CN105010760B - A kind of wide spectrum feed montmorillonite takes off mould dose and preparation method thereof and application method - Google Patents
A kind of wide spectrum feed montmorillonite takes off mould dose and preparation method thereof and application method Download PDFInfo
- Publication number
- CN105010760B CN105010760B CN201510495977.XA CN201510495977A CN105010760B CN 105010760 B CN105010760 B CN 105010760B CN 201510495977 A CN201510495977 A CN 201510495977A CN 105010760 B CN105010760 B CN 105010760B
- Authority
- CN
- China
- Prior art keywords
- montmorillonite
- feed
- added
- raw material
- sodium salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229910052901 montmorillonite Inorganic materials 0.000 title claims abstract description 64
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 238000000034 method Methods 0.000 title claims abstract description 22
- 238000001228 spectrum Methods 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title abstract description 20
- 159000000000 sodium salts Chemical class 0.000 claims abstract description 38
- 238000003756 stirring Methods 0.000 claims abstract description 27
- 241001474374 Blennius Species 0.000 claims abstract description 18
- 210000005253 yeast cell Anatomy 0.000 claims abstract description 18
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 13
- 239000000843 powder Substances 0.000 claims description 57
- 239000002994 raw material Substances 0.000 claims description 45
- 239000000706 filtrate Substances 0.000 claims description 27
- 238000002156 mixing Methods 0.000 claims description 21
- 239000002002 slurry Substances 0.000 claims description 14
- 239000012266 salt solution Substances 0.000 claims description 13
- 239000007787 solid Substances 0.000 claims description 13
- 239000012530 fluid Substances 0.000 claims description 9
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 8
- 229910021536 Zeolite Inorganic materials 0.000 claims description 7
- 239000012141 concentrate Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 238000002203 pretreatment Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000010457 zeolite Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 6
- 230000001954 sterilising effect Effects 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 abstract description 16
- 241001465754 Metazoa Species 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 20
- 229910000029 sodium carbonate Inorganic materials 0.000 description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 8
- 239000002270 dispersing agent Substances 0.000 description 8
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 8
- 229940048086 sodium pyrophosphate Drugs 0.000 description 8
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 8
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 8
- 238000001694 spray drying Methods 0.000 description 6
- 239000003053 toxin Substances 0.000 description 6
- 231100000765 toxin Toxicity 0.000 description 6
- 238000005341 cation exchange Methods 0.000 description 5
- 229910001385 heavy metal Inorganic materials 0.000 description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 4
- 235000017557 sodium bicarbonate Nutrition 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- -1 concave convex rod Inorganic materials 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 235000017550 sodium carbonate Nutrition 0.000 description 3
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- 238000002604 ultrasonography Methods 0.000 description 3
- 231100000678 Mycotoxin Toxicity 0.000 description 2
- 244000052616 bacterial pathogen Species 0.000 description 2
- 235000021050 feed intake Nutrition 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 210000004400 mucous membrane Anatomy 0.000 description 2
- 239000002636 mycotoxin Substances 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 230000007096 poisonous effect Effects 0.000 description 2
- 239000001488 sodium phosphate Substances 0.000 description 2
- 229960003339 sodium phosphate Drugs 0.000 description 2
- 235000011008 sodium phosphates Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 208000011580 syndromic disease Diseases 0.000 description 2
- KWILGNNWGSNMPA-LURJTMIESA-N (R)-(-)-Mellein Natural products C1=CC(O)=C2C(=O)O[C@@H](C)CC2=C1 KWILGNNWGSNMPA-LURJTMIESA-N 0.000 description 1
- 229930195730 Aflatoxin Natural products 0.000 description 1
- 244000063299 Bacillus subtilis Species 0.000 description 1
- 235000014469 Bacillus subtilis Nutrition 0.000 description 1
- 241000606807 Glaesserella parasuis Species 0.000 description 1
- 229920002581 Glucomannan Polymers 0.000 description 1
- 240000001046 Lactobacillus acidophilus Species 0.000 description 1
- 235000013956 Lactobacillus acidophilus Nutrition 0.000 description 1
- 206010028470 Mycoplasma infections Diseases 0.000 description 1
- 208000030852 Parasitic disease Diseases 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 239000004113 Sepiolite Substances 0.000 description 1
- 241000194017 Streptococcus Species 0.000 description 1
- BXFOFFBJRFZBQZ-QYWOHJEZSA-N T-2 toxin Chemical compound C([C@@]12[C@]3(C)[C@H](OC(C)=O)[C@@H](O)[C@H]1O[C@H]1[C@]3(COC(C)=O)C[C@@H](C(=C1)C)OC(=O)CC(C)C)O2 BXFOFFBJRFZBQZ-QYWOHJEZSA-N 0.000 description 1
- BXFOFFBJRFZBQZ-UHFFFAOYSA-N T2 Toxin Natural products C1=C(C)C(OC(=O)CC(C)C)CC2(COC(C)=O)C1OC1C(O)C(OC(C)=O)C2(C)C11CO1 BXFOFFBJRFZBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000082085 Verticillium <Phyllachorales> Species 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- VEUACKUBDLVUAC-UHFFFAOYSA-N [Na].[Ca] Chemical compound [Na].[Ca] VEUACKUBDLVUAC-UHFFFAOYSA-N 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 239000005409 aflatoxin Substances 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 238000003975 animal breeding Methods 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 239000000404 calcium aluminium silicate Substances 0.000 description 1
- 235000012215 calcium aluminium silicate Nutrition 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- LINOMUASTDIRTM-QGRHZQQGSA-N deoxynivalenol Chemical compound C([C@@]12[C@@]3(C[C@@H](O)[C@H]1O[C@@H]1C=C(C([C@@H](O)[C@@]13CO)=O)C)C)O2 LINOMUASTDIRTM-QGRHZQQGSA-N 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical compound [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 description 1
- 210000000981 epithelium Anatomy 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229940039695 lactobacillus acidophilus Drugs 0.000 description 1
- KWILGNNWGSNMPA-UHFFFAOYSA-N mellein Chemical compound C1=CC(O)=C2C(=O)OC(C)CC2=C1 KWILGNNWGSNMPA-UHFFFAOYSA-N 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000029058 respiratory gaseous exchange Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 229910052624 sepiolite Inorganic materials 0.000 description 1
- 235000019355 sepiolite Nutrition 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229960001471 sodium selenite Drugs 0.000 description 1
- 239000011781 sodium selenite Substances 0.000 description 1
- 235000015921 sodium selenite Nutrition 0.000 description 1
- UGTZMIPZNRIWHX-UHFFFAOYSA-K sodium trimetaphosphate Chemical group [Na+].[Na+].[Na+].[O-]P1(=O)OP([O-])(=O)OP([O-])(=O)O1 UGTZMIPZNRIWHX-UHFFFAOYSA-K 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- MBMQEIFVQACCCH-UHFFFAOYSA-N trans-Zearalenon Natural products O=C1OC(C)CCCC(=O)CCCC=CC2=CC(O)=CC(O)=C21 MBMQEIFVQACCCH-UHFFFAOYSA-N 0.000 description 1
- 229960005486 vaccine Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- LINOMUASTDIRTM-UHFFFAOYSA-N vomitoxin hydrate Natural products OCC12C(O)C(=O)C(C)=CC1OC1C(O)CC2(C)C11CO1 LINOMUASTDIRTM-UHFFFAOYSA-N 0.000 description 1
- MBMQEIFVQACCCH-QBODLPLBSA-N zearalenone Chemical compound O=C1O[C@@H](C)CCCC(=O)CCC\C=C\C2=CC(O)=CC(O)=C21 MBMQEIFVQACCCH-QBODLPLBSA-N 0.000 description 1
Landscapes
- Fodder In General (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of wide spectrum feed montmorillonites to take off mould dose, includes the component of following weight percents：Montmorillonite 2 0-80%, yeast cell wall 10-50%, seaweed 10-50%.Preparation method includes the following steps：（1）Montmorillonite is delaminated crushing, seaweed is added, stirs evenly；（2）Copper sulphate and sodium salt are uniformly mixed, yeast cell wall is added, stirs evenly；（3）By step（2）Acquired mixture is added and step（1）The mixture of gained, stirs and evenly mixs, and obtains mould dose de-.Application method：Pre- mildew proof adds 1-5 kilograms in feed per ton；Mouldy feed adds 3-8 kilograms in feed per ton.The present invention is in good taste, and cost of material is low, without side-effects to animal, efficiently de- mould, can act on a variety of common moulds in feed, while providing de- mould dose of the preparation method and application method, simple for process, of low cost, is convenient for industrialized production.
Description
Technical field
De- mould dose the present invention relates to one kind, specifically a kind of wide spectrum feed montmorillonite take off mould dose and preparation method thereof with make
With method, belong to feed additive field.
Background technology
Feed raw grain and finished product feedstuff go mouldy caused by Moisture high UCL or storage are improper.Edible animal breeding can be induced
Breathing syndrome, system failure syndrome, pseudoabies, pest heat symptom-complex, haemophilus parasuis, streptococcus, eperythrozoonosis, bow
Some epidemy diseases such as shape parasitosis.Vomiting, food refusal, feed intake decline；Although immune programme is reasonable, vaccine is also inoculated on time, move
Object group antibody level does not increase always but.
Currently, also have the mould dose de- of many brands, but effect is general, and ingredient safety is poor, can cause two to animal
Secondary injury.Patent No. CN1817170A discloses a kind of mineral substance and takes off mould dose and preparation method thereof, with montmorillonite, concave convex rod,
Sepiolite, hydration sodium calcium aluminium silicate are component, but poor taste, after being added to feed, animal apocleisis, food refusal, and also it is edible
It is easy to cause the abdomen full sense of animal afterwards, feed intake declines, slow-growing.
Patent No. CN103461677A also discloses that a kind of animal feed takes off mould dose and the preparation method and application thereof, presses
Mass fraction meter includes following components：50-150 parts of bacillus subtilis, 5-15 parts of lactobacillus acidophilus freeze-drying powder, sodium selenite
0.1-1 parts, 5-55 parts of vitamin E2, feeding active dry yeast 100-300 parts, 5-15 parts of glucomannans, montmorillonite 50-150
Part and 350-700 parts of hydrated aluminosilicate of improvement.Mould dose of green non-pollution is taken off prepared by the present invention, to various common moulds
Toxin has extremely strong adsorption capacity.But high expensive, popularization in the market are restricted.
Invention content
The object of the present invention is to provide a kind of wide spectrum feed montmorillonites to take off mould dose, and in good taste, cost of material is low, to animal without
Side effect, it is efficiently de- mould, a variety of common moulds in feed can be acted on, while de- mould dose of the preparation method being provided and is made
It is simple for process, of low cost with method, it is convenient for industrialized production.
The present invention adopts the following technical scheme that：A kind of wide spectrum feed montmorillonite takes off mould dose, including following weight percents
Component：Montmorillonite 2 0-80%, yeast cell wall 10-50%, seaweed 10-50%.
Montmorillonite can effectively remove a variety of harmful mycotoxins in feed, remove damage of the toxin to animal body,
There is extremely strong adsorb, admittedly to mycotoxins such as aflatoxins, ochracin, zearalenone toxin, vomitoxin, T2 toxin
Fixed, inhibiting effect；After animal edible, yeast cell wall is cooperateed with montmorillonite, to pathogenic bacteria in the digestive tract and their institutes
Toxin, gas of generation etc. have it is extremely strong adsorb and fix, inhibiting effect, so that it is lost pathogenic, with a seaweed, can promote
The alimentary canal mucous membrane epithelium regeneration of damage, restores the normal rhythm of enterocinesia, safeguards the conveying and absorption of enteron aisle, improves alimentary canal
Immune function.Montmorillonite itself is not digested, and is carried various poisonous substances and is excreted, ensures the health of animal.
Preferably, it is 1-10% sodium salts to also have the copper sulphate, weight percent that weight percent is 1-10% in mould dose de-.
Copper sulphate has synergistic effect to the mould suction-operated of montmorillonite, can improve its percent 20 or so adsorption rate,
Sodium salt can not only reinforce adsorption effect, be significantly increased effect to the absorption of pathogenic bacteria in enteron aisle to montmorillonite.
Preferably, taking off the mould dose of component for including following weight percents：Montmorillonite 30-50%, yeast cell wall 20-
30%, seaweed 20-30%, copper sulphate 1-10%, sodium salt 1-10%.
Preferably, the sodium salt is the mixture of sodium carbonate or sodium bicarbonate or sodium carbonate and sodium bicarbonate.
A kind of wide spectrum feed montmorillonite takes off mould dose of preparation method, includes the following steps：（1）Montmorillonite is delaminated crushing,
Seaweed is added, stirs evenly；（2）Copper sulphate and sodium salt are uniformly mixed, yeast cell wall is added, stirs evenly；（3）By step
（2）Acquired mixture is added and step（1）The mixture of gained, stirs and evenly mixs, and obtains mould dose de-.
Preferably, the montmorillonite is made by the following method：（a）Montmorillonite raw material is dried under the conditions of 70-90 DEG C
Afterwards, it is crushed to 300-500 mesh, obtains raw material powder；（b）To step（a）Obtained raw material powder carries out pre-treatment：Raw material powder is added
It into sodium salt solution, handles 2-5 hours, filtering obtains treatment fluid；The weight ratio of raw material powder and sodium salt solution is 1:1-3；（c）
The zeolite that grain size is 0.2mm is added in treatment fluid, in mixing plant, stir process 1-3 hours, mixing speed 200-300
Rev/min, it then concentrates, be dried to obtain processing powder；（d）Water is added into processing powder, is stirred and evenly mixed with processing powder, is made and contains admittedly
Amount is the slurries of 10-25%；（e）The slurries cross 300-500 mesh sieve, obtain the first filtrate；（f）First filtrate is sent into ultra-fine equipment
Middle progress is ultra-fine to delaminate, and removes solid particle using classifying equipoment after delaminating, obtains the second filtrate；（g）Described second is filtered
Liquid sterilizing, concentration, drying, obtain montmorillonite.
Preferably, the sodium salt is the mixture of one or more of sodium carbonate or sodium bicarbonate or sodium pyrophosphate,
A concentration of 50-80% of sodium salt.
Preferably, the sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, mass mixing ratio 3-5:1.
Wide spectrum feed montmorillonite provided by the present invention takes off mould dose of application method：Pre- mildew proof is added in feed per ton
1-5 kilograms；Mouldy feed adds 3-8 kilograms in feed per ton.
By implementing above-mentioned technical proposal, cost of material of the present invention is low, green non-poisonous evil, being capable of common mould of efficient absorption
Verticillium toxin, can inhibit the breeding of mould in feed, after animal edible, can protect mucous membrane, but do not absorbed by animal body, carry
The toxin adsorbed excretes；Preparation method, it is simple for process, of low cost, it is convenient for industrialized production；Application method is simple.
Specific implementation mode
With reference to embodiment, further description is done to the present invention.
Embodiment 1：
A kind of wide spectrum feed montmorillonite takes off mould dose, includes the component of following weight percents：Powdered montmorillonite 2 0%,
Yeast cell wall 40%, powdered seaweed 40%.
Preparation process：（1）Montmorillonite is delaminated crushing, seaweed is added, stirs evenly；（2）Yeast cell wall, stirring is added
Uniformly.
The preparation method for the montmorillonite used includes：（a）It is 5% that montmorillonite raw material to moisture content is dried under the conditions of 70 DEG C
Afterwards, 400 mesh are crushed to, raw material powder is obtained；（b）Pre-treatment is carried out to obtained raw material powder, steps are as follows：By a concentration of 50%
Sodium salt solution is added in raw material powder, is handled 3 hours under conditions of temperature is 70 DEG C, and filtering obtains treatment fluid；Sodium salt is carbon
The mixture of sour sodium and sodium pyrophosphate, mass mixing ratio 3:1；The weight ratio of raw material powder and sodium salt solution is 1:1；（c）Processing
The zeolite that grain size is 0.2mm is added in liquid, in mixing plant, stir process 1 hour, mixing speed is 250 revs/min, so
After concentrate, be dried to obtain processing powder；（c）Water and dispersant is added into processing powder, is stirred and evenly mixed with raw material powder, solid content is made
For 25% slurries；Dispersant is the 0.05% of raw material powder weight, selects calgon；（d）The slurries cross 500 mesh
Sieve, obtains the first filtrate；（e）First filtrate be sent into ultra-fine equipment carry out it is ultra-fine delaminate, removed using classifying equipoment after delaminating
Solid particle obtains the second filtrate；（f）By second filtrate sterilizing, concentration, dry, montmorillonite is obtained, purity 99.3%,
Heavy metal lead is 3ppn, whiteness 86%, cation exchange capacity 150mmol/100g.
Wide spectrum feed montmorillonite takes off mould dose of application method：Pre- mildew proof adds 2 kilograms in feed per ton；It is mouldy
Feed, 6 kilograms are added in feed per ton.
Embodiment 2：
A kind of wide spectrum feed montmorillonite takes off mould dose, includes the component of following weight percents：Powdered montmorillonite 80%,
Yeast cell wall 10%, powdered seaweed 10%.
Preparation process：（1）Montmorillonite is delaminated crushing, seaweed is added, stirs evenly；（2）Yeast cell wall, stirring is added
Uniformly.
The preparation method for the montmorillonite used includes：（a）It is 5% that montmorillonite raw material to moisture content is dried under the conditions of 70 DEG C
Afterwards, 400 mesh are crushed to, raw material powder is obtained；（b）Pre-treatment is carried out to obtained raw material powder, steps are as follows：By a concentration of 50%
Sodium salt solution is added in raw material powder, is handled 3 hours under conditions of temperature is 70 DEG C, and filtering obtains treatment fluid；Sodium salt is carbon
The mixture of sour sodium and sodium pyrophosphate, mass mixing ratio 3:1；The weight ratio of raw material powder and sodium salt solution is 1:1；（c）Processing
The zeolite that grain size is 0.2mm is added in liquid, in mixing plant, stir process 1 hour, mixing speed is 250 revs/min, so
After concentrate, be dried to obtain processing powder；（c）Water and dispersant is added into processing powder, is stirred and evenly mixed with raw material powder, solid content is made
For 25% slurries；Dispersant is the 0.05% of raw material powder weight, selects calgon；（d）The slurries cross 300 mesh
Sieve, obtains the first filtrate；（e）First filtrate be sent into ultra-fine equipment carry out it is ultra-fine delaminate, removed using classifying equipoment after delaminating
Solid particle obtains the second filtrate；（f）By second filtrate sterilizing, concentration, dry, montmorillonite is obtained, purity 99.3%,
Heavy metal lead is 3ppn, whiteness 86%, cation exchange capacity 150mmol/100g.
Wide spectrum feed montmorillonite takes off mould dose of application method：Pre- mildew proof adds 2 kilograms in feed per ton；It is mouldy
Feed, 6 kilograms are added in feed per ton.
Embodiment 3：
A kind of wide spectrum feed montmorillonite takes off mould dose, includes the component of following weight percents：Powdered montmorillonite 60%,
Yeast cell wall 20%, powdered seaweed 10%, copper sulphate 5%, sodium salt 5%；Sodium salt selects sodium carbonate.
Preparation process：（1）Montmorillonite is delaminated crushing, seaweed is added, stirs evenly；（2）Copper sulphate and sodium salt are mixed
Uniformly, yeast cell wall is added, stirs evenly；（3）By step（2）Acquired mixture is added and step（1）The mixing of gained
Object stirs and evenly mixs, and obtains mould dose de-.
The preparation method for the montmorillonite used includes：（a）It is 4% that montmorillonite raw material to moisture content is dried under the conditions of 80 DEG C
Afterwards, after, 500 mesh are crushed to, obtain raw material powder；（b）Pre-treatment is carried out to obtained raw material powder, steps are as follows：By a concentration of 70%
Sodium salt solution be added in raw material powder, handled 5 hours under the conditions of at a temperature of 90 °C, filter, obtain treatment fluid；Treatment fluid
In add grain size be 0.2mm zeolite, in mixing plant, stir process 2 hours, mixing speed be 200 revs/min, so
It concentrates afterwards, obtain processing powder after spray drying；Sodium salt is sodium carbonate；The weight ratio of raw material powder and sodium carbonate liquor is 1:2；（c）
00.1% dispersant of water and raw material powder weight is added into processing powder, is stirred and evenly mixed with raw material powder, it is 20% that solid content, which is made,
Slurries；The dispersant is sodium pyrophosphate；（d）The slurries cross 400 mesh sieve, obtain the first filtrate；（e）First filtrate is sent into super
Carried out in thin equipment it is ultra-fine delaminate, using solid particle is removed in classifying equipoment centrifuge after delaminating, obtain the second filtrate；
（f）To ultrasound sterilizing under the second filtrate high-temperature and high-pressure conditions, after carrying out sour processing to it, concentration, spray drying are covered
De- stone, purity 99.6%, heavy metal lead 3ppn, whiteness 87%, cation exchange capacity 155mmol/100g.
Wide spectrum feed montmorillonite takes off mould dose of application method：Pre- mildew proof adds 1 kilogram in feed per ton；It is mouldy
Feed, 3 kilograms are added in feed per ton.
Embodiment 4：
A kind of wide spectrum feed montmorillonite takes off mould dose, includes the component of following weight percents：Powdered montmorillonite 75%,
Yeast cell wall 11%, powdered seaweed 12%, copper sulphate 1%, sodium salt 1%；Sodium salt selects sodium bicarbonate.
Preparation process：（1）Montmorillonite is delaminated crushing, seaweed is added, stirs evenly；（2）Copper sulphate and sodium salt are mixed
Uniformly, yeast cell wall is added, stirs evenly；（3）By step（2）Acquired mixture is added and step（1）The mixing of gained
Object stirs and evenly mixs, and obtains mould dose de-.
The preparation method for the montmorillonite used includes：（a）Montmorillonite raw material to moisture content is dried under the conditions of 80 DEG C is
After 4.5%, after, 500 mesh are crushed to, raw material powder is obtained；（b）Pre-treatment is carried out to obtained raw material powder, steps are as follows：By concentration
80% sodium salt solution is added in raw material powder, is handled 5 hours under the conditions of at a temperature of 90 °C, and filtering obtains treatment fluid；Place
The zeolite that grain size is 0.3mm is added in reason liquid, in mixing plant, stir process 1.5 hours, mixing speed is 250 revs/min
Then clock concentrates, obtains processing powder after spray drying；Sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is
5:1；The weight ratio of raw material powder and sodium salt solution is 1:2；（c）0.01% point of water and raw material powder weight is added into processing powder
Powder is stirred and evenly mixed with raw material powder, and the slurries that solid content is 20% are made；The dispersant is calgon and sodium pyrophosphate
In mass ratio 1:2 mixture；（d）The slurries cross 400 mesh sieve, obtain the first filtrate；（e）First filtrate is sent into ultra-fine equipment
Carry out it is ultra-fine delaminate, using solid particle is removed in classifying equipoment centrifuge after delaminating, obtain the second filtrate；（f）To second
Ultrasound sterilizing under filtrate high-temperature and high-pressure conditions, after carrying out sour processing to it, concentration, spray drying obtain montmorillonite, purity
For 99.8%, heavy metal lead 1ppn, whiteness 80%, cation exchange capacity 180mmol/100g.
Wide spectrum feed montmorillonite takes off mould dose of application method：Pre- mildew proof adds 5 kilograms in feed per ton；It is mouldy
Feed, 8 kilograms are added in feed per ton.
Embodiment 5：
A kind of wide spectrum feed montmorillonite takes off mould dose, includes the component of following weight percents：Powdered montmorillonite 50%,
Yeast cell wall 25%, powdered seaweed 20%, copper sulphate 3%, sodium salt 2%；It is 3 that sodium salt, which selects mass ratio,：1 sodium carbonate and carbon
The mixture of sour hydrogen sodium.
Preparation process：（1）Montmorillonite is delaminated crushing, seaweed is added, stirs evenly；（2）Copper sulphate and sodium salt are mixed
Uniformly, yeast cell wall is added, stirs evenly；（3）By step（2）Acquired mixture is added and step（1）The mixing of gained
Object stirs and evenly mixs, and obtains mould dose de-.
The preparation method for the montmorillonite used includes：（a）It is 3% that montmorillonite raw material to moisture content is dried under the conditions of 85 DEG C
Afterwards, after, 450 mesh are crushed to, obtain raw material powder；（b）Pre-treatment is carried out to obtained raw material powder, steps are as follows：By a concentration of 60%
Sodium salt solution be added in raw material powder, temperature be 80 DEG C under conditions of handle 4 hours, filtering, obtain treatment fluid；(c) place
The zeolite that grain size is 0.2mm is added in reason liquid, in mixing plant, stir process 1 hour, mixing speed is 300 revs/min
Then clock concentrates, obtains processing powder after spray drying；Sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is
4:1；The weight ratio of raw material powder and sodium salt solution is 1:3；（d）0.08% point of water and raw material powder weight is added into processing powder
Powder is stirred and evenly mixed with raw material powder, and the slurries that solid content is 20% are made；The dispersant is sodium trimetaphosphate；（e）The slurry
Liquid crosses 400 mesh sieve, obtains the first filtrate；（f）First filtrate be sent into ultra-fine equipment carry out it is ultra-fine delaminate, using classification after delaminating
Solid particle is removed in equipment centrifuge, obtains the second filtrate；（g）It sterilizes to ultrasound under the second filtrate high-temperature and high-pressure conditions,
After carrying out sour processing to it, concentration, spray drying obtain montmorillonite, purity 99.9%, heavy metal lead 0ppn, whiteness are
90%, cation exchange capacity 200mmol/100g.
Wide spectrum feed montmorillonite takes off mould dose of application method：Pre- mildew proof adds 1-5 kilograms in feed per ton；It has sent out
Mould feed adds 3-8 kilograms in feed per ton.
Claims (2)
1. a kind of wide spectrum feed montmorillonite takes off mould dose, which is characterized in that the component including following weight percents：Montmorillonite 2 0-
80%, yeast cell wall 10-50%, seaweed 10-50%, copper sulphate 1-10%, sodium salt 1-10%；The montmorillonite is by the following method
It is made：（a）After drying montmorillonite raw material under the conditions of 70-90 DEG C, it is crushed to 300-500 mesh, obtains raw material powder；（b）To step（a）
Obtained raw material powder carries out pre-treatment：Raw material powder is added in sodium salt solution, is handled 2-5 hours, filtering is handled
Liquid；The weight ratio of raw material powder and sodium salt solution is 1:1-3；（c）The zeolite that grain size is 0.2mm is added in treatment fluid, is set in stirring
In standby, stir process 1-3 hours, mixing speed is 200-300 revs/min, then concentrates, is dried to obtain processing powder；（d）To place
Water is added in reason powder, is stirred and evenly mixed with processing powder, the slurries that solid content is 10-25% are made；（e）The slurries cross 300-500 mesh
Sieve, obtains the first filtrate；（f）First filtrate be sent into ultra-fine equipment carry out it is ultra-fine delaminate, removed using classifying equipoment after delaminating
Solid particle obtains the second filtrate；（g）By second filtrate sterilizing, concentration, drying, montmorillonite product is obtained.
2. a kind of wide spectrum feed montmorillonite takes off mould dose according to claim 1, which is characterized in that including following weight percents
Component：Montmorillonite 30-50%, yeast cell wall 20-30%, seaweed 20-30%, copper sulphate 1-10%, sodium salt 1-10%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510495977.XA CN105010760B (en) | 2015-08-14 | 2015-08-14 | A kind of wide spectrum feed montmorillonite takes off mould dose and preparation method thereof and application method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510495977.XA CN105010760B (en) | 2015-08-14 | 2015-08-14 | A kind of wide spectrum feed montmorillonite takes off mould dose and preparation method thereof and application method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105010760A CN105010760A (en) | 2015-11-04 |
| CN105010760B true CN105010760B (en) | 2018-11-06 |
Family
ID=54401395
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510495977.XA Expired - Fee Related CN105010760B (en) | 2015-08-14 | 2015-08-14 | A kind of wide spectrum feed montmorillonite takes off mould dose and preparation method thereof and application method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105010760B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106306425A (en) * | 2016-08-22 | 2017-01-11 | 四川恒通动保生物科技有限公司 | Feed mold removal agent and preparation method thereof |
| CN107136388A (en) * | 2017-05-22 | 2017-09-08 | 青岛海大海糖生物科技有限公司 | It is a kind of compound de- mould dose and preparation method thereof containing chitosan oligosaccharide |
| CN107497563A (en) * | 2017-09-22 | 2017-12-22 | 安吉高纯蒙脱石有限公司 | A kind of anti-clogging pulverizer |
| CN109673849A (en) * | 2019-01-04 | 2019-04-26 | 联技精细材料(珠海)有限公司 | A kind of feeding Smecta additive and its preparation method and application |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101602509A (en) * | 2008-06-11 | 2009-12-16 | 浙江海力生制药有限公司 | A kind of montmorillonite that utilizes the method for electrophoresis purifying montmorillonite and make and its application |
| CN101340979B (en) * | 2006-02-09 | 2010-06-16 | 浙江海力生制药有限公司 | Method for purifying montmorillonite, purified montmorillonite and combination thereof |
| CN102940131A (en) * | 2012-12-11 | 2013-02-27 | 江西新世纪民星动物保健品有限公司 | Novel mycotoxin detoxification agent and preparation method thereof |
| CN102948679A (en) * | 2012-07-03 | 2013-03-06 | 山东绿都安特动物药业有限公司 | Multifunctional mildew removal feed premixing agent with physical, chemical and biological mildew removal functions |
| CN103243028A (en) * | 2012-02-02 | 2013-08-14 | 安琪酵母股份有限公司 | Yeast cell wall and preparation method thereof, forage additive and preparation method thereof, and forage |
| CN103461677A (en) * | 2013-09-25 | 2013-12-25 | 南京日升昌生物技术有限公司 | Mold removal agent for animal feed as well as preparation method and application of mold removal agent |
| CN103829113A (en) * | 2014-03-06 | 2014-06-04 | 苏州万生源生物科技有限公司 | Mycotoxin detoxication agent for foods, preparation method and application of mycotoxin detoxication agent |
| CN104171421A (en) * | 2014-08-08 | 2014-12-03 | 河南牧翔动物药业有限公司 | Feed additive for conditioning intestines of animals |
| CN104431375A (en) * | 2014-12-31 | 2015-03-25 | 湖北泱盛生物科技有限公司 | Mycotoxin adsorbent and preparation method thereof |
-
2015
- 2015-08-14 CN CN201510495977.XA patent/CN105010760B/en not_active Expired - Fee Related
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101340979B (en) * | 2006-02-09 | 2010-06-16 | 浙江海力生制药有限公司 | Method for purifying montmorillonite, purified montmorillonite and combination thereof |
| CN101602509A (en) * | 2008-06-11 | 2009-12-16 | 浙江海力生制药有限公司 | A kind of montmorillonite that utilizes the method for electrophoresis purifying montmorillonite and make and its application |
| CN103243028A (en) * | 2012-02-02 | 2013-08-14 | 安琪酵母股份有限公司 | Yeast cell wall and preparation method thereof, forage additive and preparation method thereof, and forage |
| CN102948679A (en) * | 2012-07-03 | 2013-03-06 | 山东绿都安特动物药业有限公司 | Multifunctional mildew removal feed premixing agent with physical, chemical and biological mildew removal functions |
| CN102940131A (en) * | 2012-12-11 | 2013-02-27 | 江西新世纪民星动物保健品有限公司 | Novel mycotoxin detoxification agent and preparation method thereof |
| CN103461677A (en) * | 2013-09-25 | 2013-12-25 | 南京日升昌生物技术有限公司 | Mold removal agent for animal feed as well as preparation method and application of mold removal agent |
| CN103829113A (en) * | 2014-03-06 | 2014-06-04 | 苏州万生源生物科技有限公司 | Mycotoxin detoxication agent for foods, preparation method and application of mycotoxin detoxication agent |
| CN104171421A (en) * | 2014-08-08 | 2014-12-03 | 河南牧翔动物药业有限公司 | Feed additive for conditioning intestines of animals |
| CN104431375A (en) * | 2014-12-31 | 2015-03-25 | 湖北泱盛生物科技有限公司 | Mycotoxin adsorbent and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| "猪场霉菌毒素的危害与控制策略";李铁军等;《中国畜牧兽医报》;20140413;第1-2页 * |
| "霉菌毒素对家禽养殖的危害及控制措施";张丞;《中国禽业导刊》;20051231;第22卷(第22期);第36-37页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105010760A (en) | 2015-11-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105010760B (en) | A kind of wide spectrum feed montmorillonite takes off mould dose and preparation method thereof and application method | |
| CN100397998C (en) | Composite mold toxin sorbent | |
| CN104431375A (en) | Mycotoxin adsorbent and preparation method thereof | |
| CN1810145A (en) | Production process of natural mineral feed additive | |
| CN103721533A (en) | Deoxidizing and drying agent and preparation method thereof | |
| EP2408315B1 (en) | A method of reducing the rate of degradation of a biological material | |
| CN107114584B (en) | Feed additive for lactating sows and preparation and use methods thereof | |
| CN103734864A (en) | Deoxidizing and drying agent for food and feed and preparation method thereof | |
| RU2502319C1 (en) | Method for production of fodder additive for prevention of animals and birds mycotoxicosis | |
| WO2003077673A1 (en) | A process for producing a feed additive adsorbing the mycotoxin in the animal feed | |
| CN1927803A (en) | Method of preparing calcium propionate and calcium lactate with oyster shell as calcium source | |
| CN103918589A (en) | Animal health product capable of improving survival rate of shrimp fry in long distance transportation | |
| CN104546908A (en) | Pharmaceutical composition as well as preparation method and application thereof | |
| CN102499290A (en) | Nutrient milk powder with selenium-enriched lentinus edodes and method for producing nutrient milk powder with selenium-enriched lentinus edodes | |
| BG107098A (en) | Organomineral adsorbent of mycotoxin as animal feed additive, procedure for production and application | |
| CN106616717A (en) | Preparation process of cell-wall-disrupytion bee pollen beans or bee pollen sheets without additives | |
| CN102919559B (en) | Feed additive for ewe | |
| CN101803695A (en) | Calcium and iron supplement product being applicable to children | |
| KR101109756B1 (en) | Method for production of fermented composition using guava leaf powder | |
| CN113273647A (en) | Fermented selenium-rich pig feed | |
| CN103736462A (en) | Deoxidizing and drying agent for medical medicines and preparation method thereof | |
| CN101248829A (en) | Preparation technique of maggot activity albumen powder | |
| CN103721534A (en) | Deoxidizing and drying agent for instruments and meters and preparation method thereof | |
| EP3330224A1 (en) | A method for producing a modified saponite, the modified saponite and an inter-packet water obtained by said method, a combination comprising them, use of the modified saponite and the combination and products comprising them | |
| CN106343221A (en) | Edible healthcare composition with effect of promoting growth of meat pigeons, method for preparing edible healthcare composition and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181106 |