CN105030650B - A kind of mild face cream and preparation method thereof - Google Patents
A kind of mild face cream and preparation method thereof Download PDFInfo
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- CN105030650B CN105030650B CN201510401575.9A CN201510401575A CN105030650B CN 105030650 B CN105030650 B CN 105030650B CN 201510401575 A CN201510401575 A CN 201510401575A CN 105030650 B CN105030650 B CN 105030650B
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Abstract
The invention discloses a kind of mild face cream, and including component A, B component and component C, component A is made of water, glycerine, carrageenan sodium, xanthans, trehalose, hydrolytic collagen and citric acid；B component is made of olive oil, prinsepia utilis royle oil, caprylic/capric triglyceride, beeswax and sucrose stearate；Component C is made of sunflower seed oil and rosemary leaf extract, vitamin E and bright string coccus/radish root tunning filtrate.The face cream of the present invention, recipe ingredient derive from food additives or raw-food material, and using natural bacteriostatic ingredient and natural, compatibility is good, and cutaneous safety test is non-stimulated, are a kind of mild, the permanent moisturizing of safe and stable and energy cosmetics；The present invention provides a kind of above-mentioned preparation methods of mild face cream simultaneously.
Description
Technical field
The invention belongs to daily cosmetics field, more particularly, to a kind of mild face cream and preparation method thereof.
Background technology
With the development of society, the progress of science, people increasingly pay attention to health, pay close attention to the quality of life, from
Emphatically color, smell and taste to pay attention to collocation, nutrition, health, safety.The Cosmetic Market of China is the emerging market of whole world maximum, is protected
Emerging in multitude for skin cosmetics makes people too plenty for the eye to take it all in, and people also focus more on makeup other than the cosmetics for learning to make good use of
The effect of product and safety.Therefore related " no added cosmetics ", " plant cosmetics ", " organic cosmetics ", " natural in recent years
The theories such as cosmetics ", " edible to apply some make up " receive the welcome of consumer.However, current most cosmetics on the market
It is difficult to which consumer is allowed to recognize whole components of product from product packaging, and it is difficult validity and the safety for judging product,
Even declare edible cosmetics, formula is also that constituent part derives from food additives or animal and plant raw material.
The safeties of cosmetics is to ensure the important prerequisite of cosmetics quality with stability, and grease in formula system, anti-
The selection of rotten agent etc. can have particularly important influence to the safety of cosmetics with stability again with using.Vegetable fat is rich in
Unrighted acid easily aoxidizes, and caused product discoloration, spoiled iso-metamorphism phenomenon, general preservative have slight thorn
Swash property and toxicity.Therefore, while pursuit cosmetic material is mild safely, the good compatibility of recipe ingredient is also ensured.
Olive oil is rich in abundant unrighted acid, has splendid natural health and beauty functions；Prinsepia utilis royle oil comes
From plateau plant kingdom Yunnan, rich in unrighted acid, and its composition is approached with human sebaceous's class, has skin regeneration technique
And moisture-keeping function；Hydrolytic collagen, trehalose are good nutritional ingredient and moisturizer；Rosemary leaf extract is a kind of natural excellent
Different oil-soluble inhibitor；Bright string coccus/radish root tunning filtrate is not belonging to preservative, be it is a kind of it is natural it is antibacterial into
Point.By raw materials such as these vegetable fat, moisturizer, natural, natural bacteriostatic ingredients, by scientific and reasonable experiment,
Screening is investigated and is detected, and can just produce safety, mild, stable quality face cream.
Invention content
The purpose of the invention is to overcome the deficiencies of the prior art and provide a kind of mild face cream, each raw material is equal
Using food grade raw material, food additives or raw-food material are derived from, formula uses natural bacteriostatic ingredient and natural anti-oxidation
Agent, compatibility is good, and cutaneous safety test is non-stimulated, is a kind of mild, the permanent moisturizing of safe and stable and energy makeup
Product.
Another object of the present invention is to provide a kind of preparation method of above-mentioned mild face cream.
Realizing a kind of technical solution of above-mentioned purpose is：A kind of mild face cream, including component A, B component and component C,
The component A is made of the raw material of following weight parts：
The B component is made of the raw material of following weight parts：
The component C is made of the raw material of following weight parts：
0.1~1 part of sunflower seed oil and rosemary leaf extract；
0.01~0.2 part of vitamin E；
Bright string coccus/2~2.4 parts of radish root tunning filtrate.
A kind of above-mentioned mild face cream, wherein, each raw material of the component A, each raw material of B component and component C
Each raw material use food grade raw material.
Above-mentioned raw materials are commercial product.
The present invention's additionally provides a kind of preparation method of mild face cream, includes the following steps：
Component A dissolving step：First carrageenan sodium and xanthans are added successively in glycerine and disperseed with glycerine, is formed
Glycerine dispersion, then water, glycerine dispersion, trehalose, hydrolytic collagen and citric acid are sequentially added in kettle, it is heated with stirring to
75~80 DEG C, component A is made in insulated and stirred 10~30 minutes；
B component dissolving step：By olive oil, prinsepia utilis royle oil, caprylic/capric triglyceride, beeswax and sucrose stearate
It adds in oil cauldron, is heated with stirring to 70~75 DEG C, is completely dissolved, B component is made；
Emulsifying step：Component A in the kettle through 200 mesh screens and is pumped into emulsification pot, opens homogeneous, homogeneous
Speed is 3000rpm, then the B component in the oil cauldron through 200 mesh screens and is pumped into the emulsification pot, at 70~75 DEG C
Homogeneous 5~10 minutes, then cools down under stirring；
Add in component C step：When the temperature cooling in the emulsification pot is not higher than 40 DEG C, sunflower seed oil and fan are changed
Herba Pelargonii Graveolentis extract, vitamin E and bright string coccus/radish root tunning filtrate are sequentially added in the emulsification pot, homogeneous 2-5
Minute, homogeneous speed is 2000-3000rpm, vacuum outgas under stirring, filtering and discharging after natural cooling.
The preparation method of above-mentioned mild face cream, wherein, each raw material of the component A, each raw material of B component and
Each raw material of component C uses food grade raw material.
Employ a kind of technical solution of mild face cream of the present invention, compared with prior art, mild shield of the invention
Skin frost has the advantages that：
(1) mild face cream of the invention, each raw material of recipe ingredient using food grade materials, derive from food additive
Add agent or raw-food material, it is safe and non-stimulating, even if eating by mistake, damage and security risk will not be generated to human body.
(2) mild face cream of the invention can allow ordinary consumer to be easier to recognize each in formula according to common sense
Component, and the safety of principium identification each component.
(3) the more demanding raw materials of compatibilities such as mild face cream of the invention, vegetable oil, natural bacteriostatic ingredient,
Stability is good in this formula system, safety is good.
A kind of technical solution of the preparation method of mild face cream using the present invention, can also realize more than technique effect.
Description of the drawings
Fig. 1 is the flow chart of the preparation method of the mild face cream of the present invention；
Fig. 2 is the test result figure using the skin moisture content before and after the mild face cream in each embodiment.
Specific embodiment
The present inventor is in order to preferably understand technical scheme of the present invention, below by specifically real
It applies example and is described in detail with reference to attached drawing：
Embodiment 1
A kind of mild face cream, each component are made of the raw material of following weight parts：
Component A：80.45 parts of water, 2 parts of glycerine, 1 part of carrageenan sodium, 0.5 part of xanthans, 2 parts of trehalose, hydrolytic collagen
0.05 part and 0.1 part of citric acid；
B component：5 parts of olive oil, 0.5 part of prinsepia utilis royle oil, 3 parts of caprylic/capric triglyceride, 1 part of beeswax and sucrose are stearic
2 parts of acid esters；
Component C：Sunflower seed oil and 0.3 part of rosemary leaf extract, 0.1 part of vitamin and bright string coccus/radish root fermentation
2 parts of Product filtrate.
Embodiment 2
A kind of mild face cream, each component are made of the raw material of following weight parts：
Component A：68.82 parts of water, 4 parts of glycerine, 0.8 part of carrageenan sodium, 0.2 part of xanthans, 3 parts of trehalose, hydrolysis glue
Former 0.03 part and 0.1 part of citric acid；
B component：10 parts of olive oil, 1.5 parts of prinsepia utilis royle oil, 5 parts of caprylic/capric triglyceride, 0.8 part of beeswax and sucrose are hard
3 parts of resin acid ester；
Component C：Sunflower seed oil and 0.5 part of rosemary leaf extract, 0.05 part of vitamin E and bright string coccus/radish root
2.2 parts of tunning filtrate.
Embodiment 3
A kind of mild face cream, each component are made of the raw material of following weight parts：
Component A：56.77 parts of water, 7 parts of glycerine, 0.5 part of carrageenan sodium, 0.1 part of xanthans, 1 part of trehalose, hydrolysis glue
Former 0.01 part and 0.1 part of citric acid；
B component：13 parts of olive oil, 2.5 parts of prinsepia utilis royle oil, 10 parts of caprylic/capric triglyceride, 2 parts of beeswax and sucrose are hard
4 parts of resin acid ester；
Component C：Sunflower seed oil and 0.6 part of rosemary leaf extract, 0.02 part of vitamin E and bright string coccus/radish root
2.4 parts of tunning filtrate.
Each raw material of each component of embodiment 1-3 using food grade raw material, derives from food additives or food is former
Material.
Water is prepared using the Laboratory Pure Water system Master-S of Shanghai Hitech Instruments Co., Ltd.；Glycerine uses section
The trade name Glycerine 99.5% of Ninghua work (China) Co., Ltd production；Carrageenan sodium is using hundred taste of Hebei biology
The trade name carragheen of Science and Technology Ltd.'s production；Xanthans uses the trade name RHODI CARE of Rhodia's production
H；The trade name TREHALOSE that trehalose is produced using Lin Yuan companies of Japan；Hydrolytic collagen is using prompt into trade Co., Ltd
The trade name Naticol 1000 of production；The trade name one of citric acid Chinasun Specialty Products Co., Ltd production
Citric acid monohydrate；The trade name Akogreen O of this grease (Shanghai) Co., Ltd. of olive oil A Husi karrs production；Blueness thorn
Fruit oil uses the trade name prinsepia utilis royle oil of Lijiang Gonghe Industrial Co., Ltd.'s production；Caprylic/capric triglyceride uses
The trade name TEGOSOFT CT of EVONIK companies production；Beeswax uses the trade name of Shanghai Zi Bang Chemical Co., Ltd.s production
For SOLI BEE WAX；Sucrose stearate uses the trade name PYOTO SUGAR ESTER S- of Mitsubishi Corporation of Japan production
1170；Sunflower seed oil and rosemary leaf extract use the trade name Rosamox of KEMI N companies production；Vitamin E is adopted
With the trade name dl- α-Tocopherol of DSM N. V.；Bright string coccus/radish root tunning filtrate uses Active
The trade name AMS Leucidal Liquid of Concepts companies production.
Mild face cream provided by the invention is prepared by following steps：
Component A dissolving step：First carrageenan sodium and xanthans are added successively in glycerine and disperseed with glycerine, is formed
Glycerine dispersion, then water, glycerine dispersion, trehalose, hydrolytic collagen and citric acid are sequentially added in kettle, it is heated with stirring to
75~80 DEG C, component A is made in insulated and stirred 10~30 minutes；
B component dissolving step：By olive oil, prinsepia utilis royle oil, caprylic/capric triglyceride, beeswax and sucrose stearate
It adds in oil cauldron, is heated with stirring to 70~75 DEG C, is completely dissolved, B component is made；
Emulsifying step：Component A in the kettle through 200 mesh screens and is pumped into emulsification pot, opens homogeneous, homogeneous
Speed is 3000rpm, then the B component in the oil cauldron through 200 mesh screens and is pumped into the emulsification pot, at 70~75 DEG C
Homogeneous 5~10 minutes, then cools down under stirring；
Add in component C step：When the temperature cooling in the emulsification pot is not higher than 40 DEG C, sunflower seed oil and fan are changed
Herba Pelargonii Graveolentis extract, vitamin E and bright string coccus/radish root tunning filtrate are sequentially added in the emulsification pot, homogeneous 2-5
Minute, homogeneous speed is 2000-3000rpm, vacuum outgas under stirring, filtering and discharging after natural cooling.
Performance detection is carried out to the mild face cream of embodiment 1-3, including stability test, anti-corrosion function test, safety
Property test and moisture of skin test.
Stability test
Study on the stability is carried out to the mild face cream of the above-mentioned embodiment 1-3 prepared, product stability investigates reference
Standard QB/T 1857-2004《Moisturizing cream》, in order to obtain more stable product, condition requirement is investigated higher than QB/T 1857-
2004, successively at -15 DEG C, 5 DEG C, 40 DEG C and 49 DEG C, test 15 days, 30 days, 45 days, 60 days and 90 days respectively, test this hair
The stability of bright mild face cream, stability test result of the test are as shown in table 1：
Table 1
Stability test result of the test is shown in table 1：The mild face cream of embodiment 1,2,3,49 DEG C of heat-resisting investigations restore
Lotion is without water-oil separating phenomenon after to room temperature, and -15 DEG C cold-resistant to investigate, after restoring to room temperature with before experiment without apparent Traits change.
Therefore the mild face cream of the present invention has good formula compatibility and product quality stability.
Anti-corrosion function is tested
Preservative efficacy evaluation is carried out by preservation challenge experiment.The method is with reference to United States Pharmacopeia USP28 editions-anti-micro- life
Object preservative efficacy is tested.The mild face cream of embodiment 1,2,3 is mixed into the cell culture substrate of identical type respectively, then
The fungi and mould of disposable access standard volume, at a temperature of sample is deposited in 37 DEG C, regular sampling Detection residual therein
Fungi number and residual fungi count, and the antibacterial of sample effect is evaluated according to the situation of change of residual fungi number and residual fungi count
Fruit.
Criterion：The residual work bacterial population and the equal 1.0 × 103CFU/ of ＜ of fungi number living being detected in sample at the 28th day
g(ml)；From the 14th day, the residual work bacterial population and fungi number living that are detected in the sample of the 21st day and the 28th day cannot be again
Increase.
Preservative efficacy test result is as shown in table 2：
Table 2
By 2 preservative efficacy test result of table it is found that at the 7th day, the residual that is detected in 1,2,3 sample of embodiment is lived bacterium
Number equal 1.0 × 103CFU/g of ＜, at the 14th day, the equal 1.0 × 103CFU/g of ＜ of remaining bacteria number, and clump count does not increase.Cause
The mild face cream of this present invention has good preservative efficacy.
Security test
Security test includes acute skin irritation test and acute eye irritation test.
(1) acute skin irritation test：
Acute skin irritation test is carried out to the mild face cream of embodiment 1,2,3, each embodiment selects 4 whites
Cavy is tested, and tests room temperature：20-24 DEG C, relative humidity：60-70%.Before experiment about for 24 hours, by experimental animal back ridge
Column both sides hair is cut, and unhairing range is respectively 2cm × 3cm, application area 2.5cm × 2.5cm.Tested material about 0.5mL is taken to smear
On the skin of side, when tested material is prepared using nonirritant solvent, opposite side applies solvent as compareing, and smears 1 time daily,
It is continuous to smear 14 days.Since second day, cropping is answered before smearing every time, tested material is remained with water or nonirritant solvent cleaning,
Result is observed after one hour.Reference《Cosmetics health specification (2007 editions)》Regulation carries out stimulate the reaction scoring.
Table 3
By the acute skin irritation test result of table 3 it is found that the mild face cream of embodiment 1,2,3 is to the acute skin of cavy
Skin irritant test, is showed no irritative response.Therefore a kind of mild face cream of the present invention, acute skin irritation test result table
It is bright there is no skin irritation.
(2) acute eye irritation test
Carry out acute eye irritation test to the mild face cream of embodiment 1,2,3, each embodiment select 3 health into
Year white rabbit is tested, and tests room temperature：20-24 DEG C, relative humidity：60-70%.Animal will be in experimental animal before experiment
3 day time is at least adapted in room environment.A palpebra inferior for hairy rat side eyes is gently pulled open, tested material 0.1mL (100mg) is dripped
Enter in (or being painted into) conjunctival sac, upper and lower eyelid is made passively to be closed 1s, to prevent tested material from losing.Opposite side eyes do not handle work
Own control.After instilling tested material eyes are not rinsed in 24 hours.If thinking necessary, can be rinsed when for 24 hours.If above-mentioned examination
It tests result and shows that tested material is irritant, optionally need to be rinsed effect test with 3 rabbit, i.e., instill tested material to rabbit eyes
30s is very fast with enough, flow velocity but the flow of animal eye injury will not be caused to rinse at least 30s afterwards.1 after tested material is instilled,
24th, 48,72 hours and the 4th drop and the 7th drop animal eyes are checked.If 72 hours do not occur stimulate the reaction, you can
Termination test.If it find that involve cornea or there are other Eye irritations to act on, not recuperator in 7 days, to determine the reversible of the damage
Property or irreversibility need to extend observing time, be usually no more than 21 days.Reference《Cosmetics health specification (2007 editions)》Provide into
Row stimulate the reaction scores.
Table 4
By the acute ocular stimulation test result of table 4 it is found that the mild face cream of embodiment 1,2,3 is to the eye irritation of rabbit
Experiment has no irritative response.Therefore a kind of mild face cream of the present invention, acute eye irritation test show no acute ocular thorn
Swash property.
Moisture of skin is tested
Using German CK companies moisture of skin tester MPA10, moisture measurement probe vertical is pressed in tested by when test
Inner forearm skin surface, probe top are pushed back a distance, keep the pressure of 0.16N, just shown on host in one second
Go out result.Test condition be 25 ± 2 DEG C of temperature, humidity 50 ± 10%.Test result is as shown in the figure.
By the moisture of skin test result of Fig. 1 it is found that the face cream of embodiment 1,2,3 30min reaches most after smearing
Good moistening effect, moisture growth rate is all higher than 0 after 90min, illustrates that moistening effect is good, and with stronger lasting moisturizing energy
Power, the effect of wherein embodiment 3 are best.
In conclusion the mild face cream of the present invention, each raw material using food grade raw material, derives from food addition
Agent or raw-food material, formula is using natural bacteriostatic ingredient and natural, and compatibility is good, and cutaneous safety test is stingless
Swash, be a kind of mild, the permanent moisturizing of safe and stable and energy cosmetics.
Those of ordinary skill in the art it should be appreciated that more than embodiment be intended merely to illustrate the present invention,
And be not used as limitation of the invention, as long as in the spirit of the present invention, the change to embodiment described above
Change, modification will be all fallen in the range of claims of the present invention.
Claims (1)
1. a kind of preparation method of mild face cream, which includes component A, B component and component C,
The component A is made of the raw material of following weight parts：
The B component is made of the raw material of following weight parts：
The component C is made of the raw material of following weight parts：
0.1~1 part of sunflower seed oil and rosemary leaf extract；
0.01~0.2 part of vitamin E；
Bright string coccus/2~2.4 parts of radish root tunning filtrate,
Each raw material of each raw material of the component A, each raw material of B component and component C uses food grade raw material,
Preparation method includes the following steps：
Component A dissolving step：First carrageenan sodium and xanthans are added successively in glycerine and disperseed with glycerine, forms glycerine
Dispersion, then water, glycerine dispersion, trehalose, hydrolytic collagen and citric acid are sequentially added in kettle, it is heated with stirring to 75~
80 DEG C, component A is made in insulated and stirred 10~30 minutes；
B component dissolving step：Olive oil, prinsepia utilis royle oil, caprylic/capric triglyceride, beeswax and sucrose stearate are added in
In oil cauldron, 70~75 DEG C are heated with stirring to, is completely dissolved, B component is made；
Emulsifying step：Component A in the kettle through 200 mesh screens and is pumped into emulsification pot, opens homogeneous, homogeneous speed
It through 200 mesh screens and is pumped into the emulsification pot for 3000rpm, then by the B component in the oil cauldron, in 70~75 DEG C of homogeneous
5~10 minutes, then cool down under stirring；
Add in component C step：When the temperature cooling in the emulsification pot is not higher than 40 DEG C, by sunflower seed oil and rosemary leave
Extract, vitamin E and bright string coccus/radish root tunning filtrate are sequentially added in the emulsification pot, homogeneous 2-5 minutes,
Homogeneous speed is 2000-3000rpm, vacuum outgas under stirring, filtering and discharging after natural cooling,
Each raw material of each raw material of the component A, each raw material of B component and component C uses food grade raw material.
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| CN106074225B (en) * | 2016-08-11 | 2019-07-09 | 宁波御坊堂生物科技有限公司 | Edibility watch box cream and preparation method thereof |
| CN107088176B (en) * | 2017-06-08 | 2018-10-26 | 花安堂生物科技集团有限公司 | A kind of cosmetic material of blackcurrant seed oil |
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| CN102641232A (en) * | 2012-05-18 | 2012-08-22 | 通德集团有限公司 | Rhodiola crenulata body lotion with whitening and nourishing effects |
| CN102670478A (en) * | 2012-04-20 | 2012-09-19 | 诺斯贝尔(中山)无纺日化有限公司 | Multi-effect restoring skin cream |
| CN103655273A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Moisturizing cream |
| CN104606081A (en) * | 2013-11-05 | 2015-05-13 | 邹诚杰 | Pure natural massage skin moistening oil for babies |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8124811B2 (en) * | 2007-03-20 | 2012-02-28 | Allylix, Inc. | Fragrance and methods for production of 5-epi-β-vetivone, 2-isopropyl-6,10-dimethyl-spiro[4.5]deca-2,6-dien-8-one, and 2-isopropyl-6,10-dimethyl-spiro[4.5]deca-1,6-dien-8-one |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102670478A (en) * | 2012-04-20 | 2012-09-19 | 诺斯贝尔(中山)无纺日化有限公司 | Multi-effect restoring skin cream |
| CN102641232A (en) * | 2012-05-18 | 2012-08-22 | 通德集团有限公司 | Rhodiola crenulata body lotion with whitening and nourishing effects |
| CN104606081A (en) * | 2013-11-05 | 2015-05-13 | 邹诚杰 | Pure natural massage skin moistening oil for babies |
| CN103655273A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Moisturizing cream |
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Inventor after: Zhou Yanfu Inventor after: Song Chunxiao Inventor after: Ma Xiao Inventor after: Wang Feifei Inventor after: Gao Shaoyang Inventor after: Guo Zhenyu Inventor after: He Li Inventor before: Gao Shaoyang Inventor before: Zhou Yanfu Inventor before: Ma Xiao Inventor before: Mo Juanying Inventor before: He Li |
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Effective date of registration: 20180503 Address after: 650000 Kunming hi tech Zone, Yunnan Province, Department of medicine No. 53 Applicant after: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Applicant after: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Applicant after: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Shanghai branch Address before: 200335 709 rooms, No. 999, Jinzhong Road, Changning District, Shanghai Applicant before: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. |
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Address after: 650106 No. 53, Ke Yan Road, hi tech Zone, Kunming, Yunnan. Co-patentee after: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Patentee after: Yunnan Beitani Biotechnology Group Co., Ltd. Co-patentee after: Yunnan Beitani Biotechnology Group Co., Ltd. Shanghai Branch Address before: 650000 Kunming hi tech Zone, Yunnan Province, Department of medicine No. 53 Co-patentee before: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Patentee before: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Co-patentee before: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Shanghai branch |