CN108379118A - A kind of organic mildy wash of astaxanthin and preparation method thereof - Google Patents

A kind of organic mildy wash of astaxanthin and preparation method thereof Download PDF

Info

Publication number
CN108379118A
CN108379118A CN201810258752.6A CN201810258752A CN108379118A CN 108379118 A CN108379118 A CN 108379118A CN 201810258752 A CN201810258752 A CN 201810258752A CN 108379118 A CN108379118 A CN 108379118A
Authority
CN
China
Prior art keywords
astaxanthin
organic
mildy wash
preparation
methylisothiazolinone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810258752.6A
Other languages
Chinese (zh)
Inventor
刘俊林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201810258752.6A priority Critical patent/CN108379118A/en
Publication of CN108379118A publication Critical patent/CN108379118A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35Ketones, e.g. benzophenone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/463Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P37/00Drugs for immunological or allergic disorders
    • A61P37/02Immunomodulators
    • A61P37/04Immunostimulants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

Abstract

The invention discloses a kind of organic mildy wash of astaxanthin, including following component, by weight percentage:Water 13% 15%, carbomer 0.05% 0.15%, citric acid 0.3% 0.5%, laruyl alcohol sodium sulfovinate 2% 4%, sodium cocoyl glycinate 43% 55%, 150 distearates of PEG 2% 10%, coconut oleoyl amine DEA2% 6%, Cocoamidopropyl betaine 10% 20%, methylisothiazolinone 0.5% 0.7%, astaxanthin 0.01% 0.03%, glycerine 15% 25%.The present invention using mildy wash prepared by above-mentioned raw materials there is anti-aging, ultra-violet radiation resisting also to have effects that good decontamination and moisturize the skin.

Description

A kind of organic mildy wash of astaxanthin and preparation method thereof
Technical field
The present invention relates to technical field of skin care, more particularly to seed shrimp blueness is known as machine mildy wash and its preparation side Method.
Background technology
Mildy wash is called facial cleanser, and facial cleanser is a kind of senior face washing agent, can clean facial dirt, can also remove ornaments and formal dress.Product Good facial cleanser of fine quality should have cleaning, nutrition, protection skin and other effects, and in general, common facial cleanser is that do not have to resist Aging effects.If adding suitable anti-aging ingredient again in high-quality facial cleanser, it is suitable for any skin quality skin and uses;Such as match Side's conditioning is appropriate, can meet most consumers and use, surfactant has and soaks, disperses, foam, go in facial cleanser Dirty, emulsification five effect greatly, is the chief active object of mildy wash, in addition, according to the similar principle that mixes, during washing one's face, can borrow The oil-soluble fat dirt of oil phase thing dissolving face and extra grease;Water-soluble sweat stain dirt on face is dissolved by means of its aqueous-phase material, Although mildy wash plays an important role in people's lives, mildy wash in the prior art often contains stimulation The composition of skin causes human body certain damage.
The function of astaxanthin is very big, this is a Carotenoids, and the color of extraction is red, is to have to beautifying Prodigious effect, and can be anti-aging, astaxanthin can resist ultraviolet radiation, because ultraviolet radiation is that skin is old Change and suffer from the major reason of cutaneum carcinoma, therefore takes some astaxanthins than vitamin to anti-ultraviolet with better function Greatly.
Therefore, study it is a kind of use astaxanthin for raw material can anti-aging, the mildy wash for improving skin elasticity is this field The problem of technical staff's urgent need to resolve.
Invention content
Can be anti-aging in view of this, the present invention provides a kind of mildy wash prepared by the raw material using astaxanthin, improve The mildy wash of skin elasticity.
To achieve the goals above, the present invention adopts the following technical scheme that:A kind of organic mildy wash of astaxanthin, including it is following Component, by weight percentage:
Water 13%-15%, carbomer 0.05%-0.15%, citric acid 0.3%-0.5%, laruyl alcohol sodium sulfovinate 2%- 4%, sodium cocoyl glycinate 43%-55%, PEG-150 distearates 2%-10%, coconut oleoyl amine DEA2%-6%, cocounut oil Amido propyl betaine 10%-20%, methylisothiazolinone 0.5%-0.7%, astaxanthin 0.01%-0.03%, glycerine 15%-25%.
Beneficial effects of the present invention:The mildy wash prepared using astaxanthin in the present invention can be anti-aging, resists ultraviolet light Radiation;And addition laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate and PEG-150 distearates have decontamination, emulsification, moisten Skin, sterilization and excellent foaming power, and there is good compatibility with skin.Therefore, mildy wash of the invention has anti- Aging, ultra-violet radiation resisting also have effects that good decontamination and moisturize the skin.
Preferably, further include essence 0.3%-0.6%.
Preferably, the organic mildy wash of a kind of astaxanthin, including following component, by weight percentage:Water 14.4%, card wave Nurse 0.1%, citric acid 0.4%, laruyl alcohol sodium sulfovinate 3%, sodium cocoyl glycinate 45%, PEG-150 distearates 10%, coconut oleoyl amine DEA4%, Cocoamidopropyl betaine 15%, methylisothiazolinone 0.6%, astaxanthin 0.02%, Glycerine 20%.
Preferably, the organic mildy wash of a kind of astaxanthin, including following component:Water 14.4%, 0.1% citric acid of carbomer 0.4%, laruyl alcohol sodium sulfovinate 3%, sodium cocoyl glycinate 53%, PEG-150 distearates 2%, coconut oleoyl amine DEA4%, Cocoamidopropyl betaine 15%, methylisothiazolinone 0.6%, astaxanthin 0.02%, glycerine 20%.
The present invention also provides a kind of preparation methods of the organic mildy wash of astaxanthin, include the following steps:
Step (1):Weigh each raw material in the organic mildy wash of above-mentioned astaxanthin;
Step (2):Coconut oleoyl amine, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin, essence is impartial It is divided into two parts, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, cocounut oil acyl glycine Sodium/PEG-150 distearates, PEG-150 distearates, glycerine, first part of coconut oleoyl amine DEA, cocamidopropyl propyl amide sweet tea Dish alkali, methylisothiazolinone and astaxanthin sequentially add in emulsification pot, stir, heating, and insulated and stirred is stood;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (3) Glycine betaine, stirring;
Step (5):Second part of methylisothiazolinone and astaxanthin are added in emulsification pot in step (4) after stirring, Continue to stir, sample, discharges after detection is qualified.
Preferably, mixing time is 3-6min in step (2), is warming up to 80-90 DEG C.
Preferably, insulated and stirred 25-35min in step (2), dwell temperature are 40-50 DEG C.
Preferably, mixing time is 8-12min in step (3).
Preferably, mixing time is 8-12min in step (4).
Preferably, further include essence 0.3%-0.6%, be divided into two parts, first part of essence relays astaxanthin in step (3) After be added;Second part of essence is added after step (5) relays astaxanthin.
It can be seen via above technical scheme that compared with prior art, the present disclosure provides a kind of astaxanthin is organic Mildy wash, using astaxanthin as raw material, using the anti-oxidant of astaxanthin, ultra-violet radiation resisting, the effect of enhancing autoimmunity, comes Prepare the mildy wash of beautifying face and moistering lotion.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
The embodiment of the invention discloses a kind of beautifying face and moistering lotion, anti-oxidant, ultra-violet radiation resisting mildy wash.
Embodiment 1
The organic mildy wash of astaxanthin:Water 14.4g, carbomer 0.1g, citric acid 0.4g, laruyl alcohol sodium sulfovinate 3g, cocounut oil Acyl Sodium Glycinate 45g, PEG-150 distearate 10g, coconut oleoyl amine DEA4g, Cocoamidopropyl betaine 15g, methyl are different Thiazolinone 0.6g, astaxanthin 0.02g, glycerine 20g, essence 0.3g.
Above-mentioned preparation method is as follows:Step (1):Weigh each raw material in the organic mildy wash of above-mentioned astaxanthin;
Step (2):Coconut oleoyl amine, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin, essence is impartial It is divided into two parts, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, PEG-150 bis- is firmly Resin acid ester, glycerine, first part of coconut oleoyl amine DEA, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin and essence It sequentially adds in emulsification pot, stirs 5min, be warming up to 85 DEG C, insulated and stirred 30min, stand to 45 DEG C;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (2) Glycine betaine stirs 10min;
Step (5):Be added in emulsification pot in the step (3) after stirring second part of methylisothiazolinone, astaxanthin and Essence continues to stir 10min, and sampling discharges after detection is qualified.
Embodiment 2
The organic mildy wash of astaxanthin:Water 14.4g, carbomer 0.1g, citric acid 0.4g, laruyl alcohol sodium sulfovinate 3g, cocounut oil Acyl Sodium Glycinate 53g, PEG-150 distearate 2g, coconut oleoyl amine DEA4g, Cocoamidopropyl betaine 15g, methyl are different Thiazolinone 0.6g, astaxanthin 0.02g, glycerine 20g, essence 0.3g.
Above-mentioned preparation method is as follows:Step (1):Weigh each raw material in the organic mildy wash of above-mentioned astaxanthin;
Step (2):Coconut oleoyl amine, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin, essence is impartial It is divided into two parts, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, PEG-150 bis- is firmly Resin acid ester, glycerine, first part of coconut oleoyl amine DEA, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin and essence It sequentially adds in emulsification pot, stirs 5min, be warming up to 85 DEG C, insulated and stirred 30min, stand to 45 DEG C;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (2) Glycine betaine stirs 10min;
Step (5):Be added in emulsification pot in the step (3) after stirring second part of methylisothiazolinone, astaxanthin and Essence continues to stir 10min, and sampling discharges after detection is qualified.
Embodiment 3
The organic mildy wash of astaxanthin:Water 13g, carbomer 0.05g, citric acid 0.3g, laruyl alcohol sodium sulfovinate 2g, cocounut oil acyl Sodium Glycinate 43g, PEG-150 distearate 10g, coconut oleoyl amine DEA2g, Cocoamidopropyl betaine 10g, the different thiophene of methyl Oxazoline ketone 0.5g, astaxanthin 0.01g, glycerine 15g, essence 0.3g.
Above-mentioned preparation method is as follows:Step (1):Weigh each raw material in the organic mildy wash of above-mentioned astaxanthin;
Step (2):Coconut oleoyl amine, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin, essence is impartial It is divided into two parts, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, PEG-150 bis- is firmly Resin acid ester, glycerine, first part of coconut oleoyl amine DEA, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin and essence It sequentially adds in emulsification pot, stirs 5min, be warming up to 85 DEG C, insulated and stirred 30min, stand to 45 DEG C;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (2) Glycine betaine stirs 10min;
Step (5):Be added in emulsification pot in the step (3) after stirring second part of methylisothiazolinone, astaxanthin and Essence continues to stir 10min, and sampling discharges after detection is qualified.
Embodiment 4
The organic mildy wash of astaxanthin:Water 15g, carbomer 0.15g, citric acid 0.5g, laruyl alcohol sodium sulfovinate 4g, cocounut oil acyl Sodium Glycinate 53g, PEG-150 distearate 2g, coconut oleoyl amine DEA6g, Cocoamidopropyl betaine 20g, the different thiophene of methyl Oxazoline ketone 0.7g, astaxanthin 0.03g, glycerine 25g, essence 0.6g.
Above-mentioned preparation method is as follows:Step (1):Weigh each raw material in the organic mildy wash of above-mentioned astaxanthin;
Step (2):Coconut oleoyl amine, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin, essence is impartial It is divided into two parts, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, PEG-150 bis- is firmly Resin acid ester, glycerine, first part of coconut oleoyl amine DEA, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin and essence It sequentially adds in emulsification pot, stirs 5min, be warming up to 85 DEG C, insulated and stirred 30min, stand to 45 DEG C;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (2) Glycine betaine stirs 10min;
Step (5):Be added in emulsification pot in the step (3) after stirring second part of methylisothiazolinone, astaxanthin and Essence continues to stir 10min, and sampling discharges after detection is qualified.
Embodiment 5
The organic mildy wash of astaxanthin:Water 14g, carbomer 0.08g, citric acid 0.4g, laruyl alcohol sodium sulfovinate 3g, cocounut oil acyl Sodium Glycinate 53g, PEG-150 distearate 2g, coconut oleoyl amine DEA4g, Cocoamidopropyl betaine 15g, the different thiophene of methyl Oxazoline ketone 0.6g, astaxanthin 0.02g, glycerine 20g, essence 0.4g.
Above-mentioned preparation method is as follows:Step (1):Weigh each raw material in the organic mildy wash of above-mentioned astaxanthin;
Step (2):Coconut oleoyl amine, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin, essence is impartial It is divided into two parts, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, PEG-150 bis- is firmly Resin acid ester, glycerine, first part of coconut oleoyl amine DEA, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin and essence It sequentially adds in emulsification pot, stirs 5min, be warming up to 85 DEG C, insulated and stirred 30min, stand to 45 DEG C;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (2) Glycine betaine stirs 10min;
Step (5):Be added in emulsification pot in the step (3) after stirring second part of methylisothiazolinone, astaxanthin and Essence continues to stir 10min, and sampling discharges after detection is qualified.
Embodiment 6
The organic mildy wash of astaxanthin:Water 14g, carbomer 0.08g, citric acid 0.4g, laruyl alcohol sodium sulfovinate 3g, cocounut oil acyl Sodium Glycinate 55g, PEG-150 distearate 3g, coconut oleoyl amine DEA4g, Cocoamidopropyl betaine 15g, the different thiophene of methyl Oxazoline ketone 0.6g, astaxanthin 0.02g, glycerine 20g, essence 0.4g.
Above-mentioned preparation method is as follows:Step (1):Weigh each raw material in the organic mildy wash of above-mentioned astaxanthin;
Step (2):Coconut oleoyl amine, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin, essence is impartial It is divided into two parts, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, PEG-150 bis- is firmly Resin acid ester, glycerine, first part of coconut oleoyl amine DEA, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin and essence It sequentially adds in emulsification pot, stirs 5min, be warming up to 85 DEG C, insulated and stirred 30min, stand to 45 DEG C;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (2) Glycine betaine stirs 10min;
Step (5):Be added in emulsification pot in the step (3) after stirring second part of methylisothiazolinone, astaxanthin and Essence continues to stir 10min, and sampling discharges after detection is qualified.
Performance test:
One, trial target:The mildy wash that embodiment 1-6 is prepared
Two, tested crowd's data and grouping:70 skin healths, the tested volunteer of women of no skin disease allergies, 35 ~55 years old, by average age 35 years old, it is randomly divided into 7 groups, every group of 10 people, wherein 6 groups using the face cleaning prepared in embodiment 1-6 Breast is test group;One group is control group without using mildy wash.
Three, test method:The skin elasticity manufactured using German Courage+Khazaka companies (German CK companies) CotometerMPA580 hosts, used probe is ReviscometerRV600 elastic fibrous tissues test probe, surveys five It is secondary to be averaged.Test zone:Place between the eyebrows middle up 2cm foreheads region, lower lip middle 2cm chin areas, nose down Point and left and right cheek region at pupil intersection.The blank value (R2, R5, R7) of 30min after being tested region clean is first measured, so Regulation subject adheres to using above-mentioned trial target daily sooner or later afterwards, test zone skin after testing 2 weeks, 4 weeks, 6 weeks, 8 weeks respectively Elasticity indexes R2, R5, R7 value (it is 450mbar that negative pressure is constant in test process).
Index explanation:For skin elasticity index R2, R5, R7 closer to 1, the elasticity of skin is better.
R2=Ua/Uf;R5=Ur/Ue;R7=Ur/Uf
Uf --- skin maximum tension amount
Ue --- after constant negative pressure is added on skin, the amount of tension of skin, positioning elastic part amount of tension at 0.1 second.
Ur --- after cancelling negative pressure, skin will restore to the original state rapidly state, equally be divided into elastic portion score value Ur, that is, cancel negative Pressure is after 0.1 second, the recovery value and visco-elastic portions value or plastic value of skin.
Ua --- from cancellation negative pressure to the recovery value of skin when follow-on test skin surface adds negative pressure again next time.
Four, test result is as follows table 1.
Table 1
It increased using R2, R5, R7 after embodiment 1-6 mildy wash the 2nd week, implement after the 8th week as can be seen from Table 1 R2, R5, R7 of example 1-6 rises obviously, and value levels off to 1, and R2, R5, R7 ascensional range unobvious of control group, explanation Using embodiment 1-6 anti-aging mildy wash, the skin elasticity of subject is obviously improved, and control group breast lack the present invention it is anti-ageing Certain components in old mildy wash formula, illustrate whitening anti-aging mildy wash formula of the present invention not by the simple of each component What combination obtained, further illustrate there is synergistic effect between inventive formulation each component.It can be seen that anti-aging face cleaning Breast, which has, increases skin elasticity, anti-aging function, and then slows down aging.
Each embodiment is described by the way of progressive in this specification, the highlights of each of the examples are with other The difference of embodiment, just to refer each other for identical similar portion between each embodiment.For device disclosed in embodiment For, since it is corresponded to the methods disclosed in the examples, so description is fairly simple, related place is said referring to method part It is bright.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention. Various modifications to these embodiments will be apparent to those skilled in the art, as defined herein General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one The widest range caused.

Claims (10)

1. a kind of organic mildy wash of astaxanthin, which is characterized in that including following component, by weight percentage:
2. the organic mildy wash of a kind of astaxanthin according to claim 1, which is characterized in that further include essence 0.3%- 0.6%.
3. the organic mildy wash of a kind of astaxanthin according to claim 1, which is characterized in that including following component, by weight Percentages:
4. the organic mildy wash of a kind of astaxanthin according to claim 1, which is characterized in that including following component:
5. a kind of preparation method of the organic mildy wash of astaxanthin, which is characterized in that include the following steps:
Step (1):Each raw material is weighed according to the organic mildy wash of any one of Claims 1-4 astaxanthin;
Step (2):Coconut oleoyl amine DEA, Cocoamidopropyl betaine, methylisothiazolinone, astaxanthin are divided into two Part, it is spare;
Step (3):By water, carbomer, citric acid, laruyl alcohol sodium sulfovinate, sodium cocoyl glycinate, sodium cocoyl glycinate/ PEG-150 distearates, PEG-150 distearates, glycerine, first part of coconut oleoyl amine DEA, cocamidopropyl propyl amide beet Alkali, methylisothiazolinone and astaxanthin sequentially add in emulsification pot, stir, heating, and insulated and stirred is stood;
Step (4):Second part of coconut oleoyl amine DEA and cocamidopropyl propyl amide are added in the emulsification pot stood in step (3) Glycine betaine, stirring;
Step (5):Second part of methylisothiazolinone and astaxanthin are added in emulsification pot in step (4) after stirring, continues Stirring, sampling discharge after detection is qualified.
6. a kind of preparation method of the organic mildy wash of astaxanthin according to claim 5, which is characterized in that in step (2) The mixing time is 3-6min, described to be warming up to 80-90 DEG C.
7. a kind of preparation method of the organic mildy wash of astaxanthin according to claim 5, which is characterized in that in step (2) The insulated and stirred 25-35min, the dwell temperature are 40-50 DEG C.
8. a kind of preparation method of the organic mildy wash of astaxanthin according to claim 5, which is characterized in that in step (3) The mixing time is 8-12min.
9. a kind of preparation method of the organic mildy wash of astaxanthin according to claim 5, which is characterized in that in step (4) Mixing time is 8-12min.
10. a kind of preparation method of the organic mildy wash of astaxanthin according to claim 5, which is characterized in that further include perfume (or spice) Smart 0.3%-0.6% is divided into two parts, and first part of essence is added after step (3) relays astaxanthin;Second part of essence is in step (5) it is added after relaying astaxanthin.
CN201810258752.6A 2018-03-27 2018-03-27 A kind of organic mildy wash of astaxanthin and preparation method thereof Pending CN108379118A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810258752.6A CN108379118A (en) 2018-03-27 2018-03-27 A kind of organic mildy wash of astaxanthin and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810258752.6A CN108379118A (en) 2018-03-27 2018-03-27 A kind of organic mildy wash of astaxanthin and preparation method thereof

Publications (1)

Publication Number Publication Date
CN108379118A true CN108379118A (en) 2018-08-10

Family

ID=63072268

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810258752.6A Pending CN108379118A (en) 2018-03-27 2018-03-27 A kind of organic mildy wash of astaxanthin and preparation method thereof

Country Status (1)

Country Link
CN (1) CN108379118A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101151016A (en) * 2005-01-28 2008-03-26 巴斯夫股份有限公司 Use of a water-in-water emulsion polymers in the form of a thickener for cosmetic preparations
WO2012142407A1 (en) * 2011-04-15 2012-10-18 Topmd, Inc. Sodium hypochlorite-based body wash compositions
CN105030555A (en) * 2014-04-17 2015-11-11 赢创工业集团股份有限公司 Surfactant compositions and highly oleaginous formulations containing these
CN105232442A (en) * 2015-11-18 2016-01-13 中山市艾丽意素生物科技有限公司 Plant antioxidation amino acid cleanser and preparation method thereof
CN105287331A (en) * 2015-10-19 2016-02-03 广州科玛生物科技有限公司 Anti-wrinkle cleansing lotion and preparation method thereof
EP3225231A1 (en) * 2016-03-28 2017-10-04 Sweet Distribuidora, Importacao e Exportacao de Cosmeticos Ltda. - ME Cosmetic haircare product for the straightening of hair in shampoo format

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101151016A (en) * 2005-01-28 2008-03-26 巴斯夫股份有限公司 Use of a water-in-water emulsion polymers in the form of a thickener for cosmetic preparations
WO2012142407A1 (en) * 2011-04-15 2012-10-18 Topmd, Inc. Sodium hypochlorite-based body wash compositions
CN105030555A (en) * 2014-04-17 2015-11-11 赢创工业集团股份有限公司 Surfactant compositions and highly oleaginous formulations containing these
CN105287331A (en) * 2015-10-19 2016-02-03 广州科玛生物科技有限公司 Anti-wrinkle cleansing lotion and preparation method thereof
CN105232442A (en) * 2015-11-18 2016-01-13 中山市艾丽意素生物科技有限公司 Plant antioxidation amino acid cleanser and preparation method thereof
EP3225231A1 (en) * 2016-03-28 2017-10-04 Sweet Distribuidora, Importacao e Exportacao de Cosmeticos Ltda. - ME Cosmetic haircare product for the straightening of hair in shampoo format

Similar Documents

Publication Publication Date Title
CN109589279B (en) Solid shampoo and preparation method thereof
CN105287290B (en) A kind of whitening anti-aging mildy wash and preparation method thereof
CN108096173A (en) Mild amino acid shampoo of a kind of green and preparation method thereof
CN107296771A (en) A kind of desquamation compositions and extra quality multiple-effect are without silicone oil shampoo
CN103167863B (en) Composition comprising the mixture containing isostearoyl amine, glyceride and water
CN106333901A (en) Mild moisturizing nourishing face-cleaning composition
CN103800252A (en) Hair-care composition capable of quickly and deeply repairing hair
CN108125870B (en) Scalp nourishing composition, preparation method and application thereof, and scalp nourishing shampoo
CN107427429A (en) Emulsified cosmetic preparation composition with pH buffer systems
CN109288725A (en) A kind of transparent amino acid pattern is without silicone oil shampoo
CN110037955A (en) A kind of amino acid shower cream and preparation method thereof suitable for the pregnancy period
CN107308043A (en) A kind of removing acnes and controlling oil mildy wash and preparation method thereof
CN108295010A (en) A kind of yellow ginger oil-control hair-loss preventing and hair-restoring shampoo and preparation method thereof
JP2010235572A (en) Hair dyeing pretreatment composition and hair dyeing method using the same
CN110314126A (en) A kind of amino acid strengthen the hair shampoo
DE10360688A1 (en) Two- or multi-phase cosmetic products with improved reversible mixing and separation behavior
CN108379118A (en) A kind of organic mildy wash of astaxanthin and preparation method thereof
CN110327257A (en) A kind of transparent amino acid shampoo with treatment
WO2012084338A2 (en) Hair treatment agent for smoothing keratin-containing fibres
CN110755329A (en) Washing and protecting product containing novel surfactant and manufacturing process
CN101862276A (en) Hair conditioner
CN109044881A (en) A kind of pearl shining shampoo composition and a kind of preparation method of pearl shining shampoo composition
CN108158921A (en) A kind of plant composition comprising tea bran and rosemary and its preparation method and application
CN111888298B (en) Shower gel and preparation method thereof
CN115300405A (en) Hair composition with color protection effect and preparation method and application thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180810