CN105056570B - The system of rapid extraction flavone from Rhododendron simsii Planch. leaf - Google Patents
The system of rapid extraction flavone from Rhododendron simsii Planch. leaf Download PDFInfo
- Publication number
- CN105056570B CN105056570B CN201510426874.8A CN201510426874A CN105056570B CN 105056570 B CN105056570 B CN 105056570B CN 201510426874 A CN201510426874 A CN 201510426874A CN 105056570 B CN105056570 B CN 105056570B
- Authority
- CN
- China
- Prior art keywords
- extraction
- flavone
- heat exchanger
- leaf
- outlet
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000000605 extraction Methods 0.000 title claims abstract description 92
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 title claims abstract description 29
- 229930003944 flavone Natural products 0.000 title claims abstract description 29
- 150000002212 flavone derivatives Chemical class 0.000 title claims abstract description 29
- 235000011949 flavones Nutrition 0.000 title claims abstract description 29
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 244000083724 Rhododendron simsii Species 0.000 title claims abstract description 16
- 238000003860 storage Methods 0.000 claims abstract description 18
- 239000003480 eluent Substances 0.000 claims abstract description 16
- 239000012530 fluid Substances 0.000 claims abstract description 15
- 241000196324 Embryophyta Species 0.000 claims abstract description 12
- 239000000706 filtrate Substances 0.000 claims abstract description 9
- 238000004108 freeze drying Methods 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 8
- 239000011347 resin Substances 0.000 claims abstract description 7
- 229920005989 resin Polymers 0.000 claims abstract description 7
- 230000008676 import Effects 0.000 claims abstract description 4
- 239000000463 material Substances 0.000 claims description 26
- 230000007246 mechanism Effects 0.000 claims description 24
- 239000000284 extract Substances 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 5
- 230000005484 gravity Effects 0.000 claims description 4
- 238000013507 mapping Methods 0.000 claims description 4
- 238000002604 ultrasonography Methods 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 238000004821 distillation Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 230000006837 decompression Effects 0.000 abstract description 4
- 238000009413 insulation Methods 0.000 abstract description 3
- 239000003795 chemical substances by application Substances 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 238000007599 discharging Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000007789 sealing Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- 241000208422 Rhododendron Species 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- BGOFCVIGEYGEOF-UJPOAAIJSA-N helicin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=CC=C1C=O BGOFCVIGEYGEOF-UJPOAAIJSA-N 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
- C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
- C07D311/28—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only
- C07D311/30—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3 with aromatic rings attached in position 2 only not hydrogenated in the hetero ring, e.g. flavones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/22—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4
- C07D311/26—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring with oxygen or sulfur atoms directly attached in position 4 with aromatic rings attached in position 2 or 3
- C07D311/40—Separation, e.g. from natural material; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C07H1/08—Separation; Purification from natural products
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H17/00—Compounds containing heterocyclic radicals directly attached to hetero atoms of saccharide radicals
- C07H17/04—Heterocyclic radicals containing only oxygen as ring hetero atoms
- C07H17/06—Benzopyran radicals
- C07H17/065—Benzo[b]pyrans
- C07H17/07—Benzo[b]pyran-4-ones
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The present invention relates to a kind of system of rapid extraction flavone from Rhododendron simsii Planch. leaf, including first set gradually, two extraction elements, first, two defecators, extracting solution storage tank, resin bed, eluent storage tank, vacuum concentration equipment, freeze drying plant and heat exchanger, it is provided with heat exchanger tube in eluent storage tank, the entrance of heat exchanger tube is connected with the concentrated solution outlet of vacuum concentration equipment, the outlet of heat exchanger tube is connected with freeze drying plant, exchanger heat fluid intake is connected with the gas outlet of vacuum concentration equipment, the filtrate (liquid of heat exchanger cold fluid inlet and the second defecator is connected, heat exchanger is cold, the outlet of hot fluid and first, the extractant import of two extraction elements is connected.In technique scheme, the heat energy of steam in vacuum concentration equipment is recycled, extracting solution and extractant are preheated, it is achieved the insulation/preheating before extracting solution decompression distillation and heating extraction agent, thus save the energy, reduce production cost.
Description
Technical field
The present invention relates to Rhododendron simsii Planch. extracting flavonoids field, be specifically related to a kind of quick from Rhododendron simsii Planch. leaf
Extract the system of flavone.
Background technology
Extract field in natural activity component, often need to use extraction element to the root of natural plants,
Stem, leaf, flower extract so that herbaceous plant root, stem, leaf, spend in active component dissolve
In extractant, thus realize the extraction to active component.The extraction pot of existing use exists mostly
Material add the problem loaded down with trivial details and time-consuming with discharging, have a strong impact on the production of natural activity component
Efficiency.It addition, for the extraction of natural activity component, all there is optimal material ratio (this thing
Extraction ratio and/or the extraction efficiency of the lower active component of material are maximum), but the difficulty that feeds intake of tradition extraction pot
To control material ratio accurately so that extraction ratio and/or extraction efficiency are unable to reach most preferably, seriously
Affect production efficiency and cause wastage of material.
It addition, currently used active component extraction equipment generally to there is extraction ratio low, utilization of energy
The problems such as rate is low, extracting cycle length.
Summary of the invention
It is an object of the invention to provide a kind of system of rapid extraction flavone from Rhododendron simsii Planch. leaf, its
The rapid extraction of mapping mountain reddish yellow ketone can be realized, and in extracting solution, the concentration of flavone is high, it is simple to be follow-up
Concentrating and purifying process and save the energy.
For achieving the above object, present invention employs techniques below scheme:
A kind of system of rapid extraction flavone from Rhododendron simsii Planch. leaf, it is characterised in that: include setting successively
The mapping mountain red autumnal leaves put carry out first and second extraction element of firsts and seconds extraction, to first and second
Material in extraction element carries out first and second defecator of solid-liquid separation respectively, for collection
The extracting solution storage tank of the filtrate that one defecator filters, the resin that flavone in extracting solution is adsorbed
Bed, the eluent storage tank that is collected of eluent after the flavone of resin bed absorption is carried out eluting,
The vacuum concentration equipment that eluent is concentrated, and the extracting solution after concentrating is dried system
The freeze drying plant of powder, is provided with heat exchanger between vacuum concentration equipment and the first extraction element,
Being provided with heat exchanger tube in eluent storage tank, the entrance of heat exchanger tube goes out with the concentrated solution of vacuum concentration equipment
Mouthful being connected, the outlet of heat exchanger tube is connected with freeze drying plant, exchanger heat fluid intake and
The gas outlet of vacuum concentration equipment is connected, and heat exchanger cold fluid inlet goes out with extractant storage tank
Mouth is connected and the filtrate (liquid of the second defecator is connected, going out of heat exchanger cold and hot fluid
Mouth is connected with the extractant import of first and second extraction element, and first and second extraction element includes carrying
Take tank and horizontally disposed shaft, be respectively arranged with in the middle part of the lateral wall, both sides that extraction pot is relative
Mounting seat, shaft two ends are rotatably installed in mounting seat, and shaft and the 3rd drive mechanism are connected
Connecing, shaft is positioned on the axle body of extraction pot and is provided with rabbling mechanism, and the top of extraction pot is arranged
There is the first adjusting part that dog-house and the closure state to dog-house are adjusted, extraction pot
The second adjusting part that bottom is provided with discharge port and the closure state to discharge port is adjusted,
First adjusting part includes the slide rail that the grooved part of opening upwards is constituted, the sky that grooved part bottom land is offered
The portion of lacking constitutes dog-house, and slide rail is arranged in the horizontal direction, and slide rail is provided with slide block, slide block and cunning
Rail constitutes slide-and-guide connection cooperation, the bottom surface of slide block and the groove of grooved part along the length direction of slide rail
The end, fits, and slide block is provided with the handing-over of the hopper that vertical shape is arranged, slide block and feed hopper bottom material mouth
Place offers into opening shape, slide block and the first drive mechanism and is connected.
Further scheme is: being provided with ultrasound emission assembly in extraction pot, extraction pot is arranged on machine
On frame, frame includes the spike that four vertical shapes are arranged, the bottom of a spike is provided with gravity sensitive
Device.Rabbling mechanism is included in the spaced puddler of zigzag shape, paddle on shaft axle body
It is arranged on the end of puddler, is articulated and connected for being articulated and connected and constituting between puddler and paddle
Axially the most axial with the shaft angle of jointed shaft be 30～60 °, paddle edge is away from puddler one
The plate face width degree that end points near puddler one end is gradually increased.It is provided with spiral shell on extraction pot internal face
The flow-interfering bar of spin line shape.
Detailed scheme is: slide block is that a strip plate is constituted, and the two ends of slide block are respectively arranged with
Hopper, the outside of two hoppers is respectively provided with material and adds mechanism.Second adjusting part includes a level
The flashboard arranged, flashboard and driving its feed screw nut's adjusting part moved in the horizontal direction or cylinder
Piston rod be connected.The sidewall of extraction pot is sandwich, and sandwich forms wall chamber, wall chamber
Entrance be connected with the gas outlet of vacuum concentration equipment, the outlet in wall chamber and exchanger heat fluid
Entrance is connected.
In technique scheme, the heat energy of steam in vacuum concentration equipment is recycled, right
Extracting solution and extractant preheat, it is achieved the insulation before extracting solution decompression distillation/preheat and heat
Extractant, thus save the energy, reduce production cost.Meanwhile, two-stage is used to extract, can be effective
Shorten extracting cycle, save the energy and improve the throughput rate of flavone.Obtain when extracting due to two grades
Extracting solution in flavone concentration relatively low, therefore will filter the filtrate after separating as extracting for the first time
Extractant, thus improve the concentration of flavone in extracting solution, it is simple to follow-up distillation and concentration processes.Separately
Outward, extraction element is moved by the first drive mechanism adjusting slider so that the sky on slide block
The portion of lacking is corresponding with the charge door on slide rail and different, thus realization to the rapid loading of extraction pot with
The Guan Bi of charge door, simultaneously when extracting, operator, can be by charging device to material
Bucket adds the inventory that next batch needs to add, so there is no need to complete to extract at extraction pot
After operation, weighing adds again, thus saves the time, improves extraction efficiency.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention；
Fig. 2 is the structural representation of first and second extraction element；
Fig. 3 is enlarged diagram at the A of Fig. 2；
Fig. 4 is the assembling schematic diagram of slide rail, slide block, hopper；
Fig. 5 is the upward view of the first stripper.
Detailed description of the invention
In order to make objects and advantages of the present invention clearer, below in conjunction with embodiment to this
Bright it is specifically described.Should be appreciated that following word is only in order to describe the one of the present invention or several
Planting specific embodiment, the protection domain of not concrete to present invention request carries out considered critical.
The technical scheme that the present invention takes is as it is shown in figure 1, one rapid extraction from Rhododendron simsii Planch. leaf is yellow
The system of ketone, carries out the first and second of firsts and seconds extraction including the mapping mountain red autumnal leaves set gradually
Extraction element A11, A12, carried out respectively to the material in first and second extraction element A11, A12
First and second defecator A21, A22 of solid-liquid separation, for collecting the first defecator A21 mistake
Extracting solution storage tank A3, the resin bed A8 adsorbing flavone in extracting solution of the filtrate of filter is right
The flavone of resin bed A8 absorption carry out eluting after the eluent storage tank A9 that is collected of eluent,
The vacuum concentration equipment A4 that eluent is concentrated, and the extracting solution after concentrating is dried
Set between the freeze drying plant A5 of powder process, vacuum concentration equipment A4 and the first extraction element A11
It is equipped with heat exchanger A6, is provided with heat exchanger tube in eluent storage tank A9, the entrance of heat exchanger tube and decompression
The concentrated solution outlet of enrichment facility A4 is connected, the outlet of heat exchanger tube and freeze drying plant A5 phase
Connecting, heat exchanger A6 thermal fluid inlet is connected with the gas outlet of vacuum concentration equipment A4, changes
Hot device A6 cold fluid inlet is connected and the second defecator with the outlet of extractant storage tank A7
The filtrate (liquid of A22 is connected, and the outlet of heat exchanger A6 cold and hot fluid extracts dress with first and second
The extractant import putting A11, A12 is connected.In technique scheme, to vacuum concentration equipment
The heat energy of middle steam recycles, and preheats extracting solution and extractant, it is achieved extracting solution
Insulation/preheating before decompression distillation and heating extraction agent, thus save the energy, reduce production cost.
Meanwhile, use two-stage to extract, can effectively shorten extracting cycle, save the energy and improve the life of flavone
Produce speed.Owing in two grades of extracting solution obtained when extracting, flavone concentration is relatively low, therefore by filtration point
Filtrate after from is as the extractant extracted for the first time, thus improves the concentration of flavone in extracting solution,
It is easy to follow-up distillation and concentration process.Defecator, vacuum concentration equipment, freeze drying plant,
Heat exchanger, resin bed, extracting solution storage tank all can use use in existing chemical industry to have corresponding function
Device use, eluent storage tank uses the transformation of general solution reservoir to obtain, in storage tank
Installing tubulation shape or spiral helicine heat exchanger tube, the solid material between neighboring devices uses conveyer belt defeated
Sending, liquid material uses pipeline and delivery pump conveying.
Extraction element A1 includes extraction pot 10 and horizontally disposed shaft 151, extraction pot 10
Being respectively arranged with mounting seat in the middle part of relative lateral wall, both sides, shaft 151 two ends are rotatably installed in
In mounting seat, shaft 151 is connected with the 3rd drive mechanism Q3, and shaft 151 is positioned at and carries
Take and on the axle body in tank 10, be provided with rabbling mechanism, the top of extraction pot 10 be provided with dog-house with
And the first adjusting part that the closure state of dog-house is adjusted, the bottom of extraction pot 10 sets
It is equipped with discharge port and the second adjusting part that the closure state to discharge port is adjusted, first,
Two adjusting parts can be that the horizontally disposed flashboard of extraction pot 10 top or bottom setting is constituted,
Flashboard can manually regulate, it is also possible to by flashboard and its screw mandrel moved in the horizontal direction of driving
The piston rod of nut adjusting part or cylinder is connected, and utilizes electric or pneumatic regulation.Need
Bright, in the present invention, for the ease of the scope that the present invention is claimed briefly, is clearly described,
Therefore, be not sealed into line description to existing on extraction pot 10 at extractant leakage, certainly this
Also it is the common knowledge understood of those of ordinary skill in the art and routine operation means.
In the present invention, it is preferred to use following scheme, as shown in Figure 2,4, the first adjusting part
The slide rail 12 constituted including the grooved part of opening upwards, the vacancy portion that grooved part bottom land is offered is constituted throws
Material mouth, slide rail 12 arranges in the horizontal direction, and slide rail 12 is provided with slide block 13, slide block 13 with
Slide rail 12 constitutes slide-and-guide connection cooperation, the bottom surface of slide block 13 along the length direction of slide rail 12
Fit with the bottom land of grooved part, slide block 13 is provided with the hopper 14 that vertical shape is arranged, slide block 13
With expect bottom hopper 14 that opening shape, slide block 13 and the first drive mechanism Q1 are offered in the junction of mouth
It is connected.Moved by the first drive mechanism adjusting slider 13 so that the sky on slide block 13
The portion of lacking is corresponding with the charge door on slide rail 12 and different, thus quick to extraction pot 10 of realization
Charging and the Guan Bi of charge door, simultaneously when extracting, operator, can be by feeding intake dress
Put in hopper 14, add the inventory that next batch needs to add, so there is no need to extracting
Tank 10 complete to extract operation after again weighing add, thus save the time, improve raw material extraction efficiency.
Preferably implementing according to scheme as shown in Figure 2,3, the second adjusting part includes extraction pot
The upper and lower first and second circular stripper 16,17 being arranged in parallel at 10 discharge ports, first unloads
Flitch 16 is fixed with one with extraction pot 10, and the side of the second stripper 17 offers annular
Groove, the second stripper 17 passes through the interior steel ball assembly 171 arranged of cannelure with extraction pot 10 around lead
Vertical direction constitutes the connection that is rotatably assorted, and the center of circle of first and second stripper 16,17 is positioned at same lead
On vertical line, first and second stripper is offered at the circumference of same radius size first and second respectively and unloads
Material mouth 16a, 17a, the lower face of the first stripper 16 be arranged to by first and second step surface 161,
It is step-like that 162 combinations are constituted, and second step face 162 is affixed with the upper face of the second stripper 17
Close, between First terrace 161 and the second stripper 17 upper face, form cavity, the first discharging
Mouth 16a is opened on First terrace 161, is provided with at the step that first and second step surface is joined
The step shape one of sealing member 163, the shape of sealing member 163 and first and second step surface junction
Causing, the second stripper 17 is connected with the second drive mechanism Q2, scheme the most as shown in Figure 5,
The outline of first and second step surface junction is arc, so sealing member is set to arc, close
Sealing can use O-ring seals.Regulate the second stripper 17 by the second drive mechanism Q2 to carry out
Rotate so that first and second discharge port on first and second stripper is corresponding and different, thus real
Now quickly discharging material and the Guan Bi of discharge port to extraction pot 10, it is achieved quickly discharging material, thus save
Time, improve extraction efficiency.
In the present invention, first, second and third drive mechanism can use electronic composition, and certain first drives machine
Structure also can use cylinder to constitute, and the 3rd drive mechanism may be used without arranging operating handle and manually adjusts
Joint, extraction pot 10 profile is cydariform or elliposoidal.
Further scheme is: be provided with ultrasound emission assembly or Microwave emission in extraction pot 10
Assembly, ultrasound emission assembly or Microwave emission assembly can improve the extraction effect of plant actives
Rate and extraction ratio, shorten the cycle and improve the utilization rate of raw material.Extraction pot 10 is arranged on frame 11
On, frame 11 includes the spike that four vertical shapes are arranged, the bottom of a spike is provided with gravity and passes
Sensor 111, gravity sensor 111 can measure the weight of whole extraction equipment and in real time by aobvious
Showing that device shows, such operator just can the most accurately learn the feeding quantity of each material, thus
Realize feeding intake according to optimal material ratio.Rabbling mechanism is included in spiral on shaft 151 axle body
The spaced puddler of wire 152, paddle 153 is arranged on the end of puddler 152, stirs
Mix between bar 152 and paddle 153 for be articulated and connected and constitute the jointed shaft that is articulated and connected axially with
The axial angle of shaft 151 is 30～60 °, and paddle 153 is along away from puddler 152 one end
Pointing to the plate face width degree near puddler 152 one end to be gradually increased, such rabbling mechanism can make
The stirring obtaining material is more abundant, can well protect rabbling mechanism simultaneously, prevents solid
Body material causes rabbling mechanism torsional deformation when tangling, and paddle 153 rotates on puddler 152
Angle is difficult to excessive, and the general angle rotated is 1～2 °.It is provided with on extraction pot 10 internal face
The flow-interfering bar of zigzag shape, arranging also for the adequacy realizing material stirring of flow-interfering bar.
Detailed scheme is: slide block 13 is that a strip plate is constituted, and the two ends of slide block 13 are respectively
Being provided with hopper 14, the outside of two hoppers 14 is respectively provided with material and adds mechanism, it is achieved multiple thing
Adding of material, the sidewall of extraction pot 10 is sandwich, and sandwich forms wall chamber, wall chamber
Entrance is connected with the gas outlet of vacuum concentration equipment, and the outlet in wall chamber enters with exchanger heat fluid
Mouth is connected.
In a word, the extraction system that the present invention provides, can effectively realize quickly adding and unloading of material,
Realize the high concentration rapid extraction of total Flavone of Rhododendron, improve the extraction efficiency of total Flavone of Rhododendron.
The above is only the preferred embodiment of the present invention, it is noted that for the art
Those of ordinary skill for, after knowing content described in the present invention, former without departing from the present invention
On the premise of reason, it is also possible to it is made some equal conversion and replacement, these convert on an equal basis and replace
In generation, also should be regarded as belonging to protection scope of the present invention.
Claims (8)
1. the system of rapid extraction flavone from Rhododendron simsii Planch. leaf, it is characterised in that: include depending on
The mapping mountain red autumnal leaves of secondary setting carry out first and second extraction element of firsts and seconds extraction, to first,
Material in two extraction elements carries out first and second defecator of solid-liquid separation respectively, is used for collecting
The extracting solution storage tank of the filtrate that the first defecator filters, the tree that flavone in extracting solution is adsorbed
Fat bed, to resin bed absorption flavone carry out eluting after eluent be collected eluent storage
Tank, the vacuum concentration equipment that eluent is concentrated, and the eluent after concentrating is done
The freeze drying plant of dry powder process, is provided with heat exchange between vacuum concentration equipment and the first extraction element
Device, is provided with heat exchanger tube in eluent storage tank, the entrance of heat exchanger tube and the concentration of vacuum concentration equipment
Liquid outlet is connected, and the outlet of heat exchanger tube is connected with freeze drying plant, and exchanger heat fluid enters
Mouth is connected with the gas outlet of vacuum concentration equipment, heat exchanger cold fluid inlet and extractant storage tank
Outlet be connected and the filtrate (liquid of the second defecator is connected, heat exchanger cold and hot fluid
Outlet be connected with the extractant import of first and second extraction element, first and second extraction element bag
Include extraction pot and horizontally disposed shaft, set respectively in the middle part of the lateral wall, both sides that extraction pot is relative
Being equipped with mounting seat, shaft two ends are rotatably installed in mounting seat, shaft and the 3rd drive mechanism
Being connected, shaft is positioned on the axle body of extraction pot and is provided with rabbling mechanism, the top of extraction pot
It is provided with dog-house and the first adjusting part that the closure state to dog-house is adjusted, extracts
The second regulation that the bottom of tank is provided with discharge port and the closure state to discharge port is adjusted
Assembly, the first adjusting part includes the slide rail that the grooved part of opening upwards is constituted, and grooved part bottom land is opened
If vacancy portion constitute dog-house, slide rail is arranged in the horizontal direction, and slide rail is provided with slide block, sliding
Block and slide rail constitute slide-and-guide along the length direction of slide rail and are connected cooperation, the bottom surface of slide block and grooved
The bottom land of part fits, and slide block is provided with the hopper that vertical shape is arranged, slide block and feed hopper bottom material mouth
Junction offer into opening shape, slide block and the first drive mechanism and be connected.
The system of rapid extraction flavone from Rhododendron simsii Planch. leaf the most according to claim 1, it is special
Levy and be: in extraction pot, be provided with ultrasound emission assembly.
The system of rapid extraction flavone from Rhododendron simsii Planch. leaf the most according to claim 1, it is special
Levying and be: extraction pot is arranged in frame, frame includes the spike that four vertical shapes are arranged, supports
The bottom of foot is provided with gravity sensor.
The system of rapid extraction flavone from Rhododendron simsii Planch. leaf the most according to claim 1, it is special
Levy and be: slide block is that a strip plate is constituted, and the two ends of slide block are respectively arranged with hopper, two material
The outside of bucket is respectively provided with material and adds mechanism.
The system of rapid extraction flavone from Rhododendron simsii Planch. leaf the most according to claim 1, it is special
Levy and be: the second adjusting part includes a horizontally disposed flashboard, flashboard with drive it along level side
It is connected to feed screw nut's adjusting part of movement or the piston rod of cylinder.
6. according to the rapid extraction from Rhododendron simsii Planch. leaf described in claim 1 or 2 or 3 or 4 or 5
The system of flavone, it is characterised in that: rabbling mechanism is included in zigzag shape interval on shaft axle body
The puddler arranged, paddle is arranged on the end of puddler, for hinge between puddler and paddle
The angle connect in succession and constitute the jointed shaft being articulated and connected the most axial with shaft is 30～60 °,
Paddle is gradually increased along the plate face width degree pointing to close puddler one end away from puddler one end.
The system of rapid extraction flavone from Rhododendron simsii Planch. leaf the most according to claim 6, it is special
Levy and be: on extraction pot internal face, be provided with the flow-interfering bar of zigzag shape.
The system of rapid extraction flavone from Rhododendron simsii Planch. leaf the most according to claim 6, it is special
Levy and be: the sidewall of extraction pot is sandwich, sandwich formed wall chamber, the entrance in wall chamber with
The gas outlet of vacuum concentration equipment is connected, and the outlet in wall chamber is connected with exchanger heat fluid intake
Connect.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610320994.4A CN105771313B (en) | 2014-08-10 | 2015-07-18 | A kind of azalea extracting flavonoids system |
| CN201510426874.8A CN105056570B (en) | 2014-08-10 | 2015-07-18 | The system of rapid extraction flavone from Rhododendron simsii Planch. leaf |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2014204486122 | 2014-08-10 | ||
| CN201420448612 | 2014-08-10 | ||
| CN201510426874.8A CN105056570B (en) | 2014-08-10 | 2015-07-18 | The system of rapid extraction flavone from Rhododendron simsii Planch. leaf |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610320994.4A Division CN105771313B (en) | 2014-08-10 | 2015-07-18 | A kind of azalea extracting flavonoids system |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105056570A CN105056570A (en) | 2015-11-18 |
| CN105056570B true CN105056570B (en) | 2016-12-07 |
Family
ID=54486213
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510426874.8A Active CN105056570B (en) | 2014-08-10 | 2015-07-18 | The system of rapid extraction flavone from Rhododendron simsii Planch. leaf |
| CN201610320994.4A Expired - Fee Related CN105771313B (en) | 2014-08-10 | 2015-07-18 | A kind of azalea extracting flavonoids system |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610320994.4A Expired - Fee Related CN105771313B (en) | 2014-08-10 | 2015-07-18 | A kind of azalea extracting flavonoids system |
Country Status (1)
| Country | Link |
|---|---|
| CN (2) | CN105056570B (en) |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2198016Y (en) * | 1994-07-26 | 1995-05-24 | 何晓东 | Dynamic multifunction extracting tank |
| CN1172808A (en) * | 1997-02-27 | 1998-02-11 | 罗海章 | Technology for combined preparation of starch, isoflavones and whole root beverage with root of kudzu vine |
| KR200187380Y1 (en) * | 1998-06-25 | 2000-07-01 | 이기동 | A power transmitting equipment of the centrifugal separating herbs extractor |
| CN1127507C (en) * | 1999-01-25 | 2003-11-12 | 南开大学 | Process for extracting natural flavonoid and/or terpene lactones from plant by adsorbent |
| CN1093416C (en) * | 1999-12-08 | 2002-10-30 | 中国科学院武汉植物研究所 | Plant Medicine for treating cardiovascular medicine and its preparing process |
| CN1422855A (en) * | 2001-12-03 | 2003-06-11 | 尹华清 | Industrialized production method of soybean isoflavone using soybean cake |
| CN1237896C (en) * | 2003-07-18 | 2006-01-25 | 华南理工大学 | Method for producing base material of soybean isoflavone with sugariness taste |
| CN1473822A (en) * | 2003-08-05 | 2004-02-11 | 西安翠宝首饰集团公司 | Extracting process of flavone and poly saccharide in duckweed |
| CN1927857A (en) * | 2006-09-25 | 2007-03-14 | 奈曼旗国有资产发展投资经营公司 | Extraction and purification process of buckwheat sprout total flavone |
| CL2010000003A1 (en) * | 2010-01-04 | 2010-04-16 | Natural Response S A | Apparatus for extracting active ingredients from natural sources, comprising a housing that encloses and supports a first transport screw, an input hopper with a second screw, an output hopper, a liquid extract discharge line and an acoustic transduction system , and a method for extraction. |
| US8668879B2 (en) * | 2010-03-31 | 2014-03-11 | Desmet Ballestra North America, Inc. | Low layer solvent extractor |
| CN202777910U (en) * | 2012-08-08 | 2013-03-13 | 天津必佳药业集团有限公司 | Multi-pressure regulating valve type traditional Chinese medicine extraction tank |
-
2015
- 2015-07-18 CN CN201510426874.8A patent/CN105056570B/en active Active
- 2015-07-18 CN CN201610320994.4A patent/CN105771313B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN105771313B (en) | 2017-11-24 |
| CN105771313A (en) | 2016-07-20 |
| CN105056570A (en) | 2015-11-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104922930B (en) | Two grades of extraction equipments of Rhododendron simsii Planch. | |
| CN104974549B (en) | For extracting the equipment of natural plant pigment | |
| CN105056570B (en) | The system of rapid extraction flavone from Rhododendron simsii Planch. leaf | |
| CN104971514B (en) | For extracting the equipment of total Flavone of Rhododendron | |
| CN104174183B (en) | The system of flavones is extracted from plant stem-leaf | |
| CN105062124B (en) | System for rapidly extracting pigments from rhododendron simsii planch flowers | |
| CN105062122B (en) | The equipment of rapid extraction natural pigment from plant flower | |
| CN105061379B (en) | The equipment of rapid extraction plant flavone | |
| CN104162289B (en) | The equipment of rapid extraction total Flavone of Rhododendron | |
| CN105062123B (en) | Equipment for quickly extracting azalea pigment | |
| CN105001667B (en) | The system of rapid extraction natural plant pigment | |
| CN105130937B (en) | Equipment for extracting plant flavone | |
| CN106317947A (en) | Energy-saving device for extracting plant pigments | |
| CN105038302B (en) | Device for extracting rhododendron pigment | |
| CN104983776A (en) | Energy-saving equipment for extracting rhododendron general flavone | |
| CN105062121B (en) | Energy-saving equipment for extracting pigments of rhododendron simsii | |
| CN104971515B (en) | Two grades of extraction equipments of plant actives | |
| CN105170044B (en) | The equipment of energy-saving extraction plant flavone |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Li Tinghui Inventor before: Hu Liuman |
|
| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160822 Address after: 350208, No. 187, crane Town Road, Changle, Fujian, Fuzhou Applicant after: Li Tinghui Address before: 246002 Anhui province Anqing City Daguan District Jixian Road No. 148 Applicant before: Hu Liuman |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Sha Chenguang Inventor before: Li Tinghui |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170901 Address after: 161100, Heilongjiang Province, Longjiang County, Longjiang Town, Qigihar Labor Street, a commission of 6 groups Patentee after: Sha Chenguang Address before: 350208, No. 187, crane Town Road, Changle, Fujian, Fuzhou Patentee before: Li Tinghui |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180920 Address after: 313000 2599 Hu Jie Avenue, Huzhou, Zhejiang Patentee after: ZHEJIANG DADONGWU GROUP CONSTRUCTION OF THE NEW MATERIAL LTD. Address before: 161100 group 6, labor Street, Longjiang Town, Longjiang, Qigihar, Heilongjiang. Patentee before: Sha Chenguang |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20201117 Address after: 1-16, Wanfu Street North, No.7, SUDI North Road, Quanshan District, Xuzhou City, Jiangsu Province, 221000 Patentee after: Xuzhou xinlaide Electronic Technology Co.,Ltd. Address before: 313000 No. 2599 weaving Avenue, Huzhou City, Zhejiang Province Patentee before: ZHEJIANG DADONGWU GROUP CONSTRUCTION OF THE NEW MATERIAL Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20231120 Address after: 815, 8th Floor, Building 1, No. 198 Changcui Road, Changping District, Beijing, 102200 Patentee after: Good health technology (Beijing) Co.,Ltd. Address before: 221000 1-16, Wanfu Street North, No. 7, SUDI North Road, Quanshan District, Xuzhou City, Jiangsu Province Patentee before: Xuzhou xinlaide Electronic Technology Co.,Ltd. |