CN105085023A - Foliar fertilizer prepared through Chinese medicine residue fermentation and preparation method thereof - Google Patents

Foliar fertilizer prepared through Chinese medicine residue fermentation and preparation method thereof Download PDF

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Publication number
CN105085023A
CN105085023A CN201510470801.9A CN201510470801A CN105085023A CN 105085023 A CN105085023 A CN 105085023A CN 201510470801 A CN201510470801 A CN 201510470801A CN 105085023 A CN105085023 A CN 105085023A
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China
Prior art keywords
chinese medicine
water
fermentation
preparation
medicine slag
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CN201510470801.9A
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Chinese (zh)
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陈金华
周浩
王晓亭
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Maanshan Kebang Eco Fertilizer Co Ltd
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Maanshan Kebang Eco Fertilizer Co Ltd
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Priority to CN201510470801.9A priority Critical patent/CN105085023A/en
Publication of CN105085023A publication Critical patent/CN105085023A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

Abstract

The invention discloses foliar fertilizer prepared through Chinese medicine residue fermentation and a preparation method thereof. The foliar fertilizer is prepared from, by weight, Chinese medicine residues, tea leaf residues, tea bran, industrial wastewater, rice straw, monopotassium phosphate, sodium fulvate, EM microbial agents, saturated lime water, borax, calcium ammonium nitrate, precipitating agents and an appropriate amount of water. Leftovers of the tea bran, tea leaf powder and the Chinese medicine residues are fully utilized, pollution of the leftovers to the environment is reduced, various components are decomposed into micromolecule structures through fermentation, and therefore the foliar surface can conveniently absorb the components; meanwhile, various organic substances belong to unsaturated macromoleculars and have the certain adsorption action on inorganic ions after being mixed with inorganic fertilizer, the fertilizer waste is reduced, and absorption and utilization of inorganic components are facilitated.

Description

Foliar nutrient that a kind of Chinese medicine slag fermentation is standby and preparation method thereof
Technical field
The invention belongs to the apartment technical field of fertilizer, be specifically related to standby foliar nutrient of a kind of Chinese medicine slag fermentation and preparation method thereof.
Background technology
Liquid fermenting is one of modern biotechnology, it refers in biochemical reactor, natural imitation circle is by the oxygen of edible medicinal fungus in residue process required for necessary carbohydrate, organic and inorganic some trace elements of compound, inorganic salt etc. containing nitrogen and other thalline respiratory metabolism, and control suitable ambient conditions, carry out the prolific process of mycelia.The large-scale fermentation culture of industrialization is fermentative production, also known as deep drainpipe or reticent cultivation.Industrial fermentation is produced must adopt fermentor tank, and fermentation culture many employings triangular flask in laboratory.Contain thalline in the fermented liquid obtained, be decomposed and undecomposed nutritive ingredient, the meta-bolites that thalline produces.The direct hyoscine of fermented liquid or confession separation and Extraction, also can do liquid spawn.
The energy needed for the liquid of edible medicinal fungus can use cerelose, industrial starch and Rhizoma Dioscoreae powder etc.; Nitrogenous source can adopt soybean cake powder, dried silkworm chrysalis meal, bran powder etc.In order to reduce costs, usually also adopt part trade effluent to be surrogate, as soybean wastewater, raw material sources are extensive.The nutrition distribution pattern of liquid nutrient medium is even, is conducive to abundant contact and the absorption of mushroom nourishing body.Mycelia can grow, can discharge in time the metabolism waste gas of respiration generation inside and outside reactor under optimum temperuture, pH, oxygen and carbon-nitrogen ratio condition, therefore metabolic vigorous, mycelial growth division rapidly, the meta-bolites that a large amount of mycelium and polysaccharide, polypeptide etc. have physiologically active can be accumulated at short notice, cultivated by liquid state fermentation and obtain a large amount of mycelium and physiologically active substance and generally only need the time of 2 ~ 7 days and cell age is neat, and solid culture needs 30 ~ 50 days.Liquid strain can effectively reduce strain pollution rate, has flowing fast, easily disperses, a bacterium point is many, sprout the features such as fast, can effectively reduce the pollution of edible mushrooms in seeded process.
The product of microbial metabolism is broadly divided into two classes: primary metabolite and secondary metabolite, primary metabolite is that the breeding of microbe metabolism growth is necessary, can produce in whole life cycle more always, amino acid, Nucleotide, polysaccharide, lipid and VITAMIN etc. are produced in cell, and secondary metabolite microbiotic, alkaloid, bacteriotoxin and plant growth factor etc. that to be extracellular produce, of a great variety.
Summary of the invention
The present invention, in order to improve the quality of foliar nutrient, improves the utilization ratio of liquid fertilizer, and after inventing a kind of liquid state fermentation, the effective constituent extracted in fermented liquid makes a kind of high efficiency composition liquid fertilizer, and specific practice is as follows:
The foliar nutrient that a kind of Chinese medicine slag fermentation is standby, it is characterized in that, be made up of the raw material of following weight part: Chinese medicine slag 10 ~ 15, tealeaf residue 30 ~ 45, tea bran 30 ~ 40, trade effluent 15 ~ 20, rice straw 20 ~ 25, potassium primary phosphate 10 ~ 15, SODLUM FULVATE 3 ~ 5, EM microbial inoculum 2 ~ 3, saturated limewater 8 ~ 12, borax 4 ~ 7, calcium ammonium nitrate 8 ~ 10, precipitation agent 7 ~ 9 and appropriate water;
Described sinking agent is made up of the raw material of following weight part: lime powder 15 ~ 20,10% alum liquor 12 ~ 16,10% acetic acid solution 4 ~ 6, primary isoamyl alcohol 0.6 ~ 1.0, polyvinyl alcohol 6 ~ 8, tween 80 1.5 ~ 3, industrial Viscotrol C 2 ~ 4, ethanol 4 ~ 7 and water 50; The mixing of second alcohol and water is poured in reactor by preparation method, then polyvinyl alcohol is added, be heated to 70 ~ 80 DEG C of stirring and dissolving, then add 10% alum liquor, 10% acetic acid solution, primary isoamyl alcohol and lime powder, keep temperature of reaction kettle, adjustment rotating speed 150 ~ 200r/min stirs 20 ~ 35min, finally add tween 80 and industrial Viscotrol C simultaneously, insulated and stirred 30min is emulsion uniformly, obtains residue by funnel suction filtration, pulverizes to obtain pulvis sinking agent after oven dry.
A preparation method for the foliar nutrient that Chinese medicine slag fermentation is standby, is characterized in that, comprises following step:
(1) mix Chinese medicine slag, tealeaf residue, tea bran, trade effluent and rice straw, add the water of 10 ~ 15 times of its weight parts, ball milling 30 ~ 40min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) EM microbial inoculum is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH6 ~ 7.5, temperature 25 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 6 ~ 8 days;
(3) after (2) complete, fermented liquid is separately put in container, ultrasonic cell disruption instrument is utilized to carry out microbial disruption, with flowing water, container is lowered the temperature simultaneously, then precipitation agent mixing is added, then add saturated limewater, after stirring 8 ~ 10min, keep fermented liquid inertial motion, leave standstill 20 ~ 25min and carry out precipitation adsorption process voluntarily, after completing, supernatant liquor got by wooden dipper;
(4) mixed phosphate potassium dihydrogen, SODLUM FULVATE, borax, calcium ammonium nitrate and other remaining component, is added in the supernatant liquor described in (3), after stirring at room temperature is dissolved.
By alum, (main component is KAl (SO 4) 2gain enlightenment, its principle utilizes it in water, ionize out two metal ion species, and Al 3+be easy to hydrolysis, generate the aluminium hydroxide Al of colloid 3++ 3H 2o=Al (OH) 3+ 3H +(reversible), the adsorptive power of alumine hydroxide colloid is strong, the impurity that can suspend in planar water, and form precipitation, make clarification of water, although successful, but the throw out after sedimentation is easily loose, be again diffused in water, the present invention not only will make the fermented liquid after fermentation clarify, also must possess make not allow composition granule composition to condense speed is fast, settling velocity fast, easily extract the features such as supernatant liquor after sedimentation, the present invention proposes sinking agent for this reason.
The operation instruction of sinking agent: adopt 10% alum liquor to be the main component of precipitation agent, the sedimentation effect reached is best, then 10% acetic acid is adopted to have certain promoter action as the separating effect of sedimentation medium to inorganic sinking agent, but the reaction of acetic acid and fermented liquid is comparatively slow, period, some fermented liquid was overflowed with the bubble of densification, so add primary isoamyl alcohol when preparing sinking agent as defoamer, adding the minimum lime powder of particle diameter is stablizer, secondly the weight of sorbent material is increased, avoid the sinking agent settling velocity of one-component slow, adding polyvinyl alcohol makes each ingredient adsorption of Tai-Ace S 150 and sedimentation promoter action on the surface of lime powder particle as binding agent, after all the components has adsorbed, finally adding a certain amount of vegetables oil can effectively prevent sinking agent particle to be mutually sticked together, become agglomerate, influence effect, particle aggregation agent after completing just can with an overall form storage, transport and use, successful.
The present invention adopts liquid state fermentation to ferment, first initial centrifugation, the oarse-grained particulate matter of filtering, ultrasonic cell disintegration instrument is utilized by remaining liq to carry out fragmentation to the microorganism in liquid, simultaneously in order to prevent heat production in process, cause temperature to raise and adopt flowing water stream to lower the temperature, by special sinking agent, adsorption precipitation is carried out to the residue in fermentation and unfermentable solid waste, obtain comparatively pure liquid extracting solution, some mineral substance that add that finally can be composite carry out function improvement and nutritional supplementation, it is reduce molecule to the impact of blade that pure extracting solution is used as foliar nutrient, the easy blocking blades pore of finely ground particles, affect respiration, next is unfavorable for prevention and elimination of disease and pests.
Intracellular organic matter can be discharged: the organic compositions such as amino acid, Nucleotide, nucleic acid, carbohydrate, make the nutritive ingredient of extracting solution abundanter while the meaning of microbial disruption is microorganism cells cracking.
Beneficial effect of the present invention: make full use of tea bran, tea leaf powder, the tankage of Chinese medicine slag, reduce their environmental pollutions, make use of again their organic matter and biological activity simultaneously, tea bran, in tea leaf powder, ingredient is oil tea, inorganic nutrients is absorbed in tea growth growth course, here utilize fermentation that various ingredient breakdown is become small molecule structure, be convenient to unilateral absorption, various organism belongs to undersaturated macromole simultaneously, to mineral ion, there is certain adsorption with after mineral manure mixing, reduce the waste of fertilizer, also help absorbing of inorganic components.
Embodiment
Embodiment 1:
The foliar nutrient that a kind of Chinese medicine slag fermentation is standby, it is characterized in that, be made up of the raw material of following weight part (Kg): Chinese medicine slag 12, tealeaf residue 36, tea bran 35, trade effluent 17, rice straw 22, potassium primary phosphate 12, SODLUM FULVATE 4, EM microbial inoculum 2, saturated limewater 10, borax 5, calcium ammonium nitrate 10, precipitation agent 7 and appropriate water;
Described sinking agent is made up of the raw material of following weight part: lime powder 16,10% alum liquor 15,10% acetic acid solution 5, primary isoamyl alcohol 0.7, polyvinyl alcohol 6, tween 80 1.5, industrial Viscotrol C 3, ethanol 6 and water 50; The mixing of second alcohol and water is poured in reactor by preparation method, then polyvinyl alcohol is added, be heated to 70 ~ 80 DEG C of stirring and dissolving, then add 10% alum liquor, 10% acetic acid solution, primary isoamyl alcohol and lime powder, keep temperature of reaction kettle, adjustment rotating speed 150 ~ 200r/min stirs 20 ~ 35min, finally add tween 80 and industrial Viscotrol C simultaneously, insulated and stirred 30min is emulsion uniformly, obtains residue by funnel suction filtration, pulverizes to obtain pulvis sinking agent after oven dry.
A preparation method for the foliar nutrient that Chinese medicine slag fermentation is standby, is characterized in that, comprises following step:
(1) mix Chinese medicine slag, tealeaf residue, tea bran, trade effluent and rice straw, add the water of 10 ~ 15 times of its weight parts, ball milling 30 ~ 40min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) EM microbial inoculum is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH6 ~ 7.5, temperature 25 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 6 ~ 8 days;
(3) after (2) complete, fermented liquid is separately put in container, ultrasonic cell disruption instrument is utilized to carry out microbial disruption, with flowing water, container is lowered the temperature simultaneously, then precipitation agent mixing is added, then add saturated limewater, after stirring 8 ~ 10min, keep fermented liquid inertial motion, leave standstill 20 ~ 25min and carry out precipitation adsorption process voluntarily, after completing, supernatant liquor got by wooden dipper;
(4) mixed phosphate potassium dihydrogen, SODLUM FULVATE, borax, calcium ammonium nitrate and other remaining component, is added in the supernatant liquor described in (3), after stirring at room temperature is dissolved.
Foliar nutrient standby for a kind of Chinese medicine slag fermentation of the present invention is used for planting fertilizer viny, select 5 mu of grapevine fields as experimental group, ginseng is inserted and is used fertilizer of the present invention, 1 year 2 times, every mu sprays 75 ~ 100Kg at every turn, 5 mu of grapevines of control group are left intact, the control of other curing conditions and disease and pest is all identical, and result shows the grapevine of experimental group, leaf color, limb and growing way all will due to control groups, resistance viny increases simultaneously, reduces the generation of disease and pest, environmental protection, cost is lower, Ji raising 22.1% relatively.

Claims (2)

1. the foliar nutrient that a Chinese medicine slag fermentation is standby, it is characterized in that, be made up of the raw material of following weight part: Chinese medicine slag 10 ~ 15, tealeaf residue 30 ~ 45, tea bran 30 ~ 40, trade effluent 15 ~ 20, rice straw 20 ~ 25, potassium primary phosphate 10 ~ 15, SODLUM FULVATE 3 ~ 5, EM microbial inoculum 2 ~ 3, saturated limewater 8 ~ 12, borax 4 ~ 7, calcium ammonium nitrate 8 ~ 10, precipitation agent 7 ~ 9 and appropriate water;
Described sinking agent is made up of the raw material of following weight part: lime powder 15 ~ 20,10% alum liquor 12 ~ 16,10% acetic acid solution 4 ~ 6, primary isoamyl alcohol 0.6 ~ 1.0, polyvinyl alcohol 6 ~ 8, tween 80 1.5 ~ 3, industrial Viscotrol C 2 ~ 4, ethanol 4 ~ 7 and water 50; The mixing of second alcohol and water is poured in reactor by preparation method, then polyvinyl alcohol is added, be heated to 70 ~ 80 DEG C of stirring and dissolving, then add 10% alum liquor, 10% acetic acid solution, primary isoamyl alcohol and lime powder, keep temperature of reaction kettle, adjustment rotating speed 150 ~ 200r/min stirs 20 ~ 35min, finally add tween 80 and industrial Viscotrol C simultaneously, insulated and stirred 30min is emulsion uniformly, obtains residue by funnel suction filtration, pulverizes to obtain pulvis sinking agent after oven dry.
2. the preparation method of the foliar nutrient that a kind of Chinese medicine slag fermentation is standby according to claim 1, is characterized in that, comprise following step:
(1) mix Chinese medicine slag, tealeaf residue, tea bran, trade effluent and rice straw, add the water of 10 ~ 15 times of its weight parts, ball milling 30 ~ 40min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) EM microbial inoculum is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH6 ~ 7.5, temperature 25 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 6 ~ 8 days;
(3) after (2) complete, fermented liquid is separately put in container, ultrasonic cell disruption instrument is utilized to carry out microbial disruption, with flowing water, container is lowered the temperature simultaneously, then precipitation agent mixing is added, then add saturated limewater, after stirring 8 ~ 10min, keep fermented liquid inertial motion, leave standstill 20 ~ 25min and carry out precipitation adsorption process voluntarily, after completing, supernatant liquor got by wooden dipper;
(4) mixed phosphate potassium dihydrogen, SODLUM FULVATE, borax, calcium ammonium nitrate and other remaining component, is added in the supernatant liquor described in (3), after stirring at room temperature is dissolved.
CN201510470801.9A 2015-08-05 2015-08-05 Foliar fertilizer prepared through Chinese medicine residue fermentation and preparation method thereof Withdrawn CN105085023A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106007897A (en) * 2016-05-13 2016-10-12 淄博夸克医药技术有限公司 Mild flower plant fertilizer
CN106007972A (en) * 2016-05-24 2016-10-12 南宁圣特生物科技有限公司 Tea bran biofertilizer and preparation method thereof
CN106045731A (en) * 2016-08-18 2016-10-26 广西鑫雅皇庭园林工程有限责任公司 Foliar fertilizer specially used for tea leaves and preparation method thereof
CN106187436A (en) * 2016-07-01 2016-12-07 安徽万利生态园林景观有限公司 A kind of osmanthus fragrans foliage fertilizer additives and preparation method thereof
CN109197359A (en) * 2018-11-07 2019-01-15 常宁市瑶园生态农业科技发展有限公司 A kind of implantation methods of environmental protection tea

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104177195A (en) * 2014-09-11 2014-12-03 标优美生态工程股份有限公司 Special fertilizer for foliage spraying type flowers and preparation method thereof
CN104803792A (en) * 2015-04-28 2015-07-29 云南省农业科学院热带亚热带经济作物研究所 Bagasse bio-organic fertilizer and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104177195A (en) * 2014-09-11 2014-12-03 标优美生态工程股份有限公司 Special fertilizer for foliage spraying type flowers and preparation method thereof
CN104803792A (en) * 2015-04-28 2015-07-29 云南省农业科学院热带亚热带经济作物研究所 Bagasse bio-organic fertilizer and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106007897A (en) * 2016-05-13 2016-10-12 淄博夸克医药技术有限公司 Mild flower plant fertilizer
CN106007972A (en) * 2016-05-24 2016-10-12 南宁圣特生物科技有限公司 Tea bran biofertilizer and preparation method thereof
CN106187436A (en) * 2016-07-01 2016-12-07 安徽万利生态园林景观有限公司 A kind of osmanthus fragrans foliage fertilizer additives and preparation method thereof
CN106045731A (en) * 2016-08-18 2016-10-26 广西鑫雅皇庭园林工程有限责任公司 Foliar fertilizer specially used for tea leaves and preparation method thereof
CN109197359A (en) * 2018-11-07 2019-01-15 常宁市瑶园生态农业科技发展有限公司 A kind of implantation methods of environmental protection tea

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Application publication date: 20151125