CN105287331B - A kind of crease-resistant mildy wash and preparation method thereof - Google Patents
A kind of crease-resistant mildy wash and preparation method thereof Download PDFInfo
- Publication number
- CN105287331B CN105287331B CN201510674416.6A CN201510674416A CN105287331B CN 105287331 B CN105287331 B CN 105287331B CN 201510674416 A CN201510674416 A CN 201510674416A CN 105287331 B CN105287331 B CN 105287331B
- Authority
- CN
- China
- Prior art keywords
- essence
- crease
- resistant
- skin
- mildy wash
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/447—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof containing sulfur
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to cosmetic technical fields, and in particular to a kind of crease-resistant mildy wash and preparation method thereof.The crease-resistant mildy wash includes myristic acid, palmitic acid, stearic acid, glycerine, potassium hydroxide, lauric acid sodium taurocholate, sodium cocoyl glycinate, sodium lauroyl glutamate, 14 sec alkanol polyethers 20 of C12, glycol distearate, propylene glycol, Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence, starfish essence, cortex acanthopanacis essence, Margarita extract, EDETATE SODIUM, hydroxypropyl methyl cellulose, methyl hydroxybenzoate, Nipasol, methylisothiazolinone, essence and water.The crease-resistant mild pro-skin of mildy wash of the present invention, safe and non-stimulating, deep layer cleaning skin, while moisturizing is crease-resistant.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of crease-resistant mildy wash and preparation method thereof.
Background technology
Skin aging includes internal factor and external factor.Internal factor：25 years old is spent, the collagen in skin will
It is lost in annual 5% speed or even some people just felt the apparent aging of skin less than 25 years old, increasingly coarse pore, pine
It relaxes, microgroove is all the sign of aging.Collagen is reduced, and supports the elasticated net of skin be broken, follow the string, is sagging, skin is just
Meeting atrophy collapses, and stereotype is presented.Simultaneously after 25 years old, the metabolism of skin will slow down, and neonatal cell reduces, and dead skin is just
Often metabolism is also slack-off, to cause dead skin to accumulate, enables skin obscure coarse.External factor：Light aging is lead to aging important
Factor, ultraviolet light can make skin generate microgroove, color spot, and skin can also be enabled to follow the string and gloss.It is nowadays more next in addition to light aging
More serious municipal pollution is also no small test for skin, and pore caused by haze, radiation is coarse, obscure etc., and
Very common skin problem.Urban woman is facing to the heavy pressure of live and work, and skin, which also bears a heavy burden, can't bear, and pressure can be led
It causes the sugar in blood to form harmful substance, makes protein denaturation, cause the elasticity of skin to reduce, flesh age shows.Pressure is also
It can cause sleep insufficiency and anxiety, skin is allowed to become sensitive and dull.Protect skin very urgent, cleaning skin is not at daily
Negligible work.
The mildy wash of market is mainly the following type from ingredient at present：1. soap base mildy wash：Dirt-removing power and
Degreasing ability is strong, but can be clearly felt that skin water shortage and tight after using, and is easy to damage skin；2. surfactant mildy wash：
Compare it is mild, do not stimulate, but still have tight and water shortage after using, dirt-removing power is weaker, and flushing has residual；3. emulsibility
Mildy wash：With rear without senses of discomfort such as tight, water shortages, but dirt-removing power and degreasing ability are worst, and cleaning capacity is worst；4. ammonia
Base acid mildy wash：Amino acid itself is weakly acidic, has just suited the acid-base property of skin, will not cause shadow to the acid-base value of skin
It rings, to the irritation very little of skin, skin-friendly is also especially good, and cleaning strength is moderate, with rear noresidue, avoids residuals to skin
The injury of skin natural containment, frothing capacity are good.And in terms of effect, in addition to cleanable skin, mended currently on the market with having
The face cleaning milk product of water, moisturizing and white-skinned face function is in the majority, has effects that crease-resistant product is less, and its anti-wrinkle effect unobvious.
104758223 A of Chinese patent application CN disclose a kind of hydrolysis silk mildy wash comprising myristic acid, sweet
Oil, D-sorbite, stearic acid, palmitic acid, lauric acid, butanediol, amino acid surfactant, glycol distearate, hydrogen
Potassium oxide, ceteareth -25, skin conditioning agent, hydrolysis silk, polyquaternium conditioner, gathers single stearic acid glycerine lipoprotein
Glycols and water.The mildy wash can effectively remove dirt, fat granule in pore, and blackhead etc. is not tight after washing, stingless
Swash, but the mildy wash does not have crease-resistant effect.
In conclusion for overcome the deficiencies in the prior art, while the selection that more products enrich market being provided, meet people
Demand to high-quality cosmetics, it is necessary to research and development one kind having effects that crease-resistant, effective cleaning skin, and mild non-stimulated resists
Wrinkle mildy wash.
Invention content
For overcome the deficiencies in the prior art, the purpose of the present invention is to provide a kind of crease-resistant mildy wash, mild pro-skin,
It is safe and non-stimulating, a variety of dirts of deep layer cleaning, excess oil and aging cutin, moisturizing while purification, effective delaying skin
Aging, auxiliary desalination pigment, smooth wrinkle, compact skin, improves skin gloss and elasticity.
In order to realize above-mentioned currently, technical scheme is as follows：
A kind of crease-resistant mildy wash is prepared by the raw material of following weight percent meter：Myristic acid 10%, palmitic acid
10%, stearic acid 6%, glycerine 10%, potassium hydroxide 3%, lauric acid sodium taurocholate 6%, sodium cocoyl glycinate 3%, bay
Acyl sodium glutamate 8%, C12-14 sec alkanols polyethers -201%, glycol distearate 4%, propylene glycol 0.5%, lactic acid bar
Bacterium/pomegranate fruit tunning extract 1%, arctic Ascophyllum nodosum essence 0.3%, starfish essence 1.2%, cortex acanthopanacis essence 0.3%,
Margarita extract 1%, EDETATE SODIUM 0.05%, hydroxypropyl methyl cellulose 0.2%, methyl hydroxybenzoate 0.05%, Nipasol
0.15%, methylisothiazolinone 0.01%, essence 0.2%, surplus are water.
Contain sodium lauroyl glutamate, lauric acid sodium taurocholate and cocounut oil acyl glycine in crease-resistant mildy wash of the present invention
Three kinds of amino acid surfactants of sodium, three's property is mild, soft to skin, do not cause allergy, also has excellent wetting
Property, foaming characteristic, water solubility, hard water resistance property and antibiotic property, while its faintly acid same as skin keeps skin feel comfortable, soft
Profit, the low stimulation of what is more important three, low toxicity have good biodegradability properties；And three cooperates with, and reaches mild stingless
Swash, the effect of safe and effective cleaning skin.
Bacillus acidi lactici of the present invention/pomegranate fruit tunning extract contains a large amount of ellagic acid, polyphenol and anthocyanidin,
Its inoxidizability is strong, can effectively neutralize free radical, boost metabolism, and reduces visible microgroove.
The arctic Ascophyllum nodosum essence is micro rich in phycocolloid body, brown algae polyphenols, sodium alginate, algae carrotene and ocean
Element, the mechanical performance that can increase skin thickness, improve skin improve barrier function, promote collagen and elastin laminin
And at, inhibit degrading enzyme, so as to improve the texture, color and luster and brightness of skin.
The starfish essence can promote the metabolism of skin, increase epidermal barrier regeneration, while more increasing glycosaminoglycan
(GAGS) wrinkle is effectively antagonized, keeps skin water tender flexible, and do not have with the synthesis of III, type Ⅳ collagen albumen, help skin
Any side effect and irritation.
The cortex acanthopanacis essence contains a variety of glucosides, also contains polysaccharide, Isofraxidin, chlorogenic acid, sesamin, stearic acid, β-
Sitosterol etc. has the effects that radioresistance, removing toxic substances, anti-inflammatory, antibacterial and antiviral.
The Margarita extract can effectively reduce wrinkle, eliminate blackspot, reply skin elastic.
The Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence, starfish essence, cortex acanthopanacis essence
With Margarita extract collaboration sodium lauroyl glutamate, lauric acid sodium taurocholate and sodium cocoyl glycinate, it is old dead skin can be removed
Change cutin, a variety of dirts of deep layer cleaning, excess oil and aging cutin, while timely replenishing water and preserving moisture, auxiliary desalination pigment is supplied
Nutrition needed for skin, effective delaying skin aging, smooth wrinkle, compact skin, so that skin is got well state, then coordinate Pork and beans
The basis such as cool acid, palmitic acid, stearic acid, glycerine, C12-14 sec alkanols polyethers -20, glycol distearate, propylene glycol is former
Material obtains the crease-resistant mildy wash of the present invention, each component collaboration so that stable system safety, mild non-stimulated, blistering is abundant, Yi Chong
It washes, noresidue, can be used for a long time.
The present invention also provides the preparation methods of above-mentioned crease-resistant mildy wash, specifically include following steps：
S1, myristic acid, palmitic acid, stearic acid, glycol distearate, the secondary alkanes of C12-14 are added into oil phase pot
Alcohol polyethers -20, methyl hydroxybenzoate and Nipasol are heated with stirring to 80~85 DEG C, and stirring is completely dissolved to material, obtains material A；
S2, EDETATE SODIUM, water, glycerine and potassium hydroxide are added into water phase pot, are heated with stirring to 80~85 DEG C, stirring is extremely
Material is completely dissolved, and obtains material B；
S3, the material B that 1/3 is added into emulsification pot, add material A, other 2/3 material B are slowly added under stirring,
It is uniformly mixed, obtains material C；
S4, propylene glycol and the advance mixing of hydroxypropyl methyl cellulose, be then added in material C, be heated to 80~85
DEG C, start to cool down after keeping the temperature 25~30min；
When S5, system are cooled to 60 DEG C, lauric acid sodium taurocholate, sodium cocoyl glycinate and lauroyl glutamate is added
Sodium is stirred until homogeneous；
When S6, system are cooled to 45 DEG C, be added Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence,
Starfish essence, cortex acanthopanacis essence, Margarita extract, methylisothiazolinone and essence, are stirred until homogeneous；It is cooled to room temperature, is taken out
Sample inspection discharges after qualified to get crease-resistant mildy wash.
Further, the mixing speed of the stirring is 20~50r/min.
Therefore, compared with prior art, advantage of the invention is that：
(1) the crease-resistant mildy wash of the present invention contains lauric acid sodium taurocholate, sodium lauroyl glutamate and sodium cocoyl glycinate
Three kinds of amino acids cleansings can safely and effectively clean the excess oil and dust dirt of skin surface and pore depths, day
Right faintly acid is close with skin PH, and skin-friendly is good, does not cause any burden and injury to tender skin, keeps skin moisture,
The natural sebum film of face skin will not be destroyed.
(2) present invention crease-resistant mildy wash addition Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence,
Starfish essence, cortex acanthopanacis essence and Margarita extract, clean skin while timely replenishing water and preserving moisture, and it is crease-resistant ingredient is effective
It is sent to skin deep layer, repairs impaired or innutritive cell, reduce microgroove, lighten the stain, make that skin water profit is smooth, has bullet
Property.
(3) the crease-resistant mild pro-skin of mildy wash of the present invention, blistering is abundant, easily rinses, heavy metal free, without foaming agent etc., contains
Amino acid cleaning gene and a variety of active skull cap components, it is non-stimulated to skin；Can deep layer cleaning, replenishing water and preserving moisture, whitening anti-wrinkling, together
When the crease-resistant mildy wash cost of material of the present invention it is low, preparation method is simple, process stabilizing, can be applicable.
Specific implementation mode
The present invention is further described below by way of specific implementation mode, but the present invention is not limited only to following embodiment.
In the scope of the present invention or do not departing from present disclosure, in spirit and scope, to crease-resistant mildy wash of the present invention into
Row is suitably modified, replaces the identical component of effect, it will become apparent to those skilled in the art that they are considered as
It is included within the scope of the present invention.
The information such as the producer of part material and article No. are as follows in crease-resistant mildy wash described in the embodiment of the present invention：
| Raw material of the present invention | Producer | Article No. |
| Bacillus acidi lactici/pomegranate fruit tunning extract | Active Concepts | 20440 |
| Arctic Ascophyllum nodosum essence | The Arctic Company | 254812 |
| Starfish essence | Lai Yu groups | 660415 |
| Cortex acanthopanacis essence | Guangzhou Ming Hui Fine Chemical Co., Ltd | PW1311WJ0125 |
| Margarita extract | Guangzhou Nuo Pin trade Co., Ltds | ZZ-0254 |
Embodiment 1, the crease-resistant mildy wash of the present invention and its preparation
Formula：It is prepared by the raw material of following weight percent meter：Myristic acid 10%, palmitic acid 10%, stearic acid
6%, glycerine 10%, potassium hydroxide 3%, lauric acid sodium taurocholate 6%, sodium cocoyl glycinate 3%, sodium lauroyl glutamate
8%, C12-14 sec alkanols polyethers -201%, glycol distearate 4%, propylene glycol 0.5%, Bacillus acidi lactici/pomegranate fruit
Tunning extract 1%, arctic Ascophyllum nodosum essence 0.3%, starfish essence 1.2%, cortex acanthopanacis essence 0.3%, pearl extraction
Object 1%, EDETATE SODIUM 0.05%, hydroxypropyl methyl cellulose 0.2%, methyl hydroxybenzoate 0.05%, Nipasol 0.15%, methyl
Isothiazolinone 0.01%, essence 0.2%, surplus are water.
Preparation method：S1, into oil phase pot be added myristic acid, palmitic acid, stearic acid, glycol distearate,
C12-14 sec alkanols polyethers -20, methyl hydroxybenzoate and Nipasol, are heated with stirring to 80 DEG C under the mixing speed of 50r/min,
Stirring is completely dissolved to material, obtains material A；
S2, EDETATE SODIUM, water, glycerine and potassium hydroxide are added into water phase pot, are stirred under the mixing speed of 50r/min
85 DEG C are heated to, stirring is completely dissolved to material, obtains material B；
S3, the material B that 1/3 is added into emulsification pot, add material A, are stirred under the mixing speed of 20r/min, delayed
Slowly other 2/3 material B is added, is uniformly mixed, obtains material C；
S4, propylene glycol and the advance mixing of hydroxypropyl methyl cellulose, be then added in material C, be heated to 85 DEG C, protect
Start to cool down after warm 30min；
When S5, system are cooled to 60 DEG C, lauric acid sodium taurocholate, sodium cocoyl glycinate and lauroyl glutamate is added
Sodium is stirred until homogeneous under the mixing speed of 40r/min；
When S6, system are cooled to 45 DEG C, be added Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence,
Starfish essence, cortex acanthopanacis essence, Margarita extract, methylisothiazolinone and essence, are stirred under the mixing speed of 40r/min
To uniform；It is cooled to room temperature, is surveyed sample, is discharged to get crease-resistant mildy wash after qualified.
Testing performance index is done to the crease-resistant mildy wash of embodiment 1, test result is as follows：
1, appearance：White lotion；
2, pH value：5.5~7.0；
3, viscosity：5~100,000；
4, heat-resistant stability investigates (45 DEG C × for 24 hours)：It is qualified；
5, resist cold study on the stability (- 15 DEG C × for 24 hours)：It is qualified.
Comparative example 1,
Formula：It is prepared by the raw material of following weight percent meter：Myristic acid 12%, palmitic acid 8%, stearic acid
7.5%, glycerine 8%, potassium hydroxide 5.4%, lauric acid sodium taurocholate 5%, sodium cocoyl glycinate 5%, lauroyl glutamate
Sodium 5%, C12-14 sec alkanols polyethers -202%, glycol distearate 2%, propylene glycol 1.5%, Bacillus acidi lactici/pomegranate
Fruit tunning extract 0.5%, Margarita extract 0.5%, EDETATE SODIUM 0.15%, hydroxypropyl methyl cellulose 0.15%,
Methyl hydroxybenzoate 0.15%, Nipasol 0.1%, methylisothiazolinone 0.15%, essence 0.1%, surplus are water.
Preparation method is with reference to embodiment 1.
Comparative example 2,
Formula：It is prepared by the raw material of following weight percent meter：Myristic acid 16%, stearic acid 11.5%, glycerine
10%, potassium hydroxide 5.4%, sodium cocoyl glycinate 7.5%, sodium lauroyl glutamate 7.5%, C12-14 sec alkanols are poly-
Ether -202%, propylene glycol 1.5%, Bacillus acidi lactici/pomegranate fruit tunning extract 0.5%, arctic Ascophyllum nodosum essence 0.4%,
Starfish essence 0.6%, cortex acanthopanacis essence 0.5%, Margarita extract 0.5%, EDETATE SODIUM 0.15%, hydroxypropyl methyl cellulose
0.15%, methyl hydroxybenzoate 0.15%, Nipasol 0.1%, methylisothiazolinone 0.15%, essence 0.1%, surplus are water.
Preparation method is with reference to embodiment 1.
Test example one, Product Safety evaluation (experiment of human skin patch)
One, trial target：The crease-resistant mildy wash that embodiment 1, comparative example 1~2 are prepared
Tested crowd's number：30 people, women
Age：Between 20~50 years old
Health status：Subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.
Grouping：3 groups, every group of 10 people, average age 28 ± 2 years old.
Two, patch method：Select qualified spot to try device, with closed patch experiment method, by tested material about 0.020g~
0.025g drops are in spot examination device, and external application special adhesive tape is covered on subject back, and tested material is removed after 24 hours, after removing respectively
0.5, observation dermoreaction in 6,12,24,48 hours, according to《Cosmetics health specification》Middle dermoreaction grade scale records its knot
Fruit.
Three, experimental result：Human skin patch result is shown：Each group subject passes through embodiment 1, comparative example 1~2
Crease-resistant mildy wash patch test, dermoreaction was observed at 0.5,6,12,24,48 hour, wherein 0 skin occur bad anti-
It answers, illustrates that the crease-resistant mildy wash is safe to use.
Test example two, product effect assessment
First part：The moisturizing effect of the crease-resistant mildy wash of the present invention
One, trial target：The crease-resistant mildy wash that embodiment 1, comparative example 1~2 are prepared
Two, tested crowd
Gender number：Female, 30 people
Age：Between 20~40 years old
Health status：Subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.
Grouping：It is divided into 3 groups, every group of 10 people.
Three, test method：Subject uses Fes Kai Er SK-III skin moisture detectors after cleaning face using clear water
The moisture of forehead, left face, right face and chin skin is tested respectively, and takes arithmetic mean of instantaneous value, and it is wet that subject reuses warm water
Moisten face, then clean face using above-mentioned crease-resistant mildy wash, cleaned with clear water, then with skin moisture tester test forehead,
The skin moisture content of left face, right face and chin same location, and take arithmetic mean of instantaneous value.Every group of 10 subject will be tested
As a result arithmetic mean of instantaneous value is taken.
Four, test result is as follows table 1：
1 skin moisture content test result table of table
By upper table 1 it is found that after using 1 crease-resistant mildy wash face cleaning of the embodiment of the present invention, moisture of skin can not only be kept not flow
Lose, the natural sebum film of face skin will not be destroyed, can also timely replenishing water and preserving moisture, make skin water moisten.Comparative example 1 and comparative example 2
Lack certain components compared with Example 1, moisturizing effect illustrates plant extracts collaboration of the present invention not as good as embodiment 1.
Second part：The using effect of the crease-resistant mildy wash of the present invention
One, trial target：Crease-resistant mildy wash prepared by embodiment 1, comparative example 1~2
Two, tested crowd
Gender number：Female, 90 people
Age：Between 20~50 years old
Health status：Subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.
Grouping：It is divided into 3 groups, every group of 30 people.
Three, test method：The crease-resistant mildy wash cleaning face prepared by example 1, comparative example 1~2, observation and sense are used respectively
By using effect.Application method：Subject directly uses tested products, each using primary daily morning and evening, using it is preceding by face with
Clear water drenches, and squeezes out appropriate mildy wash in the centre of the palm, a small amount of clear water is added and has rubbed abundant foam, in face message in a moment with clear
Water is rinsed well.Adhere to using one month, at least checks that once whether there is or not whole bodies and local adverse reaction with understanding weekly, and in detail
Record result.
Four, test assessment result is as follows：
(one month) on probation feedback conclusive table of 2 embodiment of table, 2 crease-resistant mildy wash
(one month) on probation feedback conclusive table of 3 comparative example of table, 1 mildy wash
(one month) on probation feedback conclusive table of 4 comparative example of table, 2 mildy wash
(1) by upper table 2 it is found that the crease-resistant mildy wash of embodiment 1 almost obtains the approval of all subjects, illustrate the present invention
Crease-resistant mildy wash does not stimulate mildly, and blistering is abundant, easily rinses, and effectively cleans the excess oil and ash of skin surface and pore depths
Dustiness dirt can keep skin moisture using the salubrious non-greasy of rear face, without tight feeling, timely moisturizing and simultaneously by crease-resistant ingredient
It is effective to be sent to skin deep layer, repair impaired or innutritive cell, reduce microgroove, lighten the stain, make skin water profit it is smooth,
It is flexible.
(2) by upper table 3~4 it is found that the using effect of 2 mildy wash of comparative example 1 and comparative example is not so good as embodiment 1, explanation
The crease-resistant mildy wash formula of the present invention is obtained not by the simple combination of each component, and inventive formulation is furtherly illustrated
There is synergistic effect between each component.
There is allergic phenomena in non-someone in whole subjects simultaneously, does not also occur the shapes such as pruitus, shouting pain, redness
Condition.Therefore, the crease-resistant mildy wash of the present invention is mildly safe, can be used for a long time.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology can all carry out modifications and changes to above-described embodiment without violating the spirit and scope of the present invention.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should by the present invention claim be covered.
Claims (3)
1. a kind of crease-resistant mildy wash, which is characterized in that be prepared by the raw material of following weight percent meter：Myristic acid
10%, palmitic acid 10%, stearic acid 6%, glycerine 10%, potassium hydroxide 3%, lauric acid sodium taurocholate 6%, cocounut oil acyl glycine
Sodium 3%, sodium lauroyl glutamate 8%, C12-14 sec alkanols polyethers -20 1%, glycol distearate 4%, propylene glycol
0.5%, Bacillus acidi lactici/pomegranate fruit tunning extract 1%, arctic Ascophyllum nodosum essence 0.3%, starfish essence 1.2%, slender acanthopanax
Skin essence 0.3%, Margarita extract 1%, EDETATE SODIUM 0.05%, hydroxypropyl methyl cellulose 0.2%, methyl hydroxybenzoate
0.05%, Nipasol 0.15%, methylisothiazolinone 0.01%, essence 0.2%, surplus are water.
2. a kind of method preparing crease-resistant mildy wash as described in claim 1, which is characterized in that include the following steps：
S1, into oil phase pot, addition myristic acid, palmitic acid, stearic acid, glycol distearate, C12-14 sec alkanols are poly-
Ether -20, methyl hydroxybenzoate and Nipasol are heated with stirring to 80~85 DEG C, and stirring is completely dissolved to material, obtains material A；
S2, EDETATE SODIUM, water, glycerine and potassium hydroxide are added into water phase pot, are heated with stirring to 80~85 DEG C, stirring to material
It is completely dissolved, obtains material B；
S3, the material B that 1/3 is added into emulsification pot, add material A, other 2/3 material B are slowly added under stirring, stir
It is uniformly mixed, obtains material C；
S4, propylene glycol and the advance mixing of hydroxypropyl methyl cellulose, be then added in material C, be heated to 80~85 DEG C, protect
Start to cool down after 25~30min of temperature；
When S5, system are cooled to 60 DEG C, lauric acid sodium taurocholate, sodium cocoyl glycinate and sodium lauroyl glutamate is added, stirs
It mixes to uniform；
When S6, system are cooled to 45 DEG C, Bacillus acidi lactici/pomegranate fruit tunning extract, arctic Ascophyllum nodosum essence, starfish is added
Essence, cortex acanthopanacis essence, Margarita extract, methylisothiazolinone and essence, are stirred until homogeneous；It is cooled to room temperature, sampling inspection
It looks into, discharges to get crease-resistant mildy wash after qualified.
3. the preparation method of crease-resistant mildy wash as claimed in claim 2, which is characterized in that the mixing speed of the stirring is 20
~50r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510674416.6A CN105287331B (en) | 2015-10-19 | 2015-10-19 | A kind of crease-resistant mildy wash and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510674416.6A CN105287331B (en) | 2015-10-19 | 2015-10-19 | A kind of crease-resistant mildy wash and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105287331A CN105287331A (en) | 2016-02-03 |
| CN105287331B true CN105287331B (en) | 2018-07-31 |
Family
ID=55185630
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510674416.6A Active CN105287331B (en) | 2015-10-19 | 2015-10-19 | A kind of crease-resistant mildy wash and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105287331B (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105902411A (en) * | 2016-05-17 | 2016-08-31 | 魏春红 | Cleansing foam and preparation method thereof |
| CN105997618A (en) * | 2016-05-18 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Acne-removal cleanser and preparation method thereof |
| CN105997733A (en) * | 2016-07-11 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Cleanser containing artemisia seleirgensis extract |
| CN105997739A (en) * | 2016-07-12 | 2016-10-12 | 广州丹奇日用化工厂有限公司 | Skin tendering facial cleanser |
| CN106727099A (en) * | 2016-11-25 | 2017-05-31 | 江苏爱西施科技服务咨询股份有限公司 | One kind is deoiled moisturizing mildy wash and preparation method thereof |
| CN106619302A (en) * | 2016-12-29 | 2017-05-10 | 广州市中通生化制品有限公司 | Mild allergy-relieving cleansing milk and preparation method thereof |
| CN108294989A (en) * | 2018-03-26 | 2018-07-20 | 广东名辰堂健康产业股份有限公司 | A kind of anti-acne facial cleanser and its production method |
| CN108379118A (en) * | 2018-03-27 | 2018-08-10 | 赵金椿 | A kind of organic mildy wash of astaxanthin and preparation method thereof |
| CN108836884A (en) * | 2018-09-26 | 2018-11-20 | 湖南御家化妆品制造有限公司 | A kind of Soap-base facial cleanser and preparation method thereof |
| IT202100010493A1 (en) * | 2021-04-26 | 2022-10-26 | Nuu Bionature S R L | IMPROVED COSMETIC PRODUCT FOR CLEANSING AND PERSONAL CARE |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103505382A (en) * | 2013-09-17 | 2014-01-15 | 广州环亚化妆品科技有限公司 | Cleanser composition with stable wire drawing effect and preparation method thereof |
| CN104622907A (en) * | 2013-11-14 | 2015-05-20 | 百岳特生物科技（上海）有限公司 | Use of starfish extract for preparing composition for promoting collagen proliferation |
| CN104758223A (en) * | 2015-03-06 | 2015-07-08 | 上海彤颜实业有限公司 | A hydrolyzed-silk face cleanser and a preparing method thereof |
| CN104825382A (en) * | 2015-05-26 | 2015-08-12 | 成都肤格特商贸有限公司 | Biotechnology skin-whitening cosmetics |
-
2015
- 2015-10-19 CN CN201510674416.6A patent/CN105287331B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103505382A (en) * | 2013-09-17 | 2014-01-15 | 广州环亚化妆品科技有限公司 | Cleanser composition with stable wire drawing effect and preparation method thereof |
| CN104622907A (en) * | 2013-11-14 | 2015-05-20 | 百岳特生物科技（上海）有限公司 | Use of starfish extract for preparing composition for promoting collagen proliferation |
| CN104758223A (en) * | 2015-03-06 | 2015-07-08 | 上海彤颜实业有限公司 | A hydrolyzed-silk face cleanser and a preparing method thereof |
| CN104825382A (en) * | 2015-05-26 | 2015-08-12 | 成都肤格特商贸有限公司 | Biotechnology skin-whitening cosmetics |
Non-Patent Citations (1)
| Title |
|---|
| 欧盟消费者安全科学委员（SCCS）建议降低化妆品中MI防腐剂限制浓度;佚名;《中国洗涤用品工业杂志》;中国洗涤工业用品协会;20150930;第81页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105287331A (en) | 2016-02-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105287331B (en) | A kind of crease-resistant mildy wash and preparation method thereof | |
| CN106038330B (en) | A kind of mildy wash and preparation method thereof | |
| CN105062731B (en) | One kind fermentation shea butter amino acid transparent soap | |
| CN107213063B (en) | Fair and bright facial mask and preparation method thereof | |
| CN102716044B (en) | Low-stimulation hair-cleaning compound | |
| CN105287290B (en) | A kind of whitening anti-aging mildy wash and preparation method thereof | |
| CN106619182B (en) | A kind of Transparent soap base bath composition of low-temperature stabilization | |
| CN110787091B (en) | Itching-relieving and anti-allergy infant washing and protecting preparation and application thereof | |
| CN110327261A (en) | A kind of compact skin skin care compositions and preparation method thereof | |
| CN111603433B (en) | Mild washing and protecting article for infants and preparation method thereof | |
| CN105232442A (en) | Plant antioxidation amino acid cleanser and preparation method thereof | |
| CN110755331B (en) | Antibacterial infant washing and caring preparation and application thereof | |
| CN104586653A (en) | Hair and body wash suitable for infants and preparation method for hair and body wash | |
| CN112957302B (en) | Amino acid facial cleanser and preparation method thereof | |
| CN108324591A (en) | A kind of hair composition containing marine bioactivity object | |
| CN105640867A (en) | Facial mask for replenishing moisture intensively with pearl essence and preparation method of facial mask | |
| CN108309866A (en) | A kind of adult's shower cream containing licorice | |
| CN108403609B (en) | Firming, skin-moistening and face-cleaning gel | |
| JP2001131049A (en) | Skin preparation for external use | |
| CN102935060B (en) | Pasties for breasts of women | |
| CN114366693B (en) | Shampoo bath lotion for infants | |
| CN109044881A (en) | A kind of pearl shining shampoo composition and a kind of preparation method of pearl shining shampoo composition | |
| CN106038392B (en) | Bubble facial mask | |
| CN109125172A (en) | A kind of Tea Saponin shower cream and preparation method thereof | |
| CN111888298B (en) | Shower gel and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information | ||
| CB02 | Change of applicant information |
Address after: Huadu District, Guangdong city of Guangzhou province 510880 Flower Town Qiyuan Road No. 28 Applicant after: Guangzhou Kema biotechnology Polytron Technologies Inc Address before: Hua Town, Huadu District, Guangdong Province, 510880 Avenue, Guangzhou City Applicant before: Kerma (unit of kinetic energy) bio tech ltd, Guangzhou |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant |