CN103478838A - Honeysuckle kudzuvine root beverage and preparation method thereof - Google Patents
Honeysuckle kudzuvine root beverage and preparation method thereof Download PDFInfo
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- CN103478838A CN103478838A CN201310439792.8A CN201310439792A CN103478838A CN 103478838 A CN103478838 A CN 103478838A CN 201310439792 A CN201310439792 A CN 201310439792A CN 103478838 A CN103478838 A CN 103478838A
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- honeysuckle
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- 235000010575 Pueraria lobata Nutrition 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- 241000205585 Aquilegia canadensis Species 0.000 title claims abstract 19
- 235000013361 beverage Nutrition 0.000 title abstract description 7
- 244000046146 Pueraria lobata Species 0.000 title abstract 7
- 239000007788 liquid Substances 0.000 claims abstract description 49
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000000706 filtrate Substances 0.000 claims abstract description 30
- 238000003756 stirring Methods 0.000 claims abstract description 30
- 238000000034 method Methods 0.000 claims abstract description 25
- 230000008569 process Effects 0.000 claims abstract description 22
- 230000001954 sterilising effect Effects 0.000 claims abstract description 20
- 235000019408 sucralose Nutrition 0.000 claims abstract description 18
- 239000002699 waste material Substances 0.000 claims abstract description 18
- 239000004376 Sucralose Substances 0.000 claims abstract description 17
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- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims abstract description 17
- 239000000811 xylitol Substances 0.000 claims abstract description 17
- 235000010447 xylitol Nutrition 0.000 claims abstract description 17
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 17
- 229960002675 xylitol Drugs 0.000 claims abstract description 17
- 238000001471 micro-filtration Methods 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 14
- 239000000047 product Substances 0.000 claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 claims abstract description 11
- 239000000243 solution Substances 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims abstract description 5
- 239000007864 aqueous solution Substances 0.000 claims description 58
- 241000219781 Pueraria montana var. lobata Species 0.000 claims description 54
- 241000219780 Pueraria Species 0.000 claims description 26
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 claims description 16
- 235000010358 acesulfame potassium Nutrition 0.000 claims description 16
- 229960004998 acesulfame potassium Drugs 0.000 claims description 16
- 239000000619 acesulfame-K Substances 0.000 claims description 16
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- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 12
- 238000004821 distillation Methods 0.000 claims description 11
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- 238000004062 sedimentation Methods 0.000 claims description 8
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- 238000000926 separation method Methods 0.000 claims description 5
- 238000012216 screening Methods 0.000 claims description 4
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- 238000007670 refining Methods 0.000 claims description 3
- 239000002893 slag Substances 0.000 claims description 3
- CEYULKASIQJZGP-UHFFFAOYSA-L disodium;2-(carboxymethyl)-2-hydroxybutanedioate Chemical compound [Na+].[Na+].[O-]C(=O)CC(O)(C(=O)O)CC([O-])=O CEYULKASIQJZGP-UHFFFAOYSA-L 0.000 claims description 2
- 238000002791 soaking Methods 0.000 claims description 2
- 239000001509 sodium citrate Substances 0.000 claims description 2
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 abstract description 5
- 235000003599 food sweetener Nutrition 0.000 abstract description 2
- 238000012545 processing Methods 0.000 abstract description 2
- 239000003765 sweetening agent Substances 0.000 abstract description 2
- YGCFIWIQZPHFLU-UHFFFAOYSA-N acesulfame Chemical compound CC1=CC(=O)NS(=O)(=O)O1 YGCFIWIQZPHFLU-UHFFFAOYSA-N 0.000 abstract 1
- 229960005164 acesulfame Drugs 0.000 abstract 1
- 238000009924 canning Methods 0.000 abstract 1
- 239000011259 mixed solution Substances 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 abstract 1
- 230000035764 nutrition Effects 0.000 abstract 1
- 241001570521 Lonicera periclymenum Species 0.000 description 38
- 235000001368 chlorogenic acid Nutrition 0.000 description 22
- CWVRJTMFETXNAD-FWCWNIRPSA-N 3-O-Caffeoylquinic acid Natural products O[C@H]1[C@@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-FWCWNIRPSA-N 0.000 description 21
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 description 21
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 description 21
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 description 21
- 229940074393 chlorogenic acid Drugs 0.000 description 21
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 description 21
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 description 21
- 239000012528 membrane Substances 0.000 description 13
- RXUWDKBZZLIASQ-UHFFFAOYSA-N Puerarin Natural products OCC1OC(Oc2c(O)cc(O)c3C(=O)C(=COc23)c4ccc(O)cc4)C(O)C(O)C1O RXUWDKBZZLIASQ-UHFFFAOYSA-N 0.000 description 9
- HKEAFJYKMMKDOR-VPRICQMDSA-N puerarin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1C1=C(O)C=CC(C2=O)=C1OC=C2C1=CC=C(O)C=C1 HKEAFJYKMMKDOR-VPRICQMDSA-N 0.000 description 9
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- 239000004480 active ingredient Substances 0.000 description 3
- 230000000840 anti-viral effect Effects 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 235000006708 antioxidants Nutrition 0.000 description 3
- 230000003796 beauty Effects 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 3
- 201000005577 familial hyperlipidemia Diseases 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 229930003944 flavone Natural products 0.000 description 3
- 150000002212 flavone derivatives Chemical class 0.000 description 3
- 235000011949 flavones Nutrition 0.000 description 3
- 150000004676 glycans Chemical class 0.000 description 3
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- 229920001282 polysaccharide Polymers 0.000 description 3
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- 239000000126 substance Substances 0.000 description 3
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 3
- 241000245240 Lonicera Species 0.000 description 2
- 230000001093 anti-cancer Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000001784 detoxification Methods 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
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- 230000001603 reducing effect Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- 208000001953 Hypotension Diseases 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
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- 230000000975 bioactive effect Effects 0.000 description 1
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- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
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- 230000007613 environmental effect Effects 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 150000002343 gold Chemical class 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000002440 hepatic effect Effects 0.000 description 1
- 208000021822 hypotensive Diseases 0.000 description 1
- 230000001077 hypotensive effect Effects 0.000 description 1
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- 239000012535 impurity Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 210000000265 leukocyte Anatomy 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
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- 238000011160 research Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/68—Acidifying substances
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
- A23L2/74—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration using membranes, e.g. osmosis, ultrafiltration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Water Supply & Treatment (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses honeysuckle kudzuvine root beverage and a preparation method thereof, and belongs to the technical field of agricultural product processing. The honeysuckle kudzuvine root beverage is prepared by the following raw materials by weight: 10 to 90 parts of a kudzuvine root water solution, 10 to 90 parts of a honeysuckle water solution, 0.006 to 0.01 part of sucralose, 0.004 to 0.008 part of acesulfame and 0.3 to 0.7 part of xylitol. The preparation method comprises the following steps: adding the kudzuvine root water solution and the honeysuckle water solution according to the ratio, stirring for 20 to 40 minutes, and obtaining a compound liquid; roughly filtrating the compound liquid through a filter, then finely filtrating through a microfiltration filter, and obtaining a fine filtrate; adding a sweetening agent into the fine filtrate according to the ratio, and adjusting the pH value of the mixed solution to be 4.5 to 6.0, stirring, and obtaining the prepared liquid until the pH value is invariant, performing the processes of microfiltrating, heating, canning and sterilizing on the prepared liquid, and obtaining the product. The honeysuckle kudzuvine root beverage provided by the invention makes full use of the waste in the kudzuvine powder and honeysuckle distillate production, the nutrition is rich, and the taste is good.
Description
Technical field
The invention belongs to technical field of agricultural product process, particularly a kind of golden Pueraria lobota drink and preparation method thereof.
Background technology
Pueraria starch, kudzu root flavone at home and abroad are favourably welcome in market in recent years, the producer that produces kudzuvine root starch is more and more, but some basis processing are just done by most of producer, its waste water, waste residue are not used, and a large amount of Flavonoid substances and polysaccharide class material run off.After the producer of distilled liquid of honeysuckle beverage has and much volatile oil in honeysuckle extracted by distillation in addition, vinasse is all fallen as discharge of wastewater, chlorogenic acids a large amount of in honeysuckle run off.Not only wasted resource, also caused to pollute to be unfavorable for environmental protection.
Summary of the invention
One of purpose of the embodiment of the present invention is to provide a kind of golden Pueraria lobota drink, takes full advantage of the refuse of producing in the distilled liquid of honeysuckle and kudzuvine root starch process, has reduced production cost and has reduced discharge of wastewater; Simultaneously, in golden Pueraria lobota drink, contain the active principles such as a large amount of Puerarins and chlorogenic acid, there is clearing heat and detoxicating, hypertension and hyperlipemia, Dealcoholic sobering-up protects the effects such as liver and beauty treatment, and good mouthfeel.Two of purpose of the present invention is to provide the preparation method of this gold Pueraria lobota drink, and production cost is low, mouthfeel good.Described technical scheme is as follows:
On the one hand, the embodiment of the present invention provides a kind of golden Pueraria lobota drink, by following raw material, is made: the root of kudzu vine aqueous solution 10～90 weight portions, the honeysuckle aqueous solution 10～90 weight portions, Sucralose 0.006～0.01 weight portion, acesulfame potassium 0.004～0.008 weight portion and xylitol 0.3～0.7 weight portion.
Preferably, the golden Pueraria lobota drink that the embodiment of the present invention provides is made by following raw material: the root of kudzu vine aqueous solution 30～70 weight portions, the honeysuckle aqueous solution 30～70 weight portions, Sucralose 0.007～0.009 weight portion, acesulfame potassium 0.005～0.007 weight portion and xylitol 0.4～0.6 weight portion.
More preferably, the golden Pueraria lobota drink that the embodiment of the present invention provides is made by following raw material: the root of kudzu vine aqueous solution 40～60 weight portions, the honeysuckle aqueous solution 40～60 weight portions, Sucralose 0.0075～0.0085 weight portion, acesulfame potassium 0.0055～0.0065 weight portion and xylitol 0.45～0.55 weight portion.
Most preferably, the golden Pueraria lobota drink that the embodiment of the present invention provides is made by following raw material: the root of kudzu vine aqueous solution 50 weight portions, the honeysuckle aqueous solution 50 weight portions, Sucralose 0.008 weight portion, acesulfame potassium 0.006 weight portion and xylitol 0.5 weight portion.
Wherein, the aforesaid root of kudzu vine aqueous solution, for waste water and the waste residue produced from the kudzuvine root starch production process reclaims, adopts waste water lixiviate waste residue to obtain.The concentration of its Puerarin can reach 0.35mg/ml, guarantees in product that the content of material such as Puerarin is very high.That this root of kudzu vine aqueous solution has is anti-oxidant, delay senility, improve osteoporosis, remove rubbish in body, and improves the functions such as circulation, lowering blood-fat and reducing weight, adjusting blood pressure.
Particularly, referring to Fig. 1, the source of the aforesaid root of kudzu vine aqueous solution is:
Screenings separates: bright Ge Jingxuan is cut into 2～3 centimetres of segments after cleaning, and the limit extruding is pulverized limit and added the washing powder, and the defibre waste residue obtains slurries, and the quality of the fibroid waste residue of generation is about 20～30% of bright Ge Zhiliang.
Refining: slurries are carried out to sedimentation, and separation of supernatant obtains meal, and water rinse sedimentation 1～3 time for meal separates wet fine powder and obtains the meal rinsing liquid, and wet fine powder is for the production of kudzuvine root starch.
Lixiviate: merge supernatant and meal rinsing liquid and obtain kudzuvine root juice, by kudzuvine root juice, divide lixiviate fibroid waste residue 1～3 time, extraction temperature is 70～80 ℃, and the time of each lixiviate is 1～3 hour; The quality of kudzuvine root juice is 12～13 times of bright Ge Chongliang, and the mass ratio of kudzuvine root juice and fibroid waste residue is about 1:40～50.
Separate rinsing: after lixiviate completes, the defibre slag (fibrous residue obtained after lixiviate is after process by routine, can be used for producing dietary fiber) filtrate, the about water rinse of 1～3 times of bright Ge Chongliang for fibrous residue, merging filtrate and fibrous residue rinsing liquid obtain the root of kudzu vine aqueous solution, and the bright root of kudzu vine of 1 part of weight obtains the root of kudzu vine aqueous solution of 14～16 parts of weight.
More specifically, referring to Fig. 1, the preparation method of the aforesaid root of kudzu vine aqueous solution is:
Screenings separates: bright Ge Jingxuan is cut into 2～3 centimetres of segments after cleaning, and pulverizes limit with the waterside extruding of 7～9 times of bright Ge Chongliang and adds the washing powder, and isolated by filtration fibroid waste residue obtains slurries.
Refining: the slurries sedimentation that the screenings separation process is obtained 10～14 hours (preferably 12 hours), separation of supernatant obtains meal, use the water rinse sedimentation of totally 1～3 times of (being preferably 3 times) bright Ge Chongliang (to be preferably 3 times for 1～3 time meal, as can be at every turn with the water rinse sedimentation of about 1 times of bright Ge Chongliang 3 times), separate wet fine powder and obtain the meal rinsing liquid, after wet fine powder vacuum drying, obtain kudzuvine root starch.
Lixiviate: the supernatant and the meal rinsing liquid that merge the subtractive process generation obtain kudzuvine root juice, by kudzuvine root juice, divide (being preferably 3 times) lixiviate fibroid waste residue 1～3 time, and extraction temperature is 70～80 ℃, and the time of each lixiviate is 1～3 hour (being preferably 3 hours).
Separate rinsing: after lixiviate completes, the defibre slag obtains filtrate, the about water rinse of 2～4 times of bright Ge Chongliang for fibrous residue, and merging filtrate and fibrous residue rinsing liquid obtain the root of kudzu vine aqueous solution.
Wherein, the aforesaid honeysuckle aqueous solution reclaims for the distillation leftover from distilled liquid of honeysuckle production process.It obtains by the hot water centrifugal rinsing, and the chlorogenic acid loss is little, and its chlorogenic acid concentration is greater than 0.30mg/ml, and the content of material such as assurance product Content of Chlorogenic Acid are very high.Chlorogenic acid has biologically active widely, and to chlorogenic acid, bioactive research has been deep into a plurality of fields such as food, health care, medicine and daily-use chemical industry to modern science.Chlorogenic acid is a kind of important bioactivator, have antibiotic, antiviral, increase the effects such as white blood cell, hepatic cholagogic, antitumor, hypotensive, reducing blood lipid, removing free radical and stimulating central nervous system system.
Particularly, referring to Fig. 1, the source of the honeysuckle aqueous solution is:
Soak distillation: the water soaking 0.5～1 hour that dry honeysuckle after crushed adds 32～34 times of weight, soaked rear intensification air-distillation, collect the fraction of 24～26 times of weight of dry honeysuckle for the production of the distilled liquid of honeysuckle.
Centrifugal rinsing: vinasse is separated to residue and obtain centrifugate, residue carries out centrifugal rinsing with the hot water of 40～42 times of dry honeysuckle weight of dry honeysuckle, the temperature of centrifugal rinsing is 60～80 ℃, centrifugal dehydration again after centrifugal rinsing completes, obtain residue rinsing liquid and centrifugal residue (can be used for making fertilizer), merge centrifugate and residue rinsing liquid and obtain the honeysuckle aqueous solution, the dry honeysuckle of 1 weight portion obtains the honeysuckle aqueous solution of 44～46 weight portions.
Preferably, in the centrifugal rinsing process, the temperature of centrifugal rinsing is 65～75 ℃, and optimum is 70 ℃.
Particularly, referring to Fig. 1, the preparation method of the honeysuckle aqueous solution is:
Soak distillation: dry honeysuckle after crushed adds under the water normal temperature condition of 32～34 times of dry honeysuckle weight to be soaked 0.5～1 hour, after having soaked, is warming up to boiling, and air-distillation, collect the fraction of 24～26 times of weight of dry honeysuckle for the production of the distilled liquid of honeysuckle.
Centrifugal rinsing: will soak the vinasse that still-process obtains centrifugal while hot, separate residue and obtain centrifugate, residue carries out centrifugal rinsing with 60～80 ℃ of hot water of 40～42 times of weight of dry honeysuckle, the temperature of centrifugal rinsing is 60～80 ℃, after centrifugal rinsing completes again centrifugal dehydration 8～15 minutes (preferably 10 minutes) it is fully dried, merge centrifugal rinsing liquid and centrifugal dehydration liquid and obtain the residue rinsing liquid, remerge centrifugate and the residue rinsing liquid obtains the honeysuckle aqueous solution.Rotating speed when wherein, centrifugal rinsing and centrifugal dehydration are dewatered is more than or equal to 1200 rpms.
Utilize the chlorogenic acid isoreactivity composition in the method extraction residue of hot water centrifugal rinsing in the gold and silver aqueous solution of the present invention preparation, following benefit arranged:
(1) because of after fraction is extracted in air-distillation, the cell wall structure of honeysuckle has all suffered to destroy fully, and active ingredient can be dissolved, and does not need to be decocted again, can reduce input the steam saving of equipment, the destruction that also can reduce chlorogenic acid.
(2) solubility of chlorogenic acid in hot water is far longer than the solubility in cold water, so select hot water to make the extraction solvent, is conducive to stripping.
(3) the centrifugal rinsing process is actual is that solvent has been divided into to N extraction, a small amount of hot water enters, after residue contacts, separated by high speed centrifugation rapidly after the stripping chlorogenic acid, and have a small amount of hot water to supplement into, keep larger concentration gradient, effect of extracting is good, and chlorogenic acid yield is high, and simply fixedly less investment of equipment, easy to operate, production cost is low.
(4), because chlorogenic acid belongs to heat-sensitive substance, it is long just easily destroyed that temperature surpasses 90 ℃ of heated times, adopts the hot water rinsing process, and separated fast after the chlorogenic acid stripping, reduced its heated time.
On the other hand, referring to Fig. 1, the embodiment of the present invention also provides the preparation method of aforementioned golden Pueraria lobota drink, and this preparation method comprises:
Composite: as to add the root of kudzu vine aqueous solution and the honeysuckle aqueous solution by proportioning, stir 20～40 minutes to obtain compositional liquor.
Essence filter: compositional liquor is carried out to coarse filtration through filter, then carry out essence through the micro-filtration filter and filter and obtain smart filtrate.
Allotment: add Sucralose, acesulfame potassium and xylitol by proportioning in smart filtrate, and the pH value of mixed liquor is adjusted into to 4.5～6.0, stir the constant preparation liquid that obtains of pH value.
Filling sterilizing: will prepare liquid and obtain golden Pueraria lobota drink product after micro-filtration, heating, tinning and sterilization process.
Wherein, in essence, filter in journey, the piping filter that the filter used while slightly considering is 80～120 orders (being preferably 100 orders), certainly, used other filters passable equally.When filter essence the micro-filtration filter that uses be 5 microns, 2 microns double-deck microporous filtrations (coarse filtration liquid prevents from stopping up micro-filtration membrane by 5 microns, 2 microns micro-filtration membrane successively, certainly adopt other micro-filtration membrane of 2～5 microns equally can).
Preferably, in compound process, mixing time is 25-35 minute.More preferably, in compound process, mixing time is 30 minutes.
Wherein, in allocation process, use citric acid or natrium citricum (all being preferably the solution that mass concentration is 10% left and right) to regulate the pH value, stir 20～40 minutes (be preferably 25～35 minutes, optimum is 30 minutes) to the constant preparation liquid that obtains of pH value.Preferably, the pH value is controlled at 5.0～5.5, and optimum is 5.5.
Wherein, in filling sterilization process, microfiltration process adopts 0.25～0.65 micron and (is preferably 0.65 micron, can meet the demands and make product clarification) microporous filtration carry out micro-filtration, heating process is for being heated to 80～85 ℃, and sterilization process is through 115～120 ℃ of (being preferably 118 ℃) sterilizings 20～45 minutes (being preferably 30 minutes).
Further, referring to Fig. 1, the preparation method of golden Pueraria lobota drink specifically comprises:
Composite: as by proportioning, the root of kudzu vine aqueous solution and the honeysuckle aqueous solution to be joined in the composite tank of band stirring, stir 20～40 minutes to obtain compositional liquor.
Essence filter: the compositional liquor that compound process is obtained carries out coarse filtration through 100 order piping filters, then carries out essence through 5 microns, 2 microns double-deck microporous filtrations successively and filter and obtain smart filtrate.
Allotment: in the smart filtrate obtained in essence filtration journey by proportioning, add Sucralose, acesulfame potassium and xylitol to carry out seasoning, and the sodium citrate solution that the citric acid solution that is 10% by mass concentration or mass concentration are 10% is adjusted into 4.5～6.0 by the pH value of mixed liquor, stir 20～40 minutes to the constant preparation liquid that obtains of pH value.
Filling sterilizing: the preparation liquid that allocation process is obtained, after the microporous filtration of 0.65 micron, is heated to 80～85 ℃ and carries out filling and sealing, then within 30 minutes, obtains golden Pueraria lobota drink product through 118 ℃ of sterilizings.
Wherein, another patent of invention that in the present invention, the preparation method of the root of kudzu vine aqueous solution can apply on the same day referring to our company (denomination of invention is a kind of kudzuvine root starch factory effluent, waste reside comprehensive utilization method).
The beneficial effect that the technical scheme that the embodiment of the present invention provides is brought is:
Golden Pueraria lobota drink prepared by the present invention utilizes general flavone and the active ingredients such as Puerarin and water-soluble polysaccharide in the root of kudzu vine aqueous solution, there is hemangiectasis, improve microcirculation, improve myocardial metabolism, improve the function such as liver detoxification, recycle chlorogenic acid in the composite honeysuckle aqueous solution have anti-oxidant, remove free radical, anticancer change, antibiotic, antiviral, regulate the effect such as immunity.The golden Pueraria lobota beverage of producing, not only cost is low, mouthfeel is good, and applicable crowd is wide, and has clearing heat and detoxicating, hypertension and hyperlipemia, Dealcoholic sobering-up, protects the effects such as liver, beauty treatment.
The accompanying drawing explanation
Fig. 1 is the flow chart of golden Pueraria lobota drink preparation process provided by the invention.
The specific embodiment
For making the purpose, technical solutions and advantages of the present invention clearer, below the present invention is described in further detail.
Embodiment mono-:
Get 20 kilograms of the selected fresh roots of kudzu vine, clean up, be broken into 2～3 centimetre lengths, pulverize, wash powder and remove by filter fiber impurity with about 160 kg of water extruding, slurries through sedimentation after 12 hours separation of supernatant obtain meal, then by the fine powder that must wet for 3 times of totally 60～80 kg of water rinsing meal approximately, wet fine powder must be done 3.82 kilograms of kudzuvine root starch by vacuum drying, 242 kilograms of kudzuvine root juices; And 4.1 kilograms of wet fiber waste residues.The fibroid waste residue is thrown in the lixiviate still, divide stirring and leaching fibroid waste residue 3 times with 242 kilograms of kudzuvine root juices, 60～70 ℃ of extraction temperatures, be incubated lixiviate 3 hours at every turn, centrifugation while hot obtains centrifugate and fibrous residue, fibrous residue dries standby with about 60～80 kg of water rinsings, merge centrifugate, washing lotion, obtains 300.5 kilograms of the root of kudzu vine aqueous solution, detecting puerarin content through HPLC is 0.35mg/ml, and the recovery rate of Puerarin is 0.53%.
Embodiment bis-:
Get 10 kilograms of the selected fresh roots of kudzu vine, by embodiment mono-, got the powder operation, obtain 1.95 kilograms of dry kudzuvine root starch; 145 kilograms of kudzuvine root juices, and 2 kilograms of wet fiber waste residues.Detecting puerarin content in kudzuvine root juice through HPLC is 0.26mg/l, and the recovery rate of Puerarin is 0.38%.
From embodiment mono-and two, can find out, embodiment mono-adopts lixiviate fibroid waste residue effectively to increase the recovery rate of Puerarin.
Embodiment tri-:
Get 20 kilograms of dry honeysuckles after crushed, add 660 kilograms, water, soak 1 hour, 501 kilograms of fractions are collected in the intensification air-distillation.Vinasse is centrifugal filtrate while hot, then uses 820 kilograms of centrifugal rinsing filter residues of hot water of 70～75 ℃, and rinsing is finished, high speed centrifugation dehydration 10 minutes, and merging filtrate and rinsing liquid obtain 903 kilograms of the honeysuckle aqueous solution.Detecting chlorogenic acid concentration through HPLC is 0.35mg/ml, and chlorogenic acid yield is 1.5%.
Embodiment tetra-:
Get 20 kilograms of dry honeysuckles after crushed, add 660 kilograms, water, soak 1 hour, 500 kilograms of fractions are collected in the intensification air-distillation, and vinasse is centrifugal filtrate while hot, 410 kg of water decoction 1.5 hours for residue, centrifugal while hot, residue decocts 1 hour with 410 kilograms again, and centrifugal to dry while hot, merging filtrate obtains 910 kilograms of the honeysuckle aqueous solution.Detecting chlorogenic acid concentration through HPLC is 0.26mg/ml, and chlorogenic acid yield is 1.2%.
From embodiment tri-and four, can find out, embodiment tri-adopts hot water rinsing extraction effectively to increase the recovery rate of chlorogenic acid.
Embodiment five:
By in 100 kilograms of the root of kudzu vine aqueous solution and 100 kilograms of composite tanks that are added to stirring of the honeysuckle aqueous solution, stir 30 minutes to obtain compositional liquor.Compositional liquor is filtered through 100 order piping filters, then filter through 5 microns, 2 microns double-deck nuclepore membrane filters successively, obtain smart filtrate.Smart filtrate is squeezed in blend tank, add 1 kilogram of Sucralose 16 gram, acesulfame potassium 12 grams, xylitol to carry out seasoning, adjust pH 5.5, after stirring 30 minutes, the multiple adjust pH preparation liquid that do not become.To prepare liquid after 0.65 micron nuclepore membrane filter filters, and be heated to 80～85 ℃ and carry out filling and sealing, then within 30 minutes, be the get Jin Ge drink through 118 ℃ of sterilizings.This product can be clearing heat and detoxicating, again can Dealcoholic sobering-up, carry out seasoning with composite sweeteners such as Sucraloses, mouthfeel is good, applicable all people group, especially applicable diabetes patient and fat-reducing colony.
Embodiment six:
By in 40 kilograms of the root of kudzu vine aqueous solution and 60 kilograms of composite tanks that are added to stirring of the honeysuckle aqueous solution, stir 30 minutes to obtain compositional liquor.Compositional liquor is filtered through 100 order piping filters, then filter through 5 microns, 2 microns double-deck nuclepore membrane filters successively, obtain smart filtrate.Smart filtrate is squeezed in blend tank, add Sucralose 8 grams, acesulfame potassium 6 grams, xylitol 500 grams to carry out seasoning, adjust pH 5.3, after stirring 30 minutes, the multiple adjust pH preparation liquid that do not become.To prepare liquid after 0.65 micron nuclepore membrane filter filters, and be heated to 80～85 ℃ and carry out filling and sealing, then within 30 minutes, be the get Jin Ge drink through 118 ℃ of sterilizings.
Embodiment seven:
By in 35 kilograms of the root of kudzu vine aqueous solution and 15 kilograms of composite tanks that are added to stirring of the honeysuckle aqueous solution, stir 30 minutes to obtain compositional liquor.Compositional liquor is filtered through 100 order piping filters, then filter through 5 microns, 2 microns double-deck nuclepore membrane filters successively, obtain smart filtrate.Smart filtrate is squeezed in blend tank, add Sucralose 4 grams, acesulfame potassium 3 grams, xylitol 250 grams to carry out seasoning, adjust pH 5.4, after stirring 30 minutes, the multiple adjust pH preparation liquid that do not become.To prepare liquid after 0.65 micron nuclepore membrane filter filters, and be heated to 80～85 ℃ and carry out filling and sealing, then within 30 minutes, be the get Jin Ge drink through 118 ℃ of sterilizings.
Embodiment eight:
By in 20 kilograms of the root of kudzu vine aqueous solution and 80 kilograms of composite tanks that are added to stirring of the honeysuckle aqueous solution, stir 30 minutes to obtain compositional liquor.Compositional liquor is filtered through 100 order piping filters, then filter through 5 microns, 2 microns double-deck nuclepore membrane filters successively, obtain smart filtrate.Smart filtrate is squeezed in blend tank, add Sucralose 8 grams, acesulfame potassium 6 grams, xylitol 500 grams to carry out seasoning, adjust pH 5.0, after stirring 30 minutes, the multiple adjust pH preparation liquid that do not become.To prepare liquid after 0.65 micron nuclepore membrane filter filters, and be heated to 80～85 ℃ and carry out filling and sealing, then within 30 minutes, be the get Jin Ge drink through 118 ℃ of sterilizings.This product is relatively clearing heat and detoxicating.
Embodiment nine:
By in 90 kilograms of the root of kudzu vine aqueous solution and 10 kilograms of composite tanks that are added to stirring of the honeysuckle aqueous solution, stir 30 minutes to obtain compositional liquor.Compositional liquor is filtered through 100 order piping filters, then filter through 5 microns, 2 microns double-deck nuclepore membrane filters successively, obtain smart filtrate.Smart filtrate is squeezed in blend tank, add Sucralose 8 grams, acesulfame potassium 6 grams, xylitol 500 grams to carry out seasoning, adjust pH 5.0, after stirring 30 minutes, the multiple adjust pH preparation liquid that do not become.To prepare liquid after 0.65 micron nuclepore membrane filter filters, and be heated to 80～85 ℃ and carry out filling and sealing, then within 30 minutes, be the get Jin Ge drink through 118 ℃ of sterilizings.This product is partial to Dealcoholic sobering-up.
Golden Pueraria lobota drink prepared by the present invention utilizes general flavone and the active ingredients such as Puerarin and water-soluble polysaccharide in the root of kudzu vine aqueous solution, there is hemangiectasis, improve microcirculation, improve myocardial metabolism, improve the function such as liver detoxification, recycle chlorogenic acid in the composite honeysuckle aqueous solution have anti-oxidant, remove free radical, anticancer change, antibiotic, antiviral, regulate the effect such as immunity.The golden Pueraria lobota beverage of producing, not only cost is low, mouthfeel is good, and applicable crowd is wide, and has clearing heat and detoxicating, hypertension and hyperlipemia, Dealcoholic sobering-up, protects the effects such as liver, beauty treatment.
The foregoing is only preferred embodiment of the present invention, in order to limit the present invention, within the spirit and principles in the present invention not all, any modification of doing, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (10)
1. a golden Pueraria lobota drink, is characterized in that, by following raw material, made:
The root of kudzu vine aqueous solution 10～90 weight portions, the honeysuckle aqueous solution 10～90 weight portions, Sucralose 0.006～0.01 weight portion, acesulfame potassium 0.004～0.008 weight portion and xylitol 0.3～0.7 weight portion.
2. golden Pueraria lobota drink according to claim 1, is characterized in that, by following raw material, made:
The root of kudzu vine aqueous solution 30～70 weight portions, the honeysuckle aqueous solution 30～70 weight portions, Sucralose 0.007～0.009 weight portion, acesulfame potassium 0.005～0.007 weight portion and xylitol 0.4～0.6 weight portion.
3. golden Pueraria lobota drink according to claim 1, is characterized in that, by following raw material, made:
The root of kudzu vine aqueous solution 40～60 weight portions, the honeysuckle aqueous solution 40～60 weight portions, Sucralose 0.0075～0.0085 weight portion, acesulfame potassium 0.0055～0.0065 weight portion and xylitol 0.45～0.55 weight portion.
4. according to the described golden Pueraria lobota drink of claim 1～3 any one, it is characterized in that, the source of the described root of kudzu vine aqueous solution is:
Screenings separates: bright Ge Jingxuan is cut into 2～3 centimetres of segments after cleaning, and the limit extruding is pulverized limit and added the washing powder, and the defibre waste residue obtains slurries;
Refining: described slurries are carried out to sedimentation, and separation of supernatant obtains meal, and water rinse sedimentation 1～3 time for described meal separates wet fine powder and obtains the meal rinsing liquid, and described wet fine powder is for the production of kudzuvine root starch;
Lixiviate: merge described supernatant and the meal rinsing liquid obtains kudzuvine root juice, divide 1～3 lixiviate described fibroid waste residue described kudzuvine root juice, extraction temperature is 70～80 ℃, and the time of each lixiviate is 1～3 hour;
Separate rinsing: after lixiviate completes, the defibre slag obtains filtrate, and described fibrous residue water rinse merges described filtrate and fibrous residue rinsing liquid and obtains the described root of kudzu vine aqueous solution.
5. according to the described golden Pueraria lobota drink of claim 1～3 any one, it is characterized in that, the source of the described honeysuckle aqueous solution is:
Soak distillation: the water soaking 0.5～1 hour that dry honeysuckle after crushed adds 32～34 times of weight of described dry honeysuckle, soaked rear intensification, air-distillation is collected the fraction of 24～26 times of weight of described dry honeysuckle for the production of the distilled liquid of honeysuckle;
Centrifugal rinsing: vinasse is separated to residue and obtain centrifugate, described residue carries out centrifugal rinsing with the hot water of 40～42 times of weight of described dry honeysuckle, the temperature of centrifugal rinsing is 60～80 ℃, centrifugal dehydration again after centrifugal rinsing completes, obtain the residue rinsing liquid, merge described centrifugate and residue rinsing liquid and obtain the described honeysuckle aqueous solution.
6. the preparation method of golden Pueraria lobota drink as described as claim 1～3 any one, is characterized in that, described preparation method comprises:
Composite: as to add the described root of kudzu vine aqueous solution and the honeysuckle aqueous solution by proportioning, stir 20～40 minutes to obtain compositional liquor;
Essence filter: described compositional liquor is carried out to coarse filtration through filter, then carry out essence through the micro-filtration filter and filter and obtain smart filtrate;
Allotment: add Sucralose, acesulfame potassium and xylitol by proportioning in described smart filtrate, and the pH value of mixed liquor is adjusted into to 4.5～6.0, stir the constant preparation liquid that obtains of pH value;
Filling sterilizing: described preparation liquid is obtained to golden Pueraria lobota drink product after micro-filtration, heating, tinning and sterilization process.
7. preparation method according to claim 6, is characterized in that, in described essence filters journey, described filter is 80～120 purpose piping filters, and described micro-filtration filter is 5 microns, 2 microns double-deck microporous filtrations.
8. preparation method according to claim 6, is characterized in that, in allocation process, uses citric acid or natrium citricum to regulate the pH value, stirs 20～40 minutes to the constant preparation liquid that obtains of pH value.
9. preparation method according to claim 6, it is characterized in that, in filling sterilization process, described microfiltration process adopts the microporous filtration of 0.25～0.65 micron to carry out micro-filtration, described heating process is for being heated to 80～85 ℃, and described sterilization process is through 115～120 ℃ of sterilizings 20～45 minutes.
10. preparation method according to claim 6, is characterized in that, described preparation method specifically comprises:
Composite: as by proportioning, the described root of kudzu vine aqueous solution and the honeysuckle aqueous solution to be joined in the composite tank of band stirring, stir 20～40 minutes to obtain compositional liquor;
Essence filter: described compositional liquor is carried out to coarse filtration through 100 order piping filters, then carry out essence through 5 microns, 2 microns double-deck microporous filtrations and filter and obtain smart filtrate;
Allotment: by proportioning, in described smart filtrate, add Sucralose, acesulfame potassium and xylitol to carry out seasoning, and the sodium citrate solution that the citric acid solution that is 10% by mass concentration or mass concentration are 10% is adjusted into 4.5～6.0 by the pH value of mixed liquor, stir 20～40 minutes to the constant preparation liquid that obtains of pH value;
Filling sterilizing: described preparation liquid, after the microporous filtration of 0.65 micron, is heated to 80～85 ℃ and carries out filling and sealing, more obtain product in 30 minutes through 118 ℃ of sterilizings.
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| CN106616191A (en) * | 2016-11-15 | 2017-05-10 | 叶芳健 | Honeysuckle flower and radix puerariae powder effervescent tablets and preparation method |
| CN107007811A (en) * | 2017-06-05 | 2017-08-04 | 黄平县兴且民族民间中草医药科学发展有限责任公司 | A kind of pharmaceutical formulation and its medicament and preparation method for being used to treat condensed blood lipid |
| CN108464996A (en) * | 2018-04-28 | 2018-08-31 | 乌林奇 | A kind of targeting adjusts pharmaceutical composition and its application of gene |
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Address after: 438600 Fengshan City, Huanggang province Luotian County, north of the town of water Yi Road, No. 428 Patentee after: HUBEI HONGYUAN PHARMACEUTICAL TECHNOLOGY CO., LTD. Address before: 438600 Fengshan City, Huanggang province Luotian County, north of the town of water Yi Road, No. 428 Patentee before: Hubei Hongyuan Pharmaceutical Co., Ltd. |