CN104758223A - A hydrolyzed-silk face cleanser and a preparing method thereof - Google Patents
A hydrolyzed-silk face cleanser and a preparing method thereof Download PDFInfo
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- CN104758223A CN104758223A CN201510100518.7A CN201510100518A CN104758223A CN 104758223 A CN104758223 A CN 104758223A CN 201510100518 A CN201510100518 A CN 201510100518A CN 104758223 A CN104758223 A CN 104758223A
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Abstract
The invention belongs to the field of cosmetics and particularly relates to a hydrolyzed-silk face cleanser and a preparing method thereof. The face cleanser comprises following raw materials: myristic acid, glycerol, sorbitol, stearic acid, palmitic acid, lauric acid, butanediol, an amino acid surfactant, glycol distearate, potassium hydroxide, glycerol monostearate, ceteareth-25, a skin conditioning agent, hydrolyzed silk, a polyquaternium conditioning agent, polyethylene glycols, and water. The face cleanser is rich, fine and smooth in foam, rich in elasticity, and good in wire drawing. The face cleanser is fine and smooth in pasty fluid, has high pearly luster, and can effectively remove dirt, fat granules, comedo, and the like in pores. During washing, a smooth sense is strong and skin feels comfort, and the skin after being washed is not dry, not tight and free of irritation. The face cleanser is suitable for oily skin, dry skin, neutral skin, and sensitive skin with skin damage.
Description
Technical field
The invention belongs to cosmetic field, particularly a kind of hydrolyzed silkworm silk facial milk cleanser and preparation method thereof.
Background technology
Along with the quickening of people's rhythm of life, the increasing the weight of of urban air pollution, the naked face be exposed on the external is often glossy having one's face covered with.And color make-up series products is also more and more universal, as an important branch of cosmetics, it is in occupation of consequence in modern people's life, and cleaning for skin care, is the vital first step.Clean skin could absorb every nursing such as ensuing elite, emulsion, facial cream, moistens each cell.Especially in summer, skin subjects wrecking of high temperature and strong Exposure to Sunlight, and dust even in air of isolation, sun-proof, foundation cream, color make-up and antibacterial etc. are also increasing the weight of skin pressure, and clean skin is particularly important.If the oils and fats of skin surface and dirt all do not have wash clean, oils and fats and the dirt of delay not only damage skin, also can form a closed barrier, affect infiltration and the absorption of nutrient in follow-up skin care item.
At present, clean product category is very many, but its safety and cleaning effect are not fine, and has certain zest, price unusual costliness again.Therefore, a kind of gentleness, low stimulation or even non-stimulated while thoroughly can clean skin clean product be just starved of.
Summary of the invention
The object of this invention is to provide a kind of hydrolyzed silkworm silk facial milk cleanser, this facial milk cleanser is gentle, non-stimulated, and dense, the fine and smooth also high resilience of foam, cleaning effect is very good, effectively can remove dirt, fat granule in pore.
Another object of the present invention is to provide a kind of preparation method of said hydrolyzed silkworm silk facial milk cleanser.
Object of the present invention can be achieved through the following technical solutions:
A kind of hydrolyzed silkworm silk facial milk cleanser, it is characterized in that, this hydrolyzed silkworm silk facial milk cleanser is made up of the raw material of following mass fraction meter:
Described amino acid surfactant is the compositions of one or more in sodium lauroyl sarcosine, myristoyl-N-methylaminoacetic acid sodium, stearyl sarcosine sodium, methyl lauroyl sodium taurocholate, methyl myristoyl sodium taurocholate, methyl stearyl sodium taurocholate, sodium lauroyl glutamate, myristoyl glutamate sodium, stearyl sodium glutamate, lauroyl Glycine sodium, myristoyl glycine sodium, stearyl Glycine sodium.Preferably, described amino acid surfactant is the one in methyl myristoyl sodium taurocholate, methyl lauroyl sodium taurocholate, sodium lauroyl glutamate, sodium lauroyl sarcosine and lauroyl Glycine sodium.
In invention formula, add amino acid surfactant, while high-efficiency cleaning, can also work in coordination with the zest reducing other surfactants.Itself gentle pro-skin, low stimulation, child and responsive skin can use.In addition, contribute to clean product and produce fine and smooth, dense and there is elastic foam adding of amino acid surfactant.Therefore, it more contributes to the fat granule, dirt, blackhead etc. that help to go deep in pore Peppermint Extract.
Described polyquaternary ammonium salt conditioner is the compositions of one or more in polyquaternary ammonium salt-6, polyquaternary ammonium salt-7, polyquaternary ammonium salt-39, polyquaternary ammonium salt-43.Preferably, described polyquaternary ammonium salt conditioner is the one in polyquaternary ammonium salt-43, polyquaternary ammonium salt-7 or polyquaternary ammonium salt-39.
Polyquaternary amine salt can reduce the zest of other surfactants and other components, makes skin more smooth and reduces or weaken that skin is tight, sensation of dryness.
Described polyethylene glycols is the compositions of one or more in Polyethylene Glycol-7M, polyquaternary ammonium salt-14M, polyquaternary ammonium salt-2M, Polyethylene Glycol-5M, Polyethylene Glycol-45M, Polyethylene Glycol-90M.Preferably, described polyethylene glycols is the one in Polyethylene Glycol-14M, Polyethylene Glycol-7M, Polyethylene Glycol-90M or Polyethylene Glycol-45M.
Adding of polyethylene glycols component in the present invention, skinfeel can be improved tight, dry and astringent, certain wire-drawing effect can be provided simultaneously.
The mixture that described skin conditioning agent is folic acid, bacillus cereus/fermented soybean product extract and hyaluronic acid are 1:0.2-2:1-3 mixing according to weight ratio.The present invention adopts folic acid, bacillus cereus/fermented soybean product extract, hyaluronic mixture, can antiallergic, high moisturizing, promote cytothesis, anti-light aging and stimulating cellular growth and wrinkle removing etc., being highly suitable for dry skin, neutral skin and skin has the sensitivity skin of damage and the allergy of eye skin alleviate and eliminate; In addition also can be applicable to the wrinkle removing of skin, protection skin not by the injury etc. of external environment.
The preparation method of above-mentioned hydrolyzed silkworm silk facial milk cleanser, its step comprises:
(1), various raw material has been weighed according to formula;
(2), by butanediol, glycerol, polyethylene glycols, potassium hydroxide and water stir, be incubated 0.2-0.6 hour after being warming up to 80-85 DEG C, as aqueous phase; Myristic acid, stearic acid, lauric acid, Palmic acid, glycol distearate, glyceryl monostearate, ceteareth-25 are stirred, is warming up to 80-85 DEG C and is incubated 0.3-0.6 hour, as oil phase;
(3), aqueous phase stirs with the speed of 30-50rpm, stirs, keep 0.3 hour after then adding oil phase with the speed of 3000rpm;
(4) be cooled to 45-50 DEG C, then add amino acid surfactant, Pyrusussuriensis (sugar) alcohol, skin conditioning agent, hydrolyzed silkworm silk, polyquaternary ammonium salt conditioner, stir, filter.
Compared with prior art, beneficial effect of the present invention is:
1, with the addition of hydrolyzed silkworm silk component in allocation of the present invention, to whitening, puerperal speckle dispelling effective, containing high collagen protein and elastic fibers in hydrolyzed silkworm silk, the nutritions such as aminoacid, ribose, nucleic acid, it is identical with human collagen albumen, can be absorbed completely by skin, promote cell regeneration, to compact intercellular substance distance, promote skin suppleness and degree of compacting, make salubrious, white thin, the high resilience of skin, thus reach safe reduce wrinkle, effectively, lasting, be applicable to very much progressively old and feeble, matt, dryness and water deficient skin.
2, the hydrolyzed silkworm silk facial milk cleanser foam prepared of the present invention is dense, fine and smooth and high resilience, has very strong wire drawing; Mastic is fine and smooth, has very strong pearly luster.
3, described hydrolyzed silkworm silk facial milk cleanser effectively can remove dirt, the fat granule in pore, blackhead etc.; When washing, sliding sense is strong, and skinfeel is comfortable, not dry and astringent after washing, not tight, non-stimulated; Be applicable to the sensitivity flesh that oiliness skin, dry skin, neutral skin and skin have damage.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
(1), each component of following mass fraction is taken: myristic acid 18% by formula, glycerol 10%, Pyrusussuriensis (sugar) alcohol 5%, stearic acid 5%, Palmic acid 1%, lauric acid 2%, butanediol 5%, methyl lauroyl sodium taurocholate 5%, glycol distearate 2%, potassium hydroxide 5.1%, glyceryl monostearate 1%, ceteareth-25 is 2%, skin conditioning agent 0.5% (folic acid, bacillus cereus/fermented soybean product extract and hyaluronic weight ratio are 1:0.2:1), hydrolyzed silkworm silk 1%, polyquaternary ammonium salt-39 is 1%, Polyethylene Glycol-14M is 0.01%, water 36.39%,
(2), butanediol, glycerol, Polyethylene Glycol-14M, potassium hydroxide, water are added in aqueous phase agitated kettle, stir and be warming up to 80-85 DEG C and be incubated 30min; Myristic acid, stearic acid, lauric acid, Palmic acid, glycol distearate, glyceryl monostearate, ceteareth-25 etc. are added in oil phase agitated kettle, stirs and be warming up to 80-85 DEG C and be incubated 30min;
(3), under 80-85 DEG C of temperature conditions, will stir, rotating speed 30-50rpm in aqueous phase suction emulsifying pot; Then open vacuum pump, then homogenizer will be opened, rotating speed 3000rpm in oil phase suction emulsifying pot, keep 30min;
(4), stir be cooled to 50 DEG C, add methyl lauroyl sodium taurocholate, Pyrusussuriensis (sugar) alcohol, skin
Conditioner, hydrolyzed silkworm silk, polyquaternary ammonium salt-39, stir, and after the assay was approved, filters discharging fill.
Embodiment 2
(1), each component of following mass fraction is taken: myristic acid 3% by formula, glycerol 10%, Pyrusussuriensis (sugar) alcohol 5%, stearic acid 17%, Palmic acid 3%, lauric acid 3%, butanediol 5%, methyl myristoyl sodium taurocholate 8%, glycol distearate 2%, potassium hydroxide 4.9%, glyceryl monostearate 1%, ceteareth-25 is 2%, skin conditioning agent 0.5% (folic acid, bacillus cereus/fermented soybean product extract and hyaluronic weight ratio are 1:0.5:2), hydrolyzed silkworm silk 1%, polyquaternary ammonium salt-43 is 1%, Polyethylene Glycol-7M is 0.02%, water 33.58%,
(2), butanediol, glycerol, Polyethylene Glycol-7M, potassium hydroxide, water are added in aqueous phase agitated kettle, stir and be warming up to 80-85 DEG C and be incubated 30min; Myristic acid, stearic acid, lauric acid, Palmic acid, glycol distearate, glyceryl monostearate, ceteareth-25 etc. are added in oil phase agitated kettle, stirs and be warming up to 80-85 DEG C and be incubated 30min;
(3), under 80-85 DEG C of temperature conditions, will stir, rotating speed 30-50rpm in aqueous phase suction emulsifying pot; Then open vacuum pump, then homogenizer will be opened, rotating speed 3000rpm in oil phase suction emulsifying pot, keep 30min;
(4), stir and be cooled to 50 DEG C, add methyl myristoyl sodium taurocholate, Pyrusussuriensis (sugar) alcohol, skin conditioning agent, hydrolyzed silkworm silk, polyquaternary ammonium salt-43, stir, after the assay was approved, filtration discharging fill.
Embodiment 3
(1), each component of following mass fraction is taken: myristic acid 3% by formula, glycerol 10%, Pyrusussuriensis (sugar) alcohol 5%, stearic acid 19%, Palmic acid 1%, lauric acid 3%, butanediol 5%, sodium lauroyl glutamate 8%, glycol distearate 2%, potassium hydroxide 5.1%, glyceryl monostearate 1%, ceteareth-25 is 2%, skin conditioning agent 0.5% (folic acid, bacillus cereus/fermented soybean product extract and hyaluronic weight ratio are 1:0.5:2), hydrolyzed silkworm silk 1.5%, polyquaternary ammonium salt-7 is 1%, Polyethylene Glycol-90M is 0.02%, water 32.88%,
(2), butanediol, glycerol, Polyethylene Glycol, potassium hydroxide, water are added in aqueous phase agitated kettle, stir and be warming up to 80-85 DEG C and be incubated 30min; Myristic acid, stearic acid, lauric acid, Palmic acid, glycol distearate, glyceryl monostearate, ceteareth-25 etc. are added in oil phase agitated kettle, stirs and be warming up to 80-85 DEG C and be incubated 25min;
(3), under 80-85 DEG C of temperature conditions, will stir, rotating speed 30-50rpm in aqueous phase suction emulsifying pot; Then open vacuum pump, then homogenizer will be opened, rotating speed 3000rpm in oil phase suction emulsifying pot, keep 30min;
(4), stir and be cooled to 50 DEG C, add sodium lauroyl glutamate, Pyrusussuriensis (sugar) alcohol, skin conditioning agent, hydrolyzed silkworm silk, polyquaternary ammonium salt-7, stir, after the assay was approved, filtration discharging fill.
Embodiment 4
(1), each component of following mass fraction is taken: myristic acid 3% by formula, glycerol 10%, Pyrusussuriensis (sugar) alcohol 5%, stearic acid 19%, Palmic acid 1%, lauric acid 3%, butanediol 5%, lauroyl glycine potassium 8%, glycol distearate 2%, potassium hydroxide 5.1%, glyceryl monostearate 1%, ceteareth-25 is 2%, skin conditioning agent 0.5% (folic acid, bacillus cereus/fermented soybean product extract and hyaluronic weight ratio are 1:0.5:2), hydrolyzed silkworm silk 1.5%, polyquaternary ammonium salt-7 is 1%, Polyethylene Glycol-45M is 0.02%, water 32.88%,
(2), butanediol, glycerol, Polyethylene Glycol-45M, potassium hydroxide, water are added in aqueous phase agitated kettle, stir and be warming up to 80-85 DEG C and be incubated 30min; Myristic acid, stearic acid, lauric acid, Palmic acid, glycol distearate, glyceryl monostearate, ceteareth-25 etc. are added in oil phase agitated kettle, stirs and be warming up to 80-85 DEG C and be incubated 25min;
(3), under 80-85 DEG C of temperature conditions, will stir, rotating speed 30-50rpm in aqueous phase suction emulsifying pot; Then open vacuum pump, then homogenizer will be opened, rotating speed 3000rpm in oil phase suction emulsifying pot, keep 30min;
(4), stir and be cooled to 50 DEG C, add lauroyl glycine potassium, Pyrusussuriensis (sugar) alcohol, skin conditioning agent, hydrolyzed silkworm silk, polyquaternary ammonium salt-7, stir, after the assay was approved, filtration discharging fill.
Embodiment 5
(1), each component of following mass fraction is taken: myristic acid 3% by formula, glycerol 10%, Pyrusussuriensis (sugar) alcohol 5%, stearic acid 19%, Palmic acid 1%, lauric acid 3%, butanediol 5%, sodium lauroyl sarcosine 8%, glycol distearate 2%, potassium hydroxide 5.1%, glyceryl monostearate 1%, ceteareth-25 is 2%, skin conditioning agent 0.5% (folic acid, bacillus cereus/fermented soybean product extract and hyaluronic weight ratio are 1:0.5:2), hydrolyzed silkworm silk 1.5%, polyquaternary ammonium salt-7 is 1%, Polyethylene Glycol-45M is 0.02%, water 32.88%,
(2), butanediol, glycerol, Polyethylene Glycol, potassium hydroxide, water are added in aqueous phase agitated kettle, stir and be warming up to 80-85 DEG C and be incubated 30min; Myristic acid, stearic acid, lauric acid, Palmic acid, glycol distearate, glyceryl monostearate, ceteareth-25 etc. are added in oil phase agitated kettle, stirs and be warming up to 80-85 DEG C and be incubated 25min;
(3), under 80-85 DEG C of temperature conditions, will stir, rotating speed 30-50rpm in aqueous phase suction emulsifying pot; Then open vacuum pump, then homogenizer will be opened, rotating speed 3000rpm in oil phase suction emulsifying pot, keep 30min;
(4), stir and be cooled to 50 DEG C, add sodium lauroyl sarcosine, Pyrusussuriensis (sugar) alcohol, skin conditioning agent, hydrolyzed silkworm silk, polyquaternary ammonium salt-7, stir, after the assay was approved, filtration discharging fill.
Use result is tested:
1, select that there are blackhead in 25 faces, the volunteer of corse sweat pore is tested, hydrolyzed silkworm silk facial milk cleanser 100mL obtained in embodiment 1-5, use once respectively at sooner or later each, add up after using 2 weeks.Add up effective, effective and invalid number, calculate with total effective rate (%), wherein total effective rate (%)=[(efficiently individual quantity+effective number)/experiment number] * 100%.Result of the test is in table 1.
Evaluation criterion: 1) effective: blackhead, fat granule disappear substantially;
2) effective: blackhead, fat granule reduce to some extent;
3) invalid: blackhead, fat granule are without improvement.
The table with test results of table 1 blackhead and fat granule
Show from the result of the test of table 1: facial milk cleanser obtained embodiment 1-5 has good effect to minimizing blackhead and fat granule, and wherein the effect of embodiment 2 is best.
2, select 25 volunteers to test, the facial milk cleanser obtained by Example 1-5, every bottle of 100mL, sooner or later respectively use once, add up after testing 2 weeks, test data is in table 2.
The test chart of the tight sense of rear skin and sensation of dryness washed by table 2
| Embodiment | The tight sense of face | Face's sensation of dryness |
| Embodiment 1 | Nothing | Nothing |
| Embodiment 2 | Nothing | Nothing |
| Embodiment 3 | Nothing | Nothing |
| Embodiment 4 | Nothing | Nothing |
| Embodiment 5 | Nothing | Nothing |
Show from the result of the test of table 2: the skinfeel test of facial milk cleanser obtained embodiment 1-5 is all comfortable.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the content disclosed in this embodiment.The equivalence completed under not departing from spirit disclosed in this invention so every or amendment, all fall into the scope of protection of the invention.
Claims (6)
1. a hydrolyzed silkworm silk facial milk cleanser, is characterized in that, this hydrolyzed silkworm silk facial milk cleanser is made up of the raw material of following mass fraction meter:
2. hydrolyzed silkworm silk facial milk cleanser according to claim 1, is characterized in that: described amino acid surfactant is the compositions of one or more in sodium lauroyl sarcosine, myristoyl-N-methylaminoacetic acid sodium, stearyl sarcosine sodium, methyl lauroyl sodium taurocholate, methyl myristoyl sodium taurocholate, methyl stearyl sodium taurocholate, sodium lauroyl glutamate, myristoyl glutamate sodium, stearyl sodium glutamate, lauroyl Glycine sodium, myristoyl glycine sodium, stearyl Glycine sodium.
3. hydrolyzed silkworm silk facial milk cleanser according to claim 1, is characterized in that: described polyquaternary ammonium salt conditioner is the compositions of one or more in polyquaternary ammonium salt-6, polyquaternary ammonium salt-7, polyquaternary ammonium salt-39, polyquaternary ammonium salt-43.
4. hydrolyzed silkworm silk facial milk cleanser according to claim 1, is characterized in that: described polyethylene glycols is the compositions of one or more in Polyethylene Glycol-7M, polyquaternary ammonium salt-14M, polyquaternary ammonium salt-2M, Polyethylene Glycol-5M, Polyethylene Glycol-45M, Polyethylene Glycol-90M.
5. hydrolyzed silkworm silk facial milk cleanser according to claim 1, is characterized in that: the mixture that described skin conditioning agent is folic acid, bacillus cereus/fermented soybean product extract and hyaluronic acid are 1:0.2-2:1-3 mixing according to weight ratio.
6. a preparation method for hydrolyzed silkworm silk facial milk cleanser as claimed in claim 1, its step comprises:
(1), various raw material has been weighed according to formula;
(2), by butanediol, glycerol, polyethylene glycols, potassium hydroxide and water stir, be incubated 0.2-0.6 hour after being warming up to 80-85 DEG C, as aqueous phase; Myristic acid, stearic acid, lauric acid, Palmic acid, glycol distearate, glyceryl monostearate, ceteareth-25 are stirred, is warming up to 80-85 DEG C and is incubated 0.3-0.6 hour, as oil phase;
(3), aqueous phase stirs with the speed of 30-50rpm, stirs, keep 0.3 hour after then adding oil phase with the speed of 3000rpm;
(4) be cooled to 45-50 DEG C, then add amino acid surfactant, Pyrusussuriensis (sugar) alcohol, skin conditioning agent, hydrolyzed silkworm silk, polyquaternary ammonium salt conditioner, stir, filter.
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| CN201510100518.7A CN104758223B (en) | 2015-03-06 | 2015-03-06 | One kind hydrolysis silk mildy wash and preparation method thereof |
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| CN201510100518.7A CN104758223B (en) | 2015-03-06 | 2015-03-06 | One kind hydrolysis silk mildy wash and preparation method thereof |
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Cited By (7)
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| CN105287331A (en) * | 2015-10-19 | 2016-02-03 | 广州科玛生物科技有限公司 | Anti-wrinkle cleansing lotion and preparation method thereof |
| CN105686975A (en) * | 2016-03-13 | 2016-06-22 | 佛山市芊茹化妆品有限公司 | Cleansing ointment and preparation method thereof |
| CN105902411A (en) * | 2016-05-17 | 2016-08-31 | 魏春红 | Cleansing foam and preparation method thereof |
| CN108969419A (en) * | 2018-08-31 | 2018-12-11 | 陈源忠 | A kind of chest draft quintessence liquid and preparation method thereof |
| CN110946785A (en) * | 2020-01-13 | 2020-04-03 | 蝶柔化妆品(浙江)有限公司 | Mild cleansing cream |
| CN111840099A (en) * | 2020-07-28 | 2020-10-30 | 广州蜜妆生物科技有限公司 | Facial cleanser with soap base compounded with amino acid surfactant |
| CN112274446A (en) * | 2020-10-30 | 2021-01-29 | 广州市妆妍生物技术有限公司 | Ceramide refreshing amino acid facial cleanser and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105287331A (en) * | 2015-10-19 | 2016-02-03 | 广州科玛生物科技有限公司 | Anti-wrinkle cleansing lotion and preparation method thereof |
| CN105287331B (en) * | 2015-10-19 | 2018-07-31 | 广州科玛生物科技股份有限公司 | A kind of crease-resistant mildy wash and preparation method thereof |
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| CN105902411A (en) * | 2016-05-17 | 2016-08-31 | 魏春红 | Cleansing foam and preparation method thereof |
| CN108969419A (en) * | 2018-08-31 | 2018-12-11 | 陈源忠 | A kind of chest draft quintessence liquid and preparation method thereof |
| CN110946785A (en) * | 2020-01-13 | 2020-04-03 | 蝶柔化妆品(浙江)有限公司 | Mild cleansing cream |
| CN111840099A (en) * | 2020-07-28 | 2020-10-30 | 广州蜜妆生物科技有限公司 | Facial cleanser with soap base compounded with amino acid surfactant |
| CN112274446A (en) * | 2020-10-30 | 2021-01-29 | 广州市妆妍生物技术有限公司 | Ceramide refreshing amino acid facial cleanser and preparation method thereof |
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