CN105030564B - A kind of composition and its application with long-lasting moisturization - Google Patents
A kind of composition and its application with long-lasting moisturization Download PDFInfo
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Abstract
The invention particularly discloses a kind of composition with long-lasting moisturization and its application.Said composition is made up of the component of following percentage by weight：Serine 0.05 5%, pyrrolidone sodium carboxylate 0.1 5%, polysaccharide compound 0.01 10%, Sodium Hyaluronate 0.01 3%, polyquaternium 51 0.05 5%, ceramide 0.01 1.5%, cuticula softening agent 0.1 10%, polyalcohol 66.5 99.63%；Described polysaccharide compound is any of algal polysaccharides, pulullan polysaccharide, cassia angustifolia leaf polyose, GL-B, pachymaran, LBP-X, tremella polysaccharides or a variety of mixtures；Described cuticula softening agent is the mixture of one or both of allantoin, urea；Described polyalcohol is mixtures one or more in glycerine, propane diols, butanediol, sorbierite.Said composition is used to prepare moisture-keeping cosmetics, has that instant moistening effect is good, and the advantages of moistening effect is lasting.
Description
Technical field
The present invention relates to a kind of composition of compounding, said composition has long-lasting moisturization, can apply to moisturizing
The preparation of cosmetic.
Background technology
The most important process of beauty seeks to moisturizing.Particularly autumn and winter, because air starts to become very dry, add
The morning and evening temperature difference it is big, weather gradually turns cold, and causes skin pore to shrink, and the sebaceous glands of skin surface is reduced with sweat gland secretion, from
And skin surface is caused to be easy to lose moisture content.And the maximum reason of skin senescence is exactly moisture content deficiency, autumn skin is new in addition
Old metabolism is slow, so autumn wind is together, many people's has just played wrinkle or color spot, acne on the face, and original piebald, foxiness also can
Deepen, skin becomes drying, and subcutaneous fat thickens, and skin is tight, or even peeling falls bits.So moisture-keeping cosmetics are most to be in great demand
Cosmetics.
The content of the invention
It is an object of the invention to provide a kind of composition with long-lasting moisturization, said composition can make keratoderma
Moisture keeps filling for a long time, stably.
To achieve the object of the present invention, present invention employs following technical scheme：
A kind of composition with long-lasting moisturization, it is characterised in that be made up of the component of following percentage by weight：Silk
Propylhomoserin 0.05-5%, pyrrolidone sodium carboxylate 0.1-5%, polysaccharide compound 0.01-10%, Sodium Hyaluronate 0.01-3%, gather
The 0.05-5% of quaternary ammonium salt -51, ceramide 0.01-1.5%, cuticula softening agent 0.1-10%, polyalcohol 66.5-99.63%.
Preferably, a kind of composition with long-lasting moisturization, it is characterised in that by the component of following percentage by weight
It is made：Serine 0.5-4%, pyrrolidone sodium carboxylate 0.5-4%, polysaccharide compound 0.5-5%, Sodium Hyaluronate 0.1-
2.5%, the 0.5-4% of polyquaternium -51, ceramide 0.05-1%, cuticula softening agent 0.5-6%, polyalcohol 81-
97.45%。
Preferably, a kind of composition with long-lasting moisturization, it is characterised in that by the component of following percentage by weight
It is made：Serine 0.5-3%, pyrrolidone sodium carboxylate 1-3.5%, polysaccharide compound 0.5-3%, Sodium Hyaluronate 0.5-
2%, the 0.8-3% of polyquaternium -51, ceramide 0.06-0.8%, cuticula softening agent 0.5-5%, polyalcohol 82.3-
96.64%。
Preferably, a kind of composition with long-lasting moisturization, it is characterised in that by the component of following percentage by weight
It is made：Serine 1-2%, pyrrolidone sodium carboxylate 1-2.5%, polysaccharide compound 0.8-3%, Sodium Hyaluronate 0.8-2%,
The 0.8-2.5% of polyquaternium -51, ceramide 0.08-0.6%, cuticula softening agent 0.5-4%, polyalcohol 86.4-
95.82%。
Described polysaccharide compound be algal polysaccharides, pulullan polysaccharide, cassia angustifolia leaf polyose, GL-B, pachymaran,
Any of LBP-X, tremella polysaccharides or a variety of mixtures.
Described cuticula softening agent is the mixture of one or both of allantoin, urea.
Described polyalcohol is mixtures one or more in glycerine, propane diols, butanediol, sorbierite.
Above-mentioned composition preparation method：By serine, pyrrolidone sodium carboxylate, polysaccharide compound, polyquaternium -51,
Sodium Hyaluronate, ceramide, cuticula softening agent are sequentially added in polyalcohol and are uniformly dissolved, you can.
Application of the above-mentioned composition with long-lasting moisturization in preparing cosmetics, it is characterised in that contain in cosmetics
There is a kind of above-mentioned composition with long-lasting moisturization, its dosage is 0.05 ~ 25%, and preferable amount is 5 ~ 15%.Except containing
Have beyond the above-mentioned composition with long-lasting moisturization, can add as suitably desired suitable cosmetics use it is usual
Composition, such as emollient, water, emulsifying agent, preservative, essence, pigment matrix components.
The long-acting moisturizing principle of the above-mentioned composition with long-lasting moisturization：Skin keratin is made by cuticula softening agent
Layer softening, break through NMF and enter skin particles layer, have the passage of spinous layer and basalis, promote NMF to step into epidermis
Cuticula, stratum granulosum, have spinous layer and basalis；Utilize pyrrolidone sodium carboxylate, polyalcohol, serine, polysaccharide compound
These hygroscopic agents absorb moisture from corium and external environment, and polyalcohol stays in keratoderma, serine, polysaccharide compound
Due to good with skin compatibility, the stratum granulosum of skin epidermis deep layer can be stepped into, have spinous layer and basalis, thus make skin
Each layer of skin epidermis all maintains enough moisture；Ceramide has hydrone ability of associating by force very much, is formed in cuticula
Network structure, and be filled in as cytoplasm composition between skin epidermal cells, reach and maintain moisture of skin and increase skin bullet
Property purpose；Sodium Hyaluronate and polyquaternium -51 are used as macromolecule NMF, it is impossible into skin, but it is common in skin surface
One layer of fine and close film is formd, on the one hand prevents moisture of skin from volatilizing, moisture supplement on the other hand can also be absorbed from air and is stopped
NMF in skin is stayed, reaches the purpose of long-acting moisturizing.
Embodiment
Below by way of specific embodiment come the present invention is further illustrated, but these embodiments simply to illustrate that,
It is not limitation of the present invention.
A kind of composition with long-lasting moisturization of embodiment 1（Ⅰ）
A kind of composition with long-lasting moisturization（Ⅰ）, it is characterised in that it is made up of the component of following percentage by weight：
Serine 1.5%, pyrrolidone sodium carboxylate 1.5%, algal polysaccharides 1.2%, pulullan polysaccharide 1.8%, Sodium Hyaluronate 1%, gather
Quaternary ammonium salt -51 2%, ceramide 0.3%, urea 3%, glycerine 40.7%, butanediol 47%.
Preparation method：It is pulullan polysaccharide, polyquaternium -51, transparent by serine, pyrrolidone sodium carboxylate, algal polysaccharides
Matter acid sodium, ceramide, urea sequentially add to be uniformly dissolved in glycerine and mixture of butanediols, you can.
A kind of composition with long-lasting moisturization of embodiment 2（Ⅱ）
A kind of composition with long-lasting moisturization（Ⅱ）, it is characterised in that by the component system of following percentage by weight
Into：Serine 1.8%, pyrrolidone sodium carboxylate 2%, algal polysaccharides 3%, Sodium Hyaluronate 1.2%, polyquaternium -51 2%, god
Through acid amides 0.4%, urea 4%, glycerine 85.6%.
Preparation method：By serine, pyrrolidone sodium carboxylate, algal polysaccharides, polyquaternium -51, Sodium Hyaluronate, nerve
Acid amides, urea are sequentially added in glycerine and are uniformly dissolved, you can.
A kind of composition with long-lasting moisturization of embodiment 3（Ⅲ）
A kind of composition with long-lasting moisturization（Ⅲ）, it is characterised in that by the component system of following percentage by weight
Into：Serine 1.2%, pyrrolidone sodium carboxylate 1.5%, algal polysaccharides 2%, cassia angustifolia leaf polyose 1%, Sodium Hyaluronate 1.5%, gather
Quaternary ammonium salt -51 2.2%, ceramide 0.3%, allantoin 0.3%, urea 2.5%, glycerine 60%, butanediol 27.5%.
Preparation method：By serine, pyrrolidone sodium carboxylate, algal polysaccharides, cassia angustifolia leaf polyose, polyquaternium -51, transparent
Matter acid sodium, ceramide, allantoin, urea sequentially add to be uniformly dissolved in glycerine and mixture of butanediols, you can.
A kind of composition with long-lasting moisturization of embodiment 4（Ⅳ）
A kind of composition with long-lasting moisturization（Ⅳ）, it is characterised in that by the component system of following percentage by weight
Into：Serine 1.2%, pyrrolidone sodium carboxylate 1.8%, algal polysaccharides 1.6%, tremella polysaccharides 1.8%, Sodium Hyaluronate 1.2%,
Polyquaternium -51 2.5%, ceramide 0.4%, allantoin 0.2%, urea 3%, glycerine 50%, propane diols 36.3%.
Preparation method：By serine, pyrrolidone sodium carboxylate, algal polysaccharides, tremella polysaccharides, polyquaternium -51, hyalomitome
Sour sodium, ceramide, allantoin, urea sequentially add to be uniformly dissolved in glycerine and propylene glycol mixture, you can.
A kind of 1 moisture-keeping composition of comparative example（Ⅰ）
A kind of moisture-keeping composition（Ⅰ）, it is characterised in that it is made up of the component of following percentage by weight：Pyrrolidone sodium carboxylate
1.5%, Sodium Hyaluronate 7.8%, urea 3%, glycerine 40.7%, butanediol 47%.
Preparation method：Pyrrolidone sodium carboxylate, Sodium Hyaluronate, urea are sequentially added in glycerine and mixture of butanediols
It is uniformly dissolved, you can.
A kind of 2 moisture-keeping composition of comparative example（Ⅱ）
A kind of moisture-keeping composition（Ⅱ）, it is characterised in that it is made up of the component of following percentage by weight：Serine 1.5%, pyrrole
Pyrrolidone carboxylic acid's sodium 1.5%, algal polysaccharides 1.2%, pulullan polysaccharide 1.8%, Sodium Hyaluronate 3.3%, urea 3%, glycerine
40.7%, butanediol 47%.
Preparation method：By serine, pyrrolidone sodium carboxylate, algal polysaccharides, pulullan polysaccharide, Sodium Hyaluronate, urea
Sequentially add and be uniformly dissolved in glycerine and mixture of butanediols, you can.
A kind of 3 moisture-keeping composition of comparative example（Ⅲ）
A kind of moisture-keeping composition（Ⅲ）, it is characterised in that it is made up of the component of following percentage by weight：2-pyrrolidone-5-carboxylic acid
Sodium 1.5%, Sodium Hyaluronate 5.5%, polyquaternium -51 2%, ceramide 0.3%, urea 3%, glycerine 40.7%, fourth two
Alcohol 47%.
Preparation method：By pyrrolidone sodium carboxylate, Sodium Hyaluronate, polyquaternium -51, ceramide, urea add successively
Enter and be uniformly dissolved in glycerine and mixture of butanediols, you can.
The moistening effect of test example 1 is evaluated
1st, sample preparation is evaluated
The moisture-keeping composition 5g according to embodiment 1 and comparative example 1-3 preparations is taken, is added in 95g deionized waters, dissolving is equal
It is even, the assessing sample solution that mass fraction is 5% is made.
2nd, evaluation method
According to light industry standard QB/T 4256-2011 cosmetics moisture-keeping efficacy evaluation guides, made from embodiment 1
Sample, the moistening effect of determination sample.
Method of testing：Healthy volunteer 20, male 10, women 10, the age was at 25 ~ 50 years old.In isoperibol（22
±1℃）, relative humidity 50 ± 5%, after 1 hour of resting.Press（2.0±0.1）mg/ cm2Dosage sample is coated in subject's left hand
Inner forearm（4cm×4cm）With right forearm inner side（4cm×4cm）.Blank control（Do not apply）Test simultaneously.It is being painted with sample respectively
0.5 hour, 1 hour, 2 hours, the hydrauture state of the test of 4 hours, 8 hours skin of product.
3rd, evaluation result
Evaluation result is represented with hydrauture average value, is shown in Table 1.
Table 1
| Time | 0.5h | 1h | 2h | 4h | 8h |
| The sample hydrauture of embodiment 1/% | 86.45 | 83.78 | 75.71 | 63.59 | 53.28 |
| The sample hydrauture of comparative example 1/% | 63.15 | 57.23 | 45.12 | 29.34 | 15.39 |
| The sample hydrauture of comparative example 2/% | 69.30 | 60.65 | 49.38 | 33.67 | 16.97 |
| The sample hydrauture of comparative example 3/% | 64.96 | 60.67 | 56.32 | 48.37 | 34.71 |
As a result show, comparative example 2 is found with the results contrast of comparative example 1, uses serine, algal polysaccharides, pulullan polysaccharide
After replacing partially transparent matter acid sodium, hydrauture improves, and illustrates after adding serine, algal polysaccharides, pulullan polysaccharide, serves association
Same synergistic effect.
Comparative example 3 is found with the results contrast of comparative example 1, and partially transparent matter acid is replaced using polyquaternium -51, ceramide
After sodium, the instant hydrauture increase in 30min is little, but increases over time, and the speed that its hydrauture reduces is decreased obviously,
Namely moisturizing persistence serves synergistic function.
Embodiment 1 is found with comparative example 1-3 results contrasts, more with polyquaternium -51, ceramide, serine, marine alga
After sugar, pulullan polysaccharide compounding substitute Sodium Hyaluronate, hydrauture substantially increases, and moisturizing persistence also substantially improves, tool
There is long-lasting moisturization.Synergistic function is served between the composition for illustrating to obtain by compounding.
The preparation of 5 long-acting moisturiser of embodiment
Table 2 provides a kind of long-acting moisturiser formula of composition with long-lasting moisturization containing the present invention, each thing
The dosage of matter mass fraction table：
Table 2
Preparation method：The 80 DEG C of dissolvings of A phases are well mixed, and the 80 DEG C of dissolvings of B phases are well mixed, cyclomethicone emulsification
Preceding addition B phases, B is added to A phases and homogeneous 5 minutes during emulsification, and C phase and homogeneous 2 minutes, ageing 24h are added when being cooled to 50 DEG C
After pack, you can.
6 long-acting moisturizing emulsion of embodiment
Table 3 provides a kind of long-acting moisturizing emulsion formula of composition with long-lasting moisturization containing the present invention, respectively
The dosage of material is represented with mass fraction：
Table 3
Preparation method：The 80 DEG C of dissolvings of A phases are well mixed, and the 80 DEG C of dissolvings of B phases are well mixed, and C is added into B phases, breast before emulsification
A is added to B phases simultaneously homogeneous 5 minutes during change, and D simultaneously homogeneous 2 minutes are added when being cooled to 50 DEG C, are packed after being aged 24h, you can.
Claims (2)
1. a kind of composition with long-lasting moisturization, it is characterised in that be made up of the component of following percentage by weight：Silk ammonia
Sour 0.05-5%, pyrrolidone sodium carboxylate 0.1-5%, polysaccharide compound 0.01-10%, Sodium Hyaluronate 0.01-3%, poly- season
The 0.05-5% of ammonium salt -51, ceramide 0.01-1.5%, cuticula softening agent 0.1-10%, polyalcohol 66.5-99.63%；Institute
The polysaccharide compound stated be algal polysaccharides, pulullan polysaccharide, cassia angustifolia leaf polyose, GL-B, pachymaran, LBP-X,
Any of tremella polysaccharides or a variety of mixtures；Described cuticula softening agent is allantoin, one kind in urea or two
The mixture of kind；Described polyalcohol is mixtures one or more in glycerine, propane diols, butanediol, sorbierite；Described group
Compound preparation method：By serine, pyrrolidone sodium carboxylate, polysaccharide compound, polyquaternium -51, Sodium Hyaluronate, nerve
Acid amides, cuticula softening agent are sequentially added in polyalcohol and are uniformly dissolved, you can.
2. application of a kind of composition with long-lasting moisturization in preparing cosmetics described in claim 1, its feature
Containing a kind of composition with long-lasting moisturization described in claim 1, its dosage is 0.05 ~ 25% in cosmetics.
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