CN104971515B - Two grades of extraction equipments of plant actives - Google Patents

Two grades of extraction equipments of plant actives Download PDF

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Publication number
CN104971515B
CN104971515B CN201510428905.3A CN201510428905A CN104971515B CN 104971515 B CN104971515 B CN 104971515B CN 201510428905 A CN201510428905 A CN 201510428905A CN 104971515 B CN104971515 B CN 104971515B
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Prior art keywords
extractor
stripper
grades
extraction
shaft
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CN201510428905.3A
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CN104971515A (en
Inventor
曹明光
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Anhui Shenjian Grain Machinery Equipment Co ltd
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ANHUI SHENJIAN CHEMICAL MEDICINE EQUIPMENT Co Ltd
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Priority to CN201510428905.3A priority Critical patent/CN104971515B/en
Priority to CN201610307349.9A priority patent/CN105920870B/en
Publication of CN104971515A publication Critical patent/CN104971515A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0253Fluidised bed of solid materials
    • B01D11/0257Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0261Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
    • B01D11/0265Applying ultrasound

Abstract

The present invention relates to a kind of two grades of extraction equipments of plant actives, including first and second leaching device successively plant extracted and first and second filter that respectively material in first and second leaching device after extracting is carried out separation of solid and liquid, the liquid outlet of the first filter is connected with extract storage tank, and the liquid outlet of the second filter and the extractant import of the first leaching device are connected.Leaves of plants/flower is extracted in first and second leaching device by such scheme respectively, owing in the extract that leaves of plants/flower obtains when second time is extracted, pigment/flavones concentration is relatively low, therefore the filtrate after separating will be filtered as the extractant extracted for the first time, thus improve the concentration of pigment/flavones in extract, it is easy to follow-up distillation and concentration process, use two-stage to extract simultaneously, can effectively shorten extracting cycle, save the energy and improve the throughput rate of pigment/flavones.

Description

Two grades of extraction equipments of plant actives
Technical field
The present invention relates to active component and extract field, be specifically related to a kind of plant actives two grades leaching Carry equipment.
Background technology
Extract field in natural activity component, often need to use extraction element to the root of natural plants, Stem, leaf extract so that the active component in herbaceous plant root, stem, leaf is dissolved in extractant In, thus realize the extraction to active component.Mostly there is the throwing of material in the extractor of existing use Add the problem loaded down with trivial details and time-consuming with discharging, have a strong impact on the production efficiency of natural activity component.Separately Outward, for the extraction of natural activity component, all there is an optimal material ratio (active under this material The recovery rate of component and/or extraction efficiency are maximum), but feeding intake of extractor of tradition is difficult to accurately Control material ratio so that recovery rate and/or extraction efficiency are unable to reach most preferably, have a strong impact on production Efficiency and cause wastage of material.
Summary of the invention
It is an object of the invention to provide a kind of two grades of extraction equipments of plant actives, it can realize Rapid extraction to plant actives, and in extract, the concentration of active component is high, it is simple to follow-up Concentrating and purifying process and save the energy.
For achieving the above object, present invention employs techniques below scheme:
A kind of two grades of extraction equipments of plant actives, it is characterised in that: include successively plant being entered Row firsts and seconds extract first and second leaching device and respectively to extract after first and second extraction Material in device carries out first and second filter of separation of solid and liquid, the first filter go out liquid Mouth is connected with extract storage tank, the liquid outlet of the second filter and the extraction of the first leaching device Agent import is connected, and first and second leaching device includes extractor and horizontally disposed shaft, Being respectively arranged with mounting seat in the middle part of the both sides lateral wall that extractor is relative, shaft two ends rotate installs In mounting seat, shaft and the 3rd drive mechanism are connected, and shaft is positioned at the axle of extractor Being provided with rabbling mechanism with it, the top of extractor is provided with dog-house and the Guan Bi to dog-house The first adjusting part that state is adjusted, the bottom of extractor is provided with discharge port and to discharging The second adjusting part that the closure state of mouth is adjusted, the second adjusting part includes extractor discharging The upper and lower first and second circular stripper being arranged in parallel at Kou, the first stripper is solid with extractor Being connected as a single entity, the side of the second stripper offers cannelure, the second stripper passes through cannelure The steel ball assembly of interior setting and extractor constitute to be rotatably assorted around vertical and are connected, and first and second unloads The center of circle of flitch is positioned on same plumb line, the circumference of same radius size on first and second stripper Place offers first and second discharge port respectively, and the lower face of the first stripper is arranged to by first and second It is step-like that terrace combination is constituted, and second step face fits with the upper face of the second stripper, the Forming cavity between one step surface and the second stripper upper face, the first discharge port is opened in First On terrace, at the step that first and second step surface is joined, be provided with seal, the shape of seal with The step shape of first and second step surface junction is consistent, the second stripper and the second drive mechanism phase Connect.
Further scheme is: being provided with Microwave emission assembly in extractor, extractor is arranged on machine On frame, frame includes the spike that four vertical shapes are arranged, the bottom of a spike is provided with gravity sensitive Device.Rabbling mechanism is included in the spaced puddler of zigzag shape, paddle on shaft axle body It is arranged on the end of puddler, is articulated and connected for being articulated and connected and constituting between puddler and paddle Axially the most axial with the shaft angle of jointed shaft be 30~60 °, paddle edge is away from puddler one The plate face width degree that end points near puddler one end is gradually increased.It is provided with spiral shell on extractor internal face The flow-interfering bar of spin line shape, the sidewall of extractor is sandwich.
In technique scheme, in first and second leaching device, respectively leaves of plants/flower is carried out one Level and two grades of extractions, due to pigment/Huang in the extract that leaves of plants/flower obtains when second time is extracted Ketone concentration is relatively low, therefore will filter the extractant as extraction for the first time of the filtrate after separating, thus Improve the concentration of pigment/flavones in extract, it is simple to follow-up distillation and concentration processes, and uses simultaneously Two-stage is extracted, and can effectively shorten extracting cycle, saves the energy and improves the production speed of pigment/flavones Rate.Rotate it addition, extraction element regulates the second stripper by the second drive mechanism, make Obtain first and second discharge port on first and second stripper corresponding and different, thus realize extraction The quickly discharging material of tank and the Guan Bi of discharge port, thus save the time, improve extracting efficiency.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention;
Fig. 2 is the structural representation of first and second extraction element;
Fig. 3 is enlarged diagram at the A of Fig. 2;
Fig. 4 is the assembling schematic diagram of slide rail, slide block, hopper;
Fig. 5 is the upward view of the first stripper.
Detailed description of the invention
In order to make objects and advantages of the present invention clearer, below in conjunction with embodiment to this Bright it is specifically described.Should be appreciated that following word is only in order to describe the one of the present invention or several Planting specific embodiment, the protection domain of not concrete to present invention request carries out considered critical.
The technical scheme that the present invention takes is as it is shown in figure 1, include successively plant being carried out one-level and two Level extract first and second leaching device A1, A2 and respectively to extract after first and second extraction dress Put the material in A1, A2 and carry out first and second filter A3, A4 of separation of solid and liquid, the first mistake The liquid outlet of filter device A3 is connected with extract storage tank A5, and the second filter A4 goes out liquid Mouth is connected with the extractant import of the first leaching device A1.In technique scheme, first, Respectively leaves of plants/flower is extracted in two leaching devices, owing to leaves of plants/flower extracts in second time Time obtain extract in pigment/flavones concentration relatively low, therefore using filter separate after filtrate as The extractant extracted for the first time, thus improve the concentration of pigment/flavones in extract, it is simple to follow-up Distillation and concentration process, use two-stage to extract simultaneously, can effectively shorten extracting cycle, save the energy With the throughput rate improving pigment/flavones.Filter can use general equipment for separating liquid from solid, Solid material between neighboring devices uses tape transport, and liquid material uses pipeline and delivery pump defeated Send.
First and second extraction element A1, A2 includes extractor 10 and horizontally disposed shaft 151, Mounting seat, shaft 151 two ends it are respectively arranged with in the middle part of the both sides lateral wall that extractor 10 is relative Being rotatably installed in mounting seat, shaft 151 is connected with the 3rd drive mechanism Q3, shaft Being provided with rabbling mechanism on 151 axle bodies being positioned at extractor 10, the top of extractor 10 is arranged There are the first adjusting part that dog-house and the closure state to dog-house are adjusted, extractor 10 The second regulation group that bottom is provided with discharge port and the closure state to discharge port is adjusted Part, first and second adjusting part can be extractor 10 top or bottom arrange horizontally disposed Flashboard constitute, flashboard can manually regulate, it is also possible to by flashboard with drive its in the horizontal direction Feed screw nut's adjusting part of movement or the piston rod of cylinder are connected, and utilize electric or pneumatic tune Joint.It should be noted that in the present invention, for the ease of present invention request briefly, is clearly described The scope of protection, therefore, the sealing to existing on extractor 10 at extractant leakage is not carried out Describing, this is also the common knowledge understood of those of ordinary skill in the art and routine operation hand certainly Section.
In the present invention, it is preferred to use following scheme, as shown in Figure 2,4, the first adjusting part The slide rail 12 constituted including the grooved part of opening upwards, the vacancy portion that grooved part bottom land is offered is constituted throws Material mouth, slide rail 12 arranges in the horizontal direction, and slide rail 12 is provided with slide block 13, slide block 13 with Slide rail 12 constitutes slide-and-guide connection cooperation, the bottom surface of slide block 13 along the length direction of slide rail 12 Fit with the bottom land of grooved part, slide block 13 is provided with the hopper 14 that vertical shape is arranged, slide block 13 With expect bottom hopper 14 that opening shape, slide block 13 and the first drive mechanism Q1 are offered in the junction of mouth It is connected.Moved by the first drive mechanism adjusting slider 13 so that the sky on slide block 13 The portion of lacking is corresponding with the charge door on slide rail 12 and different, thus quick to extractor 10 of realization Charging and the Guan Bi of charge door, simultaneously when extracting, operating personnel, can be by feeding intake dress Put in hopper 14, add the inventory that next batch needs to add, so there is no need to extracting Tank 10 complete to extract operation after again weighing add, thus save the time, improve raw material extraction efficiency.
Preferably implementing according to scheme as shown in Figure 2,3, the second adjusting part includes extractor The upper and lower first and second circular stripper 16,17 being arranged in parallel at 10 discharge ports, first unloads Flitch 16 is fixed with one with extractor 10, and the side of the second stripper 17 offers annular Groove, the second stripper 17 passes through the interior steel ball assembly 18 arranged of cannelure with extractor 10 around lead Vertical direction constitutes the connection that is rotatably assorted, and the center of circle of first and second stripper 16,17 is positioned at same lead On vertical line, first and second stripper is offered at the circumference of same radius size first and second respectively and unloads Material mouth 16a, 17a, the lower face of the first stripper 16 be arranged to by first and second step surface 161, It is step-like that 162 combinations are constituted, and second step face 162 is affixed with the upper face of the second stripper 17 Close, between First terrace 161 and the second stripper 17 upper face, form cavity, the first discharging Mouth 16a is opened on First terrace 161, is provided with at the step that first and second step surface is joined The step shape one of seal 163, the shape of seal 163 and first and second step surface junction Causing, the second stripper 17 is connected with the second drive mechanism Q2, scheme the most as shown in Figure 5, The outline of first and second step surface junction is arc, so seal is set to arc, close Sealing can use O-ring seals.Regulate the second stripper 17 by the second drive mechanism Q2 to carry out Rotate so that first and second discharge port on first and second stripper is corresponding and different, thus real Now quickly discharging material and the Guan Bi of discharge port to extractor 10, thus save the time, improve and extract Efficiency.
In the present invention, first, second and third drive mechanism can use electronic composition, and certain first drives machine Structure also can use cylinder to constitute, and the 3rd drive mechanism may be used without arranging operating handle and manually adjusts Joint, extractor 10 profile is cydariform or elliposoidal.
Further scheme is: be provided with ultrasound emission assembly or Microwave emission in extractor 10 Assembly, ultrasound emission assembly or Microwave emission assembly can improve the extraction effect of plant actives Rate and recovery rate, shorten the cycle and improve the utilization rate of raw material.Extractor 10 is arranged on frame 11 On, frame 11 includes the spike 11 that four vertical shapes are arranged, the bottom of a spike 11 is provided with weight Force snesor 111, gravity sensor 111 can be measured the weight of whole extraction equipment in real time and lead to Crossing display to show, such operating personnel just can the most accurately learn the feeding quantity of each material, Thus realize feeding intake according to optimal material ratio.Rabbling mechanism is included on shaft 151 axle body The spaced puddler of zigzag shape 152, paddle 153 is arranged on the end of puddler 152, For being articulated and connected and to constitute the jointed shaft being articulated and connected axial between puddler 152 and paddle 153 The angle axial with shaft 151 is 30~60 °, and paddle 153 is along away from puddler 152 1 The plate face width degree that end points near puddler 152 one end is gradually increased, and such rabbling mechanism is permissible The stirring making material is more abundant, can well protect rabbling mechanism simultaneously, prevent Solid material causes rabbling mechanism torsional deformation when tangling, and paddle 153 turns on puddler 152 Dynamic angle is difficult to excessive, and the general angle rotated is 1~2 °.Arrange on extractor 10 internal face There is the flow-interfering bar of zigzag shape, arranging also for the adequacy realizing material stirring of flow-interfering bar.
Detailed scheme is: slide block 13 is that a strip plate is constituted, and the two ends of slide block 13 are respectively Being provided with hopper 14, the outside of two hoppers 14 is respectively provided with material and adds mechanism, it is achieved multiple thing Adding of material, the sidewall of extractor 10 is sandwich, and the folder chamber that sandwich is formed is used for holding Receive hot fluid, the material in extractor 10 is incubated or heats.
In a word, the present invention provide two grades of extraction equipments, can effectively realize material quickly add and Unloading, it is achieved the high concentration rapid extraction of phytochrome/flavones, improves carrying of phytochrome/flavones Take efficiency.It is natural that the present invention can be used for phytochrome, flavones, Tea Saponin, medicine activity component etc. The extraction of component.
The above is only the preferred embodiment of the present invention, it is noted that for the art Those of ordinary skill for, after knowing content described in the present invention, former without departing from the present invention On the premise of reason, it is also possible to it is made some equal conversion and replacement, these convert on an equal basis and replace In generation, also should be regarded as belonging to protection scope of the present invention.

Claims (6)

1. two grades of extraction equipments of a plant actives, it is characterised in that: include successively to planting Thing carries out first and second leaching device of firsts and seconds extraction and respectively to after extracting first and second Material in leaching device carries out first and second filter of separation of solid and liquid, the first filter Liquid outlet is connected with extract storage tank, the liquid outlet of the second filter and the first leaching device Extractant import is connected, and first and second leaching device includes extractor and horizontally disposed stirring Axle, is respectively arranged with mounting seat in the middle part of the both sides lateral wall that extractor is relative, shaft two ends rotate Being arranged in mounting seat, shaft is connected with drive mechanism B, and shaft is positioned at extractor Being provided with rabbling mechanism on axle body, the top of extractor is provided with dog-house and closes dog-house The first adjusting part that conjunction state is adjusted, the bottom of extractor is provided with discharge port and to unloading The second adjusting part that the closure state of material mouth is adjusted, the second adjusting part includes that extractor unloads The upper and lower first and second circular stripper being arranged in parallel, the first stripper and extractor at material mouth Being fixed with one, the side of the second stripper offers cannelure, the second stripper is by annular The steel ball assembly arranged in groove and extractor are rotatably assorted around vertical composition and are connected, and first and second The center of circle of stripper is positioned on same plumb line, the circle of same radius size on first and second stripper Offering first and second discharge port at Zhou respectively, the lower face of the first stripper is arranged to by first and second It is step-like that step surface combination is constituted, and second step face fits with the upper face of the second stripper, Forming cavity between First terrace and the second stripper upper face, the first discharge port is opened in first On step surface, at the step that first and second step surface is joined, it is provided with seal, the shape of seal Consistent with the step shape of first and second step surface junction, the second stripper and drive mechanism A phase Connect.
Two grades of extraction equipments of plant actives the most according to claim 1, it is characterised in that: Microwave emission assembly it is provided with in extractor.
Two grades of extraction equipments of plant actives the most according to claim 1, it is characterised in that: Extractor is arranged in frame, and frame includes the spike that four vertical shapes are arranged, the bottom of a spike It is provided with gravity sensor.
4. according to the two grades of extraction equipments of plant actives described in claim 1 or 2 or 3, its It is characterised by: rabbling mechanism is included in the spaced puddler of zigzag shape on shaft axle body, Paddle is arranged on the end of puddler, for being articulated and connected and constituting hinge between puddler and paddle The axial angle the most axial with shaft of the jointed shaft connect in succession is 30~60 °, and paddle is along away from stirring Mix the plate face width degree pointed near puddler one end bar one end to be gradually increased.
Two grades of extraction equipments of plant actives the most according to claim 4, it is characterised in that: The flow-interfering bar of zigzag shape it is provided with on extractor internal face.
Two grades of extraction equipments of plant actives the most according to claim 4, it is characterised in that: The sidewall of extractor is sandwich.
CN201510428905.3A 2014-08-10 2015-07-18 Two grades of extraction equipments of plant actives Active CN104971515B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201510428905.3A CN104971515B (en) 2014-08-10 2015-07-18 Two grades of extraction equipments of plant actives
CN201610307349.9A CN105920870B (en) 2014-08-10 2015-07-18 Two level extraction equipment applied to plant actives extraction

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Application Number Priority Date Filing Date Title
CN201420448656 2014-08-10
CN2014204486565 2014-08-10
CN201510428905.3A CN104971515B (en) 2014-08-10 2015-07-18 Two grades of extraction equipments of plant actives

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CN104971515B true CN104971515B (en) 2016-09-07

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CN104971515A (en) 2015-10-14
CN105920870B (en) 2017-11-10
CN105920870A (en) 2016-09-07

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