CN105010760A - Broad-spectrum feed montmorillonite mold removal agent and preparation method and application method thereof - Google Patents
Broad-spectrum feed montmorillonite mold removal agent and preparation method and application method thereof Download PDFInfo
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- CN105010760A CN105010760A CN201510495977.XA CN201510495977A CN105010760A CN 105010760 A CN105010760 A CN 105010760A CN 201510495977 A CN201510495977 A CN 201510495977A CN 105010760 A CN105010760 A CN 105010760A
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- montmorillonite
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- sodium salt
- sodium
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- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 title claims abstract description 75
- 229910052901 montmorillonite Inorganic materials 0.000 title claims abstract description 75
- 238000000034 method Methods 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 159000000000 sodium salts Chemical class 0.000 claims abstract description 43
- 239000000203 mixture Substances 0.000 claims abstract description 40
- 210000005253 yeast cell Anatomy 0.000 claims abstract description 19
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 235000012054 meals Nutrition 0.000 claims description 38
- 238000003756 stirring Methods 0.000 claims description 33
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 32
- 239000000706 filtrate Substances 0.000 claims description 28
- 238000001228 spectrum Methods 0.000 claims description 25
- 238000002156 mixing Methods 0.000 claims description 20
- 239000000843 powder Substances 0.000 claims description 17
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 16
- 239000012530 fluid Substances 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 14
- 239000002002 slurry Substances 0.000 claims description 14
- 239000007787 solid Substances 0.000 claims description 14
- 239000012266 salt solution Substances 0.000 claims description 13
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 10
- 229940048086 sodium pyrophosphate Drugs 0.000 claims description 10
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims description 10
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 8
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 8
- 229910021536 Zeolite Inorganic materials 0.000 claims description 7
- 238000002203 pretreatment Methods 0.000 claims description 7
- 238000010298 pulverizing process Methods 0.000 claims description 7
- 230000001954 sterilising effect Effects 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000010457 zeolite Substances 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 4
- 239000000047 product Substances 0.000 claims description 2
- 241001465754 Metazoa Species 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 4
- 239000003795 chemical substances by application Substances 0.000 abstract 7
- 229910000365 copper sulfate Inorganic materials 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 239000002270 dispersing agent Substances 0.000 description 10
- -1 concave convex rod Inorganic materials 0.000 description 6
- 238000005507 spraying Methods 0.000 description 6
- 238000005341 cation exchange Methods 0.000 description 5
- 229910001385 heavy metal Inorganic materials 0.000 description 5
- 231100000678 Mycotoxin Toxicity 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000002636 mycotoxin Substances 0.000 description 4
- 239000003053 toxin Substances 0.000 description 4
- 231100000765 toxin Toxicity 0.000 description 4
- 238000010306 acid treatment Methods 0.000 description 3
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 3
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- 244000052616 bacterial pathogen Species 0.000 description 2
- 235000021050 feed intake Nutrition 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 210000004400 mucous membrane Anatomy 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 230000007096 poisonous effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 208000011580 syndromic disease Diseases 0.000 description 2
- KWILGNNWGSNMPA-LURJTMIESA-N (R)-(-)-Mellein Natural products C1=CC(O)=C2C(=O)O[C@@H](C)CC2=C1 KWILGNNWGSNMPA-LURJTMIESA-N 0.000 description 1
- 229930195730 Aflatoxin Natural products 0.000 description 1
- 244000063299 Bacillus subtilis Species 0.000 description 1
- 235000014469 Bacillus subtilis Nutrition 0.000 description 1
- 241000606807 Glaesserella parasuis Species 0.000 description 1
- 229920002581 Glucomannan Polymers 0.000 description 1
- 240000001046 Lactobacillus acidophilus Species 0.000 description 1
- 235000013956 Lactobacillus acidophilus Nutrition 0.000 description 1
- 206010028470 Mycoplasma infections Diseases 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 239000004113 Sepiolite Substances 0.000 description 1
- 241000194017 Streptococcus Species 0.000 description 1
- BXFOFFBJRFZBQZ-QYWOHJEZSA-N T-2 toxin Chemical compound C([C@@]12[C@]3(C)[C@H](OC(C)=O)[C@@H](O)[C@H]1O[C@H]1[C@]3(COC(C)=O)C[C@@H](C(=C1)C)OC(=O)CC(C)C)O2 BXFOFFBJRFZBQZ-QYWOHJEZSA-N 0.000 description 1
- BXFOFFBJRFZBQZ-UHFFFAOYSA-N T2 Toxin Natural products C1=C(C)C(OC(=O)CC(C)C)CC2(COC(C)=O)C1OC1C(O)C(OC(C)=O)C2(C)C11CO1 BXFOFFBJRFZBQZ-UHFFFAOYSA-N 0.000 description 1
- 201000005485 Toxoplasmosis Diseases 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- VEUACKUBDLVUAC-UHFFFAOYSA-N [Na].[Ca] Chemical compound [Na].[Ca] VEUACKUBDLVUAC-UHFFFAOYSA-N 0.000 description 1
- 210000001015 abdomen Anatomy 0.000 description 1
- 239000005409 aflatoxin Substances 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 239000003674 animal food additive Substances 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 239000000404 calcium aluminium silicate Substances 0.000 description 1
- 235000012215 calcium aluminium silicate Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- LINOMUASTDIRTM-QGRHZQQGSA-N deoxynivalenol Chemical compound C([C@@]12[C@@]3(C[C@@H](O)[C@H]1O[C@@H]1C=C(C([C@@H](O)[C@@]13CO)=O)C)C)O2 LINOMUASTDIRTM-QGRHZQQGSA-N 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical compound [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000000981 epithelium Anatomy 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 230000036737 immune function Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229940039695 lactobacillus acidophilus Drugs 0.000 description 1
- KWILGNNWGSNMPA-UHFFFAOYSA-N mellein Chemical compound C1=CC(O)=C2C(=O)OC(C)CC2=C1 KWILGNNWGSNMPA-UHFFFAOYSA-N 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000001850 reproductive effect Effects 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 229910052624 sepiolite Inorganic materials 0.000 description 1
- 235000019355 sepiolite Nutrition 0.000 description 1
- 229960001471 sodium selenite Drugs 0.000 description 1
- 239000011781 sodium selenite Substances 0.000 description 1
- 235000015921 sodium selenite Nutrition 0.000 description 1
- UGTZMIPZNRIWHX-UHFFFAOYSA-K sodium trimetaphosphate Chemical group [Na+].[Na+].[Na+].[O-]P1(=O)OP([O-])(=O)OP([O-])(=O)O1 UGTZMIPZNRIWHX-UHFFFAOYSA-K 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- MBMQEIFVQACCCH-UHFFFAOYSA-N trans-Zearalenon Natural products O=C1OC(C)CCCC(=O)CCCC=CC2=CC(O)=CC(O)=C21 MBMQEIFVQACCCH-UHFFFAOYSA-N 0.000 description 1
- 229960005486 vaccine Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- LINOMUASTDIRTM-UHFFFAOYSA-N vomitoxin hydrate Natural products OCC12C(O)C(=O)C(C)=CC1OC1C(O)CC2(C)C11CO1 LINOMUASTDIRTM-UHFFFAOYSA-N 0.000 description 1
- MBMQEIFVQACCCH-QBODLPLBSA-N zearalenone Chemical compound O=C1O[C@@H](C)CCCC(=O)CCC\C=C\C2=CC(O)=CC(O)=C21 MBMQEIFVQACCCH-QBODLPLBSA-N 0.000 description 1
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- Fodder In General (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a broad-spectrum feed montmorillonite mold removal agent. The broad-spectrum feed montmorillonite mold removal agent comprises, by weight, 20-80% of montmorillonite, 10-50% of yeast cell walls and 10-50% of alga. A preparation method includes the following steps that 1, montmorillonite is peeled and smashed, the alga is added, and the mixture is evenly stirred; 2, copper sulfate and sodium salt are evenly mixed, the yeast cell walls are added, and the mixture is evenly stirred; 3, the mixture obtained in the step 2 is added to the mixture obtained in the step 2, the obtained mixture is stirred and evenly mixed, and the mold removal agent is obtained. An application method includes the steps that mold is prevented, and 1-5 kilograms of the mold removal agent is added to per tonnage of feed; 3-8 kilograms of the mold removal agent is added to per tonnage of moldy feed. The broad-spectrum feed montmorillonite mold removal agent is good in taste, low in raw material cost, free of side effects on animals and capable of efficiently removing mold and acting on multiple kinds of common mould in the feed; the preparation method and the application method of the mold removal agent are simple in process and low in cost, and industrial production is convenient.
Description
Technical field
The present invention relates to a kind of de-mould dose, be that a kind of wide spectrum feed montmorillonite takes off mould dose and preparation method thereof and using method specifically, belong to feed additive field.
Background technology
Feed raw grain and finished product feedstuff because of Moisture high UCL or store improper cause go mouldy.Some epidemy diseases such as edible animal reproductive respiratory syndrome, system failure syndrome, pseudoabies, pest heat symptom-complex, haemophilus parasuis, streptococcus, eperythrozoonosis, toxoplasmosis can be brought out.Vomiting, food refusal, feed intake decline; Although immune programme for children is reasonable, vaccine is also inoculated on time, fauna antibody horizontal does not increase always.
At present, also have de-mould dose of a lot of brand, but effect is general, and composition poor stability, secondary injury can be caused to animal.The patent No. is that CN1817170A discloses a kind of mineral substance and takes off mould dose and preparation method thereof, with montmorillonite, concave convex rod, sepiolite, hydration sodium calcium aluminium silicate for component, but mouthfeel is poor, after being added to feed, animal apocleisis, food refusal, and after eating, easily causing the full sense of the abdomen of animal, feed intake declines, poor growth.
The patent No. be CN103461677A also disclose a kind of animal feed take off mould dose and preparation method thereof with application, comprise following component according to the mass fraction: bacillus subtilis 50-150 part, lactobacillus acidophilus freeze-drying powder 5-15 part, sodium selenite 0.1-1 part, vitamin E2 5-55 part, feeding active dry yeast 100-300 part, glucomannans 5-15 part, montmorillonite 50-150 part and improvement hydrated aluminosilicate 350-700 part.De-mould dose of green non-pollution prepared by the present invention, all has extremely strong absorption affinity to various common mycotoxin.High expensive, the popularization on market is restricted.
Summary of the invention
The object of this invention is to provide a kind of wide spectrum feed montmorillonite and take off mould dose, mouthfeel is good, cost of material is low, animal is had no side effect, efficient de-mould, the multiple common mould in feed can be acted on, this its preparation method of de-mould dose and using method is provided simultaneously, technique is simple, with low cost, is convenient to suitability for industrialized production.
The present invention adopts following technical scheme: a kind of wide spectrum feed montmorillonite takes off mould dose, comprises the component of following weight percents: montmorillonite 2 0-80%, yeast cell wall 10-50%, marine alga 10-50%.
Montmorillonite effectively can remove the multiple harmful mycotoxin in feed, remove toxin to the infringement of animal body, have extremely strong absorption, fixing, inhibitory action to mycotoxins such as aflatoxins, ochracin, zearalenone toxin, vomitoxin, T2 toxin; After animal edible, yeast cell wall and montmorillonite are worked in coordination with, to the pathogenic bacteria in alimentary canal, and toxin, gas etc. that they produce have extremely strong absorption, fixing, inhibitory action, make it lose pathogenic, join a marine alga, the alimentary canal mucous membrane epithelium regeneration damaged can be promoted, recover the normal rhythm of enterocinesia, safeguard conveying and the absorption of enteron aisle, improve gastral immunologic function.Montmorillonite itself is not digested, carries various poisonous substance and excretes, and ensures the health of animal.
As preferably, in de-mould dose, also have that percentage by weight is the copper sulphate of 1-10%, percentage by weight is 1-10% sodium salt.
The mould suction-operated of copper sulphate to montmorillonite has synergy, and can improve its adsorption rate of about percent 20, sodium salt not only can strengthen adsorption effect, significantly improves effect to montmorillonite to being absorbed with of pathogenic bacteria in enteron aisle.
As preferably, take off the component that mould dose comprises following weight percents: montmorillonite 30-50%, yeast cell wall 20-30%, marine alga 20-30%, copper sulphate 1-10%, sodium salt 1-10%.
As preferably, described sodium salt is the mixture of sodium carbonate or sodium acid carbonate or sodium carbonate and sodium acid carbonate.
Wide spectrum feed montmorillonite takes off the preparation method of mould dose, comprises the steps: that montmorillonite is delaminated pulverizing by (1), adds marine alga, stir; (2) copper sulphate and sodium salt are mixed, add yeast cell wall, stir; (3) by step (2) obtain mixture and add the mixture with step (1) gained, stir and evenly mix, obtain de-mould dose.
As preferably, described montmorillonite obtains by the following method: after (a) dries montmorillonite raw material under 70-90 DEG C of condition, is crushed to 300-500 order, obtains raw meal; B () carries out pre-treatment to the raw meal that step (a) obtains: raw meal joined in sodium salt solution, and process 2-5 hour, filters, obtain treatment fluid; The weight ratio of raw meal and sodium salt solution is 1:1-3; The zeolite that particle diameter is 0.2mm is added in (c) treatment fluid, in mixing plant, stir process 1-3 hour, mixing speed is 200-300 rev/min, and then concentrated, drying obtains processing powder; D () adds water in process powder, stir and evenly mix with process powder, obtained solid content is the slurries of 10-25%; E () described slurries cross 300-500 mesh sieve, obtain the first filtrate; (f) first filtrate send in ultra-fine equipment and carry out ultra-fine delaminating, remove solid particle through classifying equipoment again after delaminating, obtain the second filtrate; G (), by described second filtrate sterilizing, concentrated, dry, obtains montmorillonite.
As preferably, described sodium salt is the mixture of one or more in sodium carbonate or sodium acid carbonate or sodium pyrophosphate, and the concentration of sodium salt is 50-80%.
As preferably, described sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is 3-5:1.
Wide spectrum feed montmorillonite provided by the present invention takes off the using method of mould dose: prevent mouldy, add 1-5 kilogram in feed per ton; Mouldy feed, adds 3-8 kilogram in feed per ton.
By implementing technique scheme, cost of material of the present invention is low, green non-poisonous evil, can the common mycotoxin of efficient adsorption, the breeding of mould in feed can be suppressed, after animal edible, can mucous membrane be protected, but do not absorbed by animal body, carry adsorbed toxin and excrete; Preparation method, technique is simple, with low cost, is convenient to suitability for industrialized production; Using method is simple.
Detailed description of the invention
Below in conjunction with detailed description of the invention, further description is done to the present invention.
Embodiment 1:
A kind of wide spectrum feed montmorillonite takes off mould dose, comprises the component of following weight percents: pulverous montmorillonite 2 0%, yeast cell wall 40%, pulverous marine alga 40%.
Preparation process: montmorillonite to be delaminated pulverizing, added marine alga, stir by (1); (2) add yeast cell wall, stir.
The preparation method of the montmorillonite used comprises: (a) dries montmorillonite raw material to moisture content under 70 DEG C of conditions is after 5%, is crushed to 400 orders, obtains raw meal; B () carries out pre-treatment to obtained raw meal, step is as follows: by concentration be 50% sodium salt solution join in raw meal, in temperature be under the condition of 70 DEG C process 3 hours, filter, obtain treatment fluid; Sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is 3:1; The weight ratio of raw meal and sodium salt solution is 1:1; The zeolite that particle diameter is 0.2mm is added in (c) treatment fluid, in mixing plant, stir process 1 hour, mixing speed is 250 revs/min, and then concentrated, drying obtains processing powder; C () adds water and dispersant in process powder, stir and evenly mix with raw meal, obtained solid content is the slurries of 25%; Dispersant is 0.05% of raw meal weight, selects calgon; D () described slurries cross 500 mesh sieves, obtain the first filtrate; (e) first filtrate send in ultra-fine equipment and carry out ultra-fine delaminating, remove solid particle through classifying equipoment again after delaminating, obtain the second filtrate; F (), by described second filtrate sterilizing, concentrated, dry, obtains montmorillonite, purity is 99.3%, heavy metal lead is 3ppn, whiteness is 86%, cation exchange capacity is 150mmol/100g.
Wide spectrum feed montmorillonite takes off the using method of mould dose: prevent mouldy, adds 2 kilograms in feed per ton; Mouldy feed, adds 6 kilograms in feed per ton.
Embodiment 2:
A kind of wide spectrum feed montmorillonite takes off mould dose, comprises the component of following weight percents: pulverous montmorillonite 80%, yeast cell wall 10%, pulverous marine alga 10%.
Preparation process: montmorillonite to be delaminated pulverizing, added marine alga, stir by (1); (2) add yeast cell wall, stir.
The preparation method of the montmorillonite used comprises: (a) dries montmorillonite raw material to moisture content under 70 DEG C of conditions is after 5%, is crushed to 400 orders, obtains raw meal; B () carries out pre-treatment to obtained raw meal, step is as follows: by concentration be 50% sodium salt solution join in raw meal, in temperature be under the condition of 70 DEG C process 3 hours, filter, obtain treatment fluid; Sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is 3:1; The weight ratio of raw meal and sodium salt solution is 1:1; The zeolite that particle diameter is 0.2mm is added in (c) treatment fluid, in mixing plant, stir process 1 hour, mixing speed is 250 revs/min, and then concentrated, drying obtains processing powder; C () adds water and dispersant in process powder, stir and evenly mix with raw meal, obtained solid content is the slurries of 25%; Dispersant is 0.05% of raw meal weight, selects calgon; D () described slurries cross 300 mesh sieves, obtain the first filtrate; (e) first filtrate send in ultra-fine equipment and carry out ultra-fine delaminating, remove solid particle through classifying equipoment again after delaminating, obtain the second filtrate; F (), by described second filtrate sterilizing, concentrated, dry, obtains montmorillonite, purity is 99.3%, heavy metal lead is 3ppn, whiteness is 86%, cation exchange capacity is 150mmol/100g.
Wide spectrum feed montmorillonite takes off the using method of mould dose: prevent mouldy, adds 2 kilograms in feed per ton; Mouldy feed, adds 6 kilograms in feed per ton.
Embodiment 3:
A kind of wide spectrum feed montmorillonite takes off mould dose, comprises the component of following weight percents: pulverous montmorillonite 60%, yeast cell wall 20%, pulverous marine alga 10%, copper sulphate 5%, sodium salt 5%; Sodium salt selects sodium carbonate.
Preparation process: montmorillonite to be delaminated pulverizing, added marine alga, stir by (1); (2) copper sulphate and sodium salt are mixed, add yeast cell wall, stir; (3) by step (2) obtain mixture and add the mixture with step (1) gained, stir and evenly mix, obtain de-mould dose.
The preparation method of the montmorillonite used comprises: (a) dries montmorillonite raw material to moisture content under 80 DEG C of conditions is after 4%, after, be crushed to 500 orders, obtain raw meal; B () carries out pre-treatment to obtained raw meal, step is as follows: by concentration be 70% sodium salt solution join in raw meal, in temperature be under the condition of 90 DEG C process 5 hours, filter, obtain treatment fluid; The zeolite that particle diameter is 0.2mm is added again in treatment fluid, in mixing plant, stir process 2 hours, mixing speed is 200 revs/min, then obtains processing powder after concentrated, spraying dry; Sodium salt is sodium carbonate; The weight ratio of raw meal and sodium carbonate liquor is 1:2; C () adds the dispersant of 00.1% of water and raw meal weight in process powder, stir and evenly mix with raw meal, obtained solid content is the slurries of 20%; Described dispersant is sodium pyrophosphate; D () described slurries cross 400 mesh sieves, obtain the first filtrate; (e) first filtrate send in ultra-fine equipment and carry out ultra-fine delaminating, in classifying equipoment centrifuge, remove solid particle again after delaminating, obtain the second filtrate; F (), to ultrasonic sterilizing under the second filtrate high-temperature and high-pressure conditions, after carrying out acid treatment to it, concentrated, spraying dry, obtains montmorillonite, purity is 99.6%, heavy metal lead is 3ppn, whiteness is 87%, cation exchange capacity is 155mmol/100g.
Wide spectrum feed montmorillonite takes off the using method of mould dose: prevent mouldy, adds 1 kilogram in feed per ton; Mouldy feed, adds 3 kilograms in feed per ton.
Embodiment 4:
A kind of wide spectrum feed montmorillonite takes off mould dose, comprises the component of following weight percents: pulverous montmorillonite 75%, yeast cell wall 11%, pulverous marine alga 12%, copper sulphate 1%, sodium salt 1%; Sodium salt selects sodium acid carbonate.
Preparation process: montmorillonite to be delaminated pulverizing, added marine alga, stir by (1); (2) copper sulphate and sodium salt are mixed, add yeast cell wall, stir; (3) by step (2) obtain mixture and add the mixture with step (1) gained, stir and evenly mix, obtain de-mould dose.
The preparation method of the montmorillonite used comprises: (a) dries montmorillonite raw material to moisture content under 80 DEG C of conditions is after 4.5%, after, be crushed to 500 orders, obtain raw meal; B () carries out pre-treatment to obtained raw meal, step is as follows: join in raw meal by the sodium salt solution of concentration 80%, is to process 5 hours under the condition of 90 DEG C in temperature, filters, obtains treatment fluid; The zeolite that particle diameter is 0.3mm is added again in treatment fluid, in mixing plant, stir process 1.5 hours, mixing speed is 250 revs/min, then obtains processing powder after concentrated, spraying dry; Sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is 5:1; The weight ratio of raw meal and sodium salt solution is 1:2; C () adds the dispersant of 0.01% of water and raw meal weight in process powder, stir and evenly mix with raw meal, obtained solid content is the slurries of 20%; Described dispersant is the mixture of calgon and sodium pyrophosphate 1:2 in mass ratio; D () described slurries cross 400 mesh sieves, obtain the first filtrate; (e) first filtrate send in ultra-fine equipment and carry out ultra-fine delaminating, in classifying equipoment centrifuge, remove solid particle again after delaminating, obtain the second filtrate; F (), to ultrasonic sterilizing under the second filtrate high-temperature and high-pressure conditions, after carrying out acid treatment to it, concentrated, spraying dry, obtains montmorillonite, purity is 99.8%, heavy metal lead is 1ppn, whiteness is 80%, cation exchange capacity is 180mmol/100g.
Wide spectrum feed montmorillonite takes off the using method of mould dose: prevent mouldy, adds 5 kilograms in feed per ton; Mouldy feed, adds 8 kilograms in feed per ton.
Embodiment 5:
A kind of wide spectrum feed montmorillonite takes off mould dose, comprises the component of following weight percents: pulverous montmorillonite 50%, yeast cell wall 25%, pulverous marine alga 20%, copper sulphate 3%, sodium salt 2%; Sodium salt selects mass ratio to be the sodium carbonate of 3:1 and the mixture of sodium acid carbonate.
Preparation process: montmorillonite to be delaminated pulverizing, added marine alga, stir by (1); (2) copper sulphate and sodium salt are mixed, add yeast cell wall, stir; (3) by step (2) obtain mixture and add the mixture with step (1) gained, stir and evenly mix, obtain de-mould dose.
The preparation method of the montmorillonite used comprises: (a) dries montmorillonite raw material to moisture content under 85 DEG C of conditions is after 3%, after, be crushed to 450 orders, obtain raw meal; B () carries out pre-treatment to obtained raw meal, step is as follows: by concentration be 60% sodium salt solution join in raw meal, in temperature be under the condition of 80 DEG C process 4 hours, filter, obtain treatment fluid; The zeolite that particle diameter is 0.2mm is added again in (c) treatment fluid, in mixing plant, stir process 1 hour, mixing speed is 300 revs/min, then obtains processing powder after concentrated, spraying dry; Sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is 4:1; The weight ratio of raw meal and sodium salt solution is 1:3; D () adds the dispersant of 0.08% of water and raw meal weight in process powder, stir and evenly mix with raw meal, obtained solid content is the slurries of 20%; Described dispersant is sodium trimetaphosphate; E () described slurries cross 400 mesh sieves, obtain the first filtrate; (f) first filtrate send in ultra-fine equipment and carry out ultra-fine delaminating, in classifying equipoment centrifuge, remove solid particle again after delaminating, obtain the second filtrate; G (), to ultrasonic sterilizing under the second filtrate high-temperature and high-pressure conditions, after carrying out acid treatment to it, concentrated, spraying dry, obtains montmorillonite, purity is 99.9%, heavy metal lead is 0ppn, whiteness is 90%, cation exchange capacity is 200mmol/100g.
Wide spectrum feed montmorillonite takes off the using method of mould dose: prevent mouldy, adds 1-5 kilogram in feed per ton; Mouldy feed, adds 3-8 kilogram in feed per ton.
Claims (9)
1. a wide spectrum feed montmorillonite takes off mould dose, it is characterized in that, comprises the component of following weight percents: montmorillonite 2 0-80%, yeast cell wall 10-50%, marine alga 10-50%.
2. a kind of wide spectrum feed montmorillonite takes off mould dose according to claim 1, it is characterized in that, also comprises copper sulphate that percentage by weight is 1-10%, percentage by weight is 1-10% sodium salt.
3. a kind of wide spectrum feed montmorillonite takes off mould dose according to claim 2, it is characterized in that, comprises the component of following weight percents: montmorillonite 30-50%, yeast cell wall 20-30%, marine alga 20-30%, copper sulphate 1-10%, sodium salt 1-10%.
4. a kind of wide spectrum feed montmorillonite takes off mould dose according to claim 2, it is characterized in that, described sodium salt is the mixture of sodium carbonate or sodium acid carbonate or sodium carbonate and sodium acid carbonate.
5. a kind of wide spectrum feed montmorillonite takes off the preparation method of mould dose as claimed in claim 2, it is characterized in that, comprises the steps: that montmorillonite is delaminated pulverizing by (1), adds marine alga, stir; (2) copper sulphate and sodium salt are mixed, add yeast cell wall, stir; (3) by step (2) obtain mixture and add the mixture with step (1) gained, stir and evenly mix, obtain de-mould dose.
6. a kind of wide spectrum feed montmorillonite takes off mould dose according to claim 1, and it is characterized in that, described montmorillonite obtains by the following method: after (a) dries montmorillonite raw material under 70-90 DEG C of condition, is crushed to 300-500 order, obtains raw meal; B () carries out pre-treatment to the raw meal that step (a) obtains: raw meal joined in sodium salt solution, and process 2-5 hour, filters, obtain treatment fluid; The weight ratio of raw meal and sodium salt solution is 1:1-3; The zeolite that particle diameter is 0.2mm is added in (c) treatment fluid, in mixing plant, stir process 1-3 hour, mixing speed is 200-300 rev/min, and then concentrated, drying obtains processing powder; D () adds water in process powder, stir and evenly mix with process powder, obtained solid content is the slurries of 10-25%; E () described slurries cross 300-500 mesh sieve, obtain the first filtrate; (f) first filtrate send in ultra-fine equipment and carry out ultra-fine delaminating, remove solid particle through classifying equipoment again after delaminating, obtain the second filtrate; G (), by described second filtrate sterilizing, concentrated, dry, obtains montmorillonite product.
7. a kind of wide spectrum feed montmorillonite takes off mould dose according to claim 6, it is characterized in that, described sodium salt is the mixture of one or more in sodium carbonate or sodium acid carbonate or sodium pyrophosphate, and the concentration of sodium salt is 50-80%.
8. a kind of wide spectrum feed montmorillonite takes off mould dose according to claim 7, it is characterized in that, described sodium salt is the mixture of sodium carbonate and sodium pyrophosphate, and mass mixing ratio is 3-5:1.
9. a kind of wide spectrum feed montmorillonite takes off the using method of mould dose as claimed in claim 1, it is characterized in that, prevents mouldy, add 1-5 kilogram in feed per ton; Mouldy feed, adds 3-8 kilogram in feed per ton.
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