CN114306156A - Milk cap cleansing product and preparation method thereof - Google Patents
Milk cap cleansing product and preparation method thereof Download PDFInfo
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- CN114306156A CN114306156A CN202111556745.2A CN202111556745A CN114306156A CN 114306156 A CN114306156 A CN 114306156A CN 202111556745 A CN202111556745 A CN 202111556745A CN 114306156 A CN114306156 A CN 114306156A
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Abstract
The application relates to the technical field of cosmetics, in particular to a milk cover makeup removing product and a preparation method thereof, wherein the milk cover makeup removing product comprises the following raw materials in percentage by weight: 30-40% of emollient, 1-11% of humectant, 1-10% of skin conditioner, 0.1-1% of preservative, 0.5-2% of emulsifier, 1-10% of thickener and the balance of water; wherein the skin conditioner is a citrus fruit extract; it has the advantages of refreshing and removing makeup, and no irritation to skin.
Description
Technical Field
The application relates to the technical field of cosmetics, in particular to a milk cap makeup removing product and a preparation method thereof.
Background
The makeup remover is a makeup remover mainly aiming at removing makeup from oil makeup cosmetics such as foundation, mascara, lipstick and the like. The existing makeup removing products comprise makeup removing water, makeup removing oil, makeup removing cream and the like. The makeup remover is mainly composed of water, a surfactant, a humectant and ethanol, and a transparent colorless liquid, and is suitable for water-based makeup removing products. However, when makeup is thick, makeup remover has low cleaning power, and is easy to generate cosmetic residues on skin, and the residual dirt can cause adverse sequelae such as pigment precipitation, black spots, whelk and the like. However, although makeup remover oil, makeup remover cream, and the like can remove a relatively thick makeup well, they often cause problems of oily feeling of the skin or red irritation to the skin after makeup removal.
Disclosure of Invention
In order to solve the problem that skin is not irritated while refreshing makeup removal, the application provides a milk cover makeup removal product and a preparation method thereof.
In a first aspect, the application provides a milk cap makeup removal product, which adopts the following technical scheme:
a milk cover makeup removing product comprises the following raw materials in percentage by weight: 30-40% of emollient, 1-11% of humectant, 1-10% of skin conditioner, 0.1-1% of preservative, 0.5-2% of emulsifier, 1-10% of thickener and the balance of water; wherein the skin conditioner is an extract of citrus fruit.
By adopting the technical scheme, the emollient is a main makeup removing component, and the humectant and the skin conditioner are added while makeup is removed, wherein the skin conditioner is a citrus fruit extract which has strong broad-spectrum antibacterial property, has good inhibition effect on acne causing bacteria, and also has the effect of removing mites; the citrus fruit extract can protect the horny layer of the skin when the makeup removing product is applied to the skin, and the humectant can keep the skin moist, so that the skin is not easy to stimulate and turn red when the makeup removing product is applied to the skin.
Preferably, the method comprises the following steps: the milk cover makeup removing product comprises the following raw materials in percentage by weight: 33-37% of emollient, 3-8% of humectant, 3-8% of skin conditioner, 0.3-0.7% of preservative, 1-1.5% of emulsifier, 3-8% of thickener and the balance of water.
By adopting the technical scheme, the makeup removing greasy feeling is reduced by optimizing the proportion of the raw materials, and the moisture content of the skin after makeup removal is higher.
Preferably, the method comprises the following steps: the humectant comprises the following raw materials in parts by weight: 1-10 parts of butanediol and 0.1-1 part of ethylhexyl glycerol.
By adopting the technical scheme, the butanediol and the ethylhexyl glycerin have a synergistic effect on the moisture retention capacity, the moisture retention effect of the butanediol and the ethylhexyl glycerin is better than that of the butanediol and the ethylhexyl glycerin which are added separately, and the ethylhexyl glycerin also has a certain antiseptic effect.
Preferably, the method comprises the following steps: the emollient comprises the following raw materials in parts by weight: 10-20 parts of isohexadecane, 1-10 parts of cyclohexasiloxane and 1-10 parts of dioctyl carbonate.
By adopting the technical scheme, when the isohexadecane and the dioctyl carbonate are added simultaneously, no obvious greasy feeling exists, and when the isohexadecane and the dioctyl carbonate are added independently, the greasy feeling is obvious, so that the isohexadecane and the dioctyl carbonate play a synergistic role in cleansing, and when the isohexadecane and the dioctyl carbonate are added simultaneously, the cleansing is cleaner.
Preferably, the method comprises the following steps: the emollient also comprises 1-10 parts by weight of cyclopentadimethylsiloxane.
By adopting the technical scheme, the cyclopentadecyldimethyl siloxane is added into the emollient, so that the refreshing feeling of the skin after makeup removal can be improved, the greasiness of the skin is reduced, and the skin is moist and bright.
Preferably, the method comprises the following steps: the emulsifier comprises the following raw materials in parts by weight: 0.1-1 part of EG-40 hydrogenated castor oil and 0.1-1 part of PG-26-butanol polyether-26.
By adopting the technical scheme, the PEG-40 hydrogenated castor oil and the PPG-26-butanol polyether-26 have mutual synergistic effect, and when the PEG-40 hydrogenated castor oil and the PPG-26-butanol polyether-26 are added separately, the emulsifying capacity is poor, the recovery time after shaking is short, and the PEG-40 hydrogenated castor oil and the PPG-26-butanol polyether-26 are not suitable for practical use.
Preferably, the method comprises the following steps: the thickening agent is sodium chloride.
In a second aspect, the application provides a preparation method of a milk cap cleansing product, which adopts the following technical scheme:
a preparation method of a milk cap makeup removing product is characterized by comprising the following steps: which comprises the following steps:
1) adding the humectant, the emulsifier, the skin conditioner, the thickener and the preservative into water, and then uniformly mixing to obtain a mixed solution, 2) mixing the emollient and the mixed solution, uniformly stirring, and standing to obtain water emulsion layering, thus obtaining the milk cover makeup removing product.
By adopting the technical scheme, the mixed solution is a water phase, the emollient is an oil phase, the water phase is firstly mixed uniformly to obtain the mixed solution, and then the mixed solution is mixed with the emollient to obtain the milk cover cleansing product.
In summary, the present application includes at least one of the following beneficial technical effects:
1. the skin lotion is a main makeup removing component, and the skin lotion is added with the humectant and the skin conditioner while makeup removing, wherein the skin conditioner is a citrus fruit extract which has strong broad-spectrum antibacterial property, has good inhibition effect on acne causing bacteria, and also has the effect of removing mites; the citrus fruit extract can protect the horny layer of the skin when the makeup removing product is applied to the skin, and the humectant can keep the skin moist, so that the skin is not easy to stimulate and turn red when the makeup removing product is applied to the skin.
2. In the microbial detection, faecal coliform, staphylococcus aureus and pseudomonas aeruginosa are not detected, the total number of bacteria is below 259CFU/g, and the total number of mould and yeast is not more than 48CFU/g, so that the microbial indexes are met; meanwhile, in metal detection, the lead content is below 1.1mg/kg, the mercury content is not more than 0.14mg/kg, the arsenic content is less than 0.21mg/kg, the content is within the limit range of toxic substances, and the production requirement is met; after the milk cap cleansing product is used for cleansing, the water content of the facial skin of the milk cap cleansing product is increased, the water content of the skin can be improved by 1.34% to the maximum extent, and the facial skin is not obviously reddened after the cleansing. When using the milk lid makeup removal product of this application, through rocking the back, its layering is eliminated, then uses, and this application is after rocking, and its recovery time is moderate, more is applicable to in-service use.
Detailed Description
The present application is described in further detail below with reference to specific contents.
Raw materials
The raw materials of the application are all common products sold in the market.
Preparation example
Preparation example 1
An emollient prepared by the steps of:
the emollient is obtained by uniformly mixing 15kg of isohexadecane, 5kg of cyclohexasiloxane and 6kg of dioctyl carbonate.
Preparation examples 2 to 4
The humectant of preparation examples 2 to 4, whose raw material amounts are shown in table 1, was prepared by the following steps:
the humectant can be obtained by weighing butanediol and ethylhexyl glycerin according to the amounts in table 1, and then mixing them uniformly.
TABLE 1 preparation examples 2-4 and the amounts (kg) of the respective raw materials
| Preparation example 2 | Preparation example 3 | Preparation example 4 | |
| Butanediol | 1 | 6 | 10 |
| Ethyl hexyl glycerol | 1 | 0.6 | 0.1 |
Preparation example 5
The emulsifier is prepared from the following raw materials in the following steps of:
0.6kg of PEG-40 hydrogenated castor oil and 0.5kg of PPG-26-butanol polyether-26 are mixed uniformly to obtain the emulsifier.
Examples
Examples 1 to 4
The milk cap cleansing product comprises the following raw materials and the dosage of the raw materials shown in the table 2, and is prepared by the following steps:
1) adding humectant, emulsifier, skin conditioner, thickener and antiseptic into water, mixing well to obtain mixed solution,
2) mixing the emollient and the mixed solution, stirring, standing for 30min to obtain water emulsion layer, and making up removing product.
Wherein, the emollient is from preparation 1, the humectant is from preparation 2, the emulsifier is from preparation 5, the skin conditioner is citrus fruit extract, the thickener is sodium chloride, and the preservative is phenoxyethanol.
TABLE 2 materials and amounts (kg) of materials of examples 1-4
| Example 1 | Example 2 | Example 3 | Example 4 | |
| Skin-moistening agent | 30 | 33 | 37 | 40 |
| Moisture-retaining agent | 11 | 8 | 3 | 1 |
| Emulsifier | 0.5 | 1 | 1.5 | 2 |
| Skin conditioning agent | 10 | 8 | 3 | 1 |
| Thickening agent | 1 | 3 | 8 | 10 |
| Preservative | 0.1 | 0.3 | 0.7 | 1 |
| Water (W) | 47.4 | 46.7 | 46.8 | 45 |
Example 5
A milk cap make-up remover product is different from example 2 in that the humectant is obtained from preparation example 3, and the rest of the procedure is the same as that of example 2.
Example 6
A milk cap make-up remover product is different from example 2 in that the humectant is obtained from preparation example 4, and the rest of the procedure is the same as that of example 2.
Example 7
A cleansing product for a milk cap, which is different from that of example 5 in that the amount of the humectant added was 1kg, and the rest of the procedure was the same as that of example 5.
Example 8
A cleansing product for a milk cap, which is different from that of example 5 in that the amount of the humectant added was 3kg, and the rest of the procedure was the same as that of example 5.
Example 9
A cleansing product for a milk cap, which is different from that of example 5 in that the amount of the humectant added was 11kg, and the rest of the procedure was the same as that of example 5.
Example 10
A milk-based make-up remover product was prepared in the same manner as in example 5 except that the amount of the skin conditioner added was 1 kg.
Example 11
A milk-based make-up remover product was prepared in the same manner as in example 5 except that the amount of the skin conditioner added was 3 kg.
Example 12
A milk-based make-up remover product was prepared in the same manner as in example 5 except that the amount of the skin conditioner added was 10 kg.
Example 13
A milk-based cleansing product was prepared in the same manner as in example 5 except that the emollient composition contained 1kg of cyclopentadimethylsiloxane, and the procedure was the same as in example 5.
Example 14
A milk-based cleansing product was prepared in the same manner as in example 5 except that the emollient composition contained 10kg of cyclopentadimethylsiloxane.
Comparative example
Comparative example 1
A milk cover makeup remover product is different from the product in the example 2 in that the added emollient formula has the addition amount of isohexadecane of 0, and the rest steps are the same as the step in the example 2.
Comparative example 2
A milk cap makeup remover product is different from the product in the example 2 in that the added emollient formula has the addition amount of dioctyl carbonate of 0, and the rest steps are the same as the step in the example 2.
Comparative example 3
A milk cover makeup remover product is different from the milk cover makeup remover product in the embodiment 2 in that the added humectant formula is 0, and the rest steps are the same as the embodiment 2.
Comparative example 4
A milk cap makeup remover product is different from the milk cap makeup remover product in example 2 in that the added humectant formula is 0 in the addition amount of ethylhexyl glycerin, and the rest steps are the same as those in example 2.
Comparative example 5
A milk-based make-up remover product was prepared in the same manner as in example 2 except that the skin conditioner was added in an amount of 0.
Comparative example 6
A milk cap makeup remover, which is different from the milk cap makeup remover in example 2 in that the emulsifier is added in the formula, the addition amount of PEG-40 hydrogenated castor oil is 0, and the rest steps are the same as those in example 2.
Comparative example 7
A milk cap makeup remover product is different from the product in the example 2 in that the added emulsifier formula has the addition amount of PPG-26-butanol polyether-26 of 0, and the rest steps are the same as the step in the example 2.
Performance test
Detection method/test method
The milk cap makeup removal products were prepared according to the preparation methods of examples 1 to 14 and comparative examples 1 to 7, and then tested according to the following methods, and the test results are shown in tables 3 and 4.
Microorganism indexes are as follows: the total amount of bacteria, the total amount of mold and yeast, the faecal coliform group, staphylococcus aureus and pseudomonas aeruginosa were detected by the method in QB/T2660-2004, as shown in Table 3;
limit of toxic substances: the detection is carried out by the method in QB/T2660-2004, and the contents of lead, mercury and arsenic are respectively detected as shown in Table 3;
sensory and physicochemical indexes: the method in QB/T2660-2004 is used for detecting, and the appearance, heat resistance and cold resistance of the material are observed, wherein the temperature is 50 ℃ and the holding time is 24 hours during heat resistance detection, and the temperature is-18 ℃ and the holding time is 24 hours during cold resistance detection; the results are shown in Table 4.
Skin moisture change rate: detecting the skin before makeup removal through a skin moisture detector, detecting the skin 5min after makeup removal, and calculating the change of the skin moisture;
skin condition after makeup removal: selecting 3 female volunteers between the ages of 25-30, removing makeup through the milk cover makeup removing product of the application after the female volunteers hold makeup for 8 hours, and then grading the skin refreshing degree after makeup removal, wherein the facial skin is smooth and moist without obvious redness: 4-5 min; the face was smooth and moist and restorable after slight redness: 2-3 min; the face is reddened and recovers for a long time: 0-1 min.
TABLE 3 examination results of the milk-cap makeup remover products of examples 1 to 14 and comparative examples 1 to 7
In the microbial detection, faecal coliform, staphylococcus aureus and pseudomonas aeruginosa are not detected, the total number of bacteria is below 259CFU/g, and the total number of mould and yeast is not more than 48CFU/g, so that the microbial indexes are met; meanwhile, in metal detection, the lead content is below 1.1mg/kg, the mercury content is not more than 0.14mg/kg, the arsenic content is less than 0.21mg/kg, the content is within the limit range of toxic substances, and the production requirement is met.
TABLE 4 test results
As can be seen from the test data of examples 1-14 and comparative examples 1-7, and Table 4, the moisture content of the facial skin was increased after makeup removal using the milk-cap makeup removal product of the present application, the moisture content of the skin was increased by up to 1.34%, and no significant redness of the facial skin occurred after makeup removal. When using the milk lid makeup removal product of this application, through rocking the back, its layering is eliminated, then uses, and this application is after rocking, and its recovery time is moderate, more is applicable to in-service use.
As can be seen from the test data of example 2 and examples 5-6, the moisturizing agent of preparation example 3 has a superior moisturizing effect, and the moisture content of the skin of the milk cap makeup remover product prepared by using the moisturizing agent of preparation example 3 is high; in the examples 7 to 9, the skin moisture change rate was gradually increased as the amount of the moisturizer added was gradually increased, but the amount of the moisturizer added was not significantly increased after the addition of 8kg, so that the amount of the moisturizer added was preferably 3 to 8 kg.
As can be seen from the test data of examples 5, 10-12 and comparative example 5, the skin redness phenomenon can be obviously improved by adding the skin conditioner, the skin damage caused by makeup removal can be reduced, and the skin irritation of the makeup removal product is obviously improved when the addition amount of the skin conditioner is more than 3 kg.
As can be seen from the test data of example 5 and examples 13-14, the addition of cyclopentadimethylsiloxane to the emollient increased the refreshing feel of the skin after makeup removal and reduced the greasiness of the skin.
As can be seen from the detection data of the example 2 and the comparative examples 1-2, when the isohexadecane and the dioctyl carbonate are added simultaneously, no obvious greasy feeling exists, when the isohexadecane and the dioctyl carbonate are added independently, the greasy feeling is obvious, the results show that the isohexadecane and the dioctyl carbonate play a synergistic role in the cleansing degree of makeup removal, and when the isohexadecane and the dioctyl carbonate are added simultaneously, the makeup removal is cleaner.
From the test results of example 2 and comparative examples 3 to 4, it can be seen that in the humectant, butylene glycol and ethylhexyl glycerin have a synergistic effect in moisture retention, and in combination with table 3, ethylhexyl glycerin also has a certain preservative effect.
As can be seen from the test data of example 2 and comparative examples 6 to 7, PEG-40 hydrogenated castor oil and PPG-26-butanol polyether-26 have a synergistic interaction, and when added alone, the emulsifying capacity is poor, and the recovery time after shaking is short, so that the PEG-40 hydrogenated castor oil and PPG-26-butanol polyether-26 are not suitable for practical use.
The embodiments of the present invention are preferred embodiments of the present application, and the scope of the present application is not limited by the embodiments of the present application, so: all equivalent changes made according to the structure, shape and principle of the present application shall be covered by the protection scope of the present application.
Claims (8)
1. A milk-cap make-up removal product characterized by: the composite material comprises the following raw materials in percentage by weight: 30-40% of emollient, 1-11% of humectant, 1-10% of skin conditioner, 0.1-1% of preservative, 0.5-2% of emulsifier, 1-10% of thickener and the balance of water; wherein the skin conditioner is an extract of citrus fruit.
2. A milk-based make-up remover product according to claim 1, wherein: the milk cover makeup removing product comprises the following raw materials in percentage by weight: 33-37% of emollient, 3-8% of humectant, 3-8% of skin conditioner, 0.3-0.7% of preservative, 1-1.5% of emulsifier, 3-8% of thickener and the balance of water.
3. A milk-based make-up remover product according to claim 1, wherein: the humectant comprises the following raw materials in parts by weight: 1-10 parts of butanediol and 0.1-1 part of ethylhexyl glycerol.
4. A milk-based make-up remover product according to claim 1, wherein: the emollient comprises the following raw materials in parts by weight: 10-20 parts of isohexadecane, 1-10 parts of cyclohexasiloxane and 1-10 parts of dioctyl carbonate.
5. A milk-based make-up remover product according to claim 1, wherein: the emollient also comprises 1-10 parts by weight of cyclopentadimethylsiloxane.
6. A milk-based make-up remover product according to claim 1, wherein: the emulsifier comprises the following raw materials in parts by weight: 0.1-1 part of EG-40 hydrogenated castor oil and 0.1-1 part of PG-26-butanol polyether-26.
7. A milk-based make-up remover product according to claim 1, wherein: the thickening agent is sodium chloride.
8. A method of preparing a milk-based make-up removal product according to any one of claims 1 to 7, characterized in that: which comprises the following steps:
1) adding humectant, emulsifier, skin conditioner, thickener and antiseptic into water, mixing well to obtain mixed solution,
2) mixing the emollient and the mixed solution, stirring uniformly, standing, and layering to obtain the final product.
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