CN105062122A - Equipment for rapidly extracting natural pigments from plant flowers - Google Patents

Equipment for rapidly extracting natural pigments from plant flowers Download PDF

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Publication number
CN105062122A
CN105062122A CN201510427020.1A CN201510427020A CN105062122A CN 105062122 A CN105062122 A CN 105062122A CN 201510427020 A CN201510427020 A CN 201510427020A CN 105062122 A CN105062122 A CN 105062122A
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CN
China
Prior art keywords
extractor
extraction
equipment
outlet
stripper
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Granted
Application number
CN201510427020.1A
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Chinese (zh)
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CN105062122B (en
Inventor
胡刘满
王选明
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GUANGXI ZHIZHEN INVESTMENT CO., LTD.
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王选明
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Priority to CN201510427020.1A priority Critical patent/CN105062122B/en
Priority to CN201610490982.6A priority patent/CN106178585B/en
Publication of CN105062122A publication Critical patent/CN105062122A/en
Application granted granted Critical
Publication of CN105062122B publication Critical patent/CN105062122B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0223Moving bed of solid material
    • B01D11/0242Moving bed of solid material in towers, e.g. comprising contacting elements
    • B01D11/0246Moving bed of solid material in towers, e.g. comprising contacting elements comprising rotating means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/028Flow sheets
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0096Purification; Precipitation; Filtration
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Abstract

The invention relates to equipment for rapidly extracting natural pigments from plant flowers. The equipment comprises a first extraction device, a second extraction device, a first filter device, a second filter device, an extracting solution storage tank, a decompressing concentration device, a spray drying device and a heat exchanger which are sequentially arranged, wherein a heat exchange pipe is arranged in the extracting solution storage tank; an inlet of the heat exchange pipe is connected with a gas outlet of the decompressing concentration device; an outlet of the heat exchange pipe is connected with a thermal fluid inlet of the heat exchanger; a cold fluid inlet of the heat exchanger is connected with an outlet of an extracting agent storage tank and a filtrate outlet of the second filter device; a cold fluid outlet and a thermal fluid outlet of the heat exchanger are connected with extracting agent inlets of the first extraction device and the second extraction device. According to the technical scheme, thermal energy of steam in the decompressing concentration device is recycled, an extracting solution and an extracting agent are preheated, thermal preservation/preheating of the extracting solution before decompressing distillation as well as extracting agent heating are realized, so that the energy is saved, and the production cost is reduced.

Description

The equipment of rapid extraction natural pigment from plant flower
Technical field
The present invention relates to nature strength field, be specifically related to a kind of equipment of rapid extraction natural pigment from plant flower.
Background technology
Extract field in natural radioactivity component, extraction element often need be used to carry out lixiviate to the root of natural phant, stem, leaf, make solubilize active ingredients in herbaceous plant root, stem, leaf in extraction agent, thus realize the extraction to active ingredient.What the extractor of existing use existed material mostly adds the problem loaded down with trivial details and consuming time with discharging, has a strong impact on the production efficiency of natural radioactivity component.In addition, for the extraction of natural radioactivity component, all there is a best material ratio (under this material the extraction yield of active ingredient and/or extraction efficiency maximum), but feeding intake of traditional extractor is difficult to control material ratio accurately, make extraction yield and/or extraction efficiency cannot reach best, have a strong impact on production efficiency and cause wastage of material.
The problems such as in addition, the active ingredient extraction equipment ubiquity extraction yield used at present is low, and energy utilization rate is low, and extracting cycle is long.
Summary of the invention
Object of the present invention is just to provide a kind of equipment of rapid extraction natural pigment from plant flower, and it can realize the rapid extraction to pigment in plant flower, and in extracting solution, the concentration of pigment is high, is convenient to follow-up concentrated and purified process and save energy.
For achieving the above object, present invention employs following technical scheme:
A kind of equipment of rapid extraction natural pigment from plant flower, it is characterized in that: comprise set gradually first of firsts and seconds extraction is carried out to plant flower, two extraction elements, to first, material in two extraction elements carries out first of solid-liquid separation respectively, two filtration units, for collecting the extracting solution storage tank of the filtrate of the first filtration devices, to the vacuum concentration equipment that extracting solution concentrates, and the extracting solution after concentrated is carried out to the spray drying unit of dry powder process, interchanger is provided with between vacuum concentration equipment and the first extraction element, heat transfer tube is provided with in extracting solution storage tank, the entrance of heat transfer tube is connected with the pneumatic outlet of vacuum concentration equipment, the outlet of heat transfer tube is connected with the hot-fluid import of interchanger, interchanger cold fluid inlet is connected with the outlet of extraction agent storage tank and the filtrate outlet of the second filtration unit, interchanger is cold, the outlet of hot-fluid and first, the extraction agent import of two extraction elements is connected, first, two extraction elements comprise extractor and horizontally disposed stir shaft, mount pad is respectively arranged with in the middle part of the both sides outer side wall that extractor is relative, stir shaft two ends are rotatably installed in mount pad, stir shaft is connected with the 3rd driving mechanism, the axle body that stir shaft is positioned at extractor is provided with stirring mechanism, the first adjusting part that the top of extractor is provided with dog-house and regulates the closure state of dog-house, the second adjusting part that the bottom of extractor is provided with discharge opening and regulates the closure state of discharge opening, second adjusting part comprises in extractor discharge opening place, under be arranged in parallel first of circle, two strippers, first stripper and extractor are fixed with one, the side of the second stripper offers ring groove, second stripper consists of to be rotatably assorted around vertical the steel ball assembly that arranges in ring groove and extractor and is connected, first, the center of circle of two strippers is positioned on same plummet, first, on two strippers, the circumference place of same radius size offers first respectively, two discharge openings, the lower face of the first stripper is arranged to by first, it is step-like that two step surface combinations are formed, the upper face of second step face and the second stripper fits, cavity is formed between First terrace and the second stripper upper face, first discharge opening is opened on First terrace, first, the step place that two step surfaces are joined is provided with sealing member, the shape of sealing member and first, the step shape of two step surface junctions is consistent, second stripper is connected with the second driving mechanism.
Further scheme is: be provided with Microwave emission assembly in extractor, and extractor is arranged in frame, and frame comprises the feet that four vertical shapes are arranged, the bottom of feet is provided with gravity sensor.Stirring mechanism is included in the spaced agitator arm of zigzag shape on stir shaft axle body, paddle is arranged on the end of agitator arm, be axially 30 ~ 60 ° with the angle of stir shaft axis for being articulated and connected and forming the jointed shaft that is articulated and connected between agitator arm and paddle, paddle increases gradually along the plate face width degree pointed near agitator arm one end away from agitator arm one end.Extractor inner-wall surface is provided with the flow-interfering bar of zigzag shape.
Detailed scheme is: slide block is that a long strip shape plate is formed, and the two ends of slide block are respectively arranged with hopper, and the outside of two hoppers arranges material respectively and adds mechanism.Second adjusting part comprises a horizontally disposed flashboard, flashboard and drive its feed screw nut's adjusting part of movement or the piston rod of cylinder are connected in the horizontal direction.The sidewall of extractor is sandwich structure.
In technique scheme, the heat energy of steam in vacuum concentration equipment is recycled, preheating is carried out to extracting solution and extraction agent, realize the insulation/preheating before extracting solution underpressure distillation and heating extraction agent, thus save energy, reduce production cost.Meanwhile, adopt two-stage to extract, effectively can shorten extracting cycle, the throughput rate of save energy and raising pigment.Because pigment concentration is lower in the extracting solution of acquisition when secondary extracts, therefore using the extraction agent that the filtrate after filtering separation was extracted as first time, thus improve the concentration of pigment in extracting solution, be convenient to follow-up distillation and concentration process.The second stripper is regulated to rotate by the second driving mechanism, make the corresponding and different layout of first and second discharge opening on first and second stripper, thus realize the quickly discharging material of extractor and the closed of discharge opening, thus save time, improve extracting efficiency.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention;
Fig. 2 is the structural representation of first and second extraction element;
Fig. 3 is the A place enlarged diagram of Fig. 2;
Fig. 4 is the assembling schematic diagram of slide rail, slide block, hopper;
Fig. 5 is the upward view of the first stripper.
Embodiment
In order to make objects and advantages of the present invention clearly understand, below in conjunction with embodiment, the present invention is specifically described.Should be appreciated that following word only in order to describe one or more concrete embodiments of the present invention, considered critical is not carried out to the protection domain that the present invention specifically asks.
The technical scheme that the present invention takes as shown in Figure 1, a kind of equipment of rapid extraction natural pigment from plant flower, comprise set gradually first of firsts and seconds extraction is carried out to plant flower, two extraction element A11, A12, to first, two extraction element A11, material in A12 carries out first of solid-liquid separation respectively, two filtration unit A21, A22, for collecting the extracting solution storage tank A3 of the filtrate that the first filtration unit A21 filters, to the vacuum concentration equipment A4 that extracting solution concentrates, and the extracting solution after concentrated is carried out to the spray drying unit A5 of dry powder process, interchanger A6 is provided with between vacuum concentration equipment A4 and the first extraction element A11, heat transfer tube is provided with in extracting solution storage tank A3, the entrance of heat transfer tube is connected with the pneumatic outlet of vacuum concentration equipment A4, the outlet of heat transfer tube is connected with the hot-fluid import of interchanger A6, interchanger A6 cold fluid inlet is connected with the outlet of extraction agent storage tank A3 and the filtrate outlet of the second filtration unit A22, interchanger A6 is cold, the outlet of hot-fluid and first, two extraction element A11, the extraction agent import of A12 is connected.In technique scheme, the heat energy of steam in vacuum concentration equipment A4 is recycled, preheating is carried out to extracting solution and extraction agent, realize the insulation/preheating before extracting solution underpressure distillation and heating extraction agent, thus save energy, reduce production cost.Meanwhile, adopt two-stage to extract, effectively can shorten extracting cycle, the throughput rate of save energy and raising pigment.Because pigment concentration is lower in the extracting solution of acquisition when secondary extracts, therefore using the extraction agent that the filtrate after filtering separation was extracted as first time, thus improve the concentration of pigment in extracting solution, be convenient to follow-up distillation and concentration process.Filtration unit, vacuum concentration equipment, spray drying unit, interchanger all can adopt the device with corresponding function used in existing chemical industry to use, extracting solution storage tank adopts general solution reservoir transformation to obtain, tubulation shape or spiral helicine heat transfer tube are installed in storage tank, solid materials between neighboring devices adopts tape transport, and liquid material adopts pipeline and transferpump conveying.
First, two extraction element A11, A12 comprises extractor 10 and horizontally disposed stir shaft 151, mount pad is respectively arranged with in the middle part of the both sides outer side wall that extractor 10 is relative, stir shaft 151 two ends are rotatably installed in mount pad, stir shaft 151 is connected with the 3rd driving mechanism Q3, the axle body that stir shaft 151 is positioned at extractor 10 is provided with stirring mechanism, the first adjusting part that the top of extractor 10 is provided with dog-house and regulates the closure state of dog-house, the second adjusting part that the bottom of extractor 10 is provided with discharge opening and regulates the closure state of discharge opening, first, the horizontally disposed flashboard that two adjusting parts can be extractor 10 top or bottom setting is formed, flashboard can manually regulate, also can by flashboard and drive its feed screw nut's adjusting part of movement or the piston rod of cylinder are connected in the horizontal direction, utilize electronic or pneumatic adjustment.It should be noted that; in the present invention, for the ease of briefly, clearly the scope that request of the present invention is protected being described, therefore; be not sealed into line description to what extractor 10 exists extraction agent leakage place, this is also the common practise understood of those of ordinary skill in the art and routine operation means certainly.
In the present invention, the following scheme of preferred employing, as Fig. 2, shown in 4, the slide rail 12 that the grooved part that first adjusting part comprises opening upwards is formed, the vacancy portion that grooved part bottom land is offered forms dog-house, slide rail 12 is arranged in the horizontal direction, slide rail 12 is provided with slide block 13, slide block 13 and slide rail 12 form slide-and-guide along the length direction of slide rail 12 and are connected and coordinate, the bottom surface of slide block 13 and the bottom land of grooved part fit, slide block 13 is provided with the hopper 14 that vertical shape is arranged, slide block 13 with expect bottom hopper 14 that opening shape is offered in the junction of mouth, slide block 13 is connected with the first driving mechanism Q1.Moved by the first driving mechanism adjusting slider 13, make the vacancy portion on slide block 13 corresponding with the charging opening on slide rail 12 and different, thus realize the rapid loading of extractor 10 and the closed of charging opening, simultaneously when extracting, operator, can add by charging device the inventory that next batch needs add in hopper 14, so just not to need after extractor 10 completes extraction operation weighing again to add, thus save time, improve raw material extraction efficiency.
Preferably according to such as Fig. 2, shown in 3, scheme is implemented, and the second adjusting part comprises in extractor 10 discharge opening place, under be arranged in parallel first of circle, two strippers 16, 17, first stripper 16 and extractor 10 are fixed with one, and the side of the second stripper 17 offers ring groove, and the second stripper 17 consists of to be rotatably assorted around vertical the steel ball assembly 18 that arranges in ring groove and extractor 10 and is connected, and first, two strippers 16, the center of circle of 17 is positioned on same plummet, and first, on two strippers, the circumference place of same radius size offers first respectively, two discharge opening 16a, 17a, the lower face of the first stripper 16 is arranged to by first, two step surfaces 161, it is step-like that 162 combinations are formed, and the upper face of second step face 162 and the second stripper 17 fits, and form cavity between First terrace 161 and the second stripper 17 upper face, the first discharge opening 16a is opened on First terrace 161, and first, the step place that two step surfaces are joined is provided with sealing member 163, the shape of sealing member 163 and first, the step shape of two step surface junctions is consistent, and the second stripper 17 is connected with the second driving mechanism Q2, preferably scheme as shown in Figure 5, and first, the outline of two step surface junctions is arc, like this sealing member is set to arc, and sealing member can adopt O-ring seals.The second stripper 17 is regulated to rotate by the second driving mechanism Q2, make first and second discharge opening on first and second stripper corresponding and different, thus realize, to the quickly discharging material of extractor 10 and the closed of discharge opening, realizing quickly discharging material, thus save time, improve extraction efficiency.
In the present invention, first, second and third driving mechanism can adopt electronic formation, and certain first driving mechanism also can adopt cylinder to form, and the 3rd driving mechanism also can adopt setting operation handle to carry out manual regulation, and extractor 10 profile is cydariform or elliposoidal.
Further scheme is: be provided with ultrasound emission assembly or Microwave emission assembly in extractor 10, and ultrasound emission assembly or Microwave emission assembly can improve extraction efficiency and the extraction yield of plant actives, shortens the utilization ratio of cycle and raising raw material.Extractor 10 is arranged in frame 11, frame 11 comprises the feet 11 that four vertical shapes are arranged, the bottom of feet 11 is provided with gravity sensor 111, gravity sensor 111 can be measured the weight of whole extraction equipment in real time and be shown by indicating meter, such operator just accurately can learn the feeding quantity of each material in real time, thus realize feeding intake according to best material ratio.Stirring mechanism is included in the spaced agitator arm 152 of zigzag shape on stir shaft 151 axle body, paddle 153 is arranged on the end of agitator arm 152, it is axially 30 ~ 60 ° with the angle of stir shaft 151 axis for being articulated and connected and forming the jointed shaft that is articulated and connected between agitator arm 152 and paddle 153, paddle 153 increases gradually along the plate face width degree pointed near agitator arm 152 one end away from agitator arm 152 one end, such stirring mechanism can make the stirring of material more abundant, well can protect stirring mechanism simultaneously, stirring mechanism torsional deformation is caused when preventing solid materials from tangling, paddle 153 rotational angle on agitator arm 152 is not easily excessive, the angle of general rotation is 1 ~ 2 °.Extractor 10 inner-wall surface is provided with the flow-interfering bar of zigzag shape, the setting of flow-interfering bar is also the adequacy in order to realize material stirring.
Detailed scheme is: slide block 13 is that a long strip shape plate is formed, the two ends of slide block 13 are respectively arranged with hopper 14, the outside of two hoppers 14 arranges material respectively and adds mechanism, realize adding of various materials, the sidewall of extractor 10 is sandwich structure, the folder chamber that sandwich structure is formed, for holding hot-fluid, is incubated the material in extractor 10 or heats.
In a word, extraction natural pigment equipment provided by the invention, effectively can realize adding fast and unloading of material, realizes the high density rapid extraction of pigment in plant flower, improves the extraction efficiency of pigment.The present invention can be used for the extraction of pigment in the plant flowers such as rhododendron, Rose, peach blossom.
The above is only the preferred embodiment of the present invention; should be understood that; for those skilled in the art; to know in the present invention after contents; under the premise without departing from the principles of the invention; can also make some equal conversion to it and substitute, these convert on an equal basis and substitute and also should be considered as belonging to protection scope of the present invention.

Claims (6)

1. the equipment of a rapid extraction natural pigment from plant flower, it is characterized in that: comprise set gradually first of firsts and seconds extraction is carried out to plant flower, two extraction elements, to first, material in two extraction elements carries out first of solid-liquid separation respectively, two filtration units, for collecting the extracting solution storage tank of the filtrate of the first filtration devices, to the vacuum concentration equipment that extracting solution concentrates, and the extracting solution after concentrated is carried out to the spray drying unit of dry powder process, interchanger is provided with between vacuum concentration equipment and the first extraction element, heat transfer tube is provided with in extracting solution storage tank, the entrance of heat transfer tube is connected with the pneumatic outlet of vacuum concentration equipment, the outlet of heat transfer tube is connected with the hot-fluid import of interchanger, interchanger cold fluid inlet is connected with the outlet of extraction agent storage tank and the filtrate outlet of the second filtration unit, interchanger is cold, the outlet of hot-fluid and first, the extraction agent import of two extraction elements is connected, first, two extraction elements comprise extractor and horizontally disposed stir shaft, mount pad is respectively arranged with in the middle part of the both sides outer side wall that extractor is relative, stir shaft two ends are rotatably installed in mount pad, stir shaft is connected with the 3rd driving mechanism, the axle body that stir shaft is positioned at extractor is provided with stirring mechanism, the first adjusting part that the top of extractor is provided with dog-house and regulates the closure state of dog-house, the second adjusting part that the bottom of extractor is provided with discharge opening and regulates the closure state of discharge opening, second adjusting part comprises in extractor discharge opening place, under be arranged in parallel first of circle, two strippers, first stripper and extractor are fixed with one, the side of the second stripper offers ring groove, second stripper consists of to be rotatably assorted around vertical the steel ball assembly that arranges in ring groove and extractor and is connected, first, the center of circle of two strippers is positioned on same plummet, first, on two strippers, the circumference place of same radius size offers first respectively, two discharge openings, the lower face of the first stripper is arranged to by first, it is step-like that two step surface combinations are formed, the upper face of second step face and the second stripper fits, cavity is formed between First terrace and the second stripper upper face, first discharge opening is opened on First terrace, first, the step place that two step surfaces are joined is provided with sealing member, the shape of sealing member and first, the step shape of two step surface junctions is consistent, second stripper is connected with the second driving mechanism.
2. the equipment of rapid extraction natural pigment from plant flower according to claim 1, is characterized in that: be provided with Microwave emission assembly in extractor.
3. the equipment of rapid extraction natural pigment from plant flower according to claim 1, is characterized in that: extractor is arranged in frame, and frame comprises the feet that four vertical shapes are arranged, the bottom of feet is provided with gravity sensor.
4. the equipment of rapid extraction natural pigment from plant flower according to claim 1 or 2 or 3, it is characterized in that: stirring mechanism is included in the spaced agitator arm of zigzag shape on stir shaft axle body, paddle is arranged on the end of agitator arm, be axially 30 ~ 60 ° with the angle of stir shaft axis for being articulated and connected and forming the jointed shaft that is articulated and connected between agitator arm and paddle, paddle increases gradually along the plate face width degree pointed near agitator arm one end away from agitator arm one end.
5. the equipment of rapid extraction natural pigment from plant flower according to claim 4, is characterized in that: flow-interfering bar extractor inner-wall surface being provided with zigzag shape.
6. the equipment of rapid extraction natural pigment from plant flower according to claim 4, is characterized in that: the sidewall of extractor is sandwich structure.
CN201510427020.1A 2014-08-10 2015-07-18 The equipment of rapid extraction natural pigment from plant flower Expired - Fee Related CN105062122B (en)

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CN201510427020.1A CN105062122B (en) 2014-08-10 2015-07-18 The equipment of rapid extraction natural pigment from plant flower
CN201610490982.6A CN106178585B (en) 2014-08-10 2015-07-18 A kind of equipment for the rapidly extracting natural pigment from plant flower

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CN2014204486207 2014-08-10
CN201420448620 2014-08-10
CN201510427020.1A CN105062122B (en) 2014-08-10 2015-07-18 The equipment of rapid extraction natural pigment from plant flower

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CN201610490982.6A Expired - Fee Related CN106178585B (en) 2014-08-10 2015-07-18 A kind of equipment for the rapidly extracting natural pigment from plant flower

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张春雨: "黑糯玉米芯黑色素提取设备的设计", 《安徽科技学院学报》 *
郭书丛等: "新型天然色素提取设备――滑槽式浸出器", 《中国油脂》 *

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