CN113755293A - Fructus cannabis fatty acid compound wine and preparation method thereof - Google Patents
Fructus cannabis fatty acid compound wine and preparation method thereof Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
- C12G3/05—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides
- C12G3/055—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with health-improving ingredients, e.g. flavonoids, flavones, polyphenols or polysaccharides extracted from plants
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
- C12G3/06—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients
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Abstract
The application discloses a fructus cannabis fatty acid compound wine, which contains fatty acid and flavone; the fatty acid contains unsaturated fatty acid. Every 100ml of fructus cannabis fatty acid compound wine contains 2-80 mg of fatty acid and 0-40 mg of total flavonoids; 2-70 mg of unsaturated fatty acid is contained in 2-80 mg of fatty acid. Also discloses a preparation method of the fructus cannabis fatty acid compound wine, which comprises the steps of processing fructus cannabis powder and fructus cannabis oil fatty acid by white spirit to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 45-65 degrees. The fructus cannabis fatty acid compound wine is transparent and yellow in color, has strong unique pleasant aroma of fructus cannabis, is high in content of nutritional functional components fatty acid and flavone, high in proportion of unsaturated fatty acid, and clear in functional components, is functional health wine with important physiological health care effects on human bodies, and promotes further development and utilization of fructus cannabis resources.
Description
Technical Field
The application relates to fructus cannabis fatty acid compound wine, and belongs to the field of compound wine.
Background
Fructus cannabis, also known as cannabis sativa, fructus cannabis, and fructus cannabis, is a dry mature fruit or seed with peel removed of cannabis sativa (Cannabissativa L.) of Moraceae, is listed as the top grade in Shennong Ben Cao Jing, is sweet in taste, neutral in nature, and has the effects of tonifying spleen and deficiency, nourishing yin and moistening dryness, and activating blood and relaxing bowels, and is clinically used for treating gastric cancer, blood deficiency and fluid deficiency, intestinal dryness and constipation, heat stranguria, rheumatism, dysentery, irregular menstruation, scabies and the like.
Fructus cannabis is a medicine and food homologous and is a good raw material for various nutritious functional foods such as beverages, vegetable oil, protein nourishments, snacks, cooking ingredients, wine and the like. At present, the fructus cannabis receives more and more attention with unique and high-quality physicochemical nutritional quality, is considered as the most centralized, complete and balanced plant source of essential amino acid and essential fatty acid by scholars at home and abroad, and the market acceptance degree is continuously increased.
The fructus cannabis wine is functional health care wine prepared by taking fructus cannabis powder as a raw material and brewing or preparing, and has wide market prospect due to unique taste, pleasant aroma and rich nutrition. Fructus cannabis wine is recorded from 'Wailai Migo', 150g fructus cannabis is ground into fine powder, and is soaked in 500g rice wine, and after taking a proper amount, spleen can be supplemented, dampness can be removed, and nourishing effect and drug efficacy can be enhanced, so that the fructus cannabis wine can be used for adjuvant treatment of beriberi, namely patients with abdominal distension and stuffiness and paralysis caused by the beriberi; the fructus cannabis wine brewed by fructus cannabis in folk has the effects of tonifying consumptive disease and relaxing bowel, and the Chinese hemp beer in foreign countries has a different flavor.
At present, the preparation method of the compound wine only taking fructus cannabis as a raw material is mainly to stir and smash fructus cannabis to be directly soaked or percolated in low-alcohol-content white spirit or rice wine with the alcohol content of about 20 percent, and the prepared fructus cannabis low-alcohol-content compound wine has low fatty acid content and low unsaturated fatty acid proportion.
Fructus cannabis contains 25-45% of rich fatty acid, the ratio of omega-6: omega-3 type unsaturated fatty acid is (2.29-3.68): 1.00, and the proportion is consistent with the proportion required by normal metabolism of human body, thus being optimal for human health. The content of unsaturated fatty acid in the fatty acid is more than 90 percent and is higher than that of soybean oil, sesame oil, olive oil and the like, wherein the content of linolenic acid in the polyunsaturated fatty acid is better than that of soybean oil, cottonseed oil and corn oil, and the content of linoleic acid is only inferior to that of peanut oil and safflower oil. Linolenic acid is essential for maintaining brain and nerve functions, and has effects of resisting thrombi, reducing blood lipid, lowering blood pressure, reducing cholesterol and improving cardiovascular disease and cerebrovascular disease; linoleic acid has effects of regulating autonomic nerve, nourishing brain cell, reducing blood lipid, and relieving inflammation. In addition, the fructus cannabis also contains antioxidant flavonoid components, and has important physiological health care effect on human bodies. Therefore, there is a need to develop a hemp seed fatty acid compound wine of higher quality, which is beneficial to the human body.
Disclosure of Invention
According to one aspect of the application, the fructus cannabis fatty acid compound wine and the preparation method thereof are provided, the fructus cannabis fatty acid compound wine with definite and high content of functional components such as series fatty acids, polyunsaturated fatty acids (linolenic acid and linoleic acid), flavones and the like is provided by adopting different fructus cannabis extraction preparation processes and a method for adding a proper amount of fructus cannabis fatty acid in the processes, the quality of the fructus cannabis fatty acid compound wine is improved, and further development and utilization of fructus cannabis resources are promoted.
A fructus Cannabis fatty acid compound wine contains fatty acid and flavone;
the fatty acid contains unsaturated fatty acid.
Optionally, in the fructus cannabis fatty acid compound wine, each 100ml of the fructus cannabis fatty acid compound wine contains 2-80 mg of fatty acid and 0-40 mg of total flavonoids;
2-70 mg of unsaturated fatty acid is contained in 2-80 mg of fatty acid.
Optionally, the fructus cannabis fatty acid compound wine comprises the fatty acid in an amount independently selected from any value of 2mg, 3mg, 5mg, 8mg, 10mg, 15mg, 20mg, 25mg, 30mg, 40mg, 50mg, 60mg, 80mg or a range between any two values per 100ml of the fructus cannabis fatty acid compound wine.
Optionally, the unsaturated fatty acid accounts for 50-100% of the contained fatty acid by mass.
Optionally, the mass percentage of the unsaturated fatty acids in the contained fatty acids is independently selected from any value of 50%, 60%, 70%, 75%, 80%, 85%, 90%, 95%, 100% or a range between any two values.
Optionally, the fructus cannabis fatty acid compound wine contains the total flavone with the mass independently selected from any value of 1mg, 3mg, 5mg, 7mg, 10mg, 15mg, 18mg, 20mg, 25mg, 28mg, 30mg, 35mg and 40mg or a range value between any two values in each 100ml of fructus cannabis fatty acid compound wine.
Optionally, the fructus cannabis fatty acid compound wine contains 2-80 mg of fatty acid, 2-70 mg of unsaturated fatty acid and 0-40 mg of total flavonoids per 100ml of fructus cannabis fatty acid compound wine.
Optionally, the fructus cannabis fatty acid compound wine contains 4-70 mg of fatty acid, 2-50 mg of unsaturated fatty acid and 0-40 mg of total flavonoids per 100ml of fructus cannabis fatty acid compound wine.
Optionally, the fructus cannabis fatty acid compound wine contains 6-40 mg of fatty acid, 3-30 mg of unsaturated fatty acid and 5-40 mg of total flavonoids per 100ml of fructus cannabis fatty acid compound wine.
Optionally, the fructus cannabis fatty acid compound wine contains 5-45 mg of fatty acid, 3-30 mg of unsaturated fatty acid and 2-40 mg of total flavonoids per 100ml of fructus cannabis fatty acid compound wine.
Optionally, the unsaturated fatty acid comprises a polyunsaturated fatty acid.
Optionally, the polyunsaturated fatty acids include linolenic acid and linoleic acid.
The fructus cannabis fatty acid compound wine is transparent and yellow in wine color, has strong unique pleasant aroma of fructus cannabis, is good in taste, has high contents of nutritional functional components fatty acid and flavone, is high in proportion of unsaturated fatty acid, has a better health care effect, and is a functional health care wine with important physiological health care effect on human bodies.
According to another aspect of the application, a preparation method of the fructus cannabis fatty acid compound wine is provided.
A preparation method of fructus cannabis fatty acid compound wine at least comprises the following steps:
processing fructus Cannabis powder and oleum Cannabis fatty acid with Chinese liquor to obtain fructus Cannabis fatty acid compound wine;
the alcohol degree of the white spirit is 45-65 degrees.
In the present application, the production place of fructus cannabis is not limited, and preferably the production place is Guangxi, Yunnan, Gansu, inner Mongolia, Heilongjiang, Shandong, Henan, Hebei, Shanxi, Shaanxi, Sichuan and Anhui.
In the application, the white spirit is only common white spirit sold on the market, and the alcohol degree is required to be 45-65 degrees, so that the white spirit is high-degree white spirit. The alcohol content is low, the contents of fatty acid, unsaturated fatty acid, general flavone and the like are low, and the aroma of fructus cannabis is weak.
Optionally, the alcohol content of the white spirit may be independently selected from any value of 45 degrees, 46 degrees, 47 degrees, 48 degrees, 49 degrees, 50 degrees, 51 degrees, 52 degrees, 53 degrees, 54 degrees, 55 degrees, 56 degrees, 57 degrees, 58 degrees, 59 degrees, 60 degrees, 61 degrees, 62 degrees, 63 degrees, 64 degrees, 65 degrees, or a range value between any two of them.
Optionally, at least comprising:
(1) parching shelled fructus Cannabis, and pulverizing to obtain processed fructus Cannabis powder;
(2) processing the processed fructus cannabis powder and fructus cannabis oil fatty acid by using white spirit to obtain fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 45-65 degrees.
Optionally, step (1) comprises at least: and (3) frying the shelled fructus cannabis for 5-10 min, and crushing to 10-40 meshes to obtain the processed fructus cannabis powder.
Optionally, the crushing degree is 20-40 meshes.
Optionally, in the step (2), 4-100L of white wine is added into each 1kg of the processed fructus cannabis powder; the volume ratio of the addition mass of the hemp oil fatty acid to the white spirit is 10-100 mg/L.
Optionally, the volume of the Chinese liquor added per 1kg of processed fructus cannabis powder is independently selected from any value of 5L, 8L, 10L, 12L, 15L, 30L, 40L, 50L, 60L, 70L, 80L, 90L, 100L or a range between any two values.
Optionally, the added mass of the hemp oil fatty acid and the volume ratio of the white spirit are independently selected from any value of 10mg/L, 15mg/L, 20mg/L, 25mg/L, 30mg/L, 40mg/L, 50mg/L, 60mg/L, 70mg/L, 80mg/L, 90mg/L, 100mg/L or a range value between any two values.
The hemp seed oil fatty acid is prepared by commercially available hemp seed oil through saponification, acidification, organic solvent extraction and other processes by adopting a conventional method. The hemp seed oil fatty acid has certain solubility in water and ethanol. The hemp oil fatty acid is not easy to dissolve in the low-concentration wine, and if the hemp oil fatty acid is added into the extracted wine base, a transparent and clear wine solution is not easy to obtain, the wine solution is mostly light yellow in color and turbid in color, the fatty acid cannot be completely dissolved, and the taste is poor. Adding the cannabis sativa oil fatty acid into the white spirit before extraction, and simultaneously improving the leaching and dissolution of the fatty acid by mass transfer and heat transfer enhancement operations of the cannabis sativa oil fatty acid in the extraction process, thereby achieving the purposes of improving the content of the fatty acid in the wine and increasing the proportion of unsaturated fatty acid. Wherein the unsaturated fatty acid contains a large amount of polyunsaturated fatty acids such as linolenic acid and linoleic acid. The prepared wine has clear wine color and good color.
Optionally, the treatment in step (2) comprises at least one of soaking extraction, shaking extraction, stirring reflux extraction and ultrasonic extraction.
Optionally, the soaking extraction at least comprises: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit in a soaking container, uniformly stirring, soaking, and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 45-65 degrees.
Optionally, in the soaking extraction, the ratio of the fructus cannabis powder to the white spirit is 1kg: 4-10L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-100 mg: 1L;
the soaking conditions are as follows: soaking for 4-100 days, and uniformly stirring for 0-3 times every day during the soaking period. When the soaking time is less than 4 days, the contents of fatty acid, unsaturated fatty acid and flavone are low, and the fragrance is weak.
When the stirring frequency is 0, standing and soaking.
Optionally, in the fructus cannabis fatty acid compound wine prepared by soaking and extracting, every 100ml of the fructus cannabis fatty acid compound wine contains 2-80 mg of fatty acid, 2-70 mg of unsaturated fatty acid and 0-40 mg of total flavonoids.
The wine prepared by soaking and extracting the fructus cannabis fatty acid is transparent and yellow in color and has strong unique aroma of fructus cannabis.
Optionally, the shaking extraction comprises at least: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit on a shaking table, shaking, and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 45-65 degrees.
Optionally, in the shaking extraction, the ratio of the fructus cannabis powder to the white spirit is 1kg: 5-15L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-50 mg: 1L;
the shaking conditions are as follows: and (5) sealing and shaking for 2-6 days, wherein the rotating speed of the shaking bed is 80-100 r/min.
Optionally, the fructus cannabis fatty acid compound wine prepared by shaking extraction contains 4-70 mg of fatty acid, 2-50 mg of unsaturated fatty acid and 0-40 mg of total flavonoids per 100ml of fructus cannabis fatty acid compound wine.
The wine prepared from the fructus cannabis fatty acid extracted by shaking is transparent yellow and has strong unique aroma of fructus cannabis.
Optionally, the agitated reflux extraction comprises at least: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit in a stirring reflux container, stirring, refluxing, leaching and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 55-65 degrees.
Optionally, in the stirring reflux extraction, the ratio of the fructus cannabis powder to the white spirit is 1kg: 10-80L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-50 mg: 1L;
the conditions of the stirring reflux leaching are as follows: stirring, refluxing and leaching for 1-2 h at the temperature of 60-80 ℃.
Optionally, the fructus cannabis fatty acid compound wine prepared by stirring reflux extraction contains 6-40 mg of fatty acid, 3-30 mg of unsaturated fatty acid and 5-40 mg of total flavonoids per 100ml of fructus cannabis fatty acid compound wine.
The fructus cannabis fatty acid compound wine prepared by stirring, refluxing and extracting is transparent and light yellow in color and has certain fructus cannabis special fragrance.
Optionally, the ultrasound extraction comprises at least: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit in an ultrasonic extraction container, performing ultrasonic-assisted extraction, and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 55-65 degrees.
Optionally, in the ultrasonic extraction, the ratio of the fructus cannabis powder to the white spirit is 1kg: 10-100L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-50 mg: 1L;
the ultrasonic-assisted extraction conditions are as follows: and (3) carrying out ultrasonic assisted extraction for 40-90 min at the temperature of 20-50 ℃ and the power of 200-500W.
Optionally, in the fructus cannabis fatty acid compound wine prepared by ultrasonic extraction, 5-45 mg of fatty acid, 3-30 mg of unsaturated fatty acid and 2-40 mg of total flavonoids are contained in each 100ml of fructus cannabis fatty acid compound wine.
The fructus cannabis fatty acid compound wine prepared by ultrasonic extraction has certain fructus cannabis special fragrance.
In the present application, "fatty acid" refers to a long aliphatic hydrocarbon chain organic substance having one carboxyl group at one end.
In the present application, "unsaturated fatty acid" refers to a fatty acid having a double bond, and is classified into monounsaturated fatty acid and polyunsaturated fatty acid.
In the present application, "total flavonoids" refers to a series of compounds in which two benzene rings (A-and B-rings) having phenolic hydroxyl groups are connected to each other through a central three carbon atom, and the basic nucleus is 2-phenylchromone.
In this application, "room temperature" means 25. + -. 5 ℃.
In this application, unless otherwise indicated, a numerical range refers to any value within the range, including the endpoints.
The beneficial effects that this application can produce include:
the fructus cannabis fatty acid compound wine is transparent and yellow in color, has strong unique pleasant aroma of fructus cannabis, is high in content of nutritional functional components fatty acid and flavone, high in proportion of unsaturated fatty acid, definite in functional components and proportion, and has better taste, unique and mellow aroma, pleasant aroma and better health-care effect, and the content of fatty acid and total flavone and the proportion of unsaturated fatty acid in the fatty acid are within the range. In the preparation process of the fructus cannabis fatty acid compound wine, a proper amount of fructus cannabis fatty acid is added, based on that fructus cannabis oil has certain solubility in water and ethanol, and the operations of mass transfer and heat transfer enhancement in the preparation process can improve the leaching and dissolution of fatty acid, improve the fatty acid content in the fructus cannabis fatty acid compound wine, and have high proportion of unsaturated fatty acid. The fructus cannabis fatty acid compound wine is functional health care wine with important physiological health care effect on human body, and further development and utilization of fructus cannabis resources are promoted.
Drawings
Fig. 1 is a gas chromatogram of the fatty acid content of sample # 1 prepared in example 1.
Detailed Description
The present application will be described in detail with reference to examples, but the present application is not limited to these examples.
The raw materials in the examples of the present application were all purchased commercially, unless otherwise specified. Wherein the production place of fructus Cannabis is Yunnan.
The hemp seed oil fatty acid is prepared by commercially available hemp seed oil through saponification, acidification, organic solvent extraction and other processes by adopting a conventional method. The preparation method of the hemp seed oil adopts a conventional squeezing method.
The analysis method in the examples of the present application is as follows:
in the fructus cannabis fatty acid compound wine, the contents of fatty acid and unsaturated fatty acid are analyzed and tested according to the national standard method of determination of fatty acid in food safety national standard food (GB 5009.168-2016). The content of the total flavone is analyzed and tested according to the national standard method spectrophotometry (GB/T20574-2006) for determining the content of the total flavone in the propolis.
The gas chromatogram of the hemp seed fatty acid blended wine was measured by taking sample # 1 of example 1 as a model, in which the peak at the retention time of 14.38 minutes was linoleic acid and the peak at the retention time of 16.10 minutes was alpha-linolenic acid.
Example 1
Parching shelled fructus Cannabis medicinal material 100g for 6min, pulverizing to 20 mesh, adding 45 degree Chinese liquor 1L, adding 10mg oleum Sesami fatty acid (10 mg oleum Cannabis fatty acid is added to every 1L Chinese liquor), soaking at room temperature for 4 days, stirring uniformly for 2 times every day during soaking, vacuum filtering the obtained soaking solution with 0.45 μm filter membrane to obtain clear and transparent filtrate, and making into fructus Cannabis fatty acid wine as sample No. 1.
Example 2
The operation was the same as in example 1 except that the soaking time was changed to 6 days. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 2.
Example 3
The operation was the same as example 1 except that the degree of added liquor was 50 degrees, the amount of added hemp oil fatty acid was 15mg (15 mg of hemp oil fatty acid was added per 1L of liquor), and the soaking time was changed to 4 days. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 3.
Example 4
The procedure of example 3 was repeated, except that the soaking time was changed to 6 days. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 4.
Example 5
The operation was the same as example 1 except that the degree of added liquor was 55 degrees, the amount of added hemp oil fatty acid was 20mg (20 mg of hemp oil fatty acid was added per 1L of liquor), and the soaking time was changed to 4 days. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 5.
Example 6
The procedure of example 5 was repeated, and the soaking time was changed to 6 days. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 6.
Example 7
Parching 1kg of shelled fructus Cannabis medicinal material for 6min, pulverizing to 20 mesh, adding 1L of 46% (v/v) Chinese liquor and 10mg of fructus Cannabis fatty acid (10 mg of fructus Cannabis fatty acid is added to 1L of Chinese liquor), standing at room temperature, soaking for 99 days, filtering with 0.45 μm filter membrane to obtain clear and transparent filtrate, and making into fructus Cannabis fatty acid wine as sample No. 7.
Example 8
The procedure is as in example 7, except that the degree of the added Chinese liquor is 56 degrees, and the addition amount of the hemp oil fatty acid is 20mg (20 mg of hemp oil fatty acid is added to 1L of Chinese liquor). Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 8.
Example 9
The procedure of example 7 was repeated, except that the degree of the added Chinese liquor was 65 degrees, and the amount of the hemp oil fatty acid added was 100mg (100 mg of hemp oil fatty acid was added per 1L of Chinese liquor). Obtaining the fructus cannabis fatty acid compound wine which is marked as sample No. 9.
The hemp seed fatty acid wine samples obtained in examples 1 to 9 were analyzed, and the characteristic indexes of the hemp seed-soaked fatty acid wine were as follows.
TABLE 1 fructus Cannabis soaking fatty acid wine characteristic index
Example 10
Parching 10g of shelled fructus Cannabis medicinal material for 6min, pulverizing to 20 mesh, adding 50ml of 45% (v/v) Chinese liquor, adding 1.0mg of oleum Sesami fatty acid (20 mg of oleum Cannabis fatty acid per 1L of Chinese liquor), shaking on shaking table at room temperature for 2 days, respectively, at shaking table rotation speed of 80r/min, vacuum filtering the obtained soaking solution with 0.45 μm filter membrane to obtain clear and transparent filtrate, and making into fructus Cannabis fatty acid wine as sample No. 10.
Example 11
The operation was carried out in the same manner as in example 10 except that the shaking time was changed to 4 days. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 11.
Example 12
The operation was carried out in the same manner as in example 10 except that the shaking time was changed to 6 days. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 12.
Example 13
The operation is the same as example 10, except that 80ml of 50-degree white spirit is added, 2mg of hemp seed oil fatty acid is added (25 mg of hemp seed oil fatty acid is added to every 1L of white spirit), and the rotating speed of the shaking table is 90r/min, so that hemp seed fatty acid blended wine is obtained and is marked as sample No. 13.
Example 14
The operation was carried out in the same manner as in example 13 except that the shaking time was changed to 4 days. And obtaining the fructus cannabis fatty acid compound wine which is marked as sample No. 14.
Example 15
The operation was carried out in the same manner as in example 13 except that the shaking time was changed to 6 days. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 15.
Example 16
The operation is the same as example 10, except that 100ml of 55-degree white spirit is added, 3mg of hemp oil fatty acid is added (30 mg of hemp oil fatty acid is added in every 1L of white spirit), and the rotating speed of the shaking table is 100 r/min. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 16.
Example 17
The operation was carried out in the same manner as in example 16 except that the shaking time was changed to 4 days. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 17.
Example 18
The operation was carried out in the same manner as in example 16 except that the shaking time was changed to 6 days. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 18.
Example 19
The operation is the same as example 10, except that 120ml of 60 degree white spirit is added, 4.8mg of hemp oil fatty acid is added (40 mg of hemp oil fatty acid is added in every 1L of white spirit), and the rotating speed of the shaking table is 80 r/min. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 19.
Example 20
The operation was carried out in the same manner as in example 19 except that the shaking time was changed to 4 days. And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 20.
Example 21
The operation was carried out in the same manner as in example 19 except that the shaking time was changed to 6 days. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 21.
Example 22
The operation is the same as example 10, except that 150ml of 65 degree white spirit is added, 7.5mg of hemp oil fatty acid is added (50 mg of hemp oil fatty acid is added in every 1L of white spirit), and the rotating speed of the shaking table is 90 r/min. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 22.
Example 23
The operation was conducted in the same manner as in example 22 except that the shaking time was changed to 4 days. Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 23.
The hemp seed fatty acid wine samples obtained in examples 10 to 23 were analyzed, and the characteristic indexes of the hemp seed shaking fatty acid wine are as follows.
TABLE 2 characteristic index of fructus Cannabis shaken fatty acid wine
Example 24
Parching 2g of shelled fructus Cannabis for 6min, pulverizing to 20 mesh, adding 160ml of 55% (v/v) Chinese liquor, adding 3.2mg of oleum Sesami fatty acid (20 mg of oleum Sesami fatty acid per 1L Chinese liquor), reflux extracting at 80 deg.C for 1 hr, filtering with 0.45 μm filter membrane to obtain clear and transparent filtrate, and making into fructus Cannabis fatty acid wine, which is designated as sample No. 24.
Example 25
The procedure is as in example 24, except that 60ml of 60% (v/v) Chinese liquor is added, and 1.8mg of hemp oil fatty acid is added (30 mg of hemp oil fatty acid per 1L of Chinese liquor). And obtaining fructus cannabis fatty acid compound wine, and marking as a sample No. 25.
Example 26
The procedure is as in example 24, except that 20ml of 65% (v/v) Chinese liquor is added, and 1mg of hemp oil fatty acid is added (50 mg of hemp oil fatty acid is added per 1L of Chinese liquor). Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 26.
The hemp seed fatty acid wine samples obtained in examples 24-26 were analyzed, and the characteristic indexes of the hemp seed reflux-extracted fatty acid wine are as follows.
TABLE 3 characteristic index of fructus Cannabis reflux extraction fatty acid wine
Example 27
Parching 5g of shelled fructus Cannabis for 6min, pulverizing to 20 mesh, adding 400ml of 55% (v/v) Chinese liquor, adding 8mg of oleum Sesami fatty acid (20 mg of oleum Cannabis fatty acid per 1L Chinese liquor), ultrasonic extracting for 40min under 200W power, filtering with 0.45 μm filter membrane to obtain clear and transparent filtrate, and making into fructus Cannabis fatty acid wine sample No. 27.
Example 28
The procedure is as in example 27, except that 50ml of 60% (v/v) Chinese liquor is added, and 1.5mg of hemp oil fatty acid is added (30 mg of hemp oil fatty acid per 1L of Chinese liquor). And (5) obtaining the fructus cannabis fatty acid compound wine, and marking as a sample No. 28.
Example 29
The procedure is as in example 27, except that 50ml of 65% (v/v) Chinese liquor is added, and 2.5mg of hemp oil fatty acid is added (50 mg of hemp oil fatty acid is added per 1L of Chinese liquor). Obtaining fructus cannabis fatty acid compound wine which is marked as sample No. 29.
The samples of the hemp seed fatty acid wine obtained in examples 27 to 29 were examined and analyzed, and the characteristic indexes of the hemp seed fatty acid wine by ultrasonic extraction were as follows.
TABLE 4 ultrasonic extraction of fructus Cannabis with fatty acid wine characteristic index
It can be seen that the application selects high-concentration white spirit, and the hemp seed oil fatty acid is added into the white spirit before being extracted, so that the content of fatty acid in the white spirit is increased, the proportion of unsaturated fatty acid is high, the content of total flavone is high, the white spirit is transparent and yellow, and the white spirit is fragrant and pleasant, and is functional health-care wine with important physiological health-care efficacy for human bodies.
Although the present application has been described with reference to a few embodiments, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the application as defined by the appended claims.
The technical scheme of the application is thank to the vigorous assistance of the institute of Process engineering of the academy of sciences of China in the research and development process.
Claims (10)
1. The fructus cannabis fatty acid compound wine is characterized by comprising fatty acid and flavone;
the fatty acid contains unsaturated fatty acid.
2. The fructus cannabis fatty acid compound wine as claimed in claim 1, wherein the fructus cannabis fatty acid compound wine contains 2-80 mg of fatty acid and 0-40 mg of total flavonoids per 100ml of fructus cannabis fatty acid compound wine;
2-70 mg of unsaturated fatty acid is contained in 2-80 mg of fatty acid.
3. A process for the preparation of a hemp seed fatty acid wine formulation according to any one of claims 1 to 2, comprising at least:
processing fructus Cannabis powder and oleum Cannabis fatty acid with Chinese liquor to obtain fructus Cannabis fatty acid compound wine;
the alcohol degree of the white spirit is 45-65 degrees.
4. The method according to claim 3, characterized by comprising at least:
(1) parching shelled fructus Cannabis, and pulverizing to obtain processed fructus Cannabis powder;
(2) processing the processed fructus cannabis powder and fructus cannabis oil fatty acid by using white spirit to obtain fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 45-65 degrees.
5. The method according to claim 4, wherein the step (1) comprises at least: stir-frying the shelled fructus cannabis for 5-10 min, and obtaining processed fructus cannabis powder with the crushing degree of 10-40 meshes;
preferably, the crushing degree is 20-40 meshes;
preferably, in the step (2), 4-100L of white wine is added to each 1kg of the processed fructus cannabis powder; the addition mass of the hemp oil fatty acid and the volume ratio of the white spirit are 10-100 mg: 1L of the compound.
6. The method according to claim 4, wherein the treatment in the step (2) includes at least one of immersion extraction, shaking extraction, agitation reflux extraction, and ultrasonic extraction.
7. The method for preparing according to claim 6, wherein said soaking extraction comprises at least: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit in a soaking container, uniformly stirring, soaking, and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 45-65 degrees;
preferably, the proportion of the fructus cannabis powder to the white spirit is 1kg: 4-10L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-100 mg: 1L;
the soaking conditions are as follows: soaking for 4-100 days, and uniformly stirring for 0-3 times every day during the soaking period.
8. The method according to claim 6, wherein the shaking extraction comprises at least: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit on a shaking table, shaking, and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 45-65 degrees;
preferably, the proportion of the fructus cannabis powder to the white spirit is 1kg: 5-15L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-50 mg: 1L;
the shaking conditions are as follows: and (5) sealing and shaking for 2-6 days, wherein the rotating speed of the shaking bed is 80-100 r/min.
9. The method for preparing according to claim 6, wherein the agitation reflux extraction comprises at least: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit in a stirring reflux container, stirring, refluxing, leaching and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 55-65 degrees;
preferably, the proportion of the fructus cannabis powder to the white spirit is 1kg to 10-80L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-50 mg: 1L;
the conditions of the stirring reflux leaching are as follows: stirring, refluxing and leaching for 1-2 h at the temperature of 60-80 ℃.
10. The method for preparing according to claim 6, wherein the ultrasonic extraction comprises at least: placing a mixture containing fructus cannabis powder, fructus cannabis fatty acid and white spirit in an ultrasonic extraction container, performing ultrasonic-assisted extraction, and filtering to obtain the fructus cannabis fatty acid compound wine; the alcohol degree of the white spirit is 55-65 degrees;
preferably, the proportion of the fructus cannabis powder to the white spirit is 1kg: 10-100L;
the proportion of the hemp seed oil fatty acid to the white spirit is as follows: 10-50 mg: 1L;
the ultrasonic-assisted extraction conditions are as follows: and (3) carrying out ultrasonic assisted extraction for 40-90 min at the temperature of 20-50 ℃ and the power of 200-500W.
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| CN105296275A (en) * | 2015-09-23 | 2016-02-03 | 黑龙江省科学院 | Fructus cannabis health care baijiu and brewing method thereof |
| CN106085752A (en) * | 2016-06-29 | 2016-11-09 | 广西天龙泉酒业有限公司 | The preparation method of Fructus Cannabis minuent health care wine |
| CN106753954A (en) * | 2016-12-15 | 2017-05-31 | 珠海聚焦先导生物研究院有限公司 | One kind weight reducing Female health wine |
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|---|---|---|---|---|
| TW200636060A (en) * | 2005-04-11 | 2006-10-16 | Chuen-Ya Wu | Suet wine and method for producing the same |
| CN105296275A (en) * | 2015-09-23 | 2016-02-03 | 黑龙江省科学院 | Fructus cannabis health care baijiu and brewing method thereof |
| CN106085752A (en) * | 2016-06-29 | 2016-11-09 | 广西天龙泉酒业有限公司 | The preparation method of Fructus Cannabis minuent health care wine |
| CN106753954A (en) * | 2016-12-15 | 2017-05-31 | 珠海聚焦先导生物研究院有限公司 | One kind weight reducing Female health wine |
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Application publication date: 20211207 |