CN1172808A - Process for producing starch, isoflavone and kudzu root beverage by using kudzu root - Google Patents
Process for producing starch, isoflavone and kudzu root beverage by using kudzu root Download PDFInfo
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- CN1172808A CN1172808A CN 97107371 CN97107371A CN1172808A CN 1172808 A CN1172808 A CN 1172808A CN 97107371 CN97107371 CN 97107371 CN 97107371 A CN97107371 A CN 97107371A CN 1172808 A CN1172808 A CN 1172808A
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- root
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- kudzu root
- kudzu vine
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- 229920002472 Starch Polymers 0.000 title claims abstract description 33
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- 239000008107 starch Substances 0.000 title claims abstract description 33
- 235000013361 beverage Nutrition 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims abstract description 13
- 241000219781 Pueraria montana var. lobata Species 0.000 title claims abstract 10
- CJWQYWQDLBZGPD-UHFFFAOYSA-N isoflavone Natural products C1=C(OC)C(OC)=CC(OC)=C1C1=COC2=C(C=CC(C)(C)O3)C3=C(OC)C=C2C1=O CJWQYWQDLBZGPD-UHFFFAOYSA-N 0.000 title description 2
- 235000008696 isoflavones Nutrition 0.000 title description 2
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- Non-Alcoholic Beverages (AREA)
Abstract
The invention provides a process method for jointly producing kudzu root starch, kudzu root isoflavone derivatives and kudzu root (whole) beverage by kudzu root. Compared with the prior art, the process method is advanced and different in that the process method is not as difficult to implement in the prior art and has effective technical means. The method has the advantages of reliability, practicability, mild process conditions, no causticity on equipment, high product quality, short production period, low production cost, and capability of saving a large amount of water, power and steam consumption, and realizing 'three-free' (no waste gas, no waste water and no waste residue) production and no environmental pollution by utilizing all the raw materials of the kudzuvine root. The economic benefit, the social benefit and the ecological environment protection are better than those of the prior art.
Description
The root of kudzu vine is the root of a kind of pulse family (Leguminosae) plant elegant jessamine [Pueraria Lobata (Wild) Chwi].Medicinal from ancient times, the successive dynasties medical book has and carries.Classify middle product in the Shennong's Herbal as." the hot flavor of property is sweet peppery.Go into lung, stomach two warps.The function expelling pathogenic factors from muscles for reducing heat, promote the production of body fluid to quench thirst.Thirsty in order to control, headache, stiff nape and back, table such as febrile disease with symptoms such as convulsion, opisthotonos, trismus, etc., pest malaria and relieving alcoholism disease." " pharmacognosy " of publishing before the sixties only be loaded with " starch-containing 8-16%, main part not quite clear " to the root of kudzu vine.
Along with to the deepening continuously of root of kudzu vine pharmacological research, find that also the main pharmacodynamics composition of the proof root of kudzu vine is the osajin derivative afterwards, be commonly referred to Radix Puerariae total flavones.Radix Puerariae total flavones has the hat of expansion, increases the effect of crown arteries and veins flow and reduction myocardial consumption of oxygen.And from the root of kudzu vine purify out big legumin (Daidyein), Daidzin (Daidyin), puerarin (Puerarin), root of kudzu vine glucoside (Sylopuerarin) and osajin derivatives such as big legumin-4,7-glucosulfone of extraction separation, further determined the general formula of molecular structure of Radix Puerariae isoflavone derivative:
Big legumin has spasmolysis like the Papaverine.The diseases such as headache that all have slow bright hypertension to cause of Daidzin, puerarin and big legumin.
| The compound title | Substituting group |
| Big legumin | 7.4′-＝OH |
| Daidzin | 4 '-OH, 7-O-glucose |
| Puerarin | 7.4 '-OH, 9-C-glucose |
| Root of kudzu vine glucoside | 8-C-glucose, the wooden sugar of D-(no-fix) |
Since the achievement of Japanese's announcement, started one pueraria starch heat in countries and regions such as Japan, the U.S., South East Asia, Hong Kong to the development research of pueraria starch.Sing the praises of and be " preventing and curing diseases ", antidotal good health and a long life powder "; also there are " kudzuvine root starch and manufacture craft thereof " (CN1093877.4; 93104516.9) and " kudzu root beverage and production method thereof " (CN1087795A; 9211758.2), " pueraria root series health drink and production method thereof " (CN1109301A; 94110898.8) in China; and the delivering of " root of kudzu vine effective ingredient extract and its production and use " patented technologies such as (CN108287A, 91110602.2).
Behind author's experimental study, find the manufacture craft of above-mentioned patent, all exist separately in implementing all difficulties and to the problems such as severe contamination of environment:
Desanding impurity elimination technology in CN1093877A, what use is that outmoded water repeatedly is towards muddy numerous and diverse technology, only got towards muddy powder slurry middle level and made high-quality starch, most starch and silt particle, impurity are mixed together, demote in the waster, and high-quality powder rate is too low, production cycle long (reaching 120-230hrs), the production cost height, the waste residue that produces in the production and a large amount of waste water do not deal with serious environment pollution.
And the production method of kudzu root beverages such as CN1087795A and CN11090301A has also only been used pressed juice and partial starch, and the waste residue after producing starch and squeezing the juice and a large amount of waste water do not deal with, with same contaminate environment.
In the patent of " root of kudzu vine effective ingredient extract and its production and use ", select for use in the preparation were established method, the root of kudzu vine is contained the ignorance of the problems such as starch higher more than hundred times than effective component, employing adds poach lixiviate taking technique, when efficacy component boils leaching, a large amount of impurity also is dissolved (as protein, tannin, phlegmatic temperament etc.) and by gelatinization (as starch), not only hinder the stripping of effective ingredient, bring all difficulties also for following each step: at first be leach liquor and gelatinization go out soak the slag separation difficulty; Secondly contain a large amount of foam material (protein, phlegmatic temperament) in the leach liquor, cause the concentrating under reduced pressure difficulty; The colloid pin mud of the alcohol precipitation of enriched material is bulky, and clear liquid is few, and yield is too low, and cost is higher.The same with above-mentioned each patent, the starch pasting that produces in producing is soaked slag and colloid pin mud does not deal with and contaminate environment.
The present invention proposes a kind of with root of kudzu vine combination producing starch, the processing method of isoflavones, beverage, and its technical scheme is as follows:
1, at first from the root of kudzu vine, isolates and produces pueraria starch;
2, the cold soaking process of root of kudzu vine efficacy component has also begun when washing root of kudzu vine dry plate powder and water (allocate quantitative antioxidant into and transfer PH to 8-9) the broken root of kudzu vine of flushing wet-milling, and in washing powder repeatedly and washing the concentration of its effective component of enrichment.
3, wash the powder rushed out after 100 mesh sieves, 200 mesh sieve secondaries screen out the fiber foreign material, remove silt particle, reenter whizzer and throw away a large amount of powder water and floating impurities washed at powerful swirling flow sand setting bucket.
4, take out powder, rinsing starch in whizzer, through in control detect qualified after, drying, drying detects qualified packing and is the pueraria starch product.
5, reach the centrifugal clarification water of shunting behind the certain density root of kudzu vine efficacy component, after filtration, go into macroporous resin/polyamides resin column and adsorb, water does not only have the flavones reaction after the absorption of emitting.The water some is returned the starch workshop for washing powder usefulness after the absorption of this no flavones reaction, and a part is used for making saturated carbon sour water filled drink.
6, carry out wash-out with an amount of alcohol, vacuum concentration, recovered alcohol with few alcohol alcohol precipitation, refining true dried recovered alcohol, promptly gets root of kudzu vine mixing isoflavone derivative product again.
7, all waste residue and filter cake mud come out (wherein most of is starch) through the content that the cellulase hydrolysis allows all contain in fiber, add the liquefaction of BF-7658 system again and add As3883 under certain acidity and temperature; Carry out saccharification.
By this saccharification liquid, with addition of an amount of sweeting agent, acidic flavoring agent and self-control spices the base-material of water quality beverage bed material syrup or solid beverage.
Embodiment one
(1) pueraria starch
Getting Yunnan dries root of kudzu vine sheet 50g (starch content～50%) and washes decortication (washing lotion clarification by rubbing with the hands with Wingdale, filter standby), again in bath (in the water with addition of an amount of antioxidant, and regulate acidity PH8-9 with saturated lime clear water, carry out wet-milling broken (granulated slag granularity 0.2～0.5mm) and washery slag secondary down together), filter with 100 mesh sieves, merging filtrate filters once with 200 mesh sieves at every turn.Powder is starched in the bomb, with certain pressure (2～3kg/cm
2) pressurized air, the powder slurry is pressed in the swirling flow sand-settling device, the powder slurry that proportion is lighter is gone up whirlpool and is overflowed, and powder is starched in the whizzer behind the separation silt particle, and centrifugal 5-10min, decant go out supernatant liquid and floating impurity.The powder that washes with water at the bottom of the bottle outlet is gone into evaporating dish, leaves standstill clarification after the stirring, and decant goes out clear liquid, adds water again and carries out rinsing repeatedly, and till the no flavones reaction, it is standby to collect centrifugate and rinse water in wash water.
Drain the water that steams in the ware, powder is scraped into watch-glass, under the sun, dry till the water content about 14%.Must do pueraria starch 23.8g.Starch is pure white glossy, free from extraneous odour, sand tooth not, foreign material such as no root of kudzu vine fiber.
(2) Radix Puerariae total flavones
Merge centrifugate, rinse water, go into macroporous resin column after the filtration, be adsorbed onto repeatedly in the liquid of back and can not detect till the flavones, collect liquid after the suction that no flavones reacts, standby.
With EtOH wash-out when absorption (elution order with opposite), be eluted in the solution of wash-out no flavones instead till.Collect elutriant.Reclaim EtOH at 60 ℃ of following concentrating under reduced pressure and end, add 95%EtOH and make concentrated solution contain EtOH to reach about 80%, cool off standing over night to the AIC. flavor.Decant filter washes in the furnace pot, vacuum-drying (reclaiming EtOH) the yellow dried piece of 0.12g, press a little press powder, flavones content 95%.
(3) Pueraria lobota (entirely) root beverage
1, will not have liquid after the absorption of flavones reaction, regulate acidity to about the PH5, join in the waste residue and filter mud behind the production starch with rare HCL, stir the retaining boil 10min after, be cooled to 55-60 ℃, add cellulase (AS32876) and produce nutrient solution 20ml, be incubated 55 ℃ of 48Hrs, transfer PH6 with liming afterwards, be warmed up to 95 ℃, add BF-7658, produce 5ml, keep 90 ℃ of 20min, the no Lan Sezhi of iodine inspection.Cool to 65 ℃ again, add Fructus Hordei Germinatus and wheat bran (starch weighs 1.5%) leach liquor and keep 60 ℃ of 3hrs, the acid adjustment degree is to PH5 again, add As3849 and produce nutrient solution 10ml, be incubated 55 ℃ of 3hrs, till survey DE value reaches more than 90%, heat up and boiling 10-15min, liquid glucose is collected in the enzyme heat of going out filter.
2, back liquid is inhaled in no flavones reaction, transfers pH value to neutral with acid, the agent of self-control functional fragrance.
3, by the DE value of saccharification liquid, the specification that bed material syrup amount of preparation and every bottle of (250ml) syrup amount and finished drink require: pol and total sugariness, acidity and wait calculate each material should the amount of getting.Above-mentioned each thing that is metered into all dissolves, boils, filters, is cooled to 30-40 ℃ in ingredients pot except that spices, the time add spices again, stir cool to room temperature, the bed material syrup, standby.
4, liquid after the suction of no flavones reaction through disinfection, is freezingly gone into the carbonating mixing tank to 8-10 ℃ and made the saturated carbon sour water, and is standby.
5, bed material syrup branch is packed in the bottle, pours into the saturated carbon sour water again, the capping decals, Pueraria lobota (entirely) the root refreshment drink of the sweet acidity of regulation.
Beverage appearance, natural faint yellow, clear, nice and cool delicate fragrance, sour and sweet palatability.
This beverage is burnt and inflammation to chronic pharyngitis and the excessive throat that causes of tobacco and wine, has than Herba Pileae Scriptae, the not bad sensation of watermelon crystal.
Embodiment two
(1) root of kudzu vine material that forms sediment: get Yunnan and dry root of kudzu vine sheet 50g (starch-containing 50%), washing decortication (the washing lotion clarification is filtered, and is standby) by rubbing with the hands with Wingdale, to carry out wet-milling again under washing by water broken.Washery slag 2 times is washed the back filter wash at every turn and is crossed 100 mesh sieves, merges filter pulp with 200 mesh sieve filter washes once, the powder slurry, washes powder with water and goes into furnace pot after the centrifugal impurity elimination through the swirling flow sand setting, leave standstill clarification after the stirring, be rinsed into repeatedly in the wash water till the reaction of no flavones, collect centrifugate, rinse water.
Drain furnace pot, scrape, dry under the sunlight till the starch moisture about 14% into watch-glass.
Pueraria starch 24g, pure white glossy, free from extraneous odour, sand tooth not, no root of kudzu vine fiber and foreign material.
(2) Radix Puerariae flavone
Collect all centrifugate and rinse water, be filtered into polyamide resin column, being adsorbed onto absorption back outflow water does not repeatedly have till the flavones reaction.Collect water after the suction of no flavones reaction, another mistake is to being eluted to repeatedly with EtOH till no flavones reacts in the wash-out effluent liquid.Collect elutriant, reclaim EtOH to no AIC flavor at 60 ℃ of following concentrating under reduced pressure, adding EtOH95% makes concentrated solution contain EtOH to reach about 80%, liquid was left standstill in cooling, the decant filter wash is gone in the furnace pot, and vacuum-drying (reclaiming EtOH) gets yellow dry substance 0.12g, press slightly press thin yellow powder, general flavone content 96.7%.
(3) Pueraria lobota (entirely) root beverage
1, back liquid is inhaled in the no flavones reaction of collecting to be transferred about PH5 with HCI, getting a part joins in waste residue and the filter cake mud, 10min is boiled in stirring, be cooled to 55-60 ℃, add As382876 and produce nutrient solution 20ml, keep 55 ℃ of 48hrs. to transfer PH6, heat up 95 ℃, add BF-7658 and produce liquid 5ml with liming, keep 90 ℃ of 20min, the no blue look of iodine inspection cools to 65 ℃, adds Fructus Hordei Germinatus wheat bran leach liquor (the same), keep 60 ℃ of 3hrs, the acid adjustment degree adds As3849 nutrient solution 10ml to PH5 again, be incubated 55 ℃ and surveys DE values 95%, heats up to boil the 10-15min enzyme heat of going out and filter collection saccharification liquid.
2, self-control functional fragrance agent.
3, by saccharification liquid DE value, the sugariness and the acidity of bed material syrup amount of preparation and every bottle of (250ml) syrup amount and finished product beverage regulation, pol etc. calculate each material of preparation bed material syrup and answer add-on.Above-mentioned metering should add each inventory, except that spices, all go into to dissolve in the ingredients pot and boil, heat filter, be cooled to add about 35 ℃ spices stir cool to room temperature the bed material syrup of water quality chafing dish beverage.This beverage has goodish alleviation sensation to the inflammation of dry of chafing dish.
Claims (6)
1, with the root of kudzu vine combination producing pueraria starch root of kudzu vine, the Radix Puerariae isoflavone analog derivative, the processing method of Pueraria lobota (entirely) root beverage contains:
2, produce the swirling flow sand setting of pueraria starch, the processing method of centrifugation floating impurity;
3, washing out the cold soaking leaching process that begins root of kudzu vine efficacy component with wet-milling is broken when flushing out starch, the backspace of centrifugal impurity elimination recycle-water go as wash-down water repeatedly in, the invention thinking and the processing method of the concentration of its efficacy component of enrichment.
4, allocate 0.5-1 ‰ S-WAT in the wash-down water into, and regulate acidity to PH8-9 with saturated limewater;
5, a large amount of root of kudzu vine effective component solution adopts macroporous resin/polymeric amide fat adsorption treatment.The water backspace of collecting the no flavones reaction in absorption back go to wash powder with outside, a part is for making beverage usefulness.
6, contain the waste residue of pueraria starch and sift out filter residue, add after the suction of no flavones reaction after the stirring and adjusting, boil mattress extremely, postcooling 55-60 ℃ adds fiber, regulate acidity to PH6 after the plain enzyme AS33876 hydrolysis treatment, be warmed up to 95 ℃ and liquefy with BF-7859, the no blue look of iodine inspection cools to 65 ℃ of acid adjustment degree and carries out the saccharification processing to PH5 with head mold A3849, to surveying DE value＞more than 90%, heat filter is boiled in intensification, collects saccharification liquid, as the invention thinking and the processing method of the base-material of Pueraria lobota (entirely) root beverage.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97107371 CN1172808A (en) | 1997-02-27 | 1997-02-27 | Process for producing starch, isoflavone and kudzu root beverage by using kudzu root |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97107371 CN1172808A (en) | 1997-02-27 | 1997-02-27 | Process for producing starch, isoflavone and kudzu root beverage by using kudzu root |
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| Publication Number | Publication Date |
|---|---|
| CN1172808A true CN1172808A (en) | 1998-02-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 97107371 Pending CN1172808A (en) | 1997-02-27 | 1997-02-27 | Process for producing starch, isoflavone and kudzu root beverage by using kudzu root |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100448369C (en) * | 2006-04-11 | 2009-01-07 | 华南农业大学 | Production method of kudzu vine root powder sheet jelly riched-in flavone kind material |
| CN103462166A (en) * | 2013-09-29 | 2013-12-25 | 湖北黄仙洞葛业食品有限公司 | Pueraria flavones functional drink and preparation method thereof |
| CN103478838A (en) * | 2013-09-25 | 2014-01-01 | 湖北省宏源药业有限公司 | Honeysuckle kudzuvine root beverage and preparation method thereof |
| CN104041771A (en) * | 2014-06-23 | 2014-09-17 | 曾世均 | Processing method for comprehensively utilizing kudzu vine root |
| CN104208921A (en) * | 2013-11-27 | 2014-12-17 | 俞勤 | Kudzu vine root powder slurry sedimentation basin with two-step decomposition unit |
| CN105056570A (en) * | 2014-08-10 | 2015-11-18 | 胡刘满 | System for rapidly extracting flavone from rhododendron simsii planch leaves |
| CN106032391A (en) * | 2015-03-17 | 2016-10-19 | 信阳思源食品科技有限公司 | Water-saving method for extracting acorn starch |
| CN108477298A (en) * | 2018-01-29 | 2018-09-04 | 长沙爱扬医药科技有限公司 | A kind of kudzu-vine root powder product rich in small peptide |
-
1997
- 1997-02-27 CN CN 97107371 patent/CN1172808A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100448369C (en) * | 2006-04-11 | 2009-01-07 | 华南农业大学 | Production method of kudzu vine root powder sheet jelly riched-in flavone kind material |
| CN103478838A (en) * | 2013-09-25 | 2014-01-01 | 湖北省宏源药业有限公司 | Honeysuckle kudzuvine root beverage and preparation method thereof |
| CN103478838B (en) * | 2013-09-25 | 2014-12-03 | 湖北省宏源药业有限公司 | Honeysuckle kudzuvine root beverage and preparation method thereof |
| CN103462166A (en) * | 2013-09-29 | 2013-12-25 | 湖北黄仙洞葛业食品有限公司 | Pueraria flavones functional drink and preparation method thereof |
| CN103462166B (en) * | 2013-09-29 | 2015-03-11 | 湖北黄仙洞葛业食品有限公司 | Pueraria flavones functional drink and preparation method thereof |
| CN104208921A (en) * | 2013-11-27 | 2014-12-17 | 俞勤 | Kudzu vine root powder slurry sedimentation basin with two-step decomposition unit |
| CN104041771A (en) * | 2014-06-23 | 2014-09-17 | 曾世均 | Processing method for comprehensively utilizing kudzu vine root |
| CN104041771B (en) * | 2014-06-23 | 2016-05-18 | 曾世均 | A kind of processing method of root of kudzu vine comprehensive utilization |
| CN105056570A (en) * | 2014-08-10 | 2015-11-18 | 胡刘满 | System for rapidly extracting flavone from rhododendron simsii planch leaves |
| CN106032391A (en) * | 2015-03-17 | 2016-10-19 | 信阳思源食品科技有限公司 | Water-saving method for extracting acorn starch |
| CN108477298A (en) * | 2018-01-29 | 2018-09-04 | 长沙爱扬医药科技有限公司 | A kind of kudzu-vine root powder product rich in small peptide |
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