CN105110899A - Humic acid foliar fertilizer and preparation method therefor - Google Patents
Humic acid foliar fertilizer and preparation method therefor Download PDFInfo
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- CN105110899A CN105110899A CN201510470624.4A CN201510470624A CN105110899A CN 105110899 A CN105110899 A CN 105110899A CN 201510470624 A CN201510470624 A CN 201510470624A CN 105110899 A CN105110899 A CN 105110899A
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Abstract
The invention relates to a humic acid foliar fertilizer and a preparation method therefor. The humic acid foliar fertilizer is prepared from the following raw materials in parts by weight: biogas residues, peat soil, fish meal, chicken, duck and fish waste materials, dry pasture, soybean meal, an EM fungicide, saturated lime water, urea, potassum fulvic acid, ammonium molybdate, ammonium nitrate, trace elements, a precipitator and a proper amount of water. By making full use of household waste materials chicken, ducks and fishes, a liquid state fertilizer obtained by fermenting the household waste materials which are effectively prevented from becoming garbage to pollute the environment. By adding inorganic components such as trace elements, the loss of the trace elements can be reduced through adsorption. The utilization ratio of the trace elements can be further improved by virtue of priority of plants on utilization of fulvic acid.
Description
Technical field
The invention belongs to the Technology field of fertilizer, be specifically related to a kind of humic acid foliar nutrient and preparation method thereof.
Background technology
Liquid fermenting is one of modern biotechnology, it refers in biochemical reactor, natural imitation circle is by the oxygen of edible medicinal fungus in residue process required for necessary carbohydrate, organic and inorganic some trace elements of compound, inorganic salt etc. containing nitrogen and other thalline respiratory metabolism, and control suitable ambient conditions, carry out the prolific process of mycelia.The large-scale fermentation culture of industrialization is fermentative production, also known as deep drainpipe or reticent cultivation.Industrial fermentation is produced must adopt fermentor tank, and fermentation culture many employings triangular flask in laboratory.Contain thalline in the fermented liquid obtained, be decomposed and undecomposed nutritive ingredient, the meta-bolites that thalline produces.The direct hyoscine of fermented liquid or confession separation and Extraction, also can do liquid spawn.
The energy needed for the liquid of edible medicinal fungus can use cerelose, industrial starch and Rhizoma Dioscoreae powder etc.; Nitrogenous source can adopt soybean cake powder, dried silkworm chrysalis meal, bran powder etc.In order to reduce costs, usually also adopt part trade effluent to be surrogate, as soybean wastewater, raw material sources are extensive.The nutrition distribution pattern of liquid nutrient medium is even, is conducive to abundant contact and the absorption of mushroom nourishing body.Mycelia can grow, can discharge in time the metabolism waste gas of respiration generation inside and outside reactor under optimum temperuture, pH, oxygen and carbon-nitrogen ratio condition, therefore metabolic vigorous, mycelial growth division rapidly, the meta-bolites that a large amount of mycelium and polysaccharide, polypeptide etc. have physiologically active can be accumulated at short notice, cultivated by liquid state fermentation and obtain a large amount of mycelium and physiologically active substance and generally only need the time of 2 ~ 7 days and cell age is neat, and solid culture needs 30 ~ 50 days.Liquid strain can effectively reduce strain pollution rate, has flowing fast, easily disperses, a bacterium point is many, sprout the features such as fast, can effectively reduce the pollution of edible mushrooms in seeded process.
The product of microbial metabolism is broadly divided into two classes: primary metabolite and secondary metabolite, primary metabolite is that the breeding of microbe metabolism growth is necessary, can produce in whole life cycle more always, amino acid, Nucleotide, polysaccharide, lipid and VITAMIN etc. are produced in cell, and secondary metabolite microbiotic, alkaloid, bacteriotoxin and plant growth factor etc. that to be extracellular produce, of a great variety.
Summary of the invention
The present invention, in order to improve the quality of foliar nutrient, improves the utilization ratio of liquid fertilizer, and after inventing a kind of liquid state fermentation, the effective constituent extracted in fermented liquid makes a kind of high efficiency composition liquid fertilizer, and specific practice is as follows:
A kind of humic acid foliar nutrient, it is characterized in that, be made up of the raw material of following weight part: natural pond slag 10 ~ 15, peat soil 10 ~ 15, fishbone powder 5 ~ 10, chicken and duck fish dead meal 60 ~ 75, tame hay 30 ~ 40, soybean cake dregs 10 ~ 15, EM microbial inoculum 2 ~ 3, saturated limewater 10 ~ 15, manganous sulfate 4 ~ 5, ammonium molybdate 1 ~ 2, ammonium nitrate 8 ~ 15, trace element 2 ~ 3, precipitation agent 7 ~ 10 and appropriate water;
Described sinking agent is made up of the raw material of following weight part: lime powder 15 ~ 20,10% alum liquor 12 ~ 16,10% acetic acid solution 4 ~ 6, primary isoamyl alcohol 0.6 ~ 1.0, polyvinyl alcohol 6 ~ 8, tween 80 1.5 ~ 3, industrial Viscotrol C 2 ~ 4, ethanol 4 ~ 7 and water 50; The mixing of second alcohol and water is poured in reactor by preparation method, then polyvinyl alcohol is added, be heated to 70 ~ 80 DEG C of stirring and dissolving, then add 10% alum liquor, 10% acetic acid solution, primary isoamyl alcohol and lime powder, keep temperature of reaction kettle, adjustment rotating speed 150 ~ 200r/min stirs 20 ~ 35min, finally add tween 80 and industrial Viscotrol C simultaneously, insulated and stirred 30min is emulsion uniformly, obtains residue by funnel suction filtration, pulverizes to obtain pulvis sinking agent after oven dry.
A preparation method for humic acid foliar nutrient, is characterized in that, comprises following step:
(1) mix natural pond slag, peat soil, fishbone powder, chicken and duck fish dead meal, tame hay, soybean cake dregs, add the water of 10 ~ 15 times of its weight parts, ball milling 30 ~ 40min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) EM microbial inoculum is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH5.5 ~ 7, temperature 25 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 6 ~ 8 days;
(3) after (2) complete, fermented liquid is separately put in container, ultrasonic cell disruption instrument is utilized to carry out microbial disruption, with flowing water, container is lowered the temperature simultaneously, then precipitation agent mixing is added, then add saturated limewater, after stirring 8 ~ 10min, keep fermented liquid inertial motion, leave standstill 20 ~ 25min and carry out precipitation adsorption process voluntarily, after completing, supernatant liquor got by wooden dipper;
(4) mix manganous sulfate, ammonium molybdate, ammonium nitrate, trace element and other remaining component, be added in the supernatant liquor described in (3), stirring at room temperature 30 ~ 40min carries out composite absorption, after completing.
By alum, (main component is KAl (SO
4)
2gain enlightenment, its principle utilizes it in water, ionize out two metal ion species, and Al
3+be easy to hydrolysis, generate the aluminium hydroxide Al of colloid
3++ 3H
2o=Al (OH)
3+ 3H
+(reversible), the adsorptive power of alumine hydroxide colloid is strong, the impurity that can suspend in planar water, and form precipitation, make clarification of water, although successful, but the throw out after sedimentation is easily loose, be again diffused in water, the present invention not only will make the fermented liquid after fermentation clarify, also must possess make not allow composition granule composition to condense speed is fast, settling velocity fast, easily extract the features such as supernatant liquor after sedimentation, the present invention proposes sinking agent for this reason.
The operation instruction of sinking agent: adopt 10% alum liquor to be the main component of precipitation agent, the sedimentation effect reached is best, then 10% acetic acid is adopted to have certain promoter action as the separating effect of sedimentation medium to inorganic sinking agent, but the reaction of acetic acid and fermented liquid is comparatively slow, period, some fermented liquid was overflowed with the bubble of densification, so add primary isoamyl alcohol when preparing sinking agent as defoamer, adding the minimum lime powder of particle diameter is stablizer, secondly the weight of sorbent material is increased, avoid the sinking agent settling velocity of one-component slow, adding polyvinyl alcohol makes each ingredient adsorption of Tai-Ace S 150 and sedimentation promoter action on the surface of lime powder particle as binding agent, after all the components has adsorbed, finally adding a certain amount of vegetables oil can effectively prevent sinking agent particle to be mutually sticked together, become agglomerate, influence effect, particle aggregation agent after completing just can with an overall form storage, transport and use, successful.
The present invention adopts liquid state fermentation to ferment, first initial centrifugation, the oarse-grained particulate matter of filtering, ultrasonic cell disintegration instrument is utilized by remaining liq to carry out fragmentation to the microorganism in liquid, simultaneously in order to prevent heat production in process, cause temperature to raise and adopt flowing water stream to lower the temperature, by special sinking agent, adsorption precipitation is carried out to the residue in fermentation and unfermentable solid waste, obtain comparatively pure liquid extracting solution, some mineral substance that add that finally can be composite carry out function improvement and nutritional supplementation, it is reduce molecule to the impact of blade that pure extracting solution is used as foliar nutrient, the easy blocking blades pore of finely ground particles, affect respiration, next is unfavorable for prevention and elimination of disease and pests.
Intracellular organic matter can be discharged: the organic compositions such as amino acid, Nucleotide, nucleic acid, carbohydrate, make the nutritive ingredient of extracting solution abundanter while the meaning of microbial disruption is microorganism cells cracking.
Beneficial effect of the present invention: make full use of the dead meal chicken and duck fish in life, a kind of fertilizer of liquid state is become after fermentation, effectively prevent it from becoming rubbish and cause environmental pollution, adopt the mode of liquid state fermentation simultaneously, make the corpse of putrefying animal be transformed into humic acids composition, then add the inorganic componentss such as trace element, by absorption, the loss of trace element can be reduced, the utilization ratio of trace element can also be improved by plant to the priority that xanthohumic acid utilizes.
Embodiment
Embodiment 1:
A kind of humic acid foliar nutrient, it is characterized in that, be made up of the raw material of following weight part (Kg): natural pond slag 12, peat soil 12, fishbone powder 6, chicken and duck fish dead meal 70, tame hay 32, soybean cake dregs 12, EM microbial inoculum 2, saturated limewater 14, manganous sulfate 5, ammonium molybdate 1, ammonium nitrate 8, trace element 2, precipitation agent 8 and appropriate water;
Described sinking agent is made up of the raw material of following weight part: lime powder 17,10% alum liquor 15,10% acetic acid solution 5, primary isoamyl alcohol 0.9, polyvinyl alcohol 7, tween 80 2.2, industrial Viscotrol C 4, ethanol 4 ~ 7 and water 50; The mixing of second alcohol and water is poured in reactor by preparation method, then polyvinyl alcohol is added, be heated to 70 ~ 80 DEG C of stirring and dissolving, then add 10% alum liquor, 10% acetic acid solution, primary isoamyl alcohol and lime powder, keep temperature of reaction kettle, adjustment rotating speed 150 ~ 200r/min stirs 20 ~ 35min, finally add tween 80 and industrial Viscotrol C simultaneously, insulated and stirred 30min is emulsion uniformly, obtains residue by funnel suction filtration, pulverizes to obtain pulvis sinking agent after oven dry.
A preparation method for humic acid foliar nutrient, is characterized in that, comprises following step:
(1) mix natural pond slag, peat soil, fishbone powder, chicken and duck fish dead meal, tame hay, soybean cake dregs, add the water of 10 ~ 15 times of its weight parts, ball milling 30 ~ 40min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) EM microbial inoculum is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH5.5 ~ 7, temperature 25 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 6 ~ 8 days;
(3) after (2) complete, fermented liquid is separately put in container, ultrasonic cell disruption instrument is utilized to carry out microbial disruption, with flowing water, container is lowered the temperature simultaneously, then precipitation agent mixing is added, then add saturated limewater, after stirring 8 ~ 10min, keep fermented liquid inertial motion, leave standstill 20 ~ 25min and carry out precipitation adsorption process voluntarily, after completing, supernatant liquor got by wooden dipper;
(4) mix manganous sulfate, ammonium molybdate, ammonium nitrate, trace element and other remaining component, be added in the supernatant liquor described in (3), stirring at room temperature 30 ~ 40min carries out composite absorption, after completing.
A kind of humic acid foliar nutrient of the present invention is used for the fertilizer of manufacturing soybean, select 5 mu of Soybean Fields as experimental group, fertilizer of the present invention is sprayed once at the growth animated period of soybean, every mu of 50 ~ 70Kg, 5 mu of soybean of control group use common fertilizer replace or be left intact, the control of other curing conditions and disease and pest is all identical, result shows the soybean of experimental group, its color and luster and dense degree are all better than control group, anti-adversity improves, reduce incidence that is dead and disease and pest, compare economic raising 19.7%.
Claims (2)
1. a humic acid foliar nutrient, it is characterized in that, be made up of the raw material of following weight part: natural pond slag 10 ~ 15, peat soil 10 ~ 15, fishbone powder 5 ~ 10, chicken and duck fish dead meal 60 ~ 75, tame hay 30 ~ 40, soybean cake dregs 10 ~ 15, EM microbial inoculum 2 ~ 3, saturated limewater 10 ~ 15, manganous sulfate 4 ~ 5, ammonium molybdate 1 ~ 2, ammonium nitrate 8 ~ 15, trace element 2 ~ 3, precipitation agent 7 ~ 10 and appropriate water;
Described sinking agent is made up of the raw material of following weight part: lime powder 15 ~ 20,10% alum liquor 12 ~ 16,10% acetic acid solution 4 ~ 6, primary isoamyl alcohol 0.6 ~ 1.0, polyvinyl alcohol 6 ~ 8, tween 80 1.5 ~ 3, industrial Viscotrol C 2 ~ 4, ethanol 4 ~ 7 and water 50; The mixing of second alcohol and water is poured in reactor by preparation method, then polyvinyl alcohol is added, be heated to 70 ~ 80 DEG C of stirring and dissolving, then add 10% alum liquor, 10% acetic acid solution, primary isoamyl alcohol and lime powder, keep temperature of reaction kettle, adjustment rotating speed 150 ~ 200r/min stirs 20 ~ 35min, finally add tween 80 and industrial Viscotrol C simultaneously, insulated and stirred 30min is emulsion uniformly, obtains residue by funnel suction filtration, pulverizes to obtain pulvis sinking agent after oven dry.
2. the preparation method of a kind of humic acid foliar nutrient according to claim 1, is characterized in that, comprise following step:
(1) mix natural pond slag, peat soil, fishbone powder, chicken and duck fish dead meal, tame hay, soybean cake dregs, add the water of 10 ~ 15 times of its weight parts, ball milling 30 ~ 40min, to homogenate, pours in fermentor tank, carries out high-temperature sterilization process;
(2) EM microbial inoculum is added the water dilution of 5 times of its weight parts, be modulated into bacterium liquid, be then seeded in the fermentor tank of (1), adjustment pH5.5 ~ 7, temperature 25 ~ 28 DEG C, passes into sterile air simultaneously and stirs, and ferments 6 ~ 8 days;
(3) after (2) complete, fermented liquid is separately put in container, ultrasonic cell disruption instrument is utilized to carry out microbial disruption, with flowing water, container is lowered the temperature simultaneously, then precipitation agent mixing is added, then add saturated limewater, after stirring 8 ~ 10min, keep fermented liquid inertial motion, leave standstill 20 ~ 25min and carry out precipitation adsorption process voluntarily, after completing, supernatant liquor got by wooden dipper;
(4) mix manganous sulfate, ammonium molybdate, ammonium nitrate, trace element and other remaining component, be added in the supernatant liquor described in (3), stirring at room temperature 30 ~ 40min carries out composite absorption, after completing.
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| CN201510470624.4A CN105110899A (en) | 2015-08-05 | 2015-08-05 | Humic acid foliar fertilizer and preparation method therefor |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105418273A (en) * | 2015-12-25 | 2016-03-23 | 常州大学 | Preparation and application of rice straw biomass carbon-base release fertilizer |
| CN105669322A (en) * | 2016-01-13 | 2016-06-15 | 临沂市林业科技开发服务中心 | Foliar fertilizer used for salix integra and preparation method thereof |
| CN106116928A (en) * | 2016-07-01 | 2016-11-16 | 安徽万利生态园林景观有限公司 | A kind of pear tree foliar fertilizer promotees effect additive and preparation method thereof |
| CN106699473A (en) * | 2017-02-22 | 2017-05-24 | 广州聚禅现代农业研究院有限公司 | Kitchen waste recycling produced microorganism fertilizer with nitrogen fixation and phosphate and potassium dissolving effects |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1343644A (en) * | 2000-09-15 | 2002-04-10 | 长春聚隆微生物制剂有限责任公司 | Active spray fertilizer |
| US6475258B1 (en) * | 1998-09-09 | 2002-11-05 | Thomas T. Yamashita | Foliar fertilizer and method for using the same |
| CN104045443A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | Foliar fertilizer |
| CN104177195A (en) * | 2014-09-11 | 2014-12-03 | 标优美生态工程股份有限公司 | Special fertilizer for foliage spraying type flowers and preparation method thereof |
-
2015
- 2015-08-05 CN CN201510470624.4A patent/CN105110899A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6475258B1 (en) * | 1998-09-09 | 2002-11-05 | Thomas T. Yamashita | Foliar fertilizer and method for using the same |
| CN1343644A (en) * | 2000-09-15 | 2002-04-10 | 长春聚隆微生物制剂有限责任公司 | Active spray fertilizer |
| CN104045443A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | Foliar fertilizer |
| CN104177195A (en) * | 2014-09-11 | 2014-12-03 | 标优美生态工程股份有限公司 | Special fertilizer for foliage spraying type flowers and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105418273A (en) * | 2015-12-25 | 2016-03-23 | 常州大学 | Preparation and application of rice straw biomass carbon-base release fertilizer |
| CN105669322A (en) * | 2016-01-13 | 2016-06-15 | 临沂市林业科技开发服务中心 | Foliar fertilizer used for salix integra and preparation method thereof |
| CN106116928A (en) * | 2016-07-01 | 2016-11-16 | 安徽万利生态园林景观有限公司 | A kind of pear tree foliar fertilizer promotees effect additive and preparation method thereof |
| CN106699473A (en) * | 2017-02-22 | 2017-05-24 | 广州聚禅现代农业研究院有限公司 | Kitchen waste recycling produced microorganism fertilizer with nitrogen fixation and phosphate and potassium dissolving effects |
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Application publication date: 20151202 |