CN106010794B - A kind of preparation method and applications increasing cigarette agalloch eaglewood note essence - Google Patents
A kind of preparation method and applications increasing cigarette agalloch eaglewood note essence Download PDFInfo
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- CN106010794B CN106010794B CN201610567645.2A CN201610567645A CN106010794B CN 106010794 B CN106010794 B CN 106010794B CN 201610567645 A CN201610567645 A CN 201610567645A CN 106010794 B CN106010794 B CN 106010794B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 62
- 241000271309 Aquilaria crassna Species 0.000 title claims abstract description 41
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 44
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000003921 oil Substances 0.000 claims abstract description 31
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 22
- 239000003205 fragrance Substances 0.000 claims abstract description 22
- 235000019441 ethanol Nutrition 0.000 claims abstract description 21
- 239000010671 sandalwood oil Substances 0.000 claims abstract description 14
- XCOJIVIDDFTHGB-UEUZTHOGSA-N Perillartine Chemical compound CC(=C)[C@H]1CCC(\C=N\O)=CC1 XCOJIVIDDFTHGB-UEUZTHOGSA-N 0.000 claims abstract description 11
- 244000182022 Salvia sclarea Species 0.000 claims abstract description 11
- 235000002911 Salvia sclarea Nutrition 0.000 claims abstract description 11
- 235000002020 sage Nutrition 0.000 claims abstract description 11
- 239000012528 membrane Substances 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 239000013049 sediment Substances 0.000 claims abstract description 9
- 239000000243 solution Substances 0.000 claims abstract description 9
- 230000003068 static effect Effects 0.000 claims abstract description 6
- 238000010790 dilution Methods 0.000 claims abstract description 4
- 239000012895 dilution Substances 0.000 claims abstract description 4
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract 4
- 241001247821 Ziziphus Species 0.000 claims description 18
- 240000000513 Santalum album Species 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 8
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 239000012141 concentrate Substances 0.000 claims description 6
- 239000000284 extract Substances 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
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- 238000000605 extraction Methods 0.000 claims description 3
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- 235000020095 red wine Nutrition 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 230000008030 elimination Effects 0.000 claims 1
- 238000003379 elimination reaction Methods 0.000 claims 1
- 239000007921 spray Substances 0.000 claims 1
- 239000000796 flavoring agent Substances 0.000 abstract description 12
- 235000019634 flavors Nutrition 0.000 abstract description 12
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract description 9
- 239000003546 flue gas Substances 0.000 abstract description 9
- 230000000391 smoking effect Effects 0.000 abstract description 7
- 239000002304 perfume Substances 0.000 abstract description 4
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- OEYQBKYISMRWQB-UHFFFAOYSA-N Santal Chemical compound C=1C(OC)=CC(O)=C(C2=O)C=1OC=C2C1=CC=C(O)C(O)=C1 OEYQBKYISMRWQB-UHFFFAOYSA-N 0.000 description 2
- 229920006221 acetate fiber Polymers 0.000 description 2
- 229910052785 arsenic Inorganic materials 0.000 description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 2
- -1 carrotene Chemical compound 0.000 description 2
- 208000017574 dry cough Diseases 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
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- 230000036039 immunity Effects 0.000 description 2
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 2
- NDTYTMIUWGWIMO-UHFFFAOYSA-N perillyl alcohol Chemical compound CC(=C)C1CCC(CO)=CC1 NDTYTMIUWGWIMO-UHFFFAOYSA-N 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 239000005060 rubber Substances 0.000 description 2
- FQTLCLSUCSAZDY-UHFFFAOYSA-N (+) E(S) nerolidol Natural products CC(C)=CCCC(C)=CCCC(C)(O)C=C FQTLCLSUCSAZDY-UHFFFAOYSA-N 0.000 description 1
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 1
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 1
- 239000001169 1-methyl-4-propan-2-ylcyclohexa-1,4-diene Substances 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000001856 Ethyl cellulose Substances 0.000 description 1
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 1
- 240000009088 Fragaria x ananassa Species 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- FQTLCLSUCSAZDY-ATGUSINASA-N Nerolidol Chemical compound CC(C)=CCC\C(C)=C\CC[C@](C)(O)C=C FQTLCLSUCSAZDY-ATGUSINASA-N 0.000 description 1
- PRNJXUQTUSFYLV-NTCAYCPXSA-N Nerolidyl acetate Chemical compound CC(C)=CCC\C(C)=C\CCC(C)(C=C)OC(C)=O PRNJXUQTUSFYLV-NTCAYCPXSA-N 0.000 description 1
- PVNIIMVLHYAWGP-UHFFFAOYSA-N Niacin Chemical compound OC(=O)C1=CC=CN=C1 PVNIIMVLHYAWGP-UHFFFAOYSA-N 0.000 description 1
- 235000004347 Perilla Nutrition 0.000 description 1
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- 201000007100 Pharyngitis Diseases 0.000 description 1
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- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 244000022370 Symplocos paniculata Species 0.000 description 1
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- JZRWCGZRTZMZEH-UHFFFAOYSA-N Thiamine Natural products CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N JZRWCGZRTZMZEH-UHFFFAOYSA-N 0.000 description 1
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- 230000015572 biosynthetic process Effects 0.000 description 1
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- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
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- 238000000576 coating method Methods 0.000 description 1
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- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229920001249 ethyl cellulose Polymers 0.000 description 1
- 235000019325 ethyl cellulose Nutrition 0.000 description 1
- 125000004494 ethyl ester group Chemical group 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000008369 fruit flavor Substances 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
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- 230000002045 lasting effect Effects 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- WASNIKZYIWZQIP-AWEZNQCLSA-N nerolidol Natural products CC(=CCCC(=CCC[C@@H](O)C=C)C)C WASNIKZYIWZQIP-AWEZNQCLSA-N 0.000 description 1
- 229960003512 nicotinic acid Drugs 0.000 description 1
- 235000001968 nicotinic acid Nutrition 0.000 description 1
- 239000011664 nicotinic acid Substances 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 150000007875 phellandrene derivatives Chemical class 0.000 description 1
- 238000013031 physical testing Methods 0.000 description 1
- 239000010318 polygalacturonic acid Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
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- 229920005989 resin Polymers 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 229930004725 sesquiterpene Natural products 0.000 description 1
- 150000004354 sesquiterpene derivatives Chemical class 0.000 description 1
- 201000009890 sinusitis Diseases 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 235000021012 strawberries Nutrition 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229930006978 terpinene Natural products 0.000 description 1
- 150000003507 terpinene derivatives Chemical class 0.000 description 1
- 235000019157 thiamine Nutrition 0.000 description 1
- KYMBYSLLVAOCFI-UHFFFAOYSA-N thiamine Chemical compound CC1=C(CCO)SCN1CC1=CN=C(C)N=C1N KYMBYSLLVAOCFI-UHFFFAOYSA-N 0.000 description 1
- 229960003495 thiamine Drugs 0.000 description 1
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- RBNWAMSGVWEHFP-UHFFFAOYSA-N trans-p-Menthane-1,8-diol Chemical compound CC(C)(O)C1CCC(C)(O)CC1 RBNWAMSGVWEHFP-UHFFFAOYSA-N 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Abstract
The present invention provides a kind of preparation method and applications for increasing cigarette agalloch eaglewood note essence.The increase cigarette agalloch eaglewood note essence is by 15~25 parts of jujube absolute oil, 0.1~1 part of East India sandalwood oil, 0.2~2 part of perillartine, 3~10 parts of ethyl acetate, 0.5~5 part of sage clary oil, 25~85 parts of ethyl alcohol, it is stirred after mixing, is static, sediment is filtered off using filter membrane again to obtain, the essence mass percent concentration is that the dilution of 50~95% ethanol solutions is sprayed directly on pipe tobacco, and cigarette is made.The present invention solves the problems, such as the harmony with the fragrance of tobacco this perfume very well, can effectively promote the quality of cigarette flavor, reduces miscellaneous gas in flue gas, reduce stimulation of the flue gas to throat, the dry sensation for reducing flue gas improves the comfort level of cigarette smoking, reduces smoking and endangers smoker's bring.
Description
Technical field
The present invention relates to technical field of cigarette flavors, in particular to a kind of system of essence for increasing cigarette agalloch eaglewood note
Preparation Method and its application.
Background technique
Flavors and fragrances can be played in cigarette cover disadvantage, improve tobacco aroma and it is jealous, improve tobacco it is physical
Can, the effect of cigarette unique taste and style be assigned, and product quality differentiation may be implemented, stablizes cigarette smoking product
Matter has a major impact the style and quality responses of cigarette.With State Bureau " blending engineering " implementation, flavors and fragrances
In Chinese-style cigarette core technology, the effect especially in terms of constructing the unique taste of cigarette and style will be more and more important.
However, existing situation is external flavors and fragrances business monopoly core technology, and China's tobacco business in terms of flavor deployment
Independent core technology is in the situation of key stage.Simultaneously as flavors and fragrances enterprise self-developing designs essence, lead to essence
And the combination defective tightness of cigarette product, therefore not can guarantee the specific aim and practicability of essence product exploitation；And cigarette enterprise
The application study of essence is only carried out, not enough, the understanding of not formed system can not construct autonomous cigarette blending core for basis accumulation
Technical system.
Agalloch eaglewood is widely used in folks of china, deep to be liked by the common people, with people's economic level continuous improvement and
Variation to cigarette consumption theory, agalloch eaglewood odor type cigarette are increasingly pursued by numerous smokers.But directly agalloch eaglewood is applied to
Considerably less in tobacco, mainly since agalloch eaglewood fragrance and tobacco this perfume (or spice) are difficult harmonious, and agalloch eaglewood is expensive.
Jujube can improve the immunity of the human body, and can inhibit cancer cell: pharmacological research discovery, jujube can promote the life of leucocyte
At reduction serum cholesterol improves seralbumin, protects liver, also contains in jujube and inhibit cancer cell, or even cancer can be made thin
Substance of the born of the same parents to normal cell turnover.Jujube contains a large amount of glucide, predominantly glucose, also containing fructose, sucrose and
Oligosaccharide, araban and galacturonan for being made of glucose and fructose etc.；And contain a large amount of vitamin C, core yellow
The multivitamins such as element, thiamine, carrotene, niacin.
East India sandalwood oil, mainly wanting composition is sesquiterpene, Oleum Ligni Santali aldehyde, and indian sandalwood is wooden, Shenmu County of India, extensively
To be used in fragrance, religious rites, drug and cosmetic product, and indian sandalwood another name for oil, then it is close with East India is grown in
What the core of the sandalwood of your Sol intermountain was extracted, quality is best；Another relatively inexpensive indian sandalwood another name for oil,
Then originate in western India Ah Mi it is auspicious this, only have and speciality as indian sandalwood another name for oils, but variant plant section
Belong to.East India sandalwood oil extracts position in colored and center wood (pith), can treat sore throat, dry cough, beneficial to respiratory system nose
Sinusitis eliminates worried, to assist deep in thought and yoga progress, conditioning drying stimulated skin, improves dry and cracked.
Current not someone is deployed into the essence of agalloch eaglewood style using jujube, East India sandalwood oil and other fragrance.
Summary of the invention
Present invention aim to overcome the shortcomings of the prior art, it is fragrant to provide a kind of increase cigarette agalloch eaglewood note
The preparation method and applications of essence.The modulator approach is simple, applied to the wind that can dramatically increase cigarette agalloch eaglewood note in cigarette
Lattice promote the graceful sense of cigarette flavor, keep the fragrance of cigarette abundant comfortable.
The present invention is achieved through the following technical solutions: a kind of essence preparation side increasing cigarette agalloch eaglewood note
Method, it is characterised in that specific step is as follows:
(1) jujube absolute oil is prepared: using extra dry red wine jujube and water according to the temperature after the ratio mixing of weight ratio 1:7-10 at 100 DEG C
It spends lower refluxing extraction 1-3 times, combined extract is simultaneously concentrated into density as 1.0-1.1；Then concentrate weight is added into concentrate
The petroleum ether or concentration of 2-5 times of amount are 95% ethyl alcohol, stand 12-48 hours, and aperture is used to filter off sediment for 0.8 micron of filter membrane
Obtaining the filtrate that relative density is 0.9~1.0 is jujube absolute oil；
(2) prepare the raw material of following parts by weight: 15~25 parts of the jujube absolute oil of preparation, East India santal in step (1)
0.1~1 part of wood oil, 0.2~2 part of perillartine, 3~10 parts of ethyl acetate, 0.5~5 part of sage clary oil, 25~85 parts of ethyl alcohol；
(3) it is stirred 2-4 hours after mixing the raw material components in step (2), it is 24-48 hours static, use aperture for 0.8
It is the perfume (or spice) for increasing cigarette agalloch eaglewood note that the filter membrane of micron, which filters off sediment and obtains the filtrate that relative density is 0.85~0.95,
Essence.
The present invention preferably technical solution: 15 parts of jujube absolute oil, 0.1 part of East Indian sandalwood oil, 0.8 part of perillartine, acetic acid
5 parts of ethyl ester, 1.5 parts of sage clary oil, 77.6 parts of ethyl alcohol.
The present invention preferably technical solution: the mass percent concentration of the ethyl alcohol is 20~80%.
The present invention preferably technical solution: by the essence mass percent of the above-mentioned increase cigarette agalloch eaglewood note prepared
Concentration is the dilution of 50~95% ethanol solutions, and the fragrance solution of the increase cigarette agalloch eaglewood note after dilution is sprayed on pipe tobacco,
And cigarette is made, wherein the essence for increasing cigarette agalloch eaglewood note accounts for the 0.01~0.30% of pipe tobacco weight
East India sandalwood oil in the present invention is by the wood chip or root of sandalwood plants Asiatic sweet leaf, branch through steam distillation institute
, it is colourless to yellow thick liquid.Unique, the lasting fragrant and sweet and radix aucklandiae fragrance of tool, main product have fixation work in India and Indonesia
With can directly buy existing finished product.
Perillartine in the present invention is white crystal, content >=99.0%.97.0-102.0 DEG C of fusing point, slightly with purple perilla
Herbal medicine fragrance, the addition of perillartine remove removal of impurities gas, flue gas are made to become softer exquisiteness first is that irritation can be reduced significantly,
Keep pleasant impression pure comfortable, to significantly improve flue gas mass；Second is that cigarette can be improved under the premise of not changing raw tobacco material
Quality grade, can also be under the premise of not changing cigarette product grade, the more low raw tobacco material of use.
Ethyl acetate in the present invention, also known as ethyl acetate are also present in the fruits such as pineapple, banana in addition to artificial synthesized
In.Pure ethyl acetate is the colorless and transparent liquid with penetrating odor, has fruit flavor, is a kind of widely used essence
Chemical product is refined, there is excellent dissolubility, quick-drying, it is widely used, it is a kind of very important Organic Chemicals and pole
Good industrial solvent is widely used in acetate fiber, ethyl cellulose, chlorinated rubber, vinyl, acetate fiber resin, synthesis
In the production process of rubber, coating and paint etc..As spice material, for fruit essences and Wei Shi such as pineapple, banana, strawberries
Avoid, the primary raw material of the fragrance such as cream, can separately make white spirit mixing fragrance etc..
Sage clary oil in the present invention is at normal temperature faint yellow to orange-yellow liquid, relative density be 0.906~
0.925, index of refraction is 1.467~1.472, and main ingredient is bergamio, linalool, geraniol, terpinol, fragrant purple perilla
Alcohol, nerolidol, nerolidyl acetate, terpinene, phellandrene etc. have herbal, faint scent, radix aucklandiae, Xin Xiang, citrus fragrance.
Beneficial effects of the present invention:
1. the present invention mixes agalloch eaglewood using East India sandalwood oil and sage clary oil, jujube absolute oil etc. in the proper ratio
Note, and, herbal fragrant and sweet with fruit, faint scent, radix aucklandiae, Xin Xiang are cooperated, and the essence with agalloch eaglewood note is adjusted to solve very well
With the harmony problem of the fragrance of tobacco this perfume, the agalloch eaglewood essence modulated assigns the Chinese style style of cigarette characteristic and price is low
Honest and clean, the allotment of agalloch eaglewood essence is independent research, helps to enhance control of the enterprise to core technology.
2. the present invention is for the first time by jujube absolute oil, East India sandalwood oil content, perillartine, ethyl acetate, sage clary oil, ethyl alcohol
It carries out compatibility and is deployed into the essence of agalloch eaglewood style, and be applied in cigarette, can effectively promote the matter of cigarette flavor
Amount reduces miscellaneous gas in flue gas, reduces stimulation of the flue gas to throat, reduces the dry sensation of flue gas, improve the comfort level of cigarette smoking,
It reduces smoking to endanger smoker's bring, and has catered to consumer and agalloch eaglewood is liked；
3. the flavor application that the present invention is deployed can dramatically increase the style of cigarette agalloch eaglewood note in cigarette, promoted
The graceful sense of cigarette flavor keeps the fragrance of cigarette abundant comfortable；
4. the present invention is in terms of Smoking is harmful to your health problem, which contains the composition of many this health of beneficial people, as red
Jujube can improve the immunity of the human body, and can inhibit the influence that cancer cell is smoked to human health, and East India sandalwood oil can treat larynx
Throat pain, dry cough, beneficial to the health etc. of human respiratory；
5. equipment of the presently claimed invention is relatively easy, cost is relatively low, easy to industrialized production, has very strong practical
Property.
Specific embodiment
The present invention is described in further detail combined with specific embodiments below, but embodiment is not to skill of the present invention
The restriction of art scheme.
The preparation process of jujube absolute oil in following embodiments: mixed according to the ratio of weight ratio 1:7-10 using extra dry red wine jujube and water
After conjunction 100 DEG C at a temperature of refluxing extraction 1-3 times, combined extract simultaneously be concentrated into density be 1.0-1.1；Then to concentrate
The middle concentration for being added 2-5 times of concentrate weight is 95% ethyl alcohol or petroleum ether, stands 12-48 hours, uses aperture for 0.8 micron
Filter membrane filter off sediment obtain relative density be 0.9~1.0 filtrate be jujube absolute oil.
A kind of preparation method for the essence for increasing cigarette agalloch eaglewood note: embodiment 1 weighs 15 parts of jujube absolute oil, East India
0.15 part of sandalwood oil, 0.8 part of perillartine, 5 parts of ethyl acetate, 1.5 parts of sage clary oil, 77.55 parts of ethyl alcohol；By the raw material group
After point mixing, stirs 2 hours, static 24 hours, use aperture to filter off sediment for 0.8 micron of filter membrane and obtain relative density and be
0.85~0.95 filtrate is the essence for increasing cigarette agalloch eaglewood note.
Agalloch eaglewood essence is dissolved in 70% ethyl alcohol of 10 times of amounts, is sprayed on pipe tobacco according to 0.1% amount, and cigarette is made,
It compares and smokes panel test.
A kind of preparation method for the essence for increasing cigarette agalloch eaglewood note: embodiment 2 weighs 20 parts of jujube absolute oil, East India
0.1 part of sandalwood oil, 0.8 part of perillartine, 7 parts of ethyl acetate, 1.5 parts of sage clary oil, 70.6 parts of ethyl alcohol；By the raw material components
After mixing, stir 2 hours, static 24 hours, using aperture to filter off sediment to obtain relative density for 0.8 micron of filter membrane was 0.85
~0.95 filtrate is the essence for increasing cigarette agalloch eaglewood note.
Agalloch eaglewood essence is dissolved in 70% ethyl alcohol of 10 times of amounts, is sprayed on pipe tobacco according to 0.1% amount, and cigarette is made,
It compares and smokes panel test.
A kind of preparation method for the essence for increasing cigarette agalloch eaglewood note: embodiment 3 weighs 15 parts of jujube absolute oil, East India
0.2 part of sandalwood oil, 0.5 part of perillartine, 5 parts of ethyl acetate, 1 part of sage clary oil, 78.3 parts of ethyl alcohol；The raw material components are mixed
After conjunction, stir 2 hours, static 24 hours, use aperture for 0.8 micron of filter membrane filter off sediment obtain relative density be 0.85~
0.95 filtrate is the essence for increasing cigarette agalloch eaglewood note.
Agalloch eaglewood essence is dissolved in 70% ethyl alcohol of 10 times of amounts, is sprayed on pipe tobacco according to 0.1% amount, and cigarette is made,
It compares and smokes panel test.
Flavouring acting embodiment, selects middle-grade blank pipe tobacco, and the essence deployed to the embodiment of the present invention 1~3 is added to
Effect in cigarette is evaluated.7 people composition is smoked panel test group, and wherein national level is smoked panel test Shi Yiming, provincial teacher of the smokeing panel test two.
Evaluation of effect of the table 1 in cigarette
Cigarette quality is promoted by the essence that smoking result in table 1 shows that the present invention is modulated, has and promotes cigarette
The graceful sense of fragrance, flue gas is smooth, sends out thoroughly, there is sense of promoting the production of body fluid, and pleasant impression stays length, and pliability has embodiment, and fragrance is abundant, and oral cavity is clean etc.
Effect, can be used as novel tobacco flavor carry out using.
Applicant will carry out physical testing by the tobacco aromaticss of above-mentioned process exploitation, and physical index is as follows:
| Title | Flavouring essence for tobacco of the present invention |
| Appearance | Clarify rufous liquid |
| Fragrance | Fragrant and sweet, radix aucklandiae |
| Relative density (20/20 DEG C) | 0.9252 |
| Refraction index (20 DEG C) | 1.4108 |
| Miscible degree (25 DEG C) in ethyl alcohol | It can be miscible with 95% ethyl alcohol of arbitrary volume |
| Lead content (mg/kg) | ≤5.0 |
| Arsenic content (mg/kg) | ≤1.0 |
It is preferable to can be seen that essence prepared by the present invention its appearance, fragrance by upper table, wherein lead content and arsenic content be all
It is relatively low, meet the standard of flavouring essence for tobacco.
Claims (3)
1. a kind of preparation method for increasing cigarette agalloch eaglewood note essence, it is characterised in that specific step is as follows:
(1) prepare jujube absolute oil: after being mixed using extra dry red wine jujube and water according to the ratio of weight ratio 1:7-10 100 DEG C at a temperature of
Refluxing extraction 1-3 times, combined extract are simultaneously concentrated into density as 1.0-1.1；Then concentrate weight 2-5 is added into concentrate
Times petroleum ether, stand 12-48 hour, use aperture for 0.8 micron of filter membrane elimination sediment obtain relative density be 0.9~
1.0 filtrate is jujube absolute oil；
(2) prepare the raw material of following parts by weight: 15~25 parts of jujube absolute oil, East India sandalwood oil prepared in step (1)
0.1~1 part, 0.2~2 part of perillartine, 3~10 parts of ethyl acetate, 0.5~5 part of sage clary oil, 25~85 parts of ethyl alcohol；The second
The mass percent concentration of alcohol is 20~80%
(3) it is stirred 2-4 hours after mixing the raw material components in step (2), it is 24-48 hours static, use aperture for 0.8 micron
Filter membrane filter off sediment obtain relative density be 0.85~0.95 filtrate be it is described increase cigarette agalloch eaglewood note essence.
2. a kind of preparation method for increasing cigarette agalloch eaglewood note essence according to claim 1, it is characterised in that the original
Expect that component is as follows: 15 parts of jujube absolute oil, 0.1 part of East Indian sandalwood oil, 0.8 part of perillartine, 5 parts of ethyl acetate, sage clary oil 1.5
Part, 77.6 parts of ethyl alcohol.
3. a kind of application of the increase cigarette agalloch eaglewood note essence according to the method preparation in claim 1, it is characterised in that: will
The essence mass percent concentration of the above-mentioned increase cigarette agalloch eaglewood note prepared is the dilution of 50~95% ethanol solutions, will be dilute
The fragrance solution of increase cigarette agalloch eaglewood note after releasing is sprayed on pipe tobacco with laryngeal spray, and cigarette is made, wherein increasing
The essence of cigarette agalloch eaglewood note accounts for the 0.01~0.30% of pipe tobacco weight.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102827693A (en) * | 2012-08-16 | 2012-12-19 | 湖北中烟工业有限责任公司 | Flower fragrance aroma essence for tobacco |
| CN105054287A (en) * | 2015-06-29 | 2015-11-18 | 湖北中烟工业有限责任公司 | Additive for compensating fragrance of low-tar cigarettes |
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2016
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102827693A (en) * | 2012-08-16 | 2012-12-19 | 湖北中烟工业有限责任公司 | Flower fragrance aroma essence for tobacco |
| CN105054287A (en) * | 2015-06-29 | 2015-11-18 | 湖北中烟工业有限责任公司 | Additive for compensating fragrance of low-tar cigarettes |
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