CN105030650A - Mild skin cream and its preparation method - Google Patents
Mild skin cream and its preparation method Download PDFInfo
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- CN105030650A CN105030650A CN201510401575.9A CN201510401575A CN105030650A CN 105030650 A CN105030650 A CN 105030650A CN 201510401575 A CN201510401575 A CN 201510401575A CN 105030650 A CN105030650 A CN 105030650A
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Abstract
The invention discloses mild skin cream, comprising a component A, a component B and a component C. The component A is composed of water, glycerin, carrageen, xanthan gum, mycose, hydrolyzed collagen, and citric acid. The component B is composed of olive oil, seed oil of Prinsepia utilis, caprylic/capric triglyceride, bee wax, and sucrose stearate. The component C is composed of sunflower seed oil, rosemary leaf extract, vitamin E and Leuconstoc/radish root fermentation product filtrate. All components of the mild skin cream are from food additives or food materials, natural antibacterial components and natural antioxidants are used, compatibility is good, a skin safety test shows that the cream is nonirritating and is a mild, safe, stable and long-acting moisturizing cosmetic; meanwhile, the invention further provides a preparation method of the mild skin cream.
Description
Technical field
The invention belongs to daily cosmetics field, especially relate to a kind of gentle protective skin cream and preparation method thereof.
Background technology
Along with the development of society, the progress of science, people more and more pay attention to health, pay close attention to the quality of life, from focusing on color, smell and taste to attention collocation, nutrition, health, safety.The Cosmetic Market of China is the maximum emerging market in the whole world, and emerging in multitude of skin cosmetic makes people too plenty for the eye to take it all in, and people, except learning the cosmetics made good use of, also pay close attention to effect and the safety of cosmetics more.Therefore in recent years about the theory such as " without adding cosmetics ", " vegetalization cosmetic ", " organise cosmetic ", " natural cosmetics ", " edible cosmetics " enjoys the welcome of consumer.But, current most cosmetics are on the market difficult to the whole components allowing consumer from identification product the packing of product, and be difficult to the effectiveness and the safety that judge product, even if declare edible cosmetics, its formula is also that constituent part derives from food additive or animal and plant raw material.
The safety of cosmetics and stability are the important prerequisites ensureing cosmetics quality, and in formula system, the selection of oils and fats, antiseptic etc. can have very important impact to the safety of cosmetics and stability with use.Vegetable oil lipoprotein is rich in unsaturated fatty acid, is easily oxidized, and the product variable color caused, spoiled iso-metamorphism phenomenon, general antiseptic has slight zest and toxicity.Therefore, while pursuit cosmetic material safety is gentle, the good compatibility of recipe ingredient to also be ensured.
Olive oil is rich in abundant unsaturated fatty acid, has splendid natural health and beauty functions; Princepia utilis oil, from plateau plant kingdom Yunnan, is rich in unsaturated fatty acid, and its composition is close with human sebaceous's class, has skin regeneration technique and moisture-keeping function; Hydrolytic collagen, trehalose are good nutritional labeling and wetting agent; Rosemary leaf extract is a kind of oil-soluble inhibitor of natural excellence; Bright string coccus/Radix Raphani root tunning filtrate does not belong to antiseptic, is a kind of natural antipathogenic composition.By raw materials such as these Vegetable oil lipoproteines, wetting agent, the Natural antioxidant, natural bacteriostatic compositions, through scientific and reasonable test, screening, investigation and detection, safety, gentle, stay-in-grade protective skin cream just can be produced.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, provide a kind of gentle protective skin cream, its each raw material all adopts food grade raw material, all derive from food additive or raw-food material, formula uses natural bacteriostatic composition and the Natural antioxidant, compatibility is good, and cutaneous safety test is non-stimulated, is a kind of gentleness, safety, stable and can the cosmetics of moisturizing for a long time.
Another object of the present invention is to provide a kind of preparation method of above-mentioned gentle protective skin cream.
A kind of technical scheme realizing above-mentioned purpose is: a kind of gentle protective skin cream, comprises component A, B component and component C,
Described component A is made up of the raw material of following weight parts:
Described B component is made up of the raw material of following weight parts:
Described component C is made up of the raw material of following weight parts:
Sunflower seed oil and rosemary leaf extract 0.1 ~ 1 part;
Vitamin E 0.01 ~ 0.2 part;
Bright string coccus/Radix Raphani root tunning filtrate 2 ~ 2.4 parts.
The gentle protective skin cream of above-mentioned one, wherein, each raw material of each raw material of described component A, each raw material of B component and component C all adopts food grade raw material.
Above-mentioned raw materials is commercially available prod.
The preparation method additionally providing a kind of gentle protective skin cream of the present invention, comprises the following steps:
Component A dissolving step: first carrageenin sodium and xanthan gum to be added on successively in glycerol and to disperse with glycerol, form glycerol dispersion, again water, glycerol dispersion, trehalose, hydrolytic collagen and citric acid are added in kettle successively, be heated with stirring to 75 ~ 80 DEG C, insulated and stirred 10 ~ 30 minutes, makes component A;
B component dissolving step: add in oil cauldron by olive oil, Princepia utilis oil, caprylic/capric triglyceride, Cera Flava and sucrose stearate, is heated with stirring to 70 ~ 75 DEG C, dissolves completely, make B component;
Emulsifying step: by the component A in described kettle through 200 mesh screen and in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, again by the B component in described oil cauldron through 200 mesh screen and in emulsifying pot described in suction, 70 ~ 75 DEG C of homogenizing 5 ~ 10 minutes, then stirring borehole cooling;
Add component C step: when the temperature cooling in described emulsifying pot is not higher than 40 DEG C, sunflower seed oil and rosemary leaf extract, vitamin E and bright string coccus/Radix Raphani root tunning filtrate are added in described emulsifying pot successively, homogenizing 2-5 minute, homogenizing speed is 2000-3000rpm, vacuum outgas under stirring, filters discharging after natural cooling.
The preparation method of above-mentioned gentle protective skin cream, wherein, each raw material of each raw material of described component A, each raw material of B component and component C all adopts food grade raw material.
Have employed the technical scheme of a kind of gentle protective skin cream of the present invention, compared with prior art, gentle protective skin cream of the present invention has following beneficial effect:
(1) gentle protective skin cream of the present invention, each raw material of its recipe ingredient all adopts food grade materials, all derives from food additive or raw-food material, safe and non-stimulating, even if eat by mistake, also can not produce damage and potential safety hazard to human body.
(2) gentle protective skin cream of the present invention, can allow ordinary consumer is easier in identification formula each component according to general knowledge, and the safety of each component of principium identification.
(3) gentle protective skin cream of the present invention, the compatibility such as its vegetable oil, natural bacteriostatic composition requires higher raw material, and in this formula system, good stability, safety are good.
Adopt the technical scheme of the preparation method of a kind of gentle protective skin cream of the present invention, also can realize above technique effect.
Accompanying drawing explanation
Fig. 1 is the flow chart of the preparation method of gentle protective skin cream of the present invention;
Fig. 2 is the test result figure of the skin moisture content used before and after the gentle protective skin cream in each embodiment.
Detailed description of the invention
The present inventor, in order to understand technical scheme of the present invention better, is described in detail by reference to the accompanying drawings below by embodiment particularly:
Embodiment 1
A kind of gentle protective skin cream, each component is made up of the raw material of following weight parts:
Component A: 80.45 parts, water, glycerol 2 parts, 1 part, carrageenin sodium, xanthan gum 0.5 part, trehalose 2 parts, hydrolytic collagen 0.05 part and citric acid 0.1 part;
B component: 5 parts, olive oil, Princepia utilis oil 0.5 part, caprylic/capric triglyceride 3 parts, 1 part, Cera Flava and sucrose stearate 2 parts;
Component C: sunflower seed oil and rosemary leaf extract 0.3 part, vitamin 0.1 part and bright string coccus/Radix Raphani root tunning filtrate 2 parts.
Embodiment 2
A kind of gentle protective skin cream, each component is made up of the raw material of following weight parts:
Component A: 68.82 parts, water, glycerol 4 parts, 0.8 part, carrageenin sodium, xanthan gum 0.2 part, trehalose 3 parts, hydrolytic collagen 0.03 part and citric acid 0.1 part;
B component: 10 parts, olive oil, Princepia utilis oil 1.5 parts, caprylic/capric triglyceride 5 parts, 0.8 part, Cera Flava and sucrose stearate 3 parts;
Component C: sunflower seed oil and rosemary leaf extract 0.5 part, vitamin E 0.05 part and bright string coccus/Radix Raphani root tunning filtrate 2.2 parts.
Embodiment 3
A kind of gentle protective skin cream, each component is made up of the raw material of following weight parts:
Component A: 56.77 parts, water, glycerol 7 parts, 0.5 part, carrageenin sodium, xanthan gum 0.1 part, trehalose 1 part, hydrolytic collagen 0.01 part and citric acid 0.1 part;
B component: 13 parts, olive oil, Princepia utilis oil 2.5 parts, caprylic/capric triglyceride 10 parts, 2 parts, Cera Flava and sucrose stearate 4 parts;
Component C: sunflower seed oil and rosemary leaf extract 0.6 part, vitamin E 0.02 part and bright string coccus/Radix Raphani root tunning filtrate 2.4 parts.
Each raw material of each component of embodiment 1-3 all adopts food grade raw material, all derives from food additive or raw-food material.
Hydromining is prepared with the Laboratory Pure Water system Master-S of Shanghai Hitech Instruments Co., Ltd. and obtains; The commodity that Ninghua work (China) company limited of glycerol employing section produces are called Glycerine99.5%; The commodity that carrageenin sodium adopts taste bio tech ltd, Hebei hundred to produce are called carrageenan; The commodity that xanthan gum adopts Rhodia to produce are called RHODICAREH; The commodity that trehalose adopts Japanese Lin Yuan company to produce are called TREHALOSE; The commodity that hydrolytic collagen adopts Jie Cheng trade Co., Ltd to produce are called Naticol1000; The commodity that citric acid Chinasun Specialty Products Co., Ltd produces are called monohydrate potassium; The commodity that olive oil Ah Hu Sikaer Si oils and fats (Shanghai) Co., Ltd. produces are called AkogreenO; The commodity that Princepia utilis oil adopts Lijiang Gonghe Industrial Co., Ltd. to produce are called Princepia utilis oil; The commodity that caprylic/capric triglyceride adopts EVONIK company to produce are called TEGOSOFTCT; The commodity that Cera Flava adopts Shanghai Zi Bang Chemical Co., Ltd. to produce are called SOLIBEEWAX; The commodity that sucrose stearate adopts MIT to produce are called PYOTOSUGARESTERS-1170; The commodity that sunflower seed oil and rosemary leaf extract adopt KEMIN company to produce are called Rosamox; Vitamin E adopts the commodity of DSM N. V. to be called dl-α-Tocopherol; The commodity that bright string coccus/Radix Raphani root tunning filtrate adopts ActiveConcepts company to produce are called AMSLeucidalLiquid.
Gentle protective skin cream provided by the invention is prepared by following steps:
Component A dissolving step: first carrageenin sodium and xanthan gum to be added on successively in glycerol and to disperse with glycerol, form glycerol dispersion, again water, glycerol dispersion, trehalose, hydrolytic collagen and citric acid are added in kettle successively, be heated with stirring to 75 ~ 80 DEG C, insulated and stirred 10 ~ 30 minutes, makes component A;
B component dissolving step: add in oil cauldron by olive oil, Princepia utilis oil, caprylic/capric triglyceride, Cera Flava and sucrose stearate, is heated with stirring to 70 ~ 75 DEG C, dissolves completely, make B component;
Emulsifying step: by the component A in described kettle through 200 mesh screen and in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, again by the B component in described oil cauldron through 200 mesh screen and in emulsifying pot described in suction, 70 ~ 75 DEG C of homogenizing 5 ~ 10 minutes, then stirring borehole cooling;
Add component C step: when the temperature cooling in described emulsifying pot is not higher than 40 DEG C, sunflower seed oil and rosemary leaf extract, vitamin E and bright string coccus/Radix Raphani root tunning filtrate are added in described emulsifying pot successively, homogenizing 2-5 minute, homogenizing speed is 2000-3000rpm, vacuum outgas under stirring, filters discharging after natural cooling.
Performance Detection is carried out to the gentle protective skin cream of embodiment 1-3, comprises stability test, anti-corrosion function test, security test and moisture of skin test.
Stability test
Study on the stability is carried out to the gentle protective skin cream of the above-mentioned embodiment 1-3 prepared, product stability investigates reference standard QB/T1857-2004 " skin lotion frost ", in order to obtain more stable product, investigate conditional request higher than QB/T1857-2004, successively at-15 DEG C, 5 DEG C, at 40 DEG C and 49 DEG C, test 15 days, 30 days respectively, 45 days, 60 days and 90 days, test the stability of gentle protective skin cream of the present invention, stability test result of the test is as shown in table 1:
Table 1
Stability test result of the test display in table 1: the gentle protective skin cream of embodiment 1,2,3,49 DEG C of heat-resisting investigations, after returning to room temperature, mastic is without oil-water separation phenomenon ,-15 DEG C of cold-resistant investigations, front without obvious Traits change with test after returning to room temperature.Therefore gentle protective skin cream of the present invention has good formula compatibility and constant product quality.
Anti-corrosion function is tested
Tested by preservation challenge and carry out preservative efficacy evaluation.The method is with reference to American Pharmacopeia USP28 version-antimicrobial preservative efficacy test.The gentle protective skin cream of embodiment 1,2,3 is mixed in the cell culture substrate of identical type respectively, then the fungus of disposable access standard volume and mycete, under sample being deposited in the temperature of 37 DEG C, regular sampling Detection residual fungus number wherein and residual fungi count, and the antibacterial effect carrying out assess sample according to the situation of change of residual fungus number and residual fungi count.
Criterion: the bacterial population residual alive be detected in sample at the 28th day and the equal < 1.0 × 103CFU/g (ml) of fungus number of living; From the 14th day, the bacterial population residual alive be detected in the sample of the 21st day and the 28th day and fungus number of living all can not increase again.
Preservative efficacy test result is as shown in table 2:
Table 2
From table 2 preservative efficacy test result, when the 7th day, the equal < 1.0 × 103CFU/g of bacterial population residual alive be detected in embodiment 1,2,3 sample, when the 14th day, the equal < 1.0 × 103CFU/g of remaining bacteria number, and clump count does not all increase.Therefore gentle protective skin cream of the present invention has good preservative efficacy.
Security test
Security test comprises acute skin irritation test and acute eye irritation test.
(1) acute skin irritation test:
Carry out acute skin irritation test to the gentle protective skin cream of embodiment 1,2,3, each embodiment all selects 4 albino guinea-pigs to test, test chamber temperature: 20-24 DEG C, relative humidity: 60-70%.Test precontract 24h, cut by hair spinal column both sides, laboratory animal back, unhairing scope is respectively 2cm × 3cm, application area 2.5cm × 2.5cm.Get tested material to be about 0.5mL and to spread upon on the skin of side, when tested material uses the preparation of nonirritant solvent, opposite side is coated with solvent in contrast, smears 1 every day, smears 14 days continuously.From second day, before smearing, answer cropping at every turn, remain tested material with water or nonirritant solvent cleaning, observed result after a hour.Irritant reaction scoring is carried out with reference to " cosmetics health specification (2007 editions) " regulation.
Table 3
From the acute skin irritation test result of table 3, the gentle protective skin cream of embodiment 1,2,3, to the acute skin irritation test of Cavia porcellus, is showed no irritative response.Therefore the gentle protective skin cream of one of the present invention, acute skin irritation test result shows do not have skin irritation.
(2) acute eye irritation test
Carry out acute eye irritation test to the gentle protective skin cream of embodiment 1,2,3, each embodiment all selects 3 healthy adult white rabbit to test, test chamber temperature: 20-24 DEG C, relative humidity: 60-70%.Before test, animal will at least adapt to 3 day time in experimental animal room environment.Pull open a palpebra inferior for hairy rat side eyes gently, tested material 0.1mL (100mg) is instilled in (or being painted into) conjunctival sac, makes the passive closed 1s of upper and lower eyelid, lose to prevent tested material.Opposite side eyes do not process and make own control.Eyes are not rinsed in 24 hours after instillation tested material.If think necessary, can rinse when 24h.If above-mentioned result of the test display tested material is irritant, need selects else and carry out developing result test with 3 rabbit, namely to 30s after rabbit eyes instillation tested material with enough, flow velocity comparatively fast but the current that animal eye can not be caused to damage rinse at least 30s.Animal eyes was checked in 1,24,48,72 hour and the 4th and the 7th after instillation tested material.If 72 hours do not occur irritant reaction, get final product termination test.If find to involve cornea or have other Eye irritation effect, not recuperator in 7 days, for the reversibility or irreversibility determining this infringement need extend observing time, is generally no more than 21 days.Irritant reaction scoring is carried out with reference to " cosmetics health specification (2007 editions) " regulation.
Table 4
From the acute ocular stimulation test result of table 4, the eye irritation test of gentle protective skin cream to rabbit of embodiment 1,2,3 has no irritative response.Therefore the gentle protective skin cream of one of the present invention, acute eye irritation test shows do not have acute ocular zest.
Moisture of skin is tested
Use German CK company moisture of skin tester MPA10, during test, moisture measurement probe vertical is pressed in tested inner forearm skin surface, probe top is pushed back a segment distance, keeps the pressure of 0.16N, in the second, main frame just demonstrates result.Test condition is temperature 25 ± 2 DEG C, humidity 50 ± 10%.Test result as shown in the figure.
From the moisture of skin test result of Fig. 1, the protective skin cream of embodiment 1,2,3 all after smearing 30min reach best moistening effect, after 90min, moisture rate of increase is all greater than 0, illustrates that moistening effect is good, and there is stronger lasting moisture-retaining capacity, wherein the effect of embodiment 3 is best.
In sum, gentle protective skin cream of the present invention, its each raw material all adopts food grade raw material, all derive from food additive or raw-food material, formula uses natural bacteriostatic composition and the Natural antioxidant, compatibility is good, and cutaneous safety test is non-stimulated, is a kind of gentleness, safety, stable and can the cosmetics of moisturizing for a long time.
Those of ordinary skill in the art will be appreciated that, above embodiment is only used to the present invention is described, and be not used as limitation of the invention, as long as in spirit of the present invention, all will drop in Claims scope of the present invention the change of the above embodiment, modification.
Claims (4)
1. a gentle protective skin cream, is characterized in that, comprises component A, B component and component C,
Described component A is made up of the raw material of following weight parts:
Described B component is made up of the raw material of following weight parts:
Described component C is made up of the raw material of following weight parts:
Sunflower seed oil and rosemary leaf extract 0.1 ~ 1 part;
Vitamin E 0.01 ~ 0.2 part;
Bright string coccus/Radix Raphani root tunning filtrate 2 ~ 2.4 parts.
2. a kind of gentle protective skin cream as claimed in claim 1, is characterized in that, each raw material of each raw material of described component A, each raw material of B component and component C all adopts food grade raw material.
3. a preparation method for gentle protective skin cream as claimed in claim 1, is characterized in that, comprise the following steps:
Component A dissolving step: first carrageenin sodium and xanthan gum to be added on successively in glycerol and to disperse with glycerol, form glycerol dispersion, again water, glycerol dispersion, trehalose, hydrolytic collagen and citric acid are added in kettle successively, be heated with stirring to 75 ~ 80 DEG C, insulated and stirred 10 ~ 30 minutes, makes component A;
B component dissolving step: add in oil cauldron by olive oil, Princepia utilis oil, caprylic/capric triglyceride, Cera Flava and sucrose stearate, is heated with stirring to 70 ~ 75 DEG C, dissolves completely, make B component;
Emulsifying step: by the component A in described kettle through 200 mesh screen and in suction emulsifying pot, open homogenizing, homogenizing speed is 3000rpm, again by the B component in described oil cauldron through 200 mesh screen and in emulsifying pot described in suction, 70 ~ 75 DEG C of homogenizing 5 ~ 10 minutes, then stirring borehole cooling;
Add component C step: when the temperature cooling in described emulsifying pot is not higher than 40 DEG C, sunflower seed oil and rosemary leaf extract, vitamin E and bright string coccus/Radix Raphani root tunning filtrate are added in described emulsifying pot successively, homogenizing 2-5 minute, homogenizing speed is 2000-3000rpm, vacuum outgas under stirring, filters discharging after natural cooling.
4. the preparation method of gentle protective skin cream as claimed in claim 3, is characterized in that, each raw material of each raw material of described component A, each raw material of B component and component C all adopts food grade raw material.
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| CN107088176A (en) * | 2017-06-08 | 2017-08-25 | 广州市花安堂生物科技有限公司 | A kind of cosmetic material of blackcurrant seed oil |
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| CN105030650B (en) | 2018-06-26 |
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Address after: 650106 No. 53, Ke Yan Road, hi tech Zone, Kunming, Yunnan. Co-patentee after: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Patentee after: Yunnan Beitani Biotechnology Group Co., Ltd. Co-patentee after: Yunnan Beitani Biotechnology Group Co., Ltd. Shanghai Branch Address before: 650000 Kunming hi tech Zone, Yunnan Province, Department of medicine No. 53 Co-patentee before: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Patentee before: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Co-patentee before: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Shanghai branch |
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