CN105038302B - Device for extracting rhododendron pigment - Google Patents

Device for extracting rhododendron pigment Download PDF

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Publication number
CN105038302B
CN105038302B CN201510426964.7A CN201510426964A CN105038302B CN 105038302 B CN105038302 B CN 105038302B CN 201510426964 A CN201510426964 A CN 201510426964A CN 105038302 B CN105038302 B CN 105038302B
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Prior art keywords
extraction
heat exchanger
extracting
slide block
extraction pot
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Application number
CN201510426964.7A
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Chinese (zh)
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CN105038302A (en
Inventor
董兰兰
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XUZHOU NAILI MACROMOLECULE TECHNOLOGY CO., LTD.
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Zhejiang Yicheng Industrial Product Design Co Ltd
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Priority to CN201610490540.1A priority Critical patent/CN105885470B/en
Priority to CN201510426964.7A priority patent/CN105038302B/en
Publication of CN105038302A publication Critical patent/CN105038302A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/10Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0096Purification; Precipitation; Filtration
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Abstract

The invention relates to a device for extracting rhododendron pigment. The device for extracting rhododendron pigment comprises an extracting device, a filtering device, an extracting solution storage tank, a reduced-pressure concentration device and a spray drying device which are arranged in sequence, wherein a heat exchanger is arranged between the reduced-pressure concentration device and the extracting device, a heat exchange tube is arranged in the extracting solution storage tank, an inlet of the heat exchange tube is connected with an air outlet of the reduced-pressure concentration device, an outlet of the heat exchange tube is connected with a thermal fluid inlet of the heat exchanger, a cold fluid inlet of the heat exchanger is connected with an outlet of an extractant storage tank, and a cold fluid outlet and a thermal fluid outlet of the heat exchanger are connected with an extractant inlet of the extracting device. In the technical scheme, heat energy of steam in the reduced-pressure concentration device is recycled, an extracting solution and an extractant are preheated to achieve heat preservation/preheating and heating of the extractant before reduced-pressure concentration of the extracting solution, accordingly energy is saved, and production cost is reduced.

Description

For extracting the equipment of Rhododendron simsii Planch. pigment
Technical field
The present invention relates to nature strength field is and in particular to one kind is used for extracting Rhododendron simsii Planch. pigment Equipment.
Background technology
Extract field in natural activity component, often need to using extraction element to the root of natural plants, Stem, leaf are extracted so that the active component in herbaceous plant root, stem, leaf is dissolved in extractant In, thus realizing the extraction to active component.Mostly there is the throwing of material in the extraction pot of existing use Plus and the loaded down with trivial details and time-consuming problem of discharging, have a strong impact on the production efficiency of natural activity component.Separately Outward, for the extraction of natural activity component, all there is an optimal material ratio (active under this material The extraction ratio of component and/or extraction efficiency are maximum), but feeding intake of traditional extraction pot is difficult to accurately Control material ratio, so that extraction ratio and/or extraction efficiency are unable to reach most preferably, has a strong impact on production Efficiency and cause wastage of material.
In addition, the current active component extraction equipment generally existing extraction ratio using is low, utilization of energy Rate is low, the problems such as extracting cycle is long.
Content of the invention
It is an object of the invention to provide a kind of equipment for extracting Rhododendron simsii Planch. pigment, it can achieve The rapid extraction of mapping mountain red pigment, and in extracting solution pigment concentration high, be easy to follow-up concentration Purification process and energy saving.
For achieving the above object, present invention employs technical scheme below:
A kind of equipment for extracting Rhododendron simsii Planch. pigment it is characterised in that:Right including set gradually The extraction element that the middle pigment of Rhododendron simsii Planch. is extracted, carries out solid-liquid to the material in extraction element and divides From defecator, for collect filter after filtrate extraction liquid storage tank, extracting solution is carried out dense The vacuum concentration equipment of contracting, and the extracting solution after concentrating is dried with the spray drying dress of powder processed Put, between vacuum concentration equipment and extraction element, be provided with heat exchanger, extract in liquid storage tank and be provided with Heat exchanger tube, the entrance of heat exchanger tube is connected with the gas outlet of vacuum concentration equipment, the going out of heat exchanger tube Mouth is connected with the hot fluid inlet of heat exchanger, and heat exchanger cold fluid inlet is gone out with extractant storage tank Mouth is connected, and the outlet of heat exchanger cold and hot fluid is connected with the extractant import of extraction element, Extraction element includes extraction pot and horizontally disposed shaft, the relative both sides lateral wall of extraction pot Middle part is respectively arranged with mounting seat, and shaft two ends are rotatably installed in mounting seat, shaft and the Three drive mechanisms are connected, and shaft is located at and is provided with rabbling mechanism on the axle body in extraction pot, carries The top taking tank is provided with the first tune that dog-house and the closure state to dog-house are adjusted Section assembly, the bottom of extraction pot is provided with discharge port and the closure state of discharge port is adjusted The second adjusting part, the first adjusting part include opening upwards grooved part constitute slide rail, groove The vacancy portion that type part bottom land opens up constitutes dog-house, and slide rail is arranged in the horizontal direction, and slide rail is arranged There is slide block, slide block is connected cooperation with slide rail along the length direction composition slide-and-guide of slide rail, slide block Bottom surface is fitted with the bottom land of grooved part, and slide block is provided with hopper, slide block and the material of vertical shape arrangement The junction of bucket bottom material mouth opens up into opening shape, and slide block is connected with the first drive mechanism.
Further scheme is:It is provided with ultrasound emission assembly, extraction pot is arranged on machine in extraction pot On frame, frame includes the support feet of four vertical shape arrangements, and the bottom of support feet is provided with gravity sensitive Device.Rabbling mechanism includes the spaced puddler of zigzag shape, paddle on shaft axle body It is arranged on the end of puddler, be to be articulated and connected and constitute to be articulated and connected between puddler and paddle Jointed shaft be axially 30~60 ° with the angle of shaft axial direction, paddle is along away from puddler one The plate face width that end is pointed near puddler one end is gradually increased.It is provided with spiral shell on extraction pot internal face The flow-interfering bar of spin line shape.
Detailed scheme is:Slide block is that a strip plate is constituted, and the two ends of slide block are respectively arranged with Hopper, the outside of two hoppers is respectively provided with material and adds mechanism.Second adjusting part includes a level The flashboard of arrangement, flashboard and the feed screw nut's adjusting part driving it to move in the horizontal direction or cylinder Piston rod be connected.The side wall of extraction pot is sandwich.
In technique scheme, the heat energy of steam in vacuum concentration equipment is recycled, right Extracting solution and extractant are preheated, and realize the insulation/preheating before extracting solution vacuum distillation and heating Extractant, thus energy saving, reduces production cost.In addition, pass through first in extraction element driving Motivation structure adjusting slider moves so that the vacancy portion on slide block is relative with the charge door on slide rail Should with different, thus realize to the rapid loading of extraction pot and the closure of charge door, carrying out simultaneously During extraction, operator, next batch can be added in hopper to need to add by charging device Inventory, so there is no need to extraction pot complete extract operation after again weighing add, thus saving Make an appointment, improve extraction efficiency.
Brief description
Fig. 1 is the structural representation of the present invention;
Fig. 2 is the structural representation of extraction element;
Fig. 3 is enlarged diagram at the A of Fig. 2;
Fig. 4 is slide rail, slide block, the assembling schematic diagram of hopper;
Fig. 5 is the upward view of the first stripper.
Specific embodiment
In order that objects and advantages of the present invention become more apparent, with reference to embodiments to this Bright it is specifically described.It should be appreciated that following word is only in order to describe one kind of the present invention or several Plant specific embodiment, considered critical is not carried out to the protection domain of the concrete request of the present invention.
Technical scheme that the present invention takes as shown in figure 1, a kind of for extracting setting of Rhododendron simsii Planch. pigment Extraction element A1 that is standby, being extracted including pigment in the mapping mountain Flos Carthami setting gradually, to extraction Material in device A1 carries out the defecator A2 of solid-liquid separation, for collecting the filtrate after filtering Extraction liquid storage tank A3, the vacuum concentration equipment A4 that extracting solution is concentrated, and to concentration Extracting solution afterwards is dried the spray-drying installation A5 of powder processed, vacuum concentration equipment A4 and extraction It is provided with heat exchanger A6 between device A1, extract in liquid storage tank A3 and be provided with heat exchanger tube, heat exchanger tube Entrance be connected with the gas outlet of vacuum concentration equipment A4, the outlet of heat exchanger tube and heat exchanger The hot fluid inlet of A6 is connected, the outlet of heat exchanger A6 cold fluid inlet and extractant storage tank A7 It is connected, the extractant import phase exporting all with extraction element A1 of heat exchanger A6 cold and hot fluid Connect.In technique scheme, the heat energy of steam in vacuum concentration equipment A4 is carried out reclaiming profit With preheating to extracting solution and extractant, realizing the insulation/preheating before extracting solution vacuum distillation With heating extraction agent, thus energy saving, reduce production cost.Defecator, concentrating under reduced pressure dress Put, spray-drying installation, heat exchanger all can have corresponding function using used in existing chemical industry Device is used, and extracts liquid storage tank and is obtained using general solution reservoir transformation, pacifies in storage tank Dress tubulation shape or spiral helicine heat exchanger tube, the solid material between neighboring devices adopts tape transport, Liquid material adopts pipeline and delivery pump conveying.
Extraction element A1 includes extraction pot 10 and horizontally disposed shaft 151, extraction pot 10 It is respectively arranged with mounting seat, shaft 151 two ends are rotatably installed in the middle part of relative both sides lateral wall In mounting seat, shaft 151 is connected with the 3rd drive mechanism Q3, and shaft 151 is located at and carries Take and rabbling mechanism be provided with the axle body in tank 10, the top of extraction pot 10 be provided with dog-house with And the first adjusting part that the closure state of dog-house is adjusted, the bottom of extraction pot 10 sets It is equipped with the second adjusting part that discharge port and the closure state to discharge port are adjusted, first, Two adjusting parts can be constituted for the horizontally disposed flashboard at extraction pot 10 top or bottom setting, Flashboard can manually adjust the screw mandrel it is also possible to it moves in the horizontal direction by flashboard and driving The piston rod of nut adjusting part or cylinder is connected, using electric or pneumatic regulation.Need Bright, in the present invention, for the ease of briefly, clearly the scope that the present invention is claimed being described, Therefore, the sealing existing at extractant leakage on extraction pot 10 is not described, certainly this It is also the common knowledge and routine operation means that those of ordinary skill in the art are understood.
In the present invention, it is preferred to adopt following scheme, as shown in Figure 2,4, the first adjusting part The slide rail 12 constituting including the grooved part of opening upwards, the vacancy portion that grooved part bottom land opens up is constituted throws Material mouth, slide rail 12 is arranged in the horizontal direction, and slide rail 12 is provided with slide block 13, slide block 13 with Slide rail 12 constitutes slide-and-guide connection cooperation, the bottom surface of slide block 13 along the length direction of slide rail 12 Fit with the bottom land of grooved part, slide block 13 is provided with the hopper 14 of vertical shape arrangement, slide block 13 Open up into opening shape, slide block 13 and the first drive mechanism Q1 with the junction of hopper 14 bottom material mouth It is connected.Sky so that on slide block 13 is moved by the first drive mechanism adjusting slider 13 Scarce portion is corresponding and different with the charge door on slide rail 12, thus realizing quick to extraction pot 10 Charging and the closure of charge door, simultaneously when being extracted, operator, can be by the dress that feeds intake Put the inventory adding next batch needs to add in hopper 14, so there is no need to extracting Tank 10 complete extract operation after again weighing add, thus saving the time, improve raw material extraction efficiency.
Preferably implemented according to scheme as shown in Figure 2,3, the second adjusting part includes extraction pot First and second stripper 16,17 of the upper and lower circle being arranged in parallel at 10 discharge ports, first unloads Flitch 16 is fixed with one with extraction pot 10, and the side of the second stripper 17 offers annular Groove, the second stripper 17 passes through the steel ball assembly 18 arranging in cannelure and extraction pot 10 around lead Vertical direction constitutes the connection that is rotatably assorted, and the center of circle of first and second stripper 16,17 is located at same lead On vertical line, open up first and second at the circumference of same radius size on first and second stripper respectively and unload Material mouth 16a, 17a, the lower face of the first stripper 16 be arranged to by first and second step surface 161, It is step-like that 162 combinations are constituted, and second step face 162 is affixed with the upper face of the second stripper 17 Close, between First terrace 161 and the second stripper 17 upper face, form cavity, the first discharging Mouth 16a is opened on First terrace 161, is provided with the step that first and second step surface is joined The step shape one of sealing member 163, the shape of sealing member 163 and first and second step surface junction Cause, the second stripper 17 is connected with the second drive mechanism Q2, scheme preferably as shown in Figure 5, The outline of first and second step surface junction is arc, so sealing member is set to arc, close Sealing can adopt O-ring seals.Adjust the second stripper 17 by the second drive mechanism Q2 to carry out Rotate so that first and second discharge port on first and second stripper is corresponding and different, thus real Now the closure of the quickly discharging material to extraction pot 10 and discharge port, realizes quickly discharging material, thus saving Time, improve extraction efficiency.
In the present invention, first, second and third drive mechanism can adopt electronic composition, certain first driving machine Structure also can be constituted using cylinder, and the 3rd drive mechanism may also be employed setting operating handle and adjusted manually Section, extraction pot 10 profile is cydariform or elliposoidal.
Further scheme is:It is provided with ultrasound emission assembly or Microwave emission in extraction pot 10 Assembly, ultrasound emission assembly or Microwave emission assembly can improve the extraction effect of plant actives Rate and extraction ratio, the utilization rate shortening the cycle and improving raw material.Extraction pot 10 is arranged on frame 11 On, frame 11 includes the support feet 11 of four vertical shape arrangements, and the bottom of support feet 11 is provided with weight Force transducer 111, gravity sensor 111 can measure the weight of whole extraction equipment in real time and lead to Cross display to show, such operator just can accurately learn the feeding quantity of each material in real time, Thus realizing being fed intake according to optimal material ratio.Rabbling mechanism is included on shaft 151 axle body The spaced puddler of zigzag shape 152, paddle 153 is arranged on the end of puddler 152, It is to be articulated and connected and constitute the jointed shaft being articulated and connected axially between puddler 152 and paddle 153 Angle with shaft 151 axial direction is 30~60 °, and paddle 153 is along away from puddler 152 1 The plate face width that end is pointed near puddler 152 one end is gradually increased, and such rabbling mechanism is permissible Make the stirring of material more abundant, rabbling mechanism can be protected well simultaneously, prevent Solid material causes rabbling mechanism torsional deformation when tangling, and paddle 153 turns on puddler 152 Dynamic angle is difficult excessive, and the general angle rotating is 1~2 °.Arrange on extraction pot 10 internal face There is the flow-interfering bar of zigzag shape, the setting of flow-interfering bar is also for the adequacy realizing material stirring.
Detailed scheme is:Slide block 13 is that a strip plate is constituted, and the two ends of slide block 13 are respectively It is provided with hopper 14, the outside of two hoppers 14 is respectively provided with material and adds mechanism, realizes multiple things That expects adds, and the side wall of extraction pot 10 is sandwich, and the folder chamber that sandwich is formed is used for holding Receive hot fluid, the material in extraction pot 10 is incubated or heats.
In a word, the extraction equipment that the present invention provides, can effectively realize quickly adding and unloading of material, Realize the high concentration rapid extraction of Rhododendron simsii Planch. pigment, improve the extraction efficiency of Rhododendron simsii Planch. pigment.
The above is only the preferred embodiment of the present invention it is noted that for the art Those of ordinary skill for, after knowing content described in the present invention, former without departing from the present invention On the premise of reason, it can also be made with some equal conversion and substitute, these convert on an equal basis and replace In generation, also should be regarded as belonging to protection scope of the present invention.

Claims (2)

1. a kind of equipment for extracting Rhododendron simsii Planch. pigment it is characterised in that:Including setting gradually Mapping mountain Flos Carthami in the extraction element that extracted of pigment, the material in extraction element is carried out solid The detached defecator of liquid, for collecting the extraction liquid storage tank of the filtrate after filtering, enters to extracting solution The vacuum concentration equipment that row concentrates, and the extracting solution after concentrating is dried with the spray dried of powder processed Dry device, is provided with heat exchanger between vacuum concentration equipment and extraction element, extract in liquid storage tank and set It is equipped with heat exchanger tube, the entrance of heat exchanger tube is connected with the gas outlet of vacuum concentration equipment, heat exchanger tube Outlet be connected with the hot fluid inlet of heat exchanger, heat exchanger cold fluid inlet and extractant storage tank Outlet be connected, the outlet of heat exchanger cold and hot fluid is connected with the extractant import of extraction element Connect, extraction element includes extraction pot and horizontally disposed shaft, outside the relative both sides of extraction pot It is respectively arranged with mounting seat, shaft two ends are rotatably installed in mounting seat, shaft in the middle part of the wall of side It is connected with drive mechanism B, shaft is located at and is provided with rabbling mechanism on the axle body in extraction pot, The top of extraction pot is provided with dog-house and the closure state to dog-house is adjusted first Adjusting part, the bottom of extraction pot is provided with discharge port and the closure state of discharge port is adjusted Second adjusting part of section, the first adjusting part includes the slide rail that the grooved part of opening upwards is constituted, The vacancy portion that grooved part bottom land opens up constitutes dog-house, and slide rail is arranged in the horizontal direction, and slide rail sets It is equipped with slide block, slide block is connected cooperation, slide block with slide rail along the length direction composition slide-and-guide of slide rail Bottom surface fit with the bottom land of grooved part, slide block is provided with the hopper of vertical shape arrangement, slide block with The junction of feed hopper bottom material mouth opens up into opening shape, and slide block is connected with drive mechanism A.
2. the equipment for extracting Rhododendron simsii Planch. pigment according to claim 1 it is characterised in that: It is provided with ultrasound emission assembly in extraction pot;Extraction pot is arranged in frame, and frame includes four and stands The support feet of shape arrangement, the bottom of support feet is provided with gravity sensor.
CN201510426964.7A 2014-08-10 2015-07-18 Device for extracting rhododendron pigment Active CN105038302B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201610490540.1A CN105885470B (en) 2014-08-10 2015-07-18 A kind of equipment that can be used in extracting azalea pigment
CN201510426964.7A CN105038302B (en) 2014-08-10 2015-07-18 Device for extracting rhododendron pigment

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN2014204486391 2014-08-10
CN201420448639 2014-08-10
CN201510426964.7A CN105038302B (en) 2014-08-10 2015-07-18 Device for extracting rhododendron pigment

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201610490540.1A Division CN105885470B (en) 2014-08-10 2015-07-18 A kind of equipment that can be used in extracting azalea pigment

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CN105038302B true CN105038302B (en) 2017-02-08

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CN201510426964.7A Active CN105038302B (en) 2014-08-10 2015-07-18 Device for extracting rhododendron pigment
CN201610490540.1A Active CN105885470B (en) 2014-08-10 2015-07-18 A kind of equipment that can be used in extracting azalea pigment

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Address before: 221000 Shenchang, Gulou District, Xuzhou City, Jiangsu Province (A2, 307, Huaihai Cultural and Technological Industrial Park)

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