CN105031187B - A kind of liquorice root honey fritillary bulb processed and preparation method - Google Patents
A kind of liquorice root honey fritillary bulb processed and preparation method Download PDFInfo
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- CN105031187B CN105031187B CN201510375959.8A CN201510375959A CN105031187B CN 105031187 B CN105031187 B CN 105031187B CN 201510375959 A CN201510375959 A CN 201510375959A CN 105031187 B CN105031187 B CN 105031187B
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Abstract
The present invention relates to a kind of liquorice root honey fritillary bulb processed, the preparation method of said preparation is also provided simultaneously, according to theory of traditional Chinese medical science basis, utilize said medicine compatibility relationship by honey moisten the lung and relieve the cough and dispelling of Radix Glycyrrhizae coughed the only mutual-assistance effect of phlegm, improve fritillary bulb moistening lung, eliminate the phlegm, cough-relieving effect. Three taste medicines are by compatibility, after the present invention's preparation, reach the moistening lung of effective increases fritillary bulb, eliminate the phlegm, antitussive action simultaneously, make the performance of fritillary bulb be tending towards sweet and put down, improved the mouthfeel of fritillary bulb, the crowd of taking is more easily taken. Under same dose, can reach the object of attenuation synergistic, to protecting and utilizing rare medicine resource to there is very big meaning.
Description
Technical field
The present invention relates to a kind of liquorice root honey fritillary bulb processed, the preparation method of said preparation be also provided simultaneously, belong to food andField of pharmaceutical technology.
Background technology
Fritillary bulb is the dry bulb of liliaceous plant fritillary bulb FritillariaussuriensisMaxim.. FlatThe bulb of fritillary has another name called level ground shellfish, the bulb of fritillary, flat shellfish. Have clearing heat and moistening lung, relieving cough and reducing sputum effect, is a kind of conventional Chinese medicine, with Bulbus Fritillariae Cirrhosae, Zhejiang shellfishMother belongs to Fritillaria together, but pharmaceutically has certain difference, is mainly distributed in Changbai Mountain arteries and veins and the south, the Xiaoxinanlin Mountains of the NortheastMountain area, the provinces such as main product Heilungkiang, Jilin, Liaoning and Shanxi, Shaanxi, Hebei.
Fritillary bulb pharmacological action is: 1, Bulbus Fritillariae Ussuriensis extractum has central inhibitory action to experimental animal models. Fritillary bulb is always rawThing alkali, pingpeimine A all have and significantly eliminate the phlegm and hypotensive activity. 2 fritillary bulb total alkali 3mg/100g, 1.5mg/100g rat skinHemostasis all has certain inhibitory action to pyloric ligation ulcers ulcer, lumbar injection to indocin type ulcer and stress ulcer,These effects may be relevant with its inhibition pepsin activity.
Fritillary bulb meridian distribution of property and flavor: bitter, sweet, be slightly cold. Return lung, the heart channel of Hang-Shaoyin. Function cures mainly as clearing heat and moistening lung, preventing phlegm from forming and stopping coughing. WithIn lung-heat type cough, the few phlegm of dry cough, deficiency of Yin labor is coughed, and coughs up sputum streaked with blood. Its effect and Bulbus Fritillariae Cirrhosae are close, medicinal effects compared with Bulbus Fritillariae Cirrhosae a little less than,Because Bulbus Fritillariae Cirrhosae belongs to wild rare medicinal herbs, resource is exhausted year by year in recent years. Because of the existing ripe artificial cultivation skill of its fritillary bulbArt, can plant in a large number, for improving the medicinal effects of fritillary bulb, improves fritillary bulb put down in cough-relieving by traditional Chinese medicine preparation methodBreathe heavily effect of aspect, reach the effect approaching with Bulbus Fritillariae Cirrhosae. Thereby improving medical value protects wild Bulbus Fritillariae Cirrhosae to have positive meaningJustice.
Summary of the invention
The invention provides a kind of liquorice root honey fritillary bulb processed, can strengthen the effect of fritillary bulb aspect cough-relieving with crossing the present inventionReally, increased the effect of relievining asthma simultaneously.
A kind of liquorice root honey of the present invention fritillary bulb processed, it is characterized in that being made up by ratio of weight and the number of copies of following medicine:
Honey 5～60, Radix Glycyrrhizae 5～30, fritillary bulb 5～100.
The preparation method of a kind of liquorice root honey of the present invention fritillary bulb processed, comprises the steps:
1) bulb of fritillary raw material of making even, choose decontamination, clean by the method for wash quickly, are placed in low-temperature vacuum drying case, warpDry 1 hour of 30 DEG C of low temperature, are dried to water content below 20%;
2) choose honey add pot in heating, refining to 105～110 DEG C and goods, refined honey water content more than 30%,Color and luster is without significant change, and slightly sticking refined honey is for subsequent use;
3) dry rhizome and the root of choosing glycyrrhizic legume clean, infiltrate, cut into slices, and add 3～6 times of decoctings and boil 2～3 times,Each 15～30 minutes, filter, collecting decoction and succus liquiritiae;
4) by step 2) and 3) mix that to obtain refined honey succus liquiritiae for subsequent use;
5) fritillary bulb being put into refined honey succus liquiritiae temperature prepared by step 4), to be controlled at 10～30 DEG C of infuses 2～48 littleTime, stirred 1 time every 6 hours during this time, it is evenly distributed, soak into fritillary bulb and absorb refined honey succus liquiritiae completely;
6) fritillary bulb after step 5) infuse is dried to water content below 15%, obtains final product.
In above-mentioned any technical scheme, refined honey is 5～60 weight portions, preferably 1～40 weight portion, more preferably 5～20Weight portion, more preferably 10～20 weight portions; Succus liquiritiae is 5～30 weight portions, preferably 5～20 weight portions, more preferably 5～15 weight portions, more preferably 6～10 weight portions; Fritillary bulb raw material is 5～100 weight portions, preferably 20～100 weight portions,Preferably 30～70 weight portions, more preferably 40～70 weight portions again.
Preparation method of the present invention also can adopt the preparation method of the conventional formulation of medicine and pharmacology.
[usage and dosage] 3～9g; Levigation is taken after mixing it with water, a 1～2g.
[indication] function cures mainly clearing heat and moistening lung, reduces phlegm, and cough-relieving. For lung-heat type cough, the few blood of dry cough, deficiency of Yin labor is coughed, and coughs upSputum streaked with blood.
[attention] should not be with monkshood, aconiti preparata,radix, radix aconiti agrestis, wild aconite root, monkshood should not be with Aconitum medicinal material with using with using.
Pharmacological effect side of the present invention separates as follows:
Honey, performance: taste is sweet, flat; Return taste, lung and large intestine channel. Function bowl spares, cough-relieving, moisturizes, removing toxic substances. For moistening lung stopsCough, the process of preparing Chinese medicine auxiliary material of tonifying middle-Jiao and Qi medicine, in order to synergy, moisturize and correct mouthfeel. As honey-moxibustion ginseng, honey are processed the tuber of stemona, honey is processed purpleGarden, sweet honey-fried FLOS FARFARAE, honey are processed mulberry leaf, sweet honey-fried CORTEX MORI, honey and are processed the fruit of Chinese magnoliavine, Radix Glycyrrhizae (processed with honey) etc.
Fritillary bulb, performance: bitter, sweet, be slightly cold. Return lung, the heart channel of Hang-Shaoyin. Clearing heat and moistening lung, reduce phlegm, cough-relieving. For lung-heat type cough, dryCough few blood, deficiency of Yin labor is coughed, and coughs up sputum streaked with blood.
Radix Glycyrrhizae, another name: old, the sweet grass of state, Glycyrrhiza Uralensis, sweet root. Pulse family, Glycyrrhiza perennial herb, root and root shapeStem is sturdy, is a kind of help Chinese herbal medicine. To the good a kind of medicine of human body, medicinal part is root and rhizome. Taste is sweet, flat, the thoughts of returning home,Lung, spleen, stomach warp, tool is invigorated the spleen and benefited qi, clearing heat and detoxicating, expelling phlegm and arresting coughing, the effect of relieving spasm to stop pain. Medicine can relax after succus liquiritiae systemThe property of medicine, reduces toxicity. As succus liquiritiae boils polygala root, evodia rutaecarpa.
The present invention is according to theory of traditional Chinese medical science basis, utilizes said medicine compatibility relationship moistening the lung and relieve the cough and Radix Glycyrrhizae honeyDispel and cough the only mutual-assistance effect of phlegm, improve fritillary bulb moistening lung, eliminate the phlegm, cough-relieving effect, increased the effect of relievining asthma simultaneously. Three taste medicinesBy compatibility, after the present invention preparation, reach the moistening lung of effective increases fritillary bulb, eliminate the phlegm, cough-relieving, antiasthmatic effect while, make flat shellfishIt is sweet flat that female performance is tending towards, and improved the mouthfeel of fritillary bulb, and the crowd of taking is more easily taken.
Carry out pharmacological evaluation for the validity that proves this invention from pharmacodynamics aspect, be reported as follows:
1, see the following form in cough-relieving experiment (ammoniacal liquor draws the method for coughing) [1]:
Fritillary bulb, liquorice liquid, the comparison of liquorice root honey fritillary bulb cough-relieving processed effect
Note: with model control group comparison: * p < 0.05.
Fritillary bulb, liquorice liquid, liquorice root honey fritillary bulb processed all can reduce mouse cough reactivity as seen from the above table, with model pairAccording to group comparing difference significance (p < 0.05), and liquorice root honey fritillary bulb group processed antitussive action is better than fritillary bulb group and liquorice liquidGroup, and suitable with codeine group.
2, the experiment (phenol red method) [1] of eliminating the phlegm
Fritillary bulb, liquorice liquid, the comparison of liquorice root honey fritillary bulb phlegm-dispelling functions processed (）
With model control group comparison: * p < 0.05, * * p < 0.01; Compare with liquorice root honey fritillary bulb group processed: #p < 0.05
As seen from the above table: relatively there were significant differences (p < 0.05 or p < 0.01) for the OD value of each administration group and model control group,Illustrative experiment group all has good phlegm-dispelling functions, and the phlegm-dispelling functions of liquorice root honey fritillary bulb group processed is obviously better than fritillary bulb group and sweetGrass group.
3, the experiment (spraying causes the method for breathing heavily) of relievining asthma
Fritillary bulb, liquorice liquid, the comparison of liquorice root honey fritillary bulb antiasthmatic effect processed (）
With model group comparison: * p < 0.05, * * p < 0.01; Compare with liquorice root honey fritillary bulb group processed: #p < 0.05
As seen from the above table: fritillary bulb group and Radix Glycyrrhizae group mouse occur Order reaction has prolongation trend incubation period, but and modelControl group comparing difference not obvious (p > 0.05), liquorice root honey fritillary bulb group processed can obviously extend mouse Order reaction incubation period(p < 0.05), points out its antiasthmatic effect to be obviously better than fritillary bulb group and Radix Glycyrrhizae group.
Cough-relieving, the effect of eliminating the phlegm, relieving asthma of the fritillary bulb of comprehensive above 3 pharmacological action contrast experiments after the present invention concoctsFruit has the effect of remarkable enhancing compared with fritillary bulb primary crude drug and Radix Glycyrrhizae.
Further illustrate good effect of the present invention below in conjunction with clinical:
One, diagnostic criteria:
Be diagnosed as according to " Diagnostics of Chinese Medicine ": lung-heat type cough, the few blood of dry cough, deficiency of Yin labor is coughed, and coughs up sputum streaked with blood.
Two, inclusive criteria:
The above-mentioned standard of all genus all can be included in clinical. Three, using method:
In composition of prescription, compatibility uses or folk prescription use. Four, curative effect judging standard:
By all reaching and improve patient's symptom after fritillary bulb treatment processed.
Good effect of the present invention is: the present invention is according to theory of traditional Chinese medical science basis, utilizes said medicine compatibility relationship to incite somebody to actionHoney moisten the lung and relieve the cough and dispelling of Radix Glycyrrhizae coughed the only mutual-assistance effect of phlegm, improve fritillary bulb moistening lung, eliminate the phlegm, cough-relieving effect. Three tastesMedicine is by compatibility, after the present invention's preparation, reach the moistening lung of effective increases fritillary bulb, eliminate the phlegm, the antitussive action while, makes fritillary bulbIt is sweet flat that performance is tending towards, and improved the mouthfeel of fritillary bulb, and the crowd of taking is more easily taken. Under same dose, can reach attenuationThe object of synergy, to protecting and utilizing rare medicine resource to have very big meaning.
Detailed description of the invention
Following embodiment and case application, be only for example of the present invention is clearly described, and not to thisThe restriction of invention. For those of ordinary skill in the field, can also make other not on the basis of the above descriptionWith variation or the variation of form. And the apparent variation of being amplified out thus or variation are still in protection scope of the present inventionAmong.
Embodiment 1:
1, get 50g fritillary bulb medicinal material, the removal of impurity, cleans by the method for wash quickly, is placed in low-temperature vacuum drying case, warpDry 1 hour of 30 DEG C of low temperature, are dried to water content 20%;
2, getting 10g honey refines 4 minutes to such an extent that refined honey water is for subsequent use 110 DEG C of temperature;
3, choose cleaning, infiltrate, cutting into slices of 30g Radix Glycyrrhizae, add 120g decocting and boil 2 times, each 15 minutes, filter, merging is decoctedLiquid and succus liquiritiae;
4, step 2 and 3 is mixed to obtain refined honey succus liquiritiae for subsequent use;
5, fritillary bulb raw material dry step 1 being placed in to step 4) refined honey succus liquiritiae stirs at 25 DEG C of infuses of constant temperature8 hours, stirred 1 time every 4 hours during this time, it is evenly distributed, soak into fritillary bulb and absorb refined honey succus liquiritiae completely;
6, step 5 is processed to the fritillary bulb obtaining and be placed in low-temperature vacuum drying case, be dried 3 hours through 30 DEG C of low temperature, dryDry to water content 15%, to obtain final product.
Embodiment 2:
1, get 300g fritillary bulb medicinal material, the removal of impurity, cleans by the method for wash quickly, is placed in low-temperature vacuum drying case, warpDry 1 hour of 30 DEG C of low temperature, are dried to water content 20%;
2, getting 200g honey refines 10 minutes to such an extent that refined honey water is for subsequent use 110 DEG C of temperature;
3, choose cleaning, infiltrate, cutting into slices of 150g Radix Glycyrrhizae, add 900g decocting and boil 3 times, each 15 minutes, filter, merging is decoctedLiquid and succus liquiritiae;
4, step 2 and 3 is mixed to obtain refined honey succus liquiritiae for subsequent use;
5, fritillary bulb raw material dry step 1 being placed in to step 4) refined honey succus liquiritiae stirs at 22 DEG C of infuses of constant temperature12 hours, stirred 1 time every 4 hours during this time, it is evenly distributed, soak into fritillary bulb and absorb refined honey succus liquiritiae completely;
6, step 5 is processed to the fritillary bulb obtaining and be placed in low-temperature vacuum drying case, be dried 5 hours through 30 DEG C of low temperature, dryDry to water content 15%, to obtain final product.
Embodiment 3:
1, get 100g fritillary bulb medicinal material, the removal of impurity, cleans by the method for wash quickly, is placed in low-temperature vacuum drying case, warpDry 1 hour of 30 DEG C of low temperature, are dried to water content 20%;
2, getting 80g honey refines 7 minutes to such an extent that refined honey water is for subsequent use 110 DEG C of temperature;
3, choose cleaning, infiltrate, cutting into slices of 50g Radix Glycyrrhizae, add 200g decocting and boil 2 times, each 15 minutes, filter, merging is decoctedLiquid and succus liquiritiae;
4, step 2 and 3 is mixed to obtain refined honey succus liquiritiae for subsequent use;
5, fritillary bulb raw material dry step 1 being placed in to step 4) refined honey succus liquiritiae stirs at 18 DEG C of infuses of constant temperature8 hours, stirred 1 time every 4 hours during this time, it is evenly distributed, soak into fritillary bulb and absorb refined honey succus liquiritiae completely;
6, step 5 is processed to the fritillary bulb obtaining and be placed in low-temperature vacuum drying case, be dried 2 hours through 25 DEG C of low temperature, dryDry to water content 15%, to obtain final product.
Further show the result for the treatment of of medicine of the present invention by following model case:
Case 1
Certain female, 53 years old, tcm diagnosis: pulse condition, number is thin; Red tongue with thin fur; Dry cough, without phlegm, few and the sticky or phlegm of phlegm as line powder notEasily bring up, tcm diagnosis is lung-heat type cough.
Treatment: 6 grams of liquorice root honey fritillary bulbs processed prepared by the embodiment of the present invention 1, grinding is taken after mixing it with water, every day 3 times.
Effect: take 3 days afterwards cough improve adhering to taking after 2 weeks and fully recover.
Case 2
Certain man, 42 years old; Tcm diagnosis: shortness of breath and fatigue, Lung-Yin deficiency chronic cough, arteries and veins is thin and delicate.
Treatment: 6 grams of liquorice root honey fritillary bulbs processed prepared by the embodiment of the present invention 2, soaked every day 3 times, 14 days courses for the treatment of.
Effect: the present invention has strengthened antitussive action, simultaneously honey has effect of moistening lung, takes the transference cure of coughing after 1 month,After taking two courses for the treatment of, chronic cough symptom is fully recovered, and shortness of breath and fatigue has obtained good improvement.
Case 3
Certain man, 60 years old; Tcm diagnosis, red tongue with a little fluid, arteries and veins is carefully heavy, belongs to prolonged illness impairment of yin, body fluid deficiency, causes dryness of the lung dry cough, phlegmFew even without phlegm.
Treatment: 6 grams of liquorice root honey fritillary bulbs prepared by the embodiment of the present invention 3, grind into powder and take after mixing it with water, 3 times on the one.
Effect: there is good moistening lung function when the present invention strengthens antitussive action, take dry cough after 1 week and obviously alleviateContinuing to take symptom after 1 month disappears completely.
Claims (1)
1. a preparation method for liquorice root honey fritillary bulb processed, is characterized in that step is as follows:
1) get 50g fritillary bulb medicinal material, the removal of impurity, cleans by the method for wash quickly, is placed in low-temperature vacuum drying case, through low temperature 30DEG C dry 1 hour, be dried to water content 20%;
2) getting 10g honey refines 4 minutes to such an extent that refined honey water is for subsequent use 110 DEG C of temperature;
3) choose cleaning, infiltrate, cutting into slices of 30g Radix Glycyrrhizae, add 120g decocting and boil 2 times, each 15 minutes, filter, collecting decoction andObtain succus liquiritiae;
4) by step 2) and 3) juice of gained mixes that to obtain refined honey succus liquiritiae for subsequent use;
5) by step 1) dry fritillary bulb raw material is placed in step 4) refined honey succus liquiritiae and stirs little at 25 DEG C of infuses 8 of constant temperatureTime, stirred 1 time every 4 hours during this time, it is evenly distributed, soak into fritillary bulb and absorb refined honey succus liquiritiae completely;
6) by step 5) process the fritillary bulb that obtains and be placed in low-temperature vacuum drying case, through dry 3 hours of 30 DEG C of low temperature, be dried toWater content 15%, to obtain final product.
2. a preparation method for liquorice root honey fritillary bulb processed, is characterized in that step is as follows:
1) get 300g fritillary bulb medicinal material, the removal of impurity, cleans by the method for wash quickly, is placed in low-temperature vacuum drying case, through low temperature30 DEG C are dried 1 hour, are dried to water content 20%;
2) getting 200g honey refines 10 minutes to such an extent that refined honey water is for subsequent use 110 DEG C of temperature;
3) choose cleaning, infiltrate, cutting into slices of 150g Radix Glycyrrhizae, add 900g decocting and boil 3 times, each 15 minutes, filter, collecting decoction andObtain succus liquiritiae;
4) by step 2) and 3) juice of gained mixes that to obtain refined honey succus liquiritiae for subsequent use;
5) by step 1) dry fritillary bulb raw material is placed in step 4) refined honey succus liquiritiae and stirs at 22 DEG C of infuses 12 of constant temperatureHour, stirred 1 time every 4 hours during this time, it is evenly distributed, soak into fritillary bulb and absorb refined honey succus liquiritiae completely;
6) by step 5) process the fritillary bulb that obtains and be placed in low-temperature vacuum drying case, through dry 5 hours of 30 DEG C of low temperature, be dried toWater content 15%, to obtain final product.
3. a preparation method for liquorice root honey fritillary bulb processed, is characterized in that step is as follows:
1) get 100g fritillary bulb medicinal material, the removal of impurity, cleans by the method for wash quickly, is placed in low-temperature vacuum drying case, through low temperature30 DEG C are dried 1 hour, are dried to water content 20%;
2) getting 80g honey refines 7 minutes to such an extent that refined honey water is for subsequent use 110 DEG C of temperature;
3) choose cleaning, infiltrate, cutting into slices of 50g Radix Glycyrrhizae, add 200g decocting and boil 2 times, each 15 minutes, filter, collecting decoction andObtain succus liquiritiae;
4) by step 2) and 3) juice of gained mixes that to obtain refined honey succus liquiritiae for subsequent use;
5) by step 1) dry fritillary bulb raw material is placed in step 4) refined honey succus liquiritiae and stirs little at 18 DEG C of infuses 8 of constant temperatureTime, stirred 1 time every 4 hours during this time, it is evenly distributed, soak into fritillary bulb and absorb refined honey succus liquiritiae completely;
6) by step 5) process the fritillary bulb that obtains and be placed in low-temperature vacuum drying case, through dry 2 hours of 25 DEG C of low temperature, be dried toWater content 15%, to obtain final product.
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