CN105054287A - Additive for compensating fragrance of low-tar cigarettes - Google Patents

Additive for compensating fragrance of low-tar cigarettes Download PDF

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Publication number
CN105054287A
CN105054287A CN201510368809.4A CN201510368809A CN105054287A CN 105054287 A CN105054287 A CN 105054287A CN 201510368809 A CN201510368809 A CN 201510368809A CN 105054287 A CN105054287 A CN 105054287A
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China
Prior art keywords
cigarette
additive
low
coke tar
red date
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Pending
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CN201510368809.4A
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Chinese (zh)
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王昊
张耀华
熊斌
刘鑫
周红审
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Priority to CN201510368809.4A priority Critical patent/CN105054287A/en
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Abstract

The invention provides an additive for compensating fragrance of low-tar cigarettes. Plant extracts containing abundant furfural components are taken as raw materials, and then the plant extracts are mixed with an organic acid and propylene glycol according to a certain proportion to form the additive. The plant extracts containing abundant furfural components comprise red date maillard reaction product red date alcohol extract, fenugreek microwave extract, tamarind fruit alcohol extract and apple juice fermentation extract. The invention also provides an application of the above additive in flavour addition of cigarettes. 1% by weight of the additive is added into low-tar cigarette tobacco, or 0.5-5% by weight of the additive is added into low-tar cigarette filters, or 0.5-5% by weight of the additive is added into cigarette paper. The additive can effectively supplement micromolecule low-boiling aroma substance such as furfural substance in low-tar cigarettes, and can supplement fragrance of low-tar cigarettes specifically.

Description

A kind of additive compensating low-coke tar cigarette note
Technical field
The present invention relates to technical field of cigarettes, specifically a kind of additive compensating low-coke tar cigarette note.
Background technology
How to reduce harm that smoking brings and become the emphasis that medical circle and tobacco business pay close attention to.The harmful components produced cigarette burning in smoking process are present in cigarette smoke, and few harmful components burst size effectively can fall in the exhaust gas volumn and the releasing content of coke tar that reduce cigarette, and the releasing content of coke tar of cigarette constantly reduces for this reason.The domestic cigarette packs mark tar content upper limit has been adjusted to 11 milligrams/in 2013.But while reduction tar content, fragrance component wherein also loses, and it is thin that Sensory Quality of Cigarette shows as fragrance, and note is single, and satisfaction is owed thereupon.For this reason, have and select the fragrance matter to loss to supplement, low-coke tar cigarette can be made to keep good fragrance and note state, improve the sensory experience of cigarette.Be that main (application number CN200710189724.5) compensates fragrance etc. as adopted latent Studies of The Aromatic Substances (application number CN200810140585.1, CN201110209568.0) or tobacco extract.
Research (Chinese tobacco journal, the 2008,3rd phase: 1-7) shows that low-coke tar cigarette is under ventilation dilution, additional fragrance material boiling point is lower, at main flume grain, middle rate of transform reduction amplitude is larger mutually, and along with fragrance material boiling point improves, the rate of transform reduces amplitude and slows down to some extent.Therefore, low-coke tar cigarette emphasis should supplement lower boiling aroma substance.
Li Yan waits (fragrance flavor and cosmetic by force, 2009,5th phase, 7-11) domestic and international 5 kinds of representative low-coke tar cigarette pipe tobacco volatility, the analysis of half volatile neutral compound are being found, four kinds of domestic cigarette aroma components have the materials such as furfural all higher than external cigarette more than 10%, wherein furfural content is 68.90-81.14 μ g/g, 5 methyl furfural content is 0.85-2.52 μ g/g, domestic cigarette furfural amount is a little more than import cigarette, and 5 methyl furfural is contrary, external cigarette product content is domestic 2-3 times.
Selectively to compensate with class low boiling flavor matter a certain in flue gas as seen, effectively can promote the perfume quantity of low burnt cigarette, enrich note, promote Sensory Quality of Cigarette.
Summary of the invention
The invention provides a kind of additive compensating low-coke tar cigarette note, effectively can to supplement in low-coke tar cigarette with the Small molecular low boiling aroma substance that chaff aldehyde material is representative, targetedly perfume (or spice) is mended to low-coke tar cigarette.
A kind of additive compensating low-coke tar cigarette note, by to be rich in the more rich plant extracts of furfural constituents content for raw material, form with organic acid, mixed with propylene glycol according to a certain percentage, described in be rich in the more rich plant extracts of furfural constituents content and comprise red date Maillard reaction products red date alcohol extract, faenum graecum Microwave Extraction thing, tamarind alcohol extract, apple juice fermentation extract.
The additive of compensation low-coke tar cigarette note as above, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 1 ~ 2%, red date alcohol extract 5 ~ 10%, faenum graecum Microwave Extraction thing 0.1 ~ 1%, tamarind alcohol extract 0.5 ~ 1%, apple juice fermentation extract 1 ~ 5%, organic acid 0.1 ~ 1%, propane diols 1%, solvent 79 ~ 91.3%.
The additive of compensation low-coke tar cigarette note as above, described solvent is 70% ethanol or propane diols or propane diols and the ethanol mixture according to mass ratio 1:4 proportioning.
The application of additive in perfuming cigarette of compensation low-coke tar cigarette note as above, described solvent is 70% ethanol, described additive adds low-coke tar cigarette pipe tobacco with the mass ratio of 1%, or is sprayed directly on cigarette paper with 0.5 ~ 5% ratio, after cigarette paper drying, roll use.
The application of additive in perfuming cigarette of compensation low-coke tar cigarette note as above, add low-coke tar cigarette filter tip, described solvent is propane diols, and described additive adds connect mouth glue with the mass ratio of 0.5 ~ 5%, stir, in the process of rolled cigarette, add filter tip.
The application of additive in perfuming cigarette of compensation low-coke tar cigarette note as above, add cigarette paper, described solvent is propane diols and the ethanol mixture according to mass ratio 1:4 proportioning, described additive adds overlapping glue with the mass ratio of 0.5 ~ 5%, mix, add in the process of rolled cigarette; Or be sprayed directly on cigarette paper, after cigarette paper drying, roll use.
Beneficial effect of the present invention is:
1, plant additive of the present invention can effectively to supplement in low-coke tar cigarette with the Small molecular low boiling aroma substance that chaff aldehyde material is representative, mends perfume (or spice) targetedly to low-coke tar cigarette.
2, plant additive of the present invention can increase fragrant and sweet rhythm, the baking note and sour note of low-coke tar cigarette.
3, plant additive of the present invention both can apply also can be applied by different modes such as cigarette materials by pipe tobacco, avoided the limitation that latent fragrant class material can only apply in pipe tobacco and coil paper.
4, because low boiling flavor matter content is higher, plant additive of the present invention also has obvious fragrant and sweet rhythm and baking note at normal temperatures, and what imparting low-coke tar cigarette was obvious, comfortable smells perfume (or spice), increases cigarette characteristic.
Detailed description of the invention
Below in conjunction with specific embodiment, the technical scheme in the present invention is clearly and completely described.
Embodiment 1: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 2%, red date alcohol extract 5%, faenum graecum Microwave Extraction thing 0.1%, tamarind alcohol extract 0.5%, apple juice fermentation extract 5%, organic acid 1%, propane diols 1%, 70% ethanol 85.4%.
Above-mentioned additive is that 1% ratio is exerted into low-coke tar cigarette pipe tobacco in perfuming link with mass percent.Adopt Chinese-style cigarette style and features sensory evaluation method evaluation, contrast the fragrant and sweet rhythm of fruit that blank cigarette can increase low-coke tar cigarette, mellow and full soft flue gas.Concrete outcome sees the following form:
Table 1 Chinese-style cigarette style and features sensory evaluation situation of change table
Embodiment 2: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 2%, red date alcohol extract 5%, faenum graecum Microwave Extraction thing 1%, tamarind alcohol extract 0.5%, apple juice fermentation extract 5%, organic acid 1%, propane diols 1%, 70% ethanol 84.5%.
Above-mentioned additive is exerted into low-coke tar cigarette pipe tobacco with 1% ratio in perfuming link.Through evaluating the roasting fragrant and sweet rhythm that can increase low-coke tar cigarette, mellow and full soft flue gas, strengthening satisfaction.Specifically see the following form:
Table 2 Chinese-style cigarette style and features sensory evaluation situation of change table
Embodiment 3: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 5%, red date alcohol extract 10%, faenum graecum Microwave Extraction thing 1%, tamarind alcohol extract 1%, apple juice fermentation extract 5%, organic acid 2%, propane diols 1%, 70% ethanol 75%.
Above-mentioned additive is exerted into low-coke tar cigarette pipe tobacco with 1% ratio in perfuming link.Through evaluating, the fruit that can increase low-coke tar cigarette is sweet, baking note, plentiful flue gas.
Embodiment 4: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 2%, red date alcohol extract 5%, faenum graecum Microwave Extraction thing 0.1%, tamarind alcohol extract 0.5%, apple juice fermentation extract 5%, organic acid 1%, propane diols 1%, solvent (propane diols) 85.4%.
Above-mentioned additive adds with 0.5 ~ 5% ratio and connects mouth glue, is exerted in low-coke tar cigarette filter tip.Through evaluating the fragrant and sweet rhythm of fruit that can increase low-coke tar cigarette, mellow and full soft flue gas.
Embodiment 5: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 2%, red date alcohol extract 5%, faenum graecum Microwave Extraction thing 1%, tamarind alcohol extract 0.5%, apple juice fermentation extract 5%, organic acid 1%, propane diols 1%, solvent (propane diols) 84.5%.
Above-mentioned additive adds with 0.5 ~ 5% ratio and connects mouth glue, is exerted in low-coke tar cigarette filter tip.Through evaluating the roasting fragrant and sweet rhythm that can increase low-coke tar cigarette, mellow and full soft flue gas, strengthening satisfaction.
Embodiment 6: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 5%, red date alcohol extract 10%, faenum graecum Microwave Extraction thing 1%, tamarind alcohol extract 1%, apple juice fermentation extract 5%, organic acid 2%, propane diols 1%, solvent (propane diols) 75%.
Above-mentioned additive adds with 0.5 ~ 5% ratio and connects mouth glue, is exerted in low-coke tar cigarette filter tip.Through evaluating, the fruit that can increase low-coke tar cigarette is sweet, baking note, plentiful flue gas.
Embodiment 7: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 2%, red date alcohol extract 5%, faenum graecum Microwave Extraction thing 0.1%, tamarind alcohol extract 0.5%, apple juice fermentation extract 5%, organic acid 1%, propane diols 1%, propane diols: ethanol (mass ratio 1:4) 85.4%.
Above-mentioned additive directly sprays with 1 ~ 5% ratio and is exerted into cigarette paper, rolling cigarette.。Through the fragrant and sweet rhythm of fruit that blank cigarette comparative evaluation can increase low-coke tar cigarette, mellow and full soft flue gas, gives cigarette sweet simultaneously, perfume (or spice) is smelt in acid.
Embodiment 8: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 2%, red date alcohol extract 5%, faenum graecum Microwave Extraction thing 1%, tamarind alcohol extract 0.5%, apple juice fermentation extract 5%, organic acid 1%, propane diols 1%, propane diols: ethanol (mass ratio 1:4) 84.5%.
Above-mentioned additive directly sprays with 1 ~ 5% ratio and is exerted into cigarette paper, rolling cigarette.Can increase the roasting fragrant and sweet rhythm of low-coke tar cigarette through blank cigarette comparative evaluation, mellow and full soft flue gas, strengthening satisfaction, gives cigarette sweet simultaneously, perfume (or spice) is smelt in acid
Embodiment 9: a kind of additive compensating low-coke tar cigarette note, be made up of according to mass percent proportioning following raw material: red date Maillard reaction products 1%, red date alcohol extract 10%, faenum graecum Microwave Extraction thing 1%, tamarind alcohol extract 1%, apple juice fermentation extract 5%, organic acid 1%, propane diols 1%, propane diols: ethanol (mass ratio 4:1) 80%.
Above-mentioned additive is being exerted into overlapping glue with 1 ~ 5% ratio, then rolling cigarette.The fruit that can increase low-coke tar cigarette through blank cigarette comparative evaluation is sweet, baking note, and plentiful flue gas, gives cigarette sweet simultaneously, perfume (or spice) is smelt in acid.
Additive of the present invention is main primarily of the plant extracts being rich in chaff aldehyde material.Furnan products is hydrolyzed generation pentose under the action of an acid by pentosan, then formed by dehydration of pentoses cyclisation, is usually considered to the catabolite of polysaccharide, is prevalent in food, essence and flavoring agent, Chinese medicine and parenteral solution.Therefore, select the natural plants that sugar content is abundant, if red date, faenum graecum, tamarind etc. are as the raw material of extract, extracted by one or more modes such as solvent extraction, biofermentation, mailland reaction, molecular clock, ultrasonic extractions, obtain after allotment.
Wherein red date Maillard reaction products is with reference to (hubei agricultural sciences such as Huanglong, 2011,8th phase, method 1673-1676) obtains, higher than chaff aldehyde matter content in general red date extract, wherein furfural content is increased to 1.52 μ g/g by 0.18 μ g/g before reacting, 5 methyl furfural content is increased to 0.70 μ g/g by 0.59 μ g/g, 5 hydroxymethyl furfural is increased to 0.32 μ g/g by not detecting,, can supplement fragrant and sweet, cure perfume (or spice), give roasting fragrant and sweet rhythm, thoroughly to be fuming perfume (or spice), round and smooth flue gas.
Faenum graecum Microwave Extraction thing, by the faenum graecum powder after curing, adds 50% alcohol solution dipping, Microwave Extraction 0.5 hour, after filtering, filtrate is concentrated obtains, supplement cure, beans are fragrant, burnt odor, give burnt, sweet, cure note, strengthen flue gas intensity, promote impulsive force.Huang Wei (Shanghai Institute Of Technology's journal, the 4th phase, 318-321 in 2005) research shows that the main aroma component of fenugreek concrete is furfural, 5 methyl furfural relative amount is up to 23.64%.
It is adopt red date or tamarind refluxing extraction after 95% alcohol solution dipping that red date and tamarind alcohol extract adopt respectively, is concentrated to certain proportion and obtains, tamarind alcohol extract can supplemental acid fragrant, fragrant and sweet, give fruit fragrant and sweet rhythm, soft fine and smooth flue gas.
Apple juice fermentation extract have employed anaerobic condition, apple liquid and a certain proportion of acetic acid bacteria is dropped in fermentation tank, carries out anaerobic fermentation.After fermentation completely, add alcohol settling, supernatant concentration obtains, and supplements fruital, acid, fragrant and sweet, fluffy flue gas.
Organic acid can be the small molecular organic acid such as acetic acid, lactic acid class material.
The above; be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, anyly belongs to those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claim.

Claims (6)

1. one kind compensates the additive of low-coke tar cigarette note, obtain by be rich in the more rich plant extracts of furfural constituents content for raw material, form with organic acid, mixed with propylene glycol according to a certain percentage, described in be rich in the more rich plant extracts of furfural constituents content and comprise red date Maillard reaction products red date alcohol extract, faenum graecum Microwave Extraction thing, tamarind alcohol extract, apple juice fermentation extract.
2. the additive compensating low-coke tar cigarette note as claimed in claim 1, it is characterized in that being made up of according to mass percent proportioning following raw material: red date Maillard reaction products 1 ~ 2%, red date alcohol extract 5 ~ 10%, faenum graecum Microwave Extraction thing 0.1 ~ 1%, tamarind alcohol extract 0.5 ~ 1%, apple juice fermentation extract 1 ~ 5%, organic acid 0.1 ~ 1%, propane diols 1%, solvent 79 ~ 91.3%.
3. the as claimed in claim 2 additive compensating low-coke tar cigarette note, is characterized in that: described solvent is 70% ethanol or propane diols or propane diols and the ethanol mixture according to mass ratio 1:4 proportioning.
4. the application of additive in perfuming cigarette as described in any one of claim 1-3, it is characterized in that: described solvent is 70% ethanol, described additive adds low-coke tar cigarette pipe tobacco with the mass ratio of 1%, or be sprayed directly on cigarette paper with 0.5 ~ 5% ratio, after cigarette paper drying, roll use.
5. the application of additive in perfuming cigarette as described in any one of claim 1-3, add low-coke tar cigarette filter tip, it is characterized in that: described solvent is propane diols, described additive adds connect mouth glue with the mass ratio of 0.5 ~ 5%, stir, in the process of rolled cigarette, add filter tip.
6. the application of additive in perfuming cigarette as described in any one of claim 1-3, add cigarette paper, it is characterized in that: described solvent is propane diols and the ethanol mixture according to mass ratio 1:4 proportioning, described additive adds overlapping glue with the mass ratio of 0.5 ~ 5%, mix, add in the process of rolled cigarette; Or be sprayed directly on cigarette paper, after cigarette paper drying, roll use.
CN201510368809.4A 2015-06-29 2015-06-29 Additive for compensating fragrance of low-tar cigarettes Pending CN105054287A (en)

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CN109082344A (en) * 2018-07-03 2018-12-25 福建中烟工业有限责任公司 Essence spice for cigarette, the cigarette paper containing the essence spice for cigarette and its application

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Publication number Priority date Publication date Assignee Title
CN106010794A (en) * 2016-07-19 2016-10-12 湖北中烟工业有限责任公司 Preparation method and application of essence for increasing agalloch eaglewood note for cigarettes
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CN109082344A (en) * 2018-07-03 2018-12-25 福建中烟工业有限责任公司 Essence spice for cigarette, the cigarette paper containing the essence spice for cigarette and its application

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Application publication date: 20151118