CN105062123B - Equipment for quickly extracting azalea pigment - Google Patents

Equipment for quickly extracting azalea pigment Download PDF

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Publication number
CN105062123B
CN105062123B CN201510427041.3A CN201510427041A CN105062123B CN 105062123 B CN105062123 B CN 105062123B CN 201510427041 A CN201510427041 A CN 201510427041A CN 105062123 B CN105062123 B CN 105062123B
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extraction
heat exchanger
extracting solution
outlet
slide block
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CN105062123A (en
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林桂花
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Pizhou Huiteng Jingfa Construction Co ltd
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Individual
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Priority to CN201610512301.1A priority Critical patent/CN106147290B/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B61/00Dyes of natural origin prepared from natural sources, e.g. vegetable sources
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0096Purification; Precipitation; Filtration
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The invention relates to equipment for quickly extracting azalea pigment, which comprises a first extraction device, a second extraction device, a first filtering device, a second filtering device, an extracting solution storage tank, a decompression concentration device, a spray drying device and a heat exchanger which are sequentially arranged, wherein a heat exchange tube is arranged in the extracting solution storage tank, the inlet of the heat exchange tube is connected with the gas outlet of the decompression concentration device, the outlet of the heat exchange tube is connected with the hot fluid inlet of the heat exchanger, the cold fluid inlet of the heat exchanger is connected with the outlet of an extractant storage tank and the filtrate outlet of the second filtering device, and the outlets of the cold fluid and the hot fluid of the heat exchanger are connected with the extractant inlets of the. According to the technical scheme, heat energy of steam in the reduced pressure concentration device is recycled, the extracting solution and the extracting agent are preheated, and heat preservation/preheating and extraction agent heating before reduced pressure distillation of the extracting solution are realized, so that energy is saved, and production cost is reduced.

Description

The equipment of rapid extraction Rhododendron simsii Planch. pigment
Technical field
The present invention relates to nature strength field, be specifically related to a kind of rapid extraction Rhododendron simsii Planch. pigment Equipment.
Background technology
Extract field in natural activity component, often need to use extraction element to the root of natural plants, Stem, leaf extract so that the active component in herbaceous plant root, stem, leaf is dissolved in extractant In, thus realize the extraction to active component.Mostly there is the throwing of material in the extraction pot of existing use Add the problem loaded down with trivial details and time-consuming with discharging, have a strong impact on the production efficiency of natural activity component.Separately Outward, for the extraction of natural activity component, all there is an optimal material ratio (active under this material The extraction ratio of component and/or extraction efficiency are maximum), but feeding intake of extraction pot of tradition is difficult to accurately Control material ratio so that extraction ratio and/or extraction efficiency are unable to reach most preferably, have a strong impact on production Efficiency and cause wastage of material.
It addition, currently used active component extraction equipment generally to there is extraction ratio low, utilization of energy The problems such as rate is low, extracting cycle length.
Summary of the invention
It is an object of the invention to provide the equipment of a kind of rapid extraction Rhododendron simsii Planch. pigment, it can realize The rapid extraction of mapping mountain red pigment, and in extracting solution, the concentration of pigment is high, it is simple to follow-up concentration Purification process and the saving energy.
For achieving the above object, present invention employs techniques below scheme:
A kind of equipment of rapid extraction Rhododendron simsii Planch. pigment, it is characterised in that: include setting gradually is right Rhododendron simsii Planch. carries out first and second extraction element of firsts and seconds extraction, extracts dress to first and second Put interior material and carry out first and second defecator of solid-liquid separation respectively, for collecting the first filtration The extracting solution storage tank of the filtrate that device filters, the vacuum concentration equipment that extracting solution is concentrated, with And the extracting solution after concentrating is dried the spray-drying installation of powder process, vacuum concentration equipment and the It is provided with heat exchanger between one extraction element, in extracting solution storage tank, is provided with heat exchanger tube, heat exchanger tube Entrance is connected with the gas outlet of vacuum concentration equipment, the outlet of heat exchanger tube and the hot-fluid of heat exchanger Body import is connected, and heat exchanger cold fluid inlet filters dress with the outlet and second of extractant storage tank The filtrate (liquid put is connected, the outlet of heat exchanger cold and hot fluid and first and second extraction element Extractant import is connected, and first and second extraction element includes extraction pot and horizontally disposed stirring Axle, is respectively arranged with mounting seat in the middle part of the lateral wall, both sides that extraction pot is relative, shaft two ends rotate Being arranged in mounting seat, shaft and the 3rd drive mechanism are connected, and shaft is positioned at extraction pot Axle body on be provided with rabbling mechanism, the top of extraction pot is provided with dog-house and to dog-house The first adjusting part that closure state is adjusted, the bottom of extraction pot is provided with discharge port and right The second adjusting part that the closure state of discharge port is adjusted, the first adjusting part include opening to On the slide rail that constitutes of grooved part, vacancy portion that grooved part bottom land is offered constitutes dog-house, slide rail edge Horizontal direction is arranged, slide rail is provided with slide block, and slide block is constituted along the length direction of slide rail with slide rail Slide-and-guide connects and coordinates, and the bottom surface of slide block fits with the bottom land of grooved part, slide block is provided with The hopper that vertical shape is arranged, slide block offers into opening shape with the junction of feed hopper bottom material mouth, slide block and First drive mechanism is connected.
Further scheme is: being provided with ultrasound emission assembly in extraction pot, extraction pot is arranged on machine On frame, frame includes the spike that four vertical shapes are arranged, the bottom of a spike is provided with gravity sensitive Device.Rabbling mechanism is included in the spaced puddler of zigzag shape, paddle on shaft axle body It is arranged on the end of puddler, is articulated and connected for being articulated and connected and constituting between puddler and paddle Axially the most axial with the shaft angle of jointed shaft be 30~60 °, paddle edge is away from puddler one The plate face width degree that end points near puddler one end is gradually increased.It is provided with spiral shell on extraction pot internal face The flow-interfering bar of spin line shape.
Detailed scheme is: slide block is that a strip plate is constituted, and the two ends of slide block are respectively arranged with Hopper, the outside of two hoppers is respectively provided with material and adds mechanism.Second adjusting part includes a level The flashboard arranged, flashboard and driving its feed screw nut's adjusting part moved in the horizontal direction or cylinder Piston rod be connected.The sidewall of extraction pot is sandwich.
In technique scheme, the heat energy of steam in vacuum concentration equipment is recycled, right Extracting solution and extractant preheat, it is achieved the insulation before extracting solution decompression distillation/preheat and heat Extractant, thus save the energy, reduce production cost.Meanwhile, two-stage is used to extract, can be effective Shorten extracting cycle, save the energy and improve the throughput rate of pigment.Obtain when extracting due to two grades Extracting solution in pigment concentration relatively low, therefore will filter the filtrate after separating as extracting for the first time Extractant, thus improve the concentration of pigment in extracting solution, it is simple to follow-up distillation and concentration processes.Separately Outward, extraction element is moved by the first drive mechanism adjusting slider so that the sky on slide block The portion of lacking is corresponding with the charge door on slide rail and different, thus realization to the rapid loading of extraction pot with The Guan Bi of charge door, simultaneously when extracting, operator, can be by charging device to material Bucket adds the inventory that next batch needs to add, so there is no need to complete to extract at extraction pot After operation, weighing adds again, thus saves the time, improves extraction efficiency.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention;
Fig. 2 is the structural representation of first and second extraction element;
Fig. 3 is enlarged diagram at the A of Fig. 2;
Fig. 4 is the assembling schematic diagram of slide rail, slide block, hopper;
Fig. 5 is the upward view of the first stripper.
Detailed description of the invention
In order to make objects and advantages of the present invention clearer, below in conjunction with embodiment to this Bright it is specifically described.Should be appreciated that following word is only in order to describe the one of the present invention or several Planting specific embodiment, the protection domain of not concrete to present invention request carries out considered critical.
Technical scheme that the present invention takes is as it is shown in figure 1, the setting of a kind of rapid extraction Rhododendron simsii Planch. pigment Standby, first and second extraction dress of firsts and seconds extraction is carried out including the mapping mountain Flos Carthami set gradually Put A11, A12, the material in first and second extraction element A11, A12 is carried out solid-liquid respectively and divides From first and second defecator A21, A22, for collect first defecator A21 filter filter The extracting solution storage tank A3 of liquid, the vacuum concentration equipment A4 that extracting solution is concentrated, and to dense Extracting solution after contracting is dried the spray-drying installation A5 of powder process, vacuum concentration equipment A4 and It is provided with heat exchanger A6 between one extraction element A11, in extracting solution storage tank A3, is provided with heat exchanger tube, The entrance of heat exchanger tube is connected with the gas outlet of vacuum concentration equipment A4, the outlet of heat exchanger tube with The hot fluid import of heat exchanger A6 is connected, heat exchanger A6 cold fluid inlet and extractant storage tank A3 Outlet and the filtrate (liquid of the second defecator A22 be connected, the hot and cold stream of heat exchanger A6 The outlet of body is connected with the extractant import of first and second extraction element A11, A12.Above-mentioned skill In art scheme, the heat energy of steam in vacuum concentration equipment A4 is recycled, to extracting solution Preheat with extractant, it is achieved the insulation/preheating before extracting solution decompression distillation and heating extraction agent, Thus save the energy, reduce production cost.Meanwhile, use two-stage to extract, can effectively shorten extraction In the cycle, save the energy and improve the throughput rate of pigment.Due to two grades of extracting solution obtained when extracting Middle pigment concentration is relatively low, therefore will filter the extractant as extraction for the first time of the filtrate after separating, Thus improving the concentration of pigment in extracting solution, it is simple to follow-up distillation and concentration processes.Defecator, Vacuum concentration equipment, spray-drying installation, heat exchanger all can use use in existing chemical industry to have The device of corresponding function uses, and extracting solution storage tank uses general solution reservoir transformation to obtain, Installing tubulation shape or spiral helicine heat exchanger tube in storage tank, the solid material between neighboring devices uses defeated Sending band to carry, liquid material uses pipeline and delivery pump conveying.
First and second extraction element A11, A12 includes extraction pot 10 and horizontally disposed shaft 151, it is respectively arranged with mounting seat, shaft 151 in the middle part of the lateral wall, both sides that extraction pot 10 is relative Two ends are rotatably installed in mounting seat, and shaft 151 is connected with the 3rd drive mechanism Q3, stirs Mix axle 151 to be positioned on the axle body of extraction pot 10 and be provided with rabbling mechanism, the top of extraction pot 10 It is provided with dog-house and the first adjusting part that the closure state to dog-house is adjusted, extracts The second tune that the bottom of tank 10 is provided with discharge port and the closure state to discharge port is adjusted Joint assembly, first and second adjusting part can be extraction pot 10 top or the horizontal cloth of bottom setting The flashboard put is constituted, and flashboard can manually regulate, it is also possible to by flashboard with drive it along level Feed screw nut's adjusting part or the piston rod of cylinder that direction is moved are connected, and utilize electronic or gas Dynamic regulation.It should be noted that in the present invention, for the ease of the present invention briefly, is clearly described The scope being claimed, therefore, not to there is the sealing at extractant leakage on extraction pot 10 Being described, this is also that the common knowledge that those of ordinary skill in the art are understood is grasped with conventional certainly Make means.
In the present invention, it is preferred to use following scheme, as shown in Figure 2,4, the first adjusting part The slide rail 12 constituted including the grooved part of opening upwards, the vacancy portion that grooved part bottom land is offered is constituted throws Material mouth, slide rail 12 arranges in the horizontal direction, and slide rail 12 is provided with slide block 13, slide block 13 with Slide rail 12 constitutes slide-and-guide connection cooperation, the bottom surface of slide block 13 along the length direction of slide rail 12 Fit with the bottom land of grooved part, slide block 13 is provided with the hopper 14 that vertical shape is arranged, slide block 13 With expect bottom hopper 14 that opening shape, slide block 13 and the first drive mechanism Q1 are offered in the junction of mouth It is connected.Moved by the first drive mechanism adjusting slider 13 so that the sky on slide block 13 The portion of lacking is corresponding with the charge door on slide rail 12 and different, thus quick to extraction pot 10 of realization Charging and the Guan Bi of charge door, simultaneously when extracting, operator, can be by feeding intake dress Put in hopper 14, add the inventory that next batch needs to add, so there is no need to extracting Tank 10 complete to extract operation after again weighing add, thus save the time, improve raw material extraction efficiency.
Preferably implementing according to scheme as shown in Figure 2,3, the second adjusting part includes extraction pot The upper and lower first and second circular stripper 16,17 being arranged in parallel at 10 discharge ports, first unloads Flitch 16 is fixed with one with extraction pot 10, and the side of the second stripper 17 offers annular Groove, the second stripper 17 passes through the interior steel ball assembly 18 arranged of cannelure with extraction pot 10 around lead Vertical direction constitutes the connection that is rotatably assorted, and the center of circle of first and second stripper 16,17 is positioned at same lead On vertical line, first and second stripper is offered at the circumference of same radius size first and second respectively and unloads Material mouth 16a, 17a, the lower face of the first stripper 16 be arranged to by first and second step surface 161, It is step-like that 162 combinations are constituted, and second step face 162 is affixed with the upper face of the second stripper 17 Close, between First terrace 161 and the second stripper 17 upper face, form cavity, the first discharging Mouth 16a is opened on First terrace 161, is provided with at the step that first and second step surface is joined The step shape one of sealing member 163, the shape of sealing member 163 and first and second step surface junction Causing, the second stripper 17 is connected with the second drive mechanism Q2, scheme the most as shown in Figure 5, The outline of first and second step surface junction is arc, so sealing member is set to arc, close Sealing can use O-ring seals.Regulate the second stripper 17 by the second drive mechanism Q2 to carry out Rotate so that first and second discharge port on first and second stripper is corresponding and different, thus real Now quickly discharging material and the Guan Bi of discharge port to extraction pot 10, it is achieved quickly discharging material, thus save Time, improve extraction efficiency.
In the present invention, first, second and third drive mechanism can use electronic composition, and certain first drives machine Structure also can use cylinder to constitute, and the 3rd drive mechanism may be used without arranging operating handle and manually adjusts Joint, extraction pot 10 profile is cydariform or elliposoidal.
Further scheme is: be provided with ultrasound emission assembly or Microwave emission in extraction pot 10 Assembly, ultrasound emission assembly or Microwave emission assembly can improve the extraction effect of plant actives Rate and extraction ratio, shorten the cycle and improve the utilization rate of raw material.Extraction pot 10 is arranged on frame 11 On, frame 11 includes the spike 11 that four vertical shapes are arranged, the bottom of a spike 11 is provided with weight Force transducer 111, gravity sensor 111 can be measured the weight of whole extraction equipment in real time and lead to Crossing display to show, such operator just can the most accurately learn the feeding quantity of each material, Thus realize feeding intake according to optimal material ratio.Rabbling mechanism is included on shaft 151 axle body The spaced puddler of zigzag shape 152, paddle 153 is arranged on the end of puddler 152, For being articulated and connected and to constitute the jointed shaft being articulated and connected axial between puddler 152 and paddle 153 The angle axial with shaft 151 is 30~60 °, and paddle 153 is along away from puddler 152 1 The plate face width degree that end points near puddler 152 one end is gradually increased, and such rabbling mechanism is permissible The stirring making material is more abundant, can well protect rabbling mechanism simultaneously, prevent Solid material causes rabbling mechanism torsional deformation when tangling, and paddle 153 turns on puddler 152 Dynamic angle is difficult to excessive, and the general angle rotated is 1~2 °.Arrange on extraction pot 10 internal face There is the flow-interfering bar of zigzag shape, arranging also for the adequacy realizing material stirring of flow-interfering bar.
Detailed scheme is: slide block 13 is that a strip plate is constituted, and the two ends of slide block 13 are respectively Being provided with hopper 14, the outside of two hoppers 14 is respectively provided with material and adds mechanism, it is achieved multiple thing Adding of material, the sidewall of extraction pot 10 is sandwich, and the folder chamber that sandwich is formed is used for holding Receive hot fluid, the material in extraction pot 10 is incubated or heats.
In a word, the extraction equipment that the present invention provides, can effectively realize quickly adding and unloading of material, Realize the high concentration rapid extraction of Rhododendron simsii Planch. pigment, improve the extraction efficiency of Rhododendron simsii Planch. pigment.
The above is only the preferred embodiment of the present invention, it is noted that for the art Those of ordinary skill for, after knowing content described in the present invention, former without departing from the present invention On the premise of reason, it is also possible to it is made some equal conversion and replacement, these convert on an equal basis and replace In generation, also should be regarded as belonging to protection scope of the present invention.

Claims (3)

1. the equipment of a rapid extraction Rhododendron simsii Planch. pigment, it is characterised in that: include setting gradually Mapping mountain Flos Carthami carry out first and second extraction element of firsts and seconds extraction, carry first and second Fetching is put interior material and is carried out first and second defecator of solid-liquid separation respectively, for collection first The extracting solution storage tank of the filtrate that defecator filters, the concentrating under reduced pressure concentrating extracting solution fills Putting, and the extracting solution after concentrating is dried the spray-drying installation of powder process, concentrating under reduced pressure fills Put and be provided with heat exchanger between the first extraction element, be provided with heat exchanger tube in extracting solution storage tank, change The entrance of heat pipe is connected with the gas outlet of vacuum concentration equipment, the outlet of heat exchanger tube and heat exchanger Hot fluid import be connected, the outlet and second of heat exchanger cold fluid inlet and extractant storage tank The filtrate (liquid of defecator is connected, the outlet of heat exchanger cold flow body and carrying of the first extraction element Take agent import to be connected, the outlet of exchanger heat fluid and the extractant import phase of the second extraction element Connecting, first and second extraction element includes extraction pot and horizontally disposed shaft, extraction pot phase To lateral wall, both sides in the middle part of be respectively arranged with mounting seat, shaft two ends are rotatably installed in mounting seat In, shaft is connected with drive mechanism B, and shaft is positioned on the axle body of extraction pot and is provided with Rabbling mechanism, the top of extraction pot is provided with dog-house and adjusts the closure state of dog-house First adjusting part of joint, the bottom of extraction pot is provided with discharge port and the closed form to discharge port The second adjusting part that state is adjusted, the first adjusting part includes that the grooved part of opening upwards is constituted Slide rail, vacancy portion that grooved part bottom land is offered constitutes dog-house, and slide rail is arranged in the horizontal direction, Being provided with slide block on slide rail, slide block and slide rail constitute slide-and-guide along the length direction of slide rail and are connected and join Closing, the bottom surface of slide block fits with the bottom land of grooved part, and slide block is provided with the hopper that vertical shape is arranged, Slide block offers into opening shape with the junction of feed hopper bottom material mouth, and slide block is connected with drive mechanism A.
The equipment of rapid extraction Rhododendron simsii Planch. pigment the most according to claim 1, it is characterised in that: Ultrasound emission assembly it is provided with in extraction pot.
The equipment of rapid extraction Rhododendron simsii Planch. pigment the most according to claim 1, it is characterised in that: Extraction pot is arranged in frame, and frame includes the spike that four vertical shapes are arranged, the bottom of a spike It is provided with gravity sensor.
CN201510427041.3A 2014-08-10 2015-07-18 Equipment for quickly extracting azalea pigment Active CN105062123B (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN201610512301.1A CN106147290B (en) 2014-08-10 2015-07-18 A kind of equipment for rapid extraction azalea pigment
CN201510427041.3A CN105062123B (en) 2014-08-10 2015-07-18 Equipment for quickly extracting azalea pigment

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN2014204486194 2014-08-10
CN201420448619 2014-08-10
CN201510427041.3A CN105062123B (en) 2014-08-10 2015-07-18 Equipment for quickly extracting azalea pigment

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CN105062123B true CN105062123B (en) 2017-01-04

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CN105062123A (en) 2015-11-18
CN106147290A (en) 2016-11-23

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