire 157-200mg, choline 150mg.
Embodiment 3
With embodiment 2 difference lies in:The numb edible raw material of fire in the step (4) after extrusion to coarse crushing after Fructus cannabis carry out deodorizing process, the weight ratio of the fermented wine and white wine is 1:10~1:4.
Embodiment 4
Same as Example 2, difference is the time of low temperature drying and the relation of drying temperature in the step (3) For:
T=-0.002t2-0.372t+55.08 40h≥t≥24h;
T=-0.21875t+45.75 72h >=t >=40h;
Wherein t represents the time, T represents drying temperature, and the fructus cannabis material bed thickness is less than or equal to 2cm, fructus cannabis material bed Wind speed≤the 3m/s on surface, preferred parameter t=26, T=44.056, t=40, T=37, t=50, T=34.81, t=60, T= 32.625。
By examining fructus cannabis under drying relation herein to make fiery fiber crops on the premise of nutriment is at utmost kept Benevolence loses moisture, i.e., had both ensured temperature below the temperature that the fructus cannabis that sets out goes bad, while maximum time dries it as far as possible In moisture.It is the schematic diagram of the difference drying temperature protein content when 40 is small as shown in Figure 1, abscissa unit degree Celsius, Ordinate is percentage composition shared by protein.Fig. 2 is schematic diagram of the temperature for 37 degrees Celsius of different time protein contents.It is horizontal Coordinate unit is hour, and ordinate is percentage composition shared by protein.By a series of experiment and data analysis, we It was found that when drying temperature is at 37 DEG C, drying effect is best during drying time 40 hours, i.e., the structure inside fructus cannabis is not sent out substantially Life changes and drying time is most short.
Embodiment 5
Same as Example 2, difference is by milling to obtain by the fire based on fiery sesame oil fat and the numb albumen of fire The magma that Solanaceae fruit is ground is added in numb edible raw material and is stirred the numb edible raw material of the fire for being made final.Pass through The poisonous fungus alkali content in fiery numb edible raw material and content of choline decline can be made by adding Solanaceae fruit magma, can be further ensured that The food security of fiery fiber crops edible raw material.
Embodiment 6
It is same as Example 5, difference be the magma that the Solanaceae fruit is ground be by Solanaceae fruit into Volume ratio 1 after row physical grinding:0.5 be watered stirring after obtain.
Embodiment 7
Same as Example 5, difference is at least selection capsicum, tomato, eggplant, the matrimony vine of preferable Solanaceae fruit One kind in son, franchet groundcherry persistent calyx or fruit, black nightshade, potato, cape gooseberry.It is that every numb edible raw material of 30 parts of fire adds the fruit of Chinese wolfberry as shown in Figure 3 The contrast schematic diagram of number and poisonous fungus alkali content.
The mass ratio for the magma that the preferred numb edible raw material of fire is ground with capsicum is 15:1;Fiery fiber crops edible raw material with The mass ratio for the magma that tomato is ground is 17:1;The mass ratio for the magma that fiery fiber crops edible raw material is ground with eggplant is 17:1;The mass ratio for the magma that fiery fiber crops edible raw material is ground with the fruit of Chinese wolfberry is 33:1;Fiery fiber crops edible raw material is ground with franchet groundcherry persistent calyx or fruit The mass ratio for grinding obtained magma is 37:1;The mass ratio for the magma that fiery fiber crops edible raw material is ground with black nightshade is 43:1;Fire The mass ratio for the magma that numb edible raw material is ground with potato is 17:1;What fiery fiber crops edible raw material was ground with cape gooseberry The mass ratio of magma is 35:1.Poisonous fungus alkali content≤0.01mg/kg, content of choline 7-8mg/ in the numb edible raw material of fire at this time kg.It is the contrast schematic diagram that every numb edible raw material of 30 parts of fire adds matrimony vine sub-number and poisonous fungus alkali content as shown in Figure 4.
Understand that in fruit of Chinese wolfberry magma mass ratio be 33 by Fig. 3, Fig. 4 and experimental analysis:As more as possible in the present invention when 1 Suppression poisonous fungus alkali content on the basis of reservation content of choline as much as possible.
Embodiment 8
Same as Example 2, difference is that the centrifugal rotational speed of centrifugally operated is 7000r/min, and centrifugation time is 20min, further includes precipitation process among the cold press and centrifugally operated, palmitic acid content is 7.2g/ in the aliphatic acid 100g, stearic acid content 2.1g/100g, oleic acid content 11g/100g, linoleic acid content are 56.3g/100g and α-flax Acid content is 21.2g/100g, and the numb protein content of the fire is 57% -70%.
Other steps are identical with any one in embodiment 4~10, and it is as follows that difference is that fiery numb protein powder passes through Step is prepared:
(1) carry out mechanical room temperature cold press using fiery numb edible raw material and centrifugally operated obtains fiery sesame oil fat and the numb protein of fire Stratified mixture;
(2) fiery sesame oil fat with the stratified mixture of fiery numb albumen separate using 0.22 μm or 0.45 μm of pellicle To fiery sesame oil fat;
(3) low pressure is carried out to the numb protein of remaining fire after separation and vacuumizes gasification process, further filtered out grease, obtain The numb protein dregs of rice of fire of purity higher;
(4) the fiery numb protein dregs of rice are subjected to fine lapping powder and obtain fiery numb protein powder.
Embodiment 9
Other steps are identical with any one in embodiment 1~8, and difference is, in fiery numb edible raw material also extremely One kind in cyanidin extract and garlic extract is added less.
The blueberry anthocyanin extract is manufactured by the following method:
A, blueberries are smashed, it is water-soluble to be incorporated as the ethanol that its 4~4.5 times concentration is 80%~90% for example in mass ratio Liquid, with the ultrasonic wave of 180W~260W in the case of temperature is 50~60 DEG C, is extracted 3 times, extract every time 60~80min when Between, extracting solution A is obtained after filtering;
B, blueberry red autumnal leaves are smashed, example is incorporated as the ethanol water that its 10~45 times concentration is 80%~90% in mass ratio Solution, with the ultrasonic wave of 180W~260W in the case of temperature is 50~60 DEG C, is extracted 3 times, extract every time 60~80min when Between, extracting solution B is obtained after filtering;
C, to being evaporated under reduced pressure after extracting solution A and extracting solution B mixing, pressure is controlled in 0.12~0.15MPa, temperature control System obtains concentrated extracting solution at 52~58 DEG C;
D, concentrated extracting solution is subjected to adsorbing separation by AB-8 macroreticular resins, after adsorption saturation, with concentration for 60~ 70% ethanol water is eluted, and obtains blueberry anthocyanin eluent;
E, be concentrated under reduced pressure to blueberry anthocyanin eluent, by blueberry anthocyanin elution hydraulic coupling control 0.12~ 0.15MPa, temperature control are concentrated at 52~58 DEG C, obtain blueberry anthocyanin extract, its proportion 1.15~1.2 it Between;
Garlic extract is obtained by the following method:
1) garlic is put into acetum and soaked 10~12 days, water cleaning, the garlic slurries after deodorization are obtained after broken;
2) the garlic slurries after deodorization will be obtained, it is 80%~90% that row, which are incorporated as its 3~5 times concentration, in mass ratio Ethanol water, it is 6 to adjust pH value, digests 50~60min, and temperature is 30~40 DEG C;
3) the garlic slurries after enzymolysis are added into the ethanol water that concentration is 80%~90% so that current garlic slurry The mass ratio of liquid and ethanol water is 1:5~1:8,10~30min of extraction is carried out using the ultrasonic wave of 50~100W, is obtained big Garlic extracting solution;
4) garlic extract is subjected to centrifugal treating, ultrafiltration is carried out after secondary filter, ultrafiltration membrane is inoranic membrane, it shuts off point Son amount is 8000~50000Da;
5) liquid will be obtained to be concentrated under reduced pressure, and will obtain garlic extract, its proportion is 1.08~1.094g/l.
Blueberry Hua Qingsu and allicin, can effectively improve body immunity, build up health, slow down aging, strengthening eyesight, simultaneously And the effect of also extensive antibacterial, especially bacillus, fungi, virus, Amoeba, Trichomonas vaginalis, pinworm etc. have suppression Killing effect, especially acts on the enteric bacteria such as Escherichia coli, shigella dysenteriae strong.
The present invention is above-mentioned except having the advantages that, the effect also with potent antitumor, anticancer, especially intestinal cancer, pass through Experiment shows, the present invention use 4:The effect of the antitumor and cancer of 1 ratio synthetic orall liquid is considerably beyond in both Any type.
Z parts of x parts of blueberry anthocyanin extract, y parts of garlic extract and water, blueberry anthocyanin extract, allicin carry The relation of thing and water is taken to meet following require:
Wherein, a is proportion scale, its value range is a ∈ (1,6), and optimal proportion can be obtained when a values are 4.When When a values are 4, the present invention to the inhibition of cancer cell survival rate apparently higher than a take 3 when situation, but with proportion scale Increase, that is, a values it is once big when, the present invention gradually reduces the inhibition of cancer cell survival rate again, as shown in Figure 5 a values For 20 when, the present invention substantially reduces the inhibition of cancer cell survival rate.
The numb health-care spirit of fire that the present invention is made obtains due to the use of the mode that low temperature drying and filter membrane directly filter The product of the present invention is arrived, without the high temperature in tradition extraction meaning, chemical reagent extracts and the process of enzymolysis, protects as far as possible Aliphatic acid, protein structure and property in fiery numb seed has been demonstrate,proved not change.Introducing the fruit magma of Solanaceae at the same time not only makes The taste of fiery fiber crops edible raw material is changed, and greatly inhibits the content of muscarine and choline in fiery fiber crops, and makes courage Alkali content is maintained in the scope beneficial to human body.According to monitoring raw material content of choline≤10mg/kg, the white wine for adding the raw material is fitted Closing the standard for meeting human body choline intake amount has effects that to promote brain growth, improves memory.

Claims (2)

1. a kind of brewing method of the numb health-care spirit of fire, it is characterised in that include the following steps:
(1) fiery numb seed screening is removed into impurity;
(2) fiery numb seed is subjected to rice huller and grinds shelling, obtain fructus cannabis;
(3) low temperature drying:Fructus cannabis material bed is paved into by being dissipated by the fructus cannabis of screening, in 30 DEG C of -45 DEG C of progress low temperature dryings, is dried When the dry time is 24-72 small, make fiery numb seed moisture≤5%;
(4) extrusion will be carried out after fructus cannabis coarse crushing, then by milling to obtain by based on fiery sesame oil fat and the numb albumen of fire Fiery fiber crops edible raw material;
(5) pure water for adding 2~4 times of weight soaks 24~36 hours;
(6) 0.2~0.5g/L of dry ferment is added, is fermented 3~5 days;
(7) fermented wine is obtained after filter residue, then add the white wine brewed into every 500mL white wine containing palmitic acid 50-72mg, The numb protein 157- of stearic acid 10-21mg, oleic acid 5-11mg, linoleic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fire 200mg, choline 150mg;
The time of low temperature drying and the relation of drying temperature are in the step (3):
T=-0.002t2-0.372t+55.08 40h≥t≥24h;
T=-0.21875t+45.75 72h >=t >=40h;
Wherein t represents the time, T represents drying temperature, and the fructus cannabis material bed thickness is less than or equal to 2cm, fructus cannabis material bed surface Wind speed≤3m/s.
A kind of 2. brewing method of the numb health-care spirit of fire according to claim 1, it is characterised in that:In the step (4) Deodorizing process will be carried out after carrying out extrusion after fructus cannabis coarse crushing, and the weight ratio of the fermented wine and white wine is 1:10~1: 4。
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CN105820909A (en) * 2016-04-29 2016-08-03 安徽恋尚你食品有限公司 Preparation method of Moringa oleifera white wine
CN109123686A (en) * 2018-08-22 2019-01-04 黑龙江黑科科技有限责任公司 Numb seed powder high protein element meat of one kind fire with health care function and preparation method thereof
CN109355156A (en) * 2018-12-04 2019-02-19 赵为兴 A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice
CN110577870A (en) * 2019-09-20 2019-12-17 云南云酒酒业有限责任公司 Brewing method of sesame-flavor liquor
CN110692881A (en) * 2019-11-01 2020-01-17 云南中医药大学 Pure fructus cannabis health drink
CN113755293A (en) * 2020-06-04 2021-12-07 云南汉盟制药有限公司 Fructus cannabis fatty acid compound wine and preparation method thereof

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CN104450156A (en) * 2014-11-21 2015-03-25 国家粮食局科学研究院 Method for extracting grease in fructus cannabis by using aqueous enzymatic method and fructus cannabis protein drink
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KR20020035367A (en) * 2000-11-06 2002-05-11 최태규 Method For Producing Refined Rice Wine Made From Swelled Barley
CN101508951A (en) * 2009-04-01 2009-08-19 覃怀忠 Wine
CN103356904A (en) * 2013-07-11 2013-10-23 秦春耀 Gastrodia elata wine and preparation method thereof
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