CN105062122B - The equipment of rapid extraction natural pigment from plant flower - Google Patents

The equipment of rapid extraction natural pigment from plant flower Download PDF

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Publication number
CN105062122B
CN105062122B CN201510427020.1A CN201510427020A CN105062122B CN 105062122 B CN105062122 B CN 105062122B CN 201510427020 A CN201510427020 A CN 201510427020A CN 105062122 B CN105062122 B CN 105062122B
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CN
China
Prior art keywords
extraction
heat exchanger
stripper
extracting solution
extraction pot
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201510427020.1A
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Chinese (zh)
Other versions
CN105062122A (en
Inventor
林桂花
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUANGXI ZHIZHEN INVESTMENT CO., LTD.
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林桂花
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Filing date
Publication date
Application filed by 林桂花 filed Critical 林桂花
Priority to CN201610490982.6A priority Critical patent/CN106178585B/en
Priority to CN201510427020.1A priority patent/CN105062122B/en
Publication of CN105062122A publication Critical patent/CN105062122A/en
Application granted granted Critical
Publication of CN105062122B publication Critical patent/CN105062122B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0223Moving bed of solid material
    • B01D11/0242Moving bed of solid material in towers, e.g. comprising contacting elements
    • B01D11/0246Moving bed of solid material in towers, e.g. comprising contacting elements comprising rotating means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/028Flow sheets
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0096Purification; Precipitation; Filtration
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The present invention relates to a kind of equipment of rapid extraction natural pigment from plant flower, including first set gradually, two extraction elements, first, two defecators, extracting solution storage tank, vacuum concentration equipment, spray-drying installation, heat exchanger, it is provided with heat exchanger tube in extracting solution storage tank, the entrance of heat exchanger tube is connected with the gas outlet of vacuum concentration equipment, the outlet of heat exchanger tube is connected with the hot fluid import of heat exchanger, heat exchanger cold fluid inlet is connected with the outlet of extractant storage tank and the filtrate (liquid of the second defecator, heat exchanger is cold, the outlet of hot fluid and first, the extractant import of two extraction elements is connected.In technique scheme, the heat energy of steam in vacuum concentration equipment is recycled, extracting solution and extractant are preheated, it is achieved the insulation/preheating before extracting solution decompression distillation and heating extraction agent, thus save the energy, reduce production cost.

Description

The equipment of rapid extraction natural pigment from plant flower
Technical field
The present invention relates to nature strength field, be specifically related to one and quickly carry from plant flower Take the equipment of natural pigment.
Background technology
Extract field in natural activity component, often need to use extraction element to the root of natural plants, Stem, leaf extract so that the active component in herbaceous plant root, stem, leaf is dissolved in extractant In, thus realize the extraction to active component.Mostly there is the throwing of material in the extraction pot of existing use Add the problem loaded down with trivial details and time-consuming with discharging, have a strong impact on the production efficiency of natural activity component.Separately Outward, for the extraction of natural activity component, all there is an optimal material ratio (active under this material The extraction ratio of component and/or extraction efficiency are maximum), but feeding intake of extraction pot of tradition is difficult to accurately Control material ratio so that extraction ratio and/or extraction efficiency are unable to reach most preferably, have a strong impact on production Efficiency and cause wastage of material.
It addition, currently used active component extraction equipment generally to there is extraction ratio low, utilization of energy The problems such as rate is low, extracting cycle length.
Summary of the invention
It is an object of the invention to provide a kind of the setting of rapid extraction natural pigment from plant flower Standby, it can realize the rapid extraction of pigment in plant flower, and in extracting solution, the concentration of pigment is high, It is easy to follow-up concentrating and purifying process and save the energy.
For achieving the above object, present invention employs techniques below scheme:
A kind of equipment of rapid extraction natural pigment from plant flower, it is characterised in that: include depending on First and second extraction element that plant flower is carried out firsts and seconds extraction of secondary setting, to first, Material in two extraction elements carries out first and second defecator of solid-liquid separation respectively, is used for collecting The extracting solution storage tank of the filtrate that the first defecator filters, the concentrating under reduced pressure that extracting solution is concentrated Device, and the extracting solution after concentrating is dried the spray-drying installation of powder process, concentrating under reduced pressure It is provided with heat exchanger between device and the first extraction element, in extracting solution storage tank, is provided with heat exchanger tube, The entrance of heat exchanger tube is connected with the gas outlet of vacuum concentration equipment, the outlet of heat exchanger tube and heat exchange The hot fluid import of device is connected, the outlet of heat exchanger cold fluid inlet and extractant storage tank and the The filtrate (liquid of two defecators is connected, and the outlet of heat exchanger cold and hot fluid carries with first and second The extractant import that fetching is put is connected, and first and second extraction element includes extraction pot and horizontal cloth The shaft put, is respectively arranged with mounting seat, shaft in the middle part of the lateral wall, both sides that extraction pot is relative Two ends are rotatably installed in mounting seat, and shaft and the 3rd drive mechanism are connected, and shaft is positioned at Being provided with rabbling mechanism on axle body in extraction pot, the top of extraction pot is provided with dog-house and right The first adjusting part that the closure state of dog-house is adjusted, the bottom of extraction pot is provided with discharging The second adjusting part that mouth and the closure state to discharge port are adjusted, the second adjusting part bag Include the upper and lower first and second circular stripper being arranged in parallel, the first discharging at extraction pot discharge port Plate is fixed with one with extraction pot, and the side of the second stripper offers cannelure, the second discharging Plate constitutes, around vertical, the company of being rotatably assorted with extraction pot by the steel ball assembly arranged in cannelure Connecing, the center of circle of first and second stripper is positioned on same plumb line, same on first and second stripper Offering first and second discharge port at the circumference of radius size respectively, the lower face of the first stripper is arranged It is step-like that one-tenth is made up of first and second step surface combination, and second step face is upper with the second stripper Plate face fits, and forms cavity, the first discharging between First terrace and the second stripper upper face Mouth is opened on First terrace, is provided with sealing member at the step that first and second step surface is joined, The shape of sealing member is consistent with the step shape of first and second step surface junction, the second stripper with Second drive mechanism is connected.
Further scheme is: being provided with Microwave emission assembly in extraction pot, extraction pot is arranged on machine On frame, frame includes the spike that four vertical shapes are arranged, the bottom of a spike is provided with gravity sensitive Device.Rabbling mechanism is included in the spaced puddler of zigzag shape, paddle on shaft axle body It is arranged on the end of puddler, is articulated and connected for being articulated and connected and constituting between puddler and paddle Axially the most axial with the shaft angle of jointed shaft be 30~60 °, paddle edge is away from puddler one The plate face width degree that end points near puddler one end is gradually increased.It is provided with spiral shell on extraction pot internal face The flow-interfering bar of spin line shape.
Detailed scheme is: slide block is that a strip plate is constituted, and the two ends of slide block are respectively arranged with Hopper, the outside of two hoppers is respectively provided with material and adds mechanism.Second adjusting part includes a level The flashboard arranged, flashboard and driving its feed screw nut's adjusting part moved in the horizontal direction or cylinder Piston rod be connected.The sidewall of extraction pot is sandwich.
In technique scheme, the heat energy of steam in vacuum concentration equipment is recycled, right Extracting solution and extractant preheat, it is achieved the insulation before extracting solution decompression distillation/preheat and heat Extractant, thus save the energy, reduce production cost.Meanwhile, two-stage is used to extract, can be effective Shorten extracting cycle, save the energy and improve the throughput rate of pigment.Obtain when extracting due to two grades Extracting solution in pigment concentration relatively low, therefore will filter the filtrate after separating as extracting for the first time Extractant, thus improve the concentration of pigment in extracting solution, it is simple to follow-up distillation and concentration processes.Logical Cross the second drive mechanism to regulate the second stripper and rotate so that on first and second stripper One, the corresponding and different layout of two discharge ports, thus realize the quickly discharging material to extraction pot and discharging The Guan Bi of mouth, thus save the time, improve extracting efficiency.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention;
Fig. 2 is the structural representation of first and second extraction element;
Fig. 3 is enlarged diagram at the A of Fig. 2;
Fig. 4 is the assembling schematic diagram of slide rail, slide block, hopper;
Fig. 5 is the upward view of the first stripper.
Detailed description of the invention
In order to make objects and advantages of the present invention clearer, below in conjunction with embodiment to this Bright it is specifically described.Should be appreciated that following word is only in order to describe the one of the present invention or several Planting specific embodiment, the protection domain of not concrete to present invention request carries out considered critical.
Technical scheme that the present invention takes is as it is shown in figure 1, one rapid extraction sky from plant flower So equipment of pigment, carries out the of firsts and seconds extraction including set gradually to plant flower One, two extraction element A11, A12, divides the material in first and second extraction element A11, A12 Do not carry out first and second defecator A21, A22 of solid-liquid separation, for collecting the first defecator Extracting solution storage tank A3, the vacuum concentration equipment A4 that extracting solution is concentrated of the filtrate that A21 filters, And the extracting solution after concentrating is dried the spray-drying installation A5 of powder process, vacuum concentration equipment It is provided with heat exchanger A6 between A4 and the first extraction element A11, is provided with in extracting solution storage tank A3 Heat exchanger tube, the entrance of heat exchanger tube is connected with the gas outlet of vacuum concentration equipment A4, heat exchanger tube Outlet be connected with the hot fluid import of heat exchanger A6, heat exchanger A6 cold fluid inlet and extraction The outlet of agent storage tank A3 and the filtrate (liquid of the second defecator A22 are connected, heat exchanger A6 The outlet of cold and hot fluid is connected with the extractant import of first and second extraction element A11, A12. In technique scheme, the heat energy of steam in vacuum concentration equipment A4 is recycled, right Extracting solution and extractant preheat, it is achieved the insulation before extracting solution decompression distillation/preheat and heat Extractant, thus save the energy, reduce production cost.Meanwhile, two-stage is used to extract, can be effective Shorten extracting cycle, save the energy and improve the throughput rate of pigment.Obtain when extracting due to two grades Extracting solution in pigment concentration relatively low, therefore will filter the filtrate after separating as extracting for the first time Extractant, thus improve the concentration of pigment in extracting solution, it is simple to follow-up distillation and concentration processes.Cross Filter device, vacuum concentration equipment, spray-drying installation, heat exchanger all can use in existing chemical industry and make The device with corresponding function use, extracting solution storage tank use general solution reservoir change Make and obtain, tubulation shape or spiral helicine heat exchanger tube, the solids between neighboring devices are installed in storage tank Material uses tape transport, and liquid material uses pipeline and delivery pump conveying.
First and second extraction element A11, A12 includes extraction pot 10 and horizontally disposed shaft 151, it is respectively arranged with mounting seat, shaft 151 in the middle part of the lateral wall, both sides that extraction pot 10 is relative Two ends are rotatably installed in mounting seat, and shaft 151 is connected with the 3rd drive mechanism Q3, stirs Mix axle 151 to be positioned on the axle body of extraction pot 10 and be provided with rabbling mechanism, the top of extraction pot 10 It is provided with dog-house and the first adjusting part that the closure state to dog-house is adjusted, extracts The second tune that the bottom of tank 10 is provided with discharge port and the closure state to discharge port is adjusted Joint assembly, first and second adjusting part can be extraction pot 10 top or the horizontal cloth of bottom setting The flashboard put is constituted, and flashboard can manually regulate, it is also possible to by flashboard with drive it along level Feed screw nut's adjusting part or the piston rod of cylinder that direction is moved are connected, and utilize electronic or gas Dynamic regulation.It should be noted that in the present invention, for the ease of the present invention briefly, is clearly described The scope being claimed, therefore, not to there is the sealing at extractant leakage on extraction pot 10 Being described, this is also that the common knowledge that those of ordinary skill in the art are understood is grasped with conventional certainly Make means.
In the present invention, it is preferred to use following scheme, as shown in Figure 2,4, the first adjusting part The slide rail 12 constituted including the grooved part of opening upwards, the vacancy portion that grooved part bottom land is offered is constituted throws Material mouth, slide rail 12 arranges in the horizontal direction, and slide rail 12 is provided with slide block 13, slide block 13 with Slide rail 12 constitutes slide-and-guide connection cooperation, the bottom surface of slide block 13 along the length direction of slide rail 12 Fit with the bottom land of grooved part, slide block 13 is provided with the hopper 14 that vertical shape is arranged, slide block 13 With expect bottom hopper 14 that opening shape, slide block 13 and the first drive mechanism Q1 are offered in the junction of mouth It is connected.Moved by the first drive mechanism adjusting slider 13 so that the sky on slide block 13 The portion of lacking is corresponding with the charge door on slide rail 12 and different, thus quick to extraction pot 10 of realization Charging and the Guan Bi of charge door, simultaneously when extracting, operator, can be by feeding intake dress Put in hopper 14, add the inventory that next batch needs to add, so there is no need to extracting Tank 10 complete to extract operation after again weighing add, thus save the time, improve raw material extraction efficiency.
Preferably implementing according to scheme as shown in Figure 2,3, the second adjusting part includes extraction pot The upper and lower first and second circular stripper 16,17 being arranged in parallel at 10 discharge ports, first unloads Flitch 16 is fixed with one with extraction pot 10, and the side of the second stripper 17 offers annular Groove, the second stripper 17 passes through the interior steel ball assembly 18 arranged of cannelure with extraction pot 10 around lead Vertical direction constitutes the connection that is rotatably assorted, and the center of circle of first and second stripper 16,17 is positioned at same lead On vertical line, first and second stripper is offered at the circumference of same radius size first and second respectively and unloads Material mouth 16a, 17a, the lower face of the first stripper 16 be arranged to by first and second step surface 161, It is step-like that 162 combinations are constituted, and second step face 162 is affixed with the upper face of the second stripper 17 Close, between First terrace 161 and the second stripper 17 upper face, form cavity, the first discharging Mouth 16a is opened on First terrace 161, is provided with at the step that first and second step surface is joined The step shape one of sealing member 163, the shape of sealing member 163 and first and second step surface junction Causing, the second stripper 17 is connected with the second drive mechanism Q2, scheme the most as shown in Figure 5, The outline of first and second step surface junction is arc, so sealing member is set to arc, close Sealing can use O-ring seals.Regulate the second stripper 17 by the second drive mechanism Q2 to carry out Rotate so that first and second discharge port on first and second stripper is corresponding and different, thus real Now quickly discharging material and the Guan Bi of discharge port to extraction pot 10, it is achieved quickly discharging material, thus save Time, improve extraction efficiency.
In the present invention, first, second and third drive mechanism can use electronic composition, and certain first drives machine Structure also can use cylinder to constitute, and the 3rd drive mechanism may be used without arranging operating handle and manually adjusts Joint, extraction pot 10 profile is cydariform or elliposoidal.
Further scheme is: be provided with ultrasound emission assembly or Microwave emission in extraction pot 10 Assembly, ultrasound emission assembly or Microwave emission assembly can improve the extraction effect of plant actives Rate and extraction ratio, shorten the cycle and improve the utilization rate of raw material.Extraction pot 10 is arranged on frame 11 On, frame 11 includes the spike 11 that four vertical shapes are arranged, the bottom of a spike 11 is provided with weight Force transducer 111, gravity sensor 111 can be measured the weight of whole extraction equipment in real time and lead to Crossing display to show, such operator just can the most accurately learn the feeding quantity of each material, Thus realize feeding intake according to optimal material ratio.Rabbling mechanism is included on shaft 151 axle body The spaced puddler of zigzag shape 152, paddle 153 is arranged on the end of puddler 152, For being articulated and connected and to constitute the jointed shaft being articulated and connected axial between puddler 152 and paddle 153 The angle axial with shaft 151 is 30~60 °, and paddle 153 is along away from puddler 152 1 The plate face width degree that end points near puddler 152 one end is gradually increased, and such rabbling mechanism is permissible The stirring making material is more abundant, can well protect rabbling mechanism simultaneously, prevent Solid material causes rabbling mechanism torsional deformation when tangling, and paddle 153 turns on puddler 152 Dynamic angle is difficult to excessive, and the general angle rotated is 1~2 °.Arrange on extraction pot 10 internal face There is the flow-interfering bar of zigzag shape, arranging also for the adequacy realizing material stirring of flow-interfering bar.
Detailed scheme is: slide block 13 is that a strip plate is constituted, and the two ends of slide block 13 are respectively Being provided with hopper 14, the outside of two hoppers 14 is respectively provided with material and adds mechanism, it is achieved multiple thing Adding of material, the sidewall of extraction pot 10 is sandwich, and the folder chamber that sandwich is formed is used for holding Receive hot fluid, the material in extraction pot 10 is incubated or heats.
In a word, the extraction natural pigment equipment that the present invention provides, can effectively realize the quick throwing of material Add and unload, it is achieved the high concentration rapid extraction of pigment in plant flower, improving the extraction effect of pigment Rate.The present invention can be used for the extraction of pigment in the plant flowers such as Folium Rhododendri Simsii, Flos Rosae Rugosae, Flos persicae.
The above is only the preferred embodiment of the present invention, it is noted that for the art Those of ordinary skill for, after knowing content described in the present invention, former without departing from the present invention On the premise of reason, it is also possible to it is made some equal conversion and replacement, these convert on an equal basis and replace In generation, also should be regarded as belonging to protection scope of the present invention.

Claims (2)

1. the equipment of rapid extraction natural pigment from plant flower, it is characterised in that: bag Include first and second extraction element that plant flower is carried out firsts and seconds extraction set gradually, right Material in first and second extraction element carries out first and second defecator of solid-liquid separation respectively, uses In the extracting solution storage tank of the filtrate collecting the first defecator filtration, concentrate extracting solution subtracts Pressure enrichment facility, and the extracting solution after concentrating is dried the spray-drying installation of powder process, subtract It is provided with heat exchanger between pressure enrichment facility and the first extraction element, is provided with in extracting solution storage tank and changes Heat pipe, the entrance of heat exchanger tube is connected with the gas outlet of vacuum concentration equipment, the outlet of heat exchanger tube It is connected with the hot fluid import of heat exchanger, heat exchanger cold fluid inlet and the outlet of extractant storage tank And second the filtrate (liquid of defecator be connected, the outlet of heat exchanger cold flow body is extracted with first The extractant import of device is connected, the outlet of exchanger heat fluid and the extraction of the second extraction element Agent import is connected, and first and second extraction element includes extraction pot and horizontally disposed shaft, Being respectively arranged with mounting seat in the middle part of the lateral wall, both sides that extraction pot is relative, shaft two ends rotate installs In mounting seat, shaft is connected with drive mechanism B, and shaft is positioned at the axle body of extraction pot On be provided with rabbling mechanism, the top of extraction pot is provided with dog-house and the closed form to dog-house The first adjusting part that state is adjusted, the bottom of extraction pot is provided with discharge port and to discharge port The second adjusting part of being adjusted of closure state, the second adjusting part includes extraction pot discharge port Locating the upper and lower first and second circular stripper being arranged in parallel, the first stripper is connected with extraction pot Being integrated, the side of the second stripper offers cannelure, the second stripper is by cannelure Steel ball assembly and the extraction pot arranged is rotatably assorted around vertical composition and is connected, first and second discharging The center of circle of plate is positioned on same plumb line, on first and second stripper at the circumference of same radius size Offering first and second discharge port respectively, the lower face of the first stripper is arranged to by first and second step It is step-like that face combination is constituted, and second step face fits with the upper face of the second stripper, and first Forming cavity between step surface and the second stripper upper face, the first discharge port is opened in first step On face, at the step that first and second step surface is joined, it is provided with sealing member, the shape of sealing member and the One, the step shape of two step surface junctions is consistent, and the second stripper is connected with drive mechanism A.
The equipment of rapid extraction natural pigment from plant flower the most according to claim 1, It is characterized in that: in extraction pot, be provided with Microwave emission assembly;Extraction pot is arranged in frame, machine Frame includes the spike that four vertical shapes are arranged, the bottom of a spike is provided with gravity sensor.
CN201510427020.1A 2014-08-10 2015-07-18 The equipment of rapid extraction natural pigment from plant flower Expired - Fee Related CN105062122B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201610490982.6A CN106178585B (en) 2014-08-10 2015-07-18 A kind of equipment for the rapidly extracting natural pigment from plant flower
CN201510427020.1A CN105062122B (en) 2014-08-10 2015-07-18 The equipment of rapid extraction natural pigment from plant flower

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN2014204486207 2014-08-10
CN201420448620 2014-08-10
CN201510427020.1A CN105062122B (en) 2014-08-10 2015-07-18 The equipment of rapid extraction natural pigment from plant flower

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CN105062122B true CN105062122B (en) 2017-01-04

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CN108408641A (en) * 2018-05-03 2018-08-17 江苏澳特丝生物科技有限公司 The installing mechanism of extractor in a kind of fibroin extraction element

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CN106178585A (en) 2016-12-07
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